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By Amanda de Angelis Vitoi

Neste trabalho foi estudado o efeito da adição de argônio à atmosfera de nitretação sob plasma sobre a resistência à corrosão do aço inoxidável austenítico AISI 316L. As nitretações foram realizadas em reator a plasma pulsado, a 420°C, por 6 h, adicionando-se 0%, 5% e 10% de argônio à mistura gasosa. Os resultados mostraram que a adição de 5% de argônio promove um aumento na espessura da camada de austenita expandida em relação ao material nitretado sem argônio. Com o aumento da concentração de argônio de 5 para 10%, no entanto, verificou-se a formação de camadas de austenita expandida mais finas e de baixa resistência à corrosão devido à presença de nitreto de cromo em sua estrutura.

Aug 8, 2018

By Beatriz Luberiaga Bezerra, André Ben-Hur da Silva Figueiredo, Leticia dos Santos Aguilera, Ana Carolina Accioly Monteiro, Thainá Lucciola Hipolito de Lima, Barbara da Costa Araujo, Ana Luiza Buse da Silva

Cerâmicas porosas foram produzidas com nanopartículas de ferrita de manganês através da técnica de freeze casting, sendo possível obter poros direcionados. Foram produzidas duas amostras dessas cerâmicas tendo como ligante-dispersante o PEG-4000 e PEG-8000, ambos em 8%p. Por MEV foi possível observar as estruturas porosas das cerâmicas. O método de Arquimedes foi utilizado para obter as medidas de porosidade e densidade aparentes e de densificação. A ferrita pura e as amostras sinterizadas foram caracterizadas por DRX e foi identificada apenas a presença da fase ferrita, para as amostras antes da sinterização e transformação de fase da ferrita para óxidos de Mn e Fe após tratamento térmico. Tais resultados possibilitam indicar a aplicação dessas cerâmicas como elementos filtrantes.

Mar 1, 2019

By Willy Ank de Morais

A Norma Regulamentadora 18 (NR 18) requisita que o trabalho em telhados e coberturas devem ser efetuados com uso de dispositivos dimensionados por profissional legalmente habilitado e que permitam a movimentação segura dos trabalhadores. A forma tradicionalmente mais segura de locomoção em telhados e coberturas é através de passarelas, que devem ser adequadamente fixadas à estrutura destes. Neste trabalho foram dimensionados e fabricados componentes de alumínio para a fixação mecânica de plataformas-escadas em alumínio. Estes componentes foram adequadamente soldados às plataformas de forma a obter um produto final mais seguro e adequado às operações de manutenção de telhados, especialmente em galpões metálicos de grandes proporções, como foi o caso dos galpões onde este produto foi empregado pela primeira vez.

Oct 30, 2017

By Vinícius de Souza Vilela

O presente trabalho tem por objetivo analisar o uso de filtros de alta pressão no tratamento de polpas decorrentes do beneficiamento mineral, em especial rejeitos e concentrados de mineração. Foram analisados os problemas da atual prática de deposição de finos em barragens de rejeitos e baias de decantação e os novos desafios encontrados pelo setor em relação a escassez de água e eficiência energética. São elencados os diferenciais tecnológicos implementados nos filtros prensa Matec e analisados os benefícios na aplicação desta tecnologia, tais como maior recuperação de água, redução dos impactos ambientais e redução dos custos operacionais para manuseio e disposição dos rejeitos. Por fim são analisados os testes de filtragem realizados com rejeitos e concentrados de minério de ferro.

Aug 16, 2017

By Dyego Irineu Silva de Almeida

O presente trabalho foi proposto em sala de aula, na disciplina de tratamento térmico de ligas metálicas, do curso de Engenharia Metalúrgica da Universidade Federal do Ceará e teve como objetivo comparar as diferenças entre microestruturas e propriedades de um aço SAE 1016 após os tratamentos térmicos de normalização, têmpera e têmpera intercrítica. Três amostras do mesmo material foram tratadas termicamente. Uma amostra foi normalizada, outra temperada e outra temperada na zona intercrítica e após as análises metalográficas e ensaios de dureza foi possível concluir que a amostra normalizada apresentou uma microestrutura ferrítica com ilhas de perlita, a amostra temperada a 930ºC apresentou microestrutura martensítica e a amostra temperada na zona intercrítica formou microestrutura bainítica em uma matriz ferrítica.

Oct 30, 2017

By Willian Facundes

Foram estudados os aspectos termoquímicos e operacionais dos aços ultrabaixo carbono com alto teor de silício e alumínio, visando eliminar a obstrução da válvula gaveta (clogging) que gera transtornos operacionais como: redução da velocidade de lingotamento, retorno de aço remanescente na panela para o convertedor e interrupções de sequenciais. Realizou-se também a caracterização do material solidificado no interior da válvula gaveta utilizando técnicas de microscopia óptica e eletrônica. Os estudos mostraram que as inclusões eram formadas principalmente por alumínio, contendo também oxigênio e cálcio. Visando reduzir a quantidade de alumina no aço, substituiu-se o alumínio pelo ferro silício como agente desoxidante e exotérmico. Após essa alteração conseguiu-se eliminar a obstrução de válvula gaveta e consequentemente, os transtornos operacionais.

Aug 16, 2017

By Tiago Fernando de Abreu e Silva Tomanik

Massa plástica refratária e placas isolantes têm sido utilizadas por um longo período em Fornos de Reaquecimento de Placas e Tarugos na Indústria Siderúrgica. Novas tecnologias para o revestimento refratário tem ganhado crescente interesse nos últimos anos em função da redução no consumo de combustíveis, redução em tempo e custos de manutenção e, consequentemente aumento de produtividade. Esse trabalho apresenta o desenvolvimento de um novo concreto isolante, de aplicação por projeção, para condições de alta temperatura, que permitiu a substituição do concreto denso na face de trabalho. Essa nova tecnologia permitiu uma redução no tempo de reparo e alta confiabilidade, pois suporta muito bem as agressivas condições da atmosfera do forno. Também será discutido o futuro desenvolvimento de projetos com significantes economias em energia.

Oct 30, 2017

By Quésia de Freitas Silva Fonseca Rodriguesr

A produção de diamante sintético pode ser influenciada por vários fatores, podendo citar o dispositivo para o tratamento á célula reativa sob Altas Pressões e Altas Temperaturas – APAT, elementos que podem ser adicionados ao sistema. No presente trabalho foi utilizado Ni-Mn-C com adição da porcentagens de 4% de Ferro, os parâmetros utilizados no processo de síntese foram 4,5GPa de pressão e 1250oC de temperatura, sendo estes parâmetros mantidos por 10 minutos no dispositivo do tipo concavidade central. O efeito de 4% de ferro adicionado a célula reativa pode ser observado a partir de análises de raio-x e microscopia eletrônica de varredura. A influência do ferro foi observada no mecanismo de nucleação e crescimento dos cristais e no rendimento do processo.

Aug 16, 2017

By Camila Mendonça Romero Sales

Este trabalho teve como objetivo observar o percentual de transformação das fases (romboédrica e hexagonal), após tratamento termobárico do hidrocarboneto aromático Antraceno. As amostras foram tratadas sob pressão fixada em 4,5GPa e temperatura variando entre 900 e 1300°C, com o intuito de obter estruturas grafíticas. O percentual de fases foi obtido a partir de dados de difração de Raios X e através de refinamento pelo método de Rietveld, sendo que na temperatura de 1300°C foi possível observar um aumento na fase romboédrica e melhores parâmetros de refinamento. Pode-se concluir que o Antraceno ao ser submetido a altas temperaturas e alta pressão torna possível o aumento da fase romboédrica do material grafítico, o que resulta em melhores condições de síntese do diamante.

Aug 16, 2017

By Gilmar Ferreira Bataglia

The possibility of parameterization of hot tensile data together with creep data is investigated, for Aluminium Alloy 7475-T7351. This study represents part of a broader research program aiming at the validation of a methodology recently proposed for analyzing both kinds of data together, considering different metallic materials. The results presented in Part 1 of this work, were analyzed according to 4 traditional methods of the literature for parameterization of creep data, namely: Larson-Miller, Orr-Sherby-Dorn, Manson-Succop and Manson-Hafferd. The compatibility of the hot tensile test results with those of creep is remarkably good, indicating the possibility of using both kind of data together also in extrapolation schemes. The criterion proposed for equivalence between hot tensile and creep data is verified to work well also for this kind of material, under the present experimental conditions.

Aug 8, 2018

By Rodrigo Fina Ferreira, Jacek Kolacz, Luciana Gois, Neymayer Pereira Lima

The recent developments on the sensor detectors together with the higher capacity of the machines, due the high-speed computing recent advances, have made possible extending the application in the mining industry. The use of x-ray fluorescence, x-ray transmission and radiometric sensor based sorting can selectively remove gangue minerals in different size fractions for different minerals. This paper summarizes the potential application of SBS for an iron ore in three size fractions aiming to increase the %Fe after the removal of particles with main gangue minerals associated. Pilot plant tests were carried out with samples of iron ore in different size fractions and different content of hematite and gangues. The use of x-ray transmission sensor showed the possibility to increase the %Fe from about 63% to above 68% for particles below 80mm and 45mm, after the removal of low density particles. The presence of fines on the feed affected the performance of the SBS X-rays transmission machine, especially for the fine fraction feed. The mineralogical determination, carried out to know the association between hematite and gangue minerals, and the density of the particles on the feed, can be used to preview the quality of products of the x-transmission sorting process.

Oct 3, 2019

By Priscilla Pessin Coppo

The prevention of dental enamel wear has particular relevance for preventive and restorative purposes in dentistry. The wear damage can increase due to salivary disorders and/or parafunction (bruxism); antagonists incisal surfaces become flat and coincident. This study aims to investigate the wear behavior and the related mechanisms in sliding pairs of conformal incisal enamel, with similar values of hardness and fracture toughness, with different applied normal loads and lubricated conditions. Bovine incisors, under pin on flat configuration, were tested in two lubrication condition (dry or with natural saliva) and two applied normal loads (8 and 16 N). The worn surfaces were investigated by 3D profilometry and SEM. The analysis of worn surfaces indicated mechanisms of brittle fracture, but with different severities. Under a normal load of 16 N and dry condition, wear is controlled by a brittle process: microcracking with flake-like wear particles, which results in high friction coefficient (> 0.85), wear rate and wear volume. On the other hand, under a normal load of 8 N and natural saliva, wear took place in the interprismatic region, with consequent exposure of prisms and fracture in localized regions. In this case, the friction coefficient was 16% lower and the wear volume was one order of magnitude lower. Under 8 N and natural saliva, the wear was greater than in the dry condition, probably due to tribochemical reactions.

Jul 31, 2018

By Jorge Madias

Se analizan las distintas alternativas para la producción de barras de refuerzo de hormigón: endurecimiento por solución sólida (“dureza natural”); endurecimiento por temple y autorevenido en línea (Tempcore, Thermex, etc.) y endurecimiento por precipitación (microaleación con niobio, vanadio o titanio) y su influencia sobre la performance de las barras, en lo que hace a la resistencia a la corrosión, al fuego y a los sismos.

Aug 17, 2017

By Johan Richaud

Achieving high surface quality steel in the continuous casting process requires optimal mould level control. The design of the casting channel from the tundish to the mould is crucial to prevent formation of undesired instabilities or biased flows that can cause level fluctuation. With the aid of CFD and with physical water models, the geometry of the stopper nose and the nozzle seat have been studied and optimized to improve the overall mould flow stability. A special stopper nose; Ripple Stopper (RST), has been developed that reduces the formation of large and unwanted eddies in the liquid steel that destabilize the port exiting jets. Instead, the RST produces a fast release of turbulence in the form of a large number of small eddies. The large sudden fluctuations in the mould level are reduced, which in turn reduces the occurrence of surface defects. An additional benefit is derived from the local pressure around the stopper nose region being greater which reduces the refractory erosion. For a tundish gate type flow regulation, a new design encompasses an offset in the Tundish Well Nozzle (TWN) that realigns the flow and reduces the bias flow that is common to tundish gate regulation. The steel recirculation regions below the throttling gate are decreased reducing the risk of oxide depositions. The RST and the Offset bore casting channel have been applied successfully leading to a superior flow control performance between the tundish and the mould.

Jul 30, 2018

By Johanna Alegría-Ortega

Cr/CrN bilayer coating was deposited on AISI 440C by Cathodic Arc. The composition and structure of the Cr/CrN coating were investigated by scanning Electron Microscope, X-Ray Diffraction and X-ray Photoelectron Spectroscopy. The results show that crystal structure obtained was CrN phase with preferred [220] orientation. The hardness and adhesion of coating also were studied. The evaluation of erosion-corrosion (EC) on 440C bare and coated with Cr/CrN was performed by carrying out wear tests using a slurry jet with impingement angle 90° at 4 and 8 m/s. Corrosion, erosion and synergism wear rate were evaluated following the procedure described in ASTM G-119-09. This study presents that the synergism wear rate exceeds 40% of the total mass loss for coating and 60% of mass loss for the 440C, being the most aggressive wear component. The increase in impact velocity generated a rise in mass loss for both 440C bare and coated. The Cr/CrN coating offers better corrosion and erosion–corrosion resistance under all the tested conditions.

Aug 8, 2018

By Marcos Paulo da Silveira, Carolina Conter Elgert, Messias Prado de Almeida, Rafael Stella Galdino

Microalloyed steels have been intensely studied as an alternative to increase strength by grain refinement and/or precipitation hardening. Long steel products have a wide range of opportunities to apply well-defined principles of controlled rolling (CR) in order to increase strength and toughness with reduced costs. To evaluate the effect of microalloying elements as Nb and Ti with thermomechanical treatment, three conditions were tested: DIN 16MnCrS5 with hot rolling (HR), DIN 16MnCrS5 with Nb and CR and DIN 16MnCrS5 with Nb+Ti and CR. Austenitic grain size, obtained by direct quenching after rolling, has shown a decrease 32% with Nb addition, and 29% when Nb and Ti was added. Controlled rolling generated higher grain refinement and pancacked grains near the surface. When comparing ferritic grain size, controlled rolling plus niobium and titanium additions resulted in significant reduction of 35%. Yield strength increased 15% with microalloying and CR and more than 270% in impact toughness, even at -40°C.

Oct 1, 2019

By Hui-bin Wu, Rui Yuan, Yang Gu, Peng-cheng Zhang, Zheng-zhi Zhao

The corrosion behavior of three kinds of medium-Cr rolled steel pipeline steels in carbon dioxide collecting and transporting environment at different temperatures was studied. The results shew that the 5Cr sample was most affected by temperature. When the temperature rised from 30 °C to 90 °C, the corrosion rate increased from 0.12 mm/a to 1.87 mm/a, which was increased 15.6 times. The corrosion rate of 7Cr steel at 30 °C was similar to that of 5Cr steel. However, as the temperature increased, the corrosion rate rised slowly, increasing by 2.4 times at 90 °C. The corrosion rate of 9Cr steel was not obvious with temperature, and it was always below 0.06 mm/a. The thickness of the corrosion product film of the three samples gradually increased below 70 °C, and suddenly increased above 70 °C. This was related to the negative temperature coefficient of the solubility of FeCO3, and the thickening of the product film also affected the ion exchange of the cathodic reaction. An increase in the Cr content contributed to grain refinement and increased the proportion of the small-angle grain boundaries. More fine grains mean an increase in the total length of the grain boundaries, which could provide a diffusion channel for the free Cr element; on the other hand, the low-angle grain boundary structure was more orderly, with a lower free volume and lower interface energy. Under the combined effect of both, 9Cr steel and 7Cr steel had high volta potential and better corrosion

Oct 1, 2019

By Sander Mul, Michael Brandner, Armin Paar

Graphitic HSS roll grades such as ESW’s brand VANIMO can be considered as the latest developments for the last finishing stands in hot strip mills. These roll grades are developed on the basis of the alloying concept of (Carbide Enhanced) Indefinite Chill work roll materials. During the development of VANIMO, the amounts and types of carbide forming elements were increased and adjusted into the direction of cast HSS roll grades. The microstructure of graphitic HSS roll grades therefore consists of tempered martensite, cementite and several different carbide types as well as a well-defined amount of free graphite. The main purpose of graphitic HSS roll grades is to combine the high surface quality of Indefinite Chill alloys as well as the high wear resistance of HSS roll grades. Several systematic steps were taken to increase the wear performance from Carbide-Enhanced Indefinite Chill grades to the more advanced VANIC grade and further on to the highest alloyed roll grade VANIMO. In every development step, the surface quality of the roll grades was carefully monitored. The decision to invest in new testing equipment at ESW’s plant was driven by the wish to see microstructural effects of different alloys in a macroscopic dimension. Usually samples are taken from cast rolls and investigation is done in comparably small areas compared to the total surface of a roll. Rolling of strip is done with the entire barrel, so effects of alloy and microstructure can appear anywhere on the barrel surface. To ensure better understanding and deeper knowledge about influences of alloying trials we decided to install the last version of LRI (Lismar Roll Inspection). LRI includes the latest technology of Eddy Current with an enormous resolution. Depending on the formation of carbide precipitations, carbide network as well as matrix and free graphite, the EC test can detect smallest differences. The possibility to analyze the different results of EC and UT surface wave inspection will be discussed. A few examples of surface effects in the mill application will be discussed and improvement strategies explained.

Oct 1, 2019

By Nelson SOUTO, Nicolas LEGRAND, Christian COUNHAYE, Don EARLEY

The work is motivated by the automotive customer requirements for a roughness with high peak density (RPc > 75 peaks/cm) on steel sheet surfaces to maintain a good strip surface finish after painting. For that purpose, a new approach is utilized to compute roughness transfer and predict final roughness on uncoated steel sheets (average roughness, skewness, peak density) as a function of temper rolling conditions. The approach is based on the Monte Carlo method combined with the Abott curves and an auto-correlation function to numerically generate roughness profiles for roll and strip respectively. To compute the roughness transfer due to the interaction between roll and strip surfaces during rolling, a composite Abott curve that combines roll and strip Abott curves is used with an asperity crushing model integrated with a rolling model. This enables simulating two roughness transfer mechanisms in the roll bite: the strip asperity crushing mechanism by roll roughness and the strip asperity ploughing mechanism due to roll-strip interfacial sliding speed. The model shows the importance of considering the two mechanisms to predict roughness transfer correctly when strip elongation is high, typically a few percent, and roll bite friction is low. In these conditions, the forward slip at the exit of the roll bite tends to erode strip roughness significantly and decrease considerably the peak density on the strip. For lower elongation levels (~1%) and high roll bite friction, the ploughing mechanism becomes negligible and roughness transfer is controlled by the crushing mechanism only. With these two mechanisms, the model reasonably predicts the evolution of average roughness and peak density over a wide range of temper rolling conditions (new/worn work rolls, hard/soft grades, various elongations), but skewness is more difficult to predict for some trials.

Oct 1, 2019

By Noan Tonini SImonassi

A indústria da construção civil e a que mais absorve mão-de-obra no Brasil, com uma significativa participação no PIB, da ordem de 15%. Em contrapartida e ainda apontada como uma grande geradora de resíduos, que variam em função da matéria-prima utilizada e também da mão-de-obra desqualificada. Dentro desta faixa de mercado, o número de edificações que empregam blocos cerâmicos como elementos de vedação ou estruturais, é bastante expressivo, principalmente pela facilidade de produção destes artefatos no Brasil. Neste trabalho buscou-se avaliar a influência dos blocos cerâmicos, quando utilizados fora de norma, em uma determinada edificação, formada por um prédio residencial multifamiliar que estava sendo construído no município de Itaperuna, RJ e se encontrava nas etapas construtivas de vedação e revestimento, cujas perdas e causas associadas foram identificadas e quantificadas.

Oct 30, 2017