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The Annual General Meeting of the Institute was held in Kelvin House, Johannesburg, on Wednesday, 27th August, 1969, at 4.15 p.m. Mr. R. C. J. Goode (President) was in the Chair. There were also present seventy Members, ten As¬sociate Members, two Affiliates, one Student and twelve Visitors making a total of ninety-five. The President declared the meeting open at 4.20 p.m. OBITUARIES The President: "It is my very sad duty to announce the deaths of the following members of the Institute: Mr James Charles Napoleon Humphreys, a Life Member who joined the Institute on 1st April, 1935, and passed away on 6th February, 1969. Mr Michael John Worrall, Graduate Member, who joined the Institute in 1960 and passed away on 2nd June, 1969. Mr Eric Adam Conrad Dickson, Associate Member, who joined the Institute on 13th June, 1952 and who passed away on 8th June, 1969. Mr Robert Jack, Associate Member, who joined the Institute on 2nd August, 1956, and passed away on 14th June, 1969. Mr R. A. H. Flugge-de-Smidt, Honorary Life Member and Gold Medallist, who joined the Institute in 1922 and passed away on 17th June, 1969. Mr John Gordon Craig, a Member who joined the Institute on 23rd August, 1960, and passed away on 6th August, 1969. As a mark of respect to the memory of the deceased, and in sympathy with the bereaved, I would ask you to rise and observe a few moments silence." MINUTES The President: "May we confirm the Minutes of the General Meeting held on 18th June, 1969, as published in the July, 1969, issue of the Journal?"-Agreed. WELCOME TO VISITORS The President: "We are honoured this afternoon by the presence of the Institute's Honorary President, Mr R. S. Cooke, President of the Chamber of Mines of South Africa, and by one of our Honorary Vice-Presidents, Mr T. L. Gibbs, the Government Mining Engineer, as well as by the presence of many distinguished guests, to all of whom I extend a most cordial welcome. We are happy to have present, Mr S. C. M. Naude, Director of the Witwatersrand Technical College, Mr G. A. P. Louw, Vice-President of the Associated Scientific and Technical Societies, Mr R. P. Randall, Senior Vice-President of the South African Institute of Electrical Engineers, Mr W. T. L. Wayman, President of the South African Institution of Mechanical Engineers, Mr D. F. Odendaal, President of the Institution of Certificated Mechanical and Electrical Engineers of South Africa, Mr E. Haacke, President of the Institute of Land Surveyors of the Transvaal, Mr B. L. Loffell, Vice-President of the South African Institution of Civil Engineers, Mr J. F. Leatherbarrow, President of the South African Institute of Assayers and Analysts, Dr W. S. Rapson, President of the Joint Council of the South African Scientific Societies, Dr P. L. Carman, President of the South African Chemical Institute, Mr F. Jackson, President of the Federation of Societies of Professional Engineers, Mr W. E. Kirkwood, President, S.E.I.F.S.A., Mr J. Steele, President of the South African Institute of Foundrymen, Mr M. Waite, President of the South African Institution of Welding, Mr M. R. Gericke, President of the South African Council of Professional Engineers, Mr G. C. Sowry, Chairman, Witbank-Middelburg Branch, Mr T. Groenewald, Chairman of the South African Chemical Institute (Southern Transvaal Section), Professor O. B. Volckman, Chairman of the South African Institution of Chemical Engineers, Mr H. W. Le Roux, Chairman of the South African Federation of University Engineer¬ing Students, Dr R. E. Robinson, Director of the National Institute for Metallurgy, Mr P. H. Anderson, Deputy-Chairman of Rand Mines Limited, Mr E. Boden, Manager of the A.S. and T.S. and Count Folchi-Vici, from Italy, who has lime interests in this country. I also extend a very special welcome to the lady guests here this afternoon, and to all the visitors." MEMBERSHIP The President: "I have pleasure in announcing that the names of the following candidates, having been published in accordance with By-Law 5.2.2, Council has elected them to membership in the following grades: NEW APPLICATIONS Members: Stuart Denston Hill, Robert Roy Richardson, Gert Paulus van der Vyver. Affiliates: Henry Clifford Read, Allen Edward Hooper, Alan Edwin Edkins. Graduates: Lester Winston Sturgess, Erroll Vincent Bosman. Students: Terence Vernon van Heerden, David Curtis Lindley. MEMBERS TRANSFERRED TO A HIGHER GRADE From Associate Member to Member: Andries Willem van Zyl, Roy Lardner, Nugent Gerald Ward Comyn. From Student to Graduate: Michael John Worrell (now passed away), Peter John Hamilton Short. I wish to welcome the new members to the Institute, and to congratulate those members who have been transferred to a higher grade." ANNUAL REPORT OF THE COUNCIL AND ACCOUNTS FOR THE YEAR ENDED 30th JUNE, 1969 The President: "Ladies and gentlemen, It is with much pleasure that I present to you the Annual Report and Accounts for the year ended 30th June, 1969. These have been laid on the chairs and before calling for their adoption I would like to make a few comments. The Accounts show an excess of expenditure over income of R2,124 and our Honorary Treasurer, Mr D. G. Maxwell, will in due course comment on this. The main difficulty has again been the cost of the Journal and I think most of you are aware of the changes that we propose to make. I shall be sorry to see the last of our old format but then I have always had rather a con¬servative outlook.

By G. van Aswegen, J. D. Bosman

Gold bearing deposits in the Witwatersrand consist predominantly of narrow tabular conglomerates with quartzite host rock. Extensive mining of these deposits at depth results in significant stresses being induced in the periphery of the tabular excavations. Where remnant pillars are created excessive stresses have resulted in the dynamic failure of the abutments. At the Hartebeestfontein Mine four brittle shear zones have recently been exposed and investigated. For most part, they represent abutment failure into the weaker hangingwall strata, striking parallel to the abutment, dipping towards the stope, with a sense of displacement consistent with closure of the stope from above. These shear zones are similar to those described in various publications by Ortlepp2: they are essentially brittle shear zones characterised by the presence of very finely comminuted ‘rock flour’ on an obviously freshly sheared surface. The angle between the shear zone wall and extension fractures indicate the sense of shear and the intersection of the extension fractures with the shear zone walls define a strong lineation normal to the direction of slip. It is suggested that these structures are referred to as ‘mining induced dynamic brittle shears’. Les gisements d’or du Witwatersrand consistent principalement de conglomérats tabulaires peu épais contenus dans une quartzite mère. Une exploitation poussée de ces gisements en profondeur a pour résultat l’apparition d’importantes contraintes induites à la périphérie des excavations tabulaires. Là où des piliers restants sont créés, des contraintes excessives ont eu pour résultat une rupture dynamique des appuis. Dans la Mine d’Hartebeestfontein, quatre zones fragiles de cisaillement ont été récemment exposées et étudiées. Dans la plupart des cas, elles représentent une rupture des appuis dans les strates moins solides de la paroi suspendue, orientée parallèlement à l’appui, inclinée en direction du chantier d’abattage avec une direction de mouvement consistante avec l’affaissement du toit de la galerie d’abattage. Ces zones de cisaillement sont similaires à celles décrites par Ortlepp2 dans diverses publications: Ce sont essentiellement des zones cisaillement fragiles caractérisées par la présence de « farine de roche » très finement réduite sur une surface évidemment fraîchement cisaillée. L’angle entre la paroi de la zone de cisaillement et les fractures de tension indiquent le sens du cisaillement et l’intersection des fractures de tension avec les parois de la zone de cisaillement définit une forte délinéation perpendiculaire à la direction du glissement. Il est suggéré que l’on se réfère à de telles structures comme des « cisaillements dynamiques fragiles induits par l‘exploitation ». Goldablagerungen im Witwatersrand bestehen überwiegend aus schmalen tabularen Konglomeraten mit Quarzitwirtgestein. Der umfangreiche Abbau dieser Ablagerungen in der Tiefe resultiert in signifikanten Drücken, die auf die Peripherie der tabularen Aushöhlungen wirken. Wo Restpfeiler hergestellt wurden, resultierten exzessive Drücke im dynamischen Versagen der Auflager. In der Hartebeestfontein Grube wurden kürzlich vier spröde Scherzonen freigelegt und untersucht. Zum größten Teil representieren sie Auflagerversagen im Stratum der schwächeren Stollenfirste, parallel zum Auflager verlaufend, in Richtung Abbaustelle abfallend, mit einem gewissen Grad an Verschiebung konsistent mit der Schliessung der Strosse von oben. Diese Scherzonen sind jenen ähnlich, die in den verschiedenen Publikationen von Ortlepp2 beschrieben werden: sie sind im Wesentlichen spröde Scherzonen, charakterisiert durch das Vorhandensein des sehr fein pulverisierten „Gesteinsmehls“ auf einer offensichtlich frisch abgescherten Oberfläche. Der Winkel zwischen der Scherzonenwand und den Bruchverlängerungen deutet die Richtung der Scherung an und die Kreuzung der Bruchverlängerungen mit der Abscherzone grenzt sich gegen eine starke Lineation normal zur Richtung der Lehne ab. Es wird vorgeschlagen, daß diese Strukturen als `vom Abbau verursachte dynamisch spröde Scherungen’ bezeichnet werden.

Jan 1, 2003

By J. M. Eriksen, T. Rosenqvist, H. Elstad, S. Seim, A. Hildal

The titanium industry demands high titanium feedstock for their processes. As rutile resources are limited, ilmenite has become the most important titanium source. Ilmenite smelting is an important part of upgrading ilmenite to high titanium feedstock. In the year 2005, upgrading of ilmenite by smelting, producing a slag with 80-90% Ti02, accounted for approximately 40% of the feedstock to the Ti02 pigment industry. In ilmenite smelting molten iron is produced together with a slag, which in addition to titanium oxide contains iron oxide as well as various impurity oxides of manganese, magnesium, silicon, aluminium, etc. Titanium is present mainly as Ti02 but partly also as Ti203. It is known that the concentration of Ti203 increases with decreasing concentration of FeO, but this dependency is affected by the nature of the impurity oxides. Sigurdson and Moore1 showed that slags high in CaO and MgO had a lower concentration of Ti203 than slags high in Si02 for the same amount of FeO. Pistorius2 showed in 2002 that if the impurity oxides MnO and MgO are counted, on a molar basis, as FeO, and Cr203, V203 and part of the A1203*), as Ti203, industrial slags will have a composition close to that of the M305 phase, where M denotes the elements Ti, Fe, Mn, etc, and which has the pseudobrookite structure. However, for equilibrium with liquid metallic iron he computed, by means of a computer program FACT, that the slag equilibrium composition is represented by a curved line in the ternary phase diagram FeTi03-TiO2-Ti2O3, but with a significantly higher concentration of trivalent titanium than actually observed in the industrial slags, and he discussed various mechanisms by which the slag during solidification could change its composition to a lower Ti203 content, but the possibility that the computed compositions might be wrong was not mentioned. Trane113 found in her research on titaniferous silicate slags a lower Ti3+/ Ti4+ ratio than that which is computed by the FACT program. The purpose of the present investigation was to study the equilibrium composition of Fe-Ti-O slag in equilibrium with liquid metallic iron, as well as the effects of impurities such as Si02, CaO and MgO on the slag composition. Industrial slags from TINFOS Titan and Iron KS (TTI) will also be discussed and their compositions will be plotted in the ternary phase diagram. These are slags produced from Tellnes ilmenite, quite high in magnesium and iron. Experimental In the past, equilibrium studies of the Fe-Ti-O slag system were difficult when it came to producing the slag. It was difficult to find a suitable crucible for the meltings. The highly corrosive slag would attack all known refractories, and the metal would attack metallic crucibles such as those made of platinum and molybdenum. In the present investigations the slag-metal combination was prepared in a high-frequency induction furnace with a vertically segmented water-cooled copper crucible. The crucible is shown in Figures 1 a and 1b. It was designed by the Australian Nuclear Science and Technology Organisation (ANSTO) with power from a 75 kVA high-frequency generator (750 kHz) supplied by Farfield Electronics Pty, Ltd, Australia. This enabled the slag-metal combination to be melted with turbulent stirring and is expected to be isothermal. The entire temperature gradient

Jan 1, 2007

By D. Bessinger, N. Rughubir

Exxaro Sands KZN produces?among other heavy mineral products?high titania slag, which is used as feedstock to the pigment industry. The titania slag is produced from the smelting of ilmenite in two 36 MW DC furnaces. In this smelting process carbon monoxide gas is produced. This gas is cooled, scrubbed and washed to remove entrained dust. This paper provides details on the gas cleaning plant system and the chemistry, mineralogy and size distribution of the particulate material contained in the off-gas stream. Characterization of the dust shows that is consists mainly of ilmenite, but with relatively high levels of SiO2and MnO. Smelting of the dust in a 500 kW DC furnace was carried out to investigate the potential for recovering valuable elements from the dust.

Jan 1, 2007

By R. L. Paul

Although it is often said that South Africa does not have suitable deposits, or the potential to develop mines on a small scale, a recent survey by the Chamber of Mines1 showed that, out of a sample of 641 producers, 41 per cent had between 10 and 19 employees, and a further 29 per cent had between 20 and 29 employees. This goes to show that minerals-related small, medium, and micro-enterprises (SMMEs) do exist, and can play an important role in the development of rural industries in South Africa. Nchaka Moloi of the Department for Mineral and Energy Affairs defined the various categories of SMMEsas shown in Table I2. An enterprise could be placed in a certain category as long as two of the variables, employees, capex or production applied.

Jan 1, 1997

NIM reports Report no. 1970 List of unrestricted NIM publications issued from 1966 to 1978. (30th Jun., 1978). Report no. 1976 The preparation and certification of two samples of chromium ore. (9th Sep., 1978). Report no. 1982 The resistivity of mixtures of Mamatwan manganese ore and reducing agents. (31st Aug., 1978). Report no. 1984 Commissioning of the AEI MS702 mass spectrometer. 31st Aug., 1978). Metallurgical slags The Basic Science Section of the Canadian Institute of Mining and Metallurgy is sponsoring an International Symposium on Metallurgical Slags, which is to be held in Halifax, Nova Scotia, during 24th to 28th August, 1980. Mining machinery An international conference on mining machinery is to be held in Brisbane, Australia, from 2nd to 6th July, 1979.

Jan 1, 1979

By B. Kenealy

A typical deep shaft is President Steyn No. 2 in the Free State, where 9 tonnes of ore are hoisted at about 15 metres per second from 2378 metres below surface. The skips and attachments each weigh 7 tonnes and they are connected by 43 tonnes of rope, so that to hoist the 9 tonnes of payload, a total of 66 tonnes is accelerated from stand still to 55 km/h for each cycle, using an average of 3185 kilowatts of power in the process. The cycle time for the hoisting is 3.22 minutes. The peak power consumption is 6954 kilowatts, which determines the size of the motor used. Is this the right approach? Are larger skips moving at higher speeds the answer? Is there another way?

Jan 1, 1996

By J. T. Davies

Note: Melting techniques in the iron foundry by J. T. DAVIES* INTRODUCTION The selection of melting equipment for use in an iron foundry has for several years been the subject of numerous discussions, papers, and conferences. The controversy that has raged throughout the world has been brought about by the following factors: IF AC Symposium The 2nd IF AC Symposium on Automation in Mining, Mineral and Metal Processing will be held from 13th to 17th September, 1976, at the Carlton Hotel, Johannesburg. Advance registration takes place on 12th September, 1976. World phosphates The Minerals Bureau of the Department of Mines has released the second publication in its series of reports on the economic aspects of minerals that are of particular importance to South Africa.

Jan 7, 1976

Mr J. Meintjes (Chairman) was in the chair. There were also present: 7 Members: Messrs B. D. McNeice, A. Bain, G. E. Carlyon, C. H. Coxon, B. F. v. d. Merwe, A. C. Hofmeyer, H. J. R. Way. 4 Associate Members: Messrs E. J. Jackson, A. C. Melvill, W. Weber, R. E. Powell. 2 Visitors. It was decided to have the visit to ETC at Barberton on 20th March. A programme will be sent to all members who indicated that they wish to go on this visit. A talk on "Billet Casting of Ferrochrome" was given by Mr. B. F. van der Merwe. After question time the chairman thanked the speaker and asked for the talk to be forwarded for possible publication in the Journal. The meeting closed at 9.10 p.m.

By J. T. M. Amphlett, C. A. Sharrad, M. D. Ogden, R. I. Foster

"A renewed interest in nuclear power around the world in order to reduce greenhouse gas emissions is going to increase demand for uranium as fuel. This will result in more uranium being mined, which will in turn increase associated environmental pressures, such as fresh water use. A move to lower quality waters containing impurities such as chloride would help alleviate these pressures. In this work, we determined the uptake characteristics of weakly basic anion exchange resin Ps-EDA towards uranium from saline solutions in a dynamic flow column. Breakthrough curves were produced, with suppression of uptake being observed for chloride concentrations above 5 g L-1. Calculated resin saturation capacities at zero and 5 g L-1 chloride are comparable with literature values for strong-base anion exchange resins, and exceed those published for weak-base resins up to 20 g L-1 chloride. Data has been fitted to multiple breakthrough models, with the modified dose-response model most effectively predicting uranium recovery. The results show that the ethylenediamine functionality could be suitable for use in future uranium processing flow sheets where a high-saline lixiviant is used. IntroductionIon exchange (IX) is a key technology in the uranium mining industry and is well established for the extraction of uranium from both acidic and alkaline leach liquors (Edwards and Oliver, 2000). It was first employed in 1952 at the West Rand mine in South Africa (Ford, 1993; Taylor, 2016). H2SO4 and Na2CO3 are the most commonly employed lixiviants used to solubilize uranium in acidic and alkaline leach conditions respectively. The chemistry of these systems causes uranium to form anionic sulphate or carbonate complexes, which can be taken advantage of by anion exchange resins.Another major technology for the extraction and purification of uranium from leach liquors is solvent extraction (SX). This technique involves the extraction of uranium from the aqueous phase into an immiscible organic layer. Although this is a commonly used method, there are major drawbacks to it, including the use of large volumes of flammable solvents, solvent loss, phase disengagement, third phase formation, and the production of problematic degradation products (Veliscek-Carolan, 2016). These problems can be circumvented through the use of IX resins."

Dec 1, 2018

By R. D. Cromarty, J. Du Toit

"Penetration of matte into tap-hole bricks causes detrimental refractory wear, which can lead to furnace breakouts. The ability of the tap-hole clay to form a protective layer on the brick, thereby limiting matte penetration was investigated by examining the interaction between platinum group metal (PGM) matte, tap-hole clay, and alumina-chrome refractory bricks on a laboratory scale.Samples containing clay and brick as well as samples containing clay, brick, and matte were heated to different temperatures to establish the clay-brick interaction and the extent of matte penetration. The greatest degree of physical contact between the brick and clay was achieved at curing temperatures of 600°C. Poor clay-brick contact was observed in the sample that was heated to 900°C.Matte displaced the clay in the clay-brick-matte sample that was heated to 1350°C, with significant matte penetration into the brick. Less matte penetration was observed when the clay-brick-matte sample was heated to 1500°C. Less matte penetration was also observed in the claybrick- matte sample in which the clay and brick were pre-baked at 800°C, and the sample then reacted with matte at 1350°C. IntroductionFloatation concentrate from ore from the eastern Bushveld Complex of South Africa, specifically the Platreef, Merensky, and UG2 reefs, forms the feed to the Polokwane platinum smelter (Hundermark, De Villiers, and Ndlovu, 2006). The ore from the UG2 Reef has a high chromite content, which requires high operating temperatures (1500–1700°C) to avoid chromium spinel build-up in the furnace hearth. These high operating temperatures lead to matte superheats in the vicinity of 500– 600°C, which put increased demands on the refractory materials (Nelson et al., 2005).Upon tapping, the matte moves through the tap-hole, which consists of an aluminachrome refractory brick-lined tapping channel (Hundermark, De Villiers, and Ndlovu, 2006). The flow of molten matte is stopped by the injection of tap-hole clay to form a plug in the tap-hole. The tap-hole clay hardens and strengthens during curing to obtain the required hardness and refractoriness against penetration, corrosion and erosion (Nelson and Hundermark, 2014)."

Jan 1, 2016

By Z-B. Cheng, X-J. Liu

"Intensive mining of shallow coal seams tends to result in severe subsidence of the ground surface. Surface subsidence is a complex dynamic spatiotemporal process that constantly changes as mining advances. With Liangshuijing coal mine as a case study, 3DEC numerical software was used to simulate the development of the moving subsidence field from open-off cut to full subsidence on the working face. The results demonstrate that the formation of a subsidence field is directly related to the coal seam depth H and the extent of the mine workings. Taking the advance distance of the working face as the unit of scale, the process of surface subsidence can be divided into four stages: micro-change (H/ p), the development of surface subsidence (2H/ p), the formation of a movement subsidence field (3H/ p), and dynamic balance (4H/ p). The changing movement of a subsidence field can be fully described by the characteristics of surface subsidence value, curve slope, and the inflection position. The results provide important technical support for predicting surface subsidence and the temporal–spatial evolution features of mining subsidence. IntroductionChina’s coal output was about 3.52 Gt in 2017 (China National Coal Association, 2018), making it the largest coal producer in the world, accounting for almost half of total world coal production. Coal production and distribution play a vital role in the energy industry of China. However, entire overlying strata, from coal seam to surface, are disturbed as a result of long-term, high-intensity and large-scale mining, causing surface subsidence. This results in groundwater loss, surface desertification, vegetation loss, and mud-rock flows. These issues have become topics of common concern throughout society. According to related research results (Liu 2008), the area of surface subsidence caused by coal mining in China has reached about 600 000 ha, some 0.2 ha (and up to 0.42 ha) of surface subsidence for every 10 000 t of coal produced. Surface subsidence disasters not only damage buildings, water conservancy, transportation infrastructure, and farmland, but also cause adverse effects on individual and community lifestyles, environmental hygiene, and economic development. Deterioration of the ecological environment in mining areas has a long history and is very harmful (Lu, 2015)."

Feb 1, 2019

1. Book reviews A report by the Monopolies and Mergers Commission on the efficiency and. costs in the development, production and supply of coal by the NCB (Chairman G. Le Quesne). London, Her Majesty's Stationery Office, Jun. 1983. £20 for report and appendices (2 vols). Reviewer: M. J. Martinson Canadian mines handbook 1983-84, edited by M. R. Brown. Toronto, Northern Miner Press Ltd, 1983. 444 pp. $22. Reviewer: Northern Miner Review Editor 2. New publications Developments in geophysical exploration methods-5, edited by A. A. Fitch. Barking. Applied Science Publishers Ltd (Ripple Road, Barking, Essex IG II OSA, England), 1983. 255 pp. £35.75. High-pressure researches in geoscience--behaviour and properties of earth materials at high pressures and temperatures, edited by W. Schreyer. Stuttgart, E. Schweizerbart'sche Verlagsbuchhandlung, 1983. 545 pp. DM 188. Dynamics of oil and gas accumulations, by Alain Perrodon. Pau, Elf Aquitaine (Documentation Centre Micoulau, 64018 Pau, France), 1983. 368 pp. 240 FF. New paths to mineral exploration, edited by F. Bender. Stuttgart, E. Schweizerbart'sche Verlagsbuchhandlung, 1983. 169 pp. DM 58. Results of the First Workshop on Standards in Geothermics, edited by R. Haenel and M. Gupta. Stuttgart, E. Schweizerbart'sche Verlagsbuchhandlung, 1983. DM 98. E&MJ book of jlowsheets edited by Paul C. Merritt. New York, McGraw-Hill, 1983. 214 pp. $42. 1983 E&MJ international directory of mining. New York, McGraw-Hill, 1983. 808 pp. $70. The future of heavy crude and tar sands - volume 11. New York, McGraw-Hill, 1983. 1300 pp. $1l0. 3. Mineral Policy and Energy publications Aluminium, by A. Johnston. 12 pp. . Arsenic, by J. J. Hogan. 4 pp. Cobalt, by D. G. Fong. 6 pp. Selenium and tellurium, by A. G. Johnston. 7 pp. Stone, by D. H. Stonehouse. 13 pp. Uranium, by R. T. Whillans. 16 pp. 4. Mintek publications Report M88 'l'he recovery of platinum-group metals and gold by the lead-collectionstep of thefire-assay procedure. Report MI04 The preparation and analysis of reference materials, and the provision of recommended values. Progress report no. 5. Report Mll1 The determination, by flow-injection analysis, of iron, sulphate, silver, and cadmium. Special publication 3 A guide to the presentation of papers.

Jan 1, 1983

By R. J. Davidson, B. Strong

The piloting and eventual large-scale operation of fixed-bed carbon columns for the recovery of gold from plant effluents is described. A fixed-bed carbon pilot plant comprising three adsorption columns was used for the recovery of gold from clarified plant effluent at the Vaal Reefs Exploration and Mining Company (West Division). The effluent ,which contained 0,1 toO,S g/t of gold and less than 10 g/t of free cyanide, was adjusted to pH 8 prior to use. Daily acid treatment of the carbon circuit with 3 per cent hydrochloric acid was shown to have a most significant effect on increasing the gold adsorption. The acid treatment involved a plant downtime of only I to 2 minutes per day. High loadings of gold (up to 30 k g/t) and copper (up to 75 k g/t) were obtained on the leading column, while the gold recoveries averaged 98 per cent over 17 weeks of continuous operation. The subsequent elution of loaded carbon in a pilot elution column indicated the use of abnormally high amounts of the pretreatment reagent (caustic soda and cyanide) used in gold elution. This was attributed to the high loading of copper on the carbon. However, the elution of both the gold and the copper at 110°C with demineralized water as the eluant was satisfactory. In a similar large-scale operation, three fixed-bed carbon columns each containing 4,5 t of carbon were used to treat 80 to 120 t/h of plant effluent with a gold concentration of about 0,15 g/t. Gold loadings of 5 to 6 k g/t were obtained regularly, while the gold recovery averaged 97 per cent over a 12-month period. The capital cost of the plant was recovered in 2 to 3 months. The evidence presented strongly suggests that copper plays a significant role in the adsorption and elution of gold under the prescribed conditions, and in the subsequent precipitation of gold following acidification of the eluates. The formation of a highly insoluble gold-copper complex produced under acid conditions appears to explain many of the observations made in the investigation.

Jan 1, 1983

1. Book reviews Phosphate rock, a bibliography of world resources. London, Mining Journal Books Limited, 1984. £10 (surface mail), £12.25 (airmail). Reviewer: P.Le. Grubb Ok Tedi, by William S. Pintz. London, Mining Journal Books Limited, 1984. 206 pp. £19 (surface mail), £22.25 (airmail). Reviewer: R.P. Plewman 2. Publications of the Canadian Mineral Policy Sector Lime by D.H. Stonehouse. 5 pp. Phosphates by G.S. Barry. 9 pp. Statistical summary of the mineral industry in Canada. 77 tables. Talc by M. Prud'homme. 6 pp. Zirconium by M.A. Boucher. 6 pp. Cement by D.H. Stonehouse. 13 pp. Gypsum and anhydrite by D.H. Stonehouse. 7 pp. Regional review by T.M. Buch. 12pp. SaltbyG.S. Barry. 7pp. Silicon, ferrosilicon and silicon carbide by D.G. Law-West. 6pp. SulphurbyB.W. Boyd. 9pp. Mineral Report 31. Canadian Minerals Yearbook 1981. Available from the above address at $40.75 per copy. 3. Mintek reports Report M18D The recovery of pyrite and gold from acid-leach residues from the Merriespruit Gold Mine. (First issued Feb. 1982; reissued Mar. 1984). Report M2OD The separation of ore from Cooke into high- and lowgrade fractions. (First issued Feb. 1982; reissued Mar. 1984). Report M33D Explanatory tests on the reduction of the sulphur content of sponge iron. (First issued Apr. 1982; reissued Mar. 1984). Report M43D Beneficiation tests on andalusite-bearing shales from a farm near Thabazimbi. (First issued Aug. 1982; reissuedMar. 1984). Report M129 The determination of tin, niobium, and tantalum in pegmatite by X-ray-fluorescence spectrometry. ReportM131 The determination of copper and nickel in iron- and chromium-bearing materials by a pressed-powder technique and X-ray-fluorescence spectrometry. Report M135 The installation of a 100 kV A plasma furnace at Mintek. The selection and installation of a 100 kV A a.c. plasma Report M136 The determination of gold in activated charcoal by use of a loose-powder technique and X-ray-fluorescence spectrometry. Report M140 The effect of physical and chemical factors on the corrosivity of a synthetic mine water.

Jan 1, 1984

By T. van Heerden

A range of supported gold catalysts was prepared by ion exchange, varying many of the preparation variables, including concentration in the precursor solution, washing procedure, as well as drying and calcination procedures. These catalysts have been characterized extensively. TEM images show essentially the same crystallite size distributions, between 2?5 nm, for almost all catalysts, the only exception being catalysts not washed in ammonia, which did not show any small crystallites. Additional characterization with SEM yielded an interesting discovery. Catalysts that appear identical on the TEM also contain some large crystallites in the range of 50?500 nm. Differences in dispersion due to the drying procedure not seen on the TEM can now be observed. Oxygen chemisorption is being investigated as an additional method to characterize gold based catalysts to complement the typically used electron microscope techniques.

Jan 1, 2012

By E. Schoeman

Ion exchange resins were investigated for the effective recovery of platinum, palladium, and gold from a pregnant cyanide heap leach solution. Screening results indicated that strong-base anion exchange resins proved to be most effective in the recovery of these metal cyanides. Gold was selectively recovered with the use of Minix, while effective recovery of gold, platinum, and palladium over the base metals, copper, and iron, was achieved with Amberlite PWA-5. Successful elution of these metal cyanides was possible from both Minix and Amberlite PWA-5, using a 2M potassium thiocyanate solution at ambient temperature. Acidic thiourea was unable to elute platinum from either Minix or Amberlite PWA-5. Effective elution of palladium and gold were, however, achieved with use of acidic thiourea. Using these results, two conceptual flow diagrams for the recovery of these metals from cyanide solutions are proposed.

Jan 1, 2012

By S. Nana, M. B. Cortie

Duplex stainless steels containing high levels of manganese and copper and lower-than-normal levels of nickel were produced and evaluated. The experimental alloys containing 3 per cent copper by mass could not be successfully hot-rolled. Alloys containing less than 2 per cent copper could be hot- and cold-rolled without difficulty. The wrought experimental alloys that contained copper were found to offer some advantages over the 2205- type duplex stainless steel in sulphuric acid at 52°C. Resistance to pitting attack was governed primarily by the chromium, molybdenum, and nitrogen contents, and one of the experimental alloys was superior to the 2205-type alloy in the ferric chloride test. It is concluded that manganese is a useful substitute for nickel in duplex alloys, but that further work is required before the present alloys, or variations of them, could be commercially viable.

Jan 1, 1993

By J. le Grange, M. Tullmin, A. Strauss, F. P. A. Robinson, C. A. O. Henning

An experimental feritic stainless steel with a chromium content of 40 per cent was welded by laser and electron beam (EB) welding processes. These techniques were found to be particularly suited to the welding of this alloy in that the impact toughness of the weld metal and heat-affected zone (HAZ) of the laser welds compared favourably with those of the parent aloy. When the EB process was used, the impact toughness of the weld metal was over 180 J/cm2. Grain growth in the HAZ was minimal for welding with these two processes. Corosion tests, conducted in a solution consisting of 20 per cent sulphuric acid and 100 p.p.m. of potassium thiocyanate, and In a highly corrosive industrial solution, indicated that the laser and EB welds were free of sensitization effects, thus confirming the metalographic results.

Jan 1, 1989

By A. J. Buchan

The wear of steel pipelines used for the transportation of backfill slurries is frequently regarded as an erosion problem only. An investigation was undertaken of the likely contribution to the total 'wear rate' made by corrosion. Use was made of a pipe flow loop with catholically protected specimens and corrosion inhibitors. Laboratory electrochemical tests utilizing a rotating-cylinder electrode were also conducted. The slurries used were classified tailings from two mines at a relative density of 1,7. The velocities were between 2 and 4,9 m/s. Substantial decreases in the wear rate of up to 80 per cent for one slurry and up to 67 per cent for the other were obtained with the use of corrosion control, showing that corrosion and, more importantly, interaction between erosion and corrosion, contribute a significant portion of the overall wear in steel pipelines

Jan 1, 1994