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By Charles W. Huggins

Knoop hardness indentations were studied and measured with the electron microscope on TiB2, HfC, and A1B12 crystals. A detailed description of replicating the indentations using collodion and Faxfilm is made. A John Hopkins grating having 28,800 lines per inch was used to accurately determine the magnification used on the electron microscope. The primary objectives were to prepare carbon replicas of hardness indentations, to measure the indenations accurately, and to compare the results with those obtained with the light microscope. The resulting data showed excellent agreement between the measurements made on the replicas with the electron microscope and those made with the optical microscope. The replicas made from collodion showed slightly better agreement with the light optical values than did the replicas made from Faxfilm.

Jan 1, 1963

By Luana de Sousa Santos

O setor Petróleo e Gás Natural vem tendo enormes gastos com as paradas de manutenção. Estes gastos estão relacionados à degradação sofrida por seus equipamentos de refino devido à corrosão. Uma possível solução seria a utilização de novas ligas de aço inoxidável ferrítico com elevados percentuais de molibdênio, o que teoricamente favoreceria um aumento da resistência à corrosão. No entanto, pelo fato dessas ligas serem aplicadas na condição como soldada mudanças microestruturais significativas podem ser geradas, além de considerar o fato da solda das ligas em estudo ser realizada com material dissimilar, e a diferença existente entre o metal de adição e a região afetada pelo calor (ZAC) pode propiciar ao surgimento do fenômeno eletroquímico conhecido como pilha galvânica. Portanto, o objetivo deste trabalho foi analisar o comportamento corrosivo na solda dissimilar de duas novas ligas de aço inoxidável ferrítico com diferentes teores de cromo e um elevado teor de molibdênio, ambas com adição de superliga de níquel, verificando a influência da pilha. O resultado da soldagem foi avaliado através de exames metalográficos e ensaios eletroquímicos. As micrografias do metal de adição utilizado na soldagem das ligas mostraram que o mesmo possui uma microestrutura dendrítica e os gráficos obtidos dos ensaios de Polarização Potenciodinâmica Cíclica não reproduziram para as ligas soldadas, o que foi melhor analisado observando os resultados dos ensaios de forma separada, para as regiões que constituem a solda das ligas, o metal de adição e ZAC. Sendo possível verificar a existência de uma maior resistência a corrosão no metal de adição.

Aug 8, 2018

By M. J. Ferrante

Enthalpy and entropy increments above 298.15° K were determined for cop-per sulfate between 298° and 1,000° K and for copper oxysulfate between 2980 and 1,146° K by the method of copper-block drop calorimetry. Enthalpies, entropies, and heat capacities are tabulated for both compounds. In addition, free-energy functions are tabulated for the sulfate. Equations representing the enthalpies are given for each compound.

Jan 1, 1972

By Fernando Kameoka

Desde o final da década de 90, com o desenvolvimento de novos parâmetros industriais para a fabricação de produtos eletroeletrônicos criou-se o conceito de obsolescência programada. Como consequência deste comportamento mercadológico e novos parâmetros de consumo, o volume de resíduos de equipamentos eletroeletrônicos gerado pelo descarte indiscriminado de produtos ainda em condições de uso tem atingido patamares alarmantes, tornando-se assim um grave problema ambiental. Com a Política Nacional de Resíduos Sólidos, estudos sobre a logística reversa dos resíduos provenientes de equipamentos eletroeletrônicos revelam-se promissores devido à presença de metais com alto valor de mercado, o que viabiliza economicamente os processos de reciclagem destes resíduos. Quando se trata da recuperação de metais e de reagentes, as rotas envolvendo etapas hidrometalúrgicas oferecem um grande benefício em relação às soluções existentes devido à não liberação de gases tóxicos durante o processo. No entanto, para a recuperação de cobre e alguns metais nobres as rotas hidrometalúrgicas tradicionais têm-se mostrado ineficientes devido à presença de ferro nos resíduos. Por esta razão, este trabalho tem como objetivo realizar estudo cinético da lixiviação de ferro de forma seletiva para a recuperação de outros metais. Foi analisado o processo de lixiviação em ácido sulfúrico na concentração de 2M, variando tempo e temperatura, com o intuito de avaliar a extração seletiva do ferro e viabilizando assim os processos subsequentes de recuperação de cobre e metais nobres através de extração sólido-líquido ou líquido-líquido. Os resultados apontam para extrações de ferro em solução de ácido com índices de pureza acima de 95%.

Aug 16, 2017

By Rudineli Demarque

Este artigo apresenta um estudo das características metalúrgicas, geométricas e microestruturais da soldagem TIG autógena aplicada em chapas de um aço AISI 304, o processo autógeno tipo cordão sobre chapa foi utilizado com a finalidade avaliar o comportamento deste aço quando submetido a ciclos térmicos distintos. A soldagem foi automatizada, na posição plana, e realizada com controle de velocidade com a finalidade de regular a energia adicionada ao material soldado. As variáveis de entrada foram a velocidade da tocha de soldagem TIG, e a corrente setada na máquina de solda. Foram avaliados os efeitos da variação da energia de soldagem sobre as características metalúrgicas do processo, sobre as características geométricas (penetração e largura) do cordão se solda, microestrutura, espaçamento dendrítico e microdureza da seção transversal da junta soldada. Os resultados indicaram uma forte influência sobre a geometria da junta soldadas, aumento de 28,5% na largura, 59,6% na profundidade e 44,6% na área, além de alterações microestruturais, aumento de 100% na quantidade de ferrita d, 12% na microdureza e 51,69% no espaçamento das dendritas no metal de solda, Além disso observaram-se ausência de defeitos nos passes isolados sobre as chapas.

Oct 30, 2017

By M. Bozorgtabar

Metal Matrix Composites (MMC) have a ductile matrix containing ceramic particles, Due to their improved wear properties, Al?SiC composites have economical applications in many industrial uses where wear is a problem, One of the most serious difficulties in manufacturing Al-SiC composites is obtaining adequate 'wetting' of the particles by the melt. In this research work, a stir casting system was designed for the improved manufacturing Al-SiC composites, The effect of some production variables such as the addition of SiC particles to the aluminum melt on wettability, was also studied. The results showed that the manual addition of particles would not be successful in manufacturing and that a system of adding silicon carbide particles through controlled temperature, atmosphere and improved mixing was needed.

Jan 1, 2005

By U B. Pal

Downsizing and decommissioning of nuclear facility operations is increasing the stockpile of various different grades of Radioactive Scrap Iron (RSI). Disposal of this material not only represents significant resource and value lost, but also necessitates long term monitoring for environmental compliance. The latter results in additional recurring expense. It is desirable to be able to decontaminate the RSI to a very low level that can be recycled or used for fabrication of containers for RSI disposal instead of using virgin metal to fabricate the container. Electro-Slag Remelting and Refining (ESR) is often used for decontaminating radioactive contaminated sources of scrap iron such as stainless steel. Non-radioactive oxides of cerium are used to simulate the radioactive oxide contaminants of Uranium and Plutonium. The success of the ESR process is strongly dependent on the capacity of the slag to rapidly incorporate the radioactive contaminant (simulant). In this study we have measured the slag-metal partition coefficient for cerium and investigated the reaction mechanism for the dissolution CeO, in the slag.

Jan 1, 2002

By P. M. Shibley

"IntroductionMine drainage, surface. drainage and process liquors are the principal mine and mill effluents. The quantity and quality of these flows varies according to mineralogy, type and scale of mining, the process, tailing disposal, local ground conditions and climate.Typical contaminants remaining after solids sedimentation are colloidal or semi-colloidal particles, acids, alkalis, metals in solution, cyanides and thiosalts. Environmental regulations and guidelines have been issued in detail by the appropriate government agencies and will not be reviewed here. Revisions and additions are being made as our comprehension and abilities increase. Some contaminants of consequence have not been specifically regulated as practical treatment technology has not been identified. Thiosalts fall into that category as do the derivatives of the first stage of cyanide oxidation - cyanates.Most mining activities have present or foreseeable water treatment requirements. Because process economics can be adversely skewed by the environmental factor, the acknowledged objective of every operation must be to identify and anticipate those requirements.The evaluation and selection of water treatment techniques for mine-mill applications is complicated by the fact that most mine-mill effluents are high volume, dilute and chemically complex systems. Treatment processes applicable to most contaminants are: chemical or biological oxidation; neutralization and/or precipitation; liquid/solids separation. Other processes such as ion exchange, electro-deposition, foam fractionation, freeze crystallization and reverse osmosis offer the possibility of selective removal or concentration of contaminents. The latter tediniques, representing a slightly higher level of technology, are less suited to the large, low value flows usually encountered in the mine environment."

Jan 1, 1989

By René Dufour

Jusqu?à son acquisition par MM René Dufour et Alain Robin en 1994, les claims miniers et les droits de surface de la propriété étaient détenus depuis 1953 par la société Québec Columbium, une filiale de la socité américaine Kennecott Copper qui y a réalisé d?importants travaux miniers. En 1995 la compagnie NIOCAN inc. fut incorporée; ses actions furent inscrites à la bourse de Montréal en 1997, et à la bourse de Toronto en décembre 1999. Jusqu?à maintenant, NIOCAN a investi plus de 7 millions de dollars dans le développement de sa propriété minière de niobium située à quelques 40 kilomètres au nord-ouest de Montréal. Le haut rendement économique des deux gisements principaux que compte exploiter la compagnie, le S-60 et le HWM-2, a été établie par des études de faisabilité effectuées par le consortium Met-Chem/SNC-Lavalin. La mission que s?est donnée NIOCAN inc. consiste à mettre en production ses deux gisements et à devenir ainsi productrice de ferroniobium dans les plus brefs délais. Figure 2 Le projet est présentement à un stade avancé d?obtention du certificat d?autorisation du ministère de l?Environnement. À plus long terme, la compagnie compte aussi exploiter les sous-produits de ses gisements (apatite, forsterite, magnétite, calcaire et terres rares).

May 1, 2003

By W. F. Scott, K. L. Somerville

"This paper outlines the development and inplementation of functional training at the Thompson Mine of Inco Metals Company, Manitoba Division. This training is an extension of similar methods implemented throughout the company to meet safety and health and productivity objectives. It consists of the orientation to the mine, induction in the basic mining skills, and specific training in drilling and other skills in the mine. Initial results indicated a positive effect on the safety performance and proficiency of the mine workforce.IntroductionThe primary mining method at the Thompson Mine is mechanized cut and fill, with secondary recovery of pillars by undercut and fill . These methods require a workforce of about 900 hourly operating employees to obtain capacity production of 6500 tons of ore per day.Historically, turnover of mine employees has been high and large numbers of new recruits are introduced to the mine every year. These men are recruited primarily in Manitoba, but also from distant areas of Canada; most of the se people have no previous mining experience.Training has always been an important component of mine operations. Mine supervisors and experienced miners have committed an appreciable amount of time and effort to training these new recruits. As well, training efforts have been directed toward upgrading the skills of experienced workers.Recently, a growing awareness of the significance of this training effort and its impact on accident frequency, productivity, turnover and other important parameters of the mine operation has led to a review of training methods. The training program described in this paper has resulted from this review."

Jan 1, 1981

By D Mather

Fibre reinforced shotcrete has long been accepted as temporary ground support in both mining and civil tunnel linings. Greater knowledge and understanding of shotcrete as an engineering material and advances in its quality have enabled designers to eliminate the requirement of a second pass lining. The initial shotcrete can be used as the permanent tunnel lining or be incorporated into the final lining design, rather than ignored and considered as sacrificial.For the initial shotcrete lining to become a suitable permanent tunnel lining it must be able to establish and maintain stability over time when subjected to all possible loads. To ensure this, best engineering practices are required during the design phase of the project to analyse; ground conditions including rock mass properties, ground and ground water quality, rock mass loadings, excavation sequencing, and construction methodologies.The increased durability of steel fibre reinforced shotcrete over traditional tunnel support, in the right ground conditions, makes it possible to achieve a serviceability design life of greater than 100 years (as required in most infrastructure projects). By specifying a good quality shotcrete mix and ensuring adequate quality control for batching, fibre dosing, preproduction testing, excavation sequencing, and application control, it is possible to eliminate the requirement of a secondary lining. The properties of a suitable permanent lining must be well established using suffi cient preproduction testing in combination with post application monitoring.A major benefit of steel fibre reinforced shotcrete in ground support applications is the removal of any requirement for workers to work under unsupported ground. Its use can also significantly reduce, if not eliminate, the manual handling associated with placing traditional reinforcement such as lattice girders and mesh. Both of these benefi ts are significant with the ever increasing focus on health and safety.This paper highlights factors that must be considered in the design and specifications to enable an initial shotcrete tunnel lining to become the permanent shotcrete tunnel lining.

Mar 8, 2011

By J. Gibson

"INTRODUCTION As one of the most pressing and important political debates of this century, climate change has captured global attention and is forcing governments to take action towards decreasing GHG and carbon emission levels below what was previously thought to be necessary. With the ever-increasing price of diesel fuel accompanied by the popular topic of carbon taxes and greenhouse gas emissions, the mining industry is looking to industry specialists for assistance. The benefits of a no-idle policy reach far beyond carbon reduction and fuel savings, ranging from decreased maintenance to increased engine life. With products like battery powered A/C systems and diesel-fired heaters, going no-idle is easier today than ever before. With both systems being manufactured to withstand the harsh environments of the mining industry, the end user will see a seamless change from conventional, inefficient belt-driven systems to future, stand-alone mobile equipment HVAC. THE HISTORY OF GHGS AND CLIMATE CHANGE In 1896 Svante Arrhenius first claimed that the combustion of fossil fuels may eventually result in enhanced global warming, but not until 1955 did Gilbert Plass draw global attention to global warming by summarizing that adding carbon dioxide to the atmosphere would intercept infrared radiation and thus warm the earth. Then in the early 1960’s Charles Keeling developed modern technology to produce concentration curves for atmospheric CO2 (Figure 1). In 1988 the Intergovernmental Panel on Climate Change (IPCC) was founded by the United Nations after acknowledgement of a rising global annual temperature. The IPCC consists of over 2500 scientific and technical experts from more than 60 countries, and because climate change could not be solved by a single country, the Kyoto Protocol was negotiated in 1998 requiring all participating countries to reduce their GHG emissions by at least 5% from the 1990 levels. The Protocol was signed by 186 countries in 2001 (since then several countries have retreated from the agreement, including the United States)."

Jan 1, 2015

By Z Tong, M Gao, X Wang

In response to the need for improved magnetic separators for beneficiation of fine grained iron ores that have been finely ground to liberate the iron minerals from the gangue, a series of high efficiency wet drum permanent magnetic separators (T-GCT) has been developed by Maanshan Tiangong Technology Co Ltd. These magnetic separators have high efficiency for separating superfine strongly magnetic minerals and the ability to produce high-grade concentrates with high recovery. They are ideal replacements for conventional drum magnetic separators, especially for treating superfine particles.

Jan 1, 2009

By Q. Zhang

Phosphate tailings through Flotation contains large amount of dolomite which is difficult to be separated from apatite. In this present research, phosphate tailings is recycled by Flotation i.e. re-processing. High-purity dolomite with purity as high as 91.17% is seperated, which contains 19.82% of MgO. The results of orthogonal test show that the effect of various levels of different factors on the high-purity dolomite floatated. Future utilization of purified dolomite is also discussed: magnesium fertiliser especially magnesium phosphate is expected to be an ideal product from high-purity dolomite.

Jan 1, 2014

Jan 1, 1968

By A. W. Fahrenwald

Many factors enter into the efficient operation of the reciprocating type of gravity concentrator. Earlier investigators who studied these factor invariably used natural (crushed ore) products for their experiments, but in the present study synthetic products were used. The variables considered were (1) specific gravity of the sand grains, (2) size of sand drains, and (3) shape of sand grains comprising the table feeds. It is recognized, also, that the percentage relationship of the different kinds of grains is a factor affecting results. This factor is variable in one group of experiments but is thereafter kept constant.

Jan 1, 1929

By Luís Marcelo Marques Tavares

Pelotas de minério de ferro representam uma parcela significativa do mercado transoceânico de minério de ferro, contando com uma participação importante de empresas brasileiras. Pelotas concorrem favoravelmente com granulados e sínteres de minério de ferro na carga metálica de fornos, em particular devido à sua elevada resistência à degradação durante o manuseio e transporte. Entretanto, pelotas ainda sofrem desse problema, que resulta na geração de finos, removidos previamente à alimentação do forno, ou de cacos, que podem resultar no aparecimento de clusters em fornos de redução direta. Esses efeitos danosos da degradação podem ser minimizados caso uma metodologia adequada de caracterização de pelotas e de simulação do processo de manuseio se encontrasse disponível. O presente trabalho trata do desenvolvimento de metodologia inédita e inovadora para previsão de resultados de degradação de pelotas, desde a usina pelotizadora até o pátio ou forno do cliente, desenvolvido como parte da parceria entre o Laboratório de Tecnologia Mineral da COPPE/UFRJ e a Samarco Mineração. O trabalho mostra ainda uma validação preliminar a partir de um ensaio de quedas múltiplas em laboratório, mostrando ótima aderência. Um simulador do processo foi desenvolvido, o qual permite inserir as características das pelotas produzidas, bem como o fluxograma de manuseio, permitindo prever a intensidade da degradação.

Aug 16, 2017

By Marc Arpin

La Bolivie possède tout pour réussir. Son vaste territoire de plus d'un million de km2 et qui occupe une position stratégique au coeur du continent sud-américain recèle des ressources naturelles (forêts, minéraux, gaz naturel, etc) variées et abondantes. Elle a une frontière avec pas moins de 5 pays dont le géant que constitue le Brésil ainsi qu'avec l'Argentine, l'autre puissance régionale. Pourtant, malgré tous ces atouts, la Bolivie demeure l'un des pays les plus pauvres du continent. Ce paradoxe n'est nulle part mieux reflété que dans le secteur minier. Celui-ci fait face à une situation de crise en dépit d'une tradition minière de plus de quatre siècles et d'un potentiel géologique indiscutable ayant conduit à la découverte et à l'exploitation de fabuleux gisements d'argent et d'étain. Les habitants des districts miniers vivent dans des conditions de pauvreté extrême et les indicateurs de développement humain de ces régions sont parmi les plus bas en Amérique du Sud. La Bolivie réussit difficilement à attirer les compagnies minières alors que, chez les voisins, et particulièrement en Argentine, qui n'a pas de tradition minière, les investissements miniers majeurs affluent. Dans cette conférence, nous chercherons à expliquer les causes de cette situation et proposerons des solutions possibles.

May 1, 2001

By Ian R. Morrison

"Abstract - The Izok Zn-Cu-Pb-Ag volcanogenic massive sulfide deposit is located 265 km south of Kugluktuk (Coppermine), Nunavut Territory, Canada, in the west-central Slave structural province. The Izok deposit is owned 100% by Inmet Mining Corporation and represents one of the largest undeveloped zinc-copper resources in North America. The Izok deposit is hosted within and near the top of a thick sequence of predominantly felsic pyroclastic rocks of late Archean age. The hanging-wall stratigraphy includes additional felsic volcaniclastic rocks, andesitic and basaltic flows, thin sulfide-rich iron formations, and turbiditic sedimentary rocks. The felsic volcanic rocks are intruded by intermediate dikes and sills, followed by gabbroic dikes and sills. Both intrusive suites are interpreted to be volcanic feeders to the overlying flows. All lithologies are subsequently cut by younger, irregular, granitic pegmatite and diabase dikes. The volcanic and sedimentary rocks are regionally metamorphosed to pyroxene hornfels grade. The massive sulfides occur within a large (kilometer-scale) Na-depleted sericitic alteration zone. The immediate footwall and hanging-wall rocks to the deposit are characterized by zones of muscovite- biotite-sillimanite, lesser chlorite-biotite-cordierite, and locally intense silicification and sodium metasomatism. All lithologies have been affected by younger Ca-metasomatism. As currently defined, the Izok deposit comprises a cluster of five complexly zoned composite lenses: the Northwest, North, Central West, Central East, and Inukshuk lenses. The first four lenses are amenable to open-pit mining, whereas the Inukshuk lens will require underground development. The total indicated mineral resource presently stands at 16.5 million tonnes with a grade of 2.2% Cu, 11.4% Zn, 1.1% Pb, and 60 g/t Ag. Inmet Mining Corporation is presently reviewing the economic feasibility of developing the property."

Jan 1, 2004

By Charles A. Seitz

This Bureau of Mines report describes a chromatographic method for analyzing impurities in helium that utilizes a helium carrier gas contain-ing 25 to 30 ppm Ne. An example of the effect of trace amounts of nitrogen, methane, and moisture on the detector's response is shown. The added neon in the carrier does away with irregularities of the analysis which were experienced when the carrier contained up to 3 ppm Ne. The addition of 25 to 30 ppm Ne causes a loss of sensitivity, but the re-maining sensitivity is adequate for routine analyses. The high-neon carrier allows positive and more linear responses for eight impurities: neon, hydrogen, argon, oxygen, nitrogen, methane, carbon dioxide, and ethane. Neon concentration levels of 0.02 to 125 ppm in helium carrier gases were studied. The high-neon carrier has been in successful rou-tine use in Bureau of Mines helium facilities since October 1981.

Jan 1, 1985