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By G. H. Gronhovd

This is the final report on a research program to develop a pilot plant gasifier for slagging gasification of lignite at high pressures and to obtain process data under various operating conditions. An operable pilot plant was developed, and the test results show that lignite is well suited for the process. Tests were run at pressures from 80 to 400 psig, and the results indicated that pressure had little effect on gas composition or the material requirements per unit gas produced. Gas production rates as high as 26,000 scfh/sq ft of reactor area were obtained at 300 psig, but limitations on auxiliary equipment prevented full-capacity operation at 400 prig. In several tests lignite having a 37-percent moisture content and 2,500° F ash-fusion temperature was successfully gasified. Refractory materials were found to have a short life in contact with high-temperature slag, and a water-cooled taphole was developed. Exploratory tests with coking coal were unsuccessful.

Jan 1, 1970

By Irving Hartmann, Edward Thomas

"INTRODUCTION Adoption of rubber-tire shuttle cars underground in conjunction with mobile coal-loading machines has introduced new problems in the control of dust on mine roadways. Where this type of loading and transportation is used, development and extraction are generally rapid, with the result that much coal is spilled from the shuttle cars during normal operation, Coal in the roadways from this source and from sloughing of the ribs is ground to fine dust by the wheels of the 'shuttle cars and by the treads of the loading and mining machines. The coal dust usually is somewhat contaminated by pulverized rock, and the mixture could not be loaded with the run-of-mine coal without undue contamination of the product even if it were cleaned up promptly.The presence of large quantities of fine, loose dust, which is constantly stirred up and kept in suspension in air by the traffic, constitutes a grave explosion hazard, reduces visibility along the roadways, and is physiologically harmful to the workmen who breathe the air. From the operating standpoint the loose material is undesirable along the roadways because it provides poor traction for the trucks and thereby increases wear and power consumption. The dust-explosion hazard could be eliminated or reduced by frequent application of sufficient rock dust on the roadbed; but this would not remedy the other difficulties, and in fact it might intensify them. Where practicable, the most direct and effective safety measure is to clean up and remove promptly all dust that forms and settles on the roadways. Unfortunately, in many cases this procedure is not feasible. A third Suggested remedy is to prevent dispersal of the dust into the air and to promote its consolidation on the floor by wetting the dust particles.During the past few years several mines have used calcium chloride on shuttle-car roadways to allay the dust thereon. When exposed to the' humid atmosphere of the mine this salt absorbs Moisture from the air and deliquesces, and in this way wets the dust on the floor of the roadway. In a survey conducted in coal mines in southern West Virginia and in eastern Kentucky where calcium chloride has been in use, somewhat conflicting re- ports were received regarding the merits of the application, and several operators have abandoned the practice either because of actual or assumed disadvantages. The purpose of the study described in this report was to collect and correlate evidence and, on the basis of experimental data obtained in the field and in laboratory tests, to present a clearer picture of the factors involved in the allaying of dust by use of salts."

Sep 1, 1945

By W. A. Grosh

In 1951 the Federal Bureau of Mines became interested in the reports of copper-nickel mineralization in northern Minnesota. Several outcrops on the north side of the Duluth gabbro in the Kawishiwi River area were sampled by the Federal Bureau of Mines and George M. Schwartz of the Minnesota Geological Survey. Because these samples showed appreciable amounts of copper and nickel, a 100-pound sample of an un-altered outcrop was obtained for metallurgical testing. Results from this preliminary work were all favorable; therefore, in the fall of 1953 the Bureau of Mines diamond-drilled three holes near the outcrop of the con-tact between the Duluth gabbro and the Algoma granite. A total of 686 feet of NX size hole was drilled, and 100 percent of the core was recovered. Each hole intersected the contact, and the strike and dip for that locality were established. The core was split, and half was used for analyses and further metallurgical tests; the remainder was retained for permanent record in the Bureau of Mines core-storage warehouse.

Jan 1, 1955

By John P. Capp

The feasibility of simultaneously burning several paths through a coalbed to develop a multiple path underground gasification system was investigated by the Bureau of Mines during two experiments, Boreholes were drilled through the overburden and into the coal and arranged in a circle approximately 50 feet from a central borehole. In the first experiment, in an area which had previously been hydraulically fractured,5 air was injected at the center borehole. The coal was ignited at the other boreholes and the fire fronts traveled toward the center, counter to the flow of air, to backward burn paths through the coalbed. Two paths were linked during the first 5 days of operation. The outlets of these two paths were throttled and air pressure was increased to maintain the flow of air, but no other linkages were made. Fourteen days after the two linkages these two paths were opened and gasification was carried on for 10 days, but with only moderate success. In an effort to overcome operating difficulties air was injected at the peripheral boreholes, and the gases were drawn off at the center borehole. Reversed flow operations continued for 12 days and two more paths linked. The heating value of the gas generally was higher than 100 British thermal units per standard cubic foot (B.t.u. per std. c.f.). Because only four of seven paths linked, however, the entire system could not be evaluated with respect to product-gas output and recovery of energy.

Jan 1, 1961

By N. A. Eilertsen

Eastern Aroostook County, Maine, contains an enormous tonnage of manganese widely distributed in manganiferous sedimentary beds composed of hematitic shale, hematitic slate, and laminated siliceous carbonate rock. The bedded deposits range in thickness from several feet to over 150 feet. Manganese minerals that occur as silicates and carbonate are so minute that they cannot be concentrated by present methods of ore dressing. From a hydrometallurgical standpoint, the deposits can best be classified by amenability to acid leaching. The deposits of Aroostook County are in three geographical groups (see fig. l), designated as the northern, central, and southern districts. At least 13 deposits are known to occur in the latter district, which covers an Ewes about 8 miles wide and 15 miles long. The Littleton Ridge deposit, on the northern boundary of the southern district, previously examined by geologists from the State and Federal Geological Surveys on the farms of Donald H. Haggerty and David A. Abernethy, was pointed out in reports as being possibly the richest and largest in the southern district. The Bureau of Mines sampled this deposit by surface trenching and diamond drilling from May 1 to September 30, 1951. A total of 23 trenches was bulldozed, aggregating 5,355 linear feet, of which 8 trenches were sampled by cutting 185 channel samples over a linear distance of 1,820 feet.

Jan 1, 1955

By C. J. Wilhelm

The disposal of brines produced with crude petroleum and natural gas has been a long-continuing problem to oil and gas operators as well as to farmers and stock-raisers in the vicinity of producing fields. An impartial appraisal of conditions pertaining to the problem of brine disposal leads to the conclusion that study of the technical consideration, with proper weight given to the economic and social factors, is the most desirable approach to this problem. Brine disposal is a problem of such magnitude in certain areas in the State of Kansas that in August 1934 a cooperative agreement was made between the Kansas State Board of Health and the U. S. Bureau of Mines for a cooperative technical study of methods of brine disposal.

Jan 1, 1935

By Homer J. Ballinger

The Krueger property was examined by an engineer of the Bureau of Mines in September 1943. The records of 23 old drill holes indicated an appreciable body of ore without delimiting the deposit. It appeared that additional drilling might increase this reserve sufficiently to justify mining. Accordingly, the Bureau of Mines drilled 5 churn-drill holes and 19 diamond-drill holes on the Krueger tract. The last of these holes concluding the Bureau?s project was completed in April 1947.

Jan 1, 1948

By Harold M. Smith

The data in this report were prepared to show how Bureau of Mines routine crude oil analyses could be used to evaluate crude oils in terms of common commercial products . The use of Bureau of Mines routine analyses to determine hydrocarbon - type relationships for the gasoline and gas - oil fractions is demonstrated . For this purpose the correlation index , the aromatic profile and the naphthene profile are used to establish reasonably acceptable values for hydrocarbontype relationships . The derivation and meaning of these indications are discussed . These analytical interpretations are applied to a group of high - sulfur crude oils from the Near East , the Permian basin of West Texas , Venezuela , Colombia , California , and other locations , and the resultant data for gasoline , gas oils , lubricating oils , and asphalt are compared by appropriate tables and graphs . Because the Near East crude oils contain higher quantities of paraffins in the gasoline and gas oil ranges , they will yield good , lowsolvency solvents and good kerosine , jet fuel , and diesel fuels , but straightrun gasoline of inferior quality compared to similar products from either West Texas or Venezuelan high - sulfur oils . The Near East oils also should be good sources of lubricating stock . However , when used as stock for catalytic cracking or reforming , the Near East oils suffer by comparison because they are deficient in naphthenes .

Jan 1, 1964

By C. C. Blade

"This report on the properties of motor fuels sold through service stations ni the Unietd States is a continuation of a series of reports made in accordance with a cooperating agreement between the Coordinating Fuel Research (CRF) Committee of the Coordinating Research Council (CRC)3/ and the Bureau of Mines of the United States Department of the Interior. The first of these reports presented data on motor gasolines sold during the winter of 1935-36.4/ Further reports were issued describing motor gasolines sold during the succeeding summers and winters to and including the summer of 1941.4/ No reports were made on motor gasolines sold during the winter of 1941-42 and during the summer of 1942. However, starting with the winter of 1942-43, the semiannual reports were resumed.4/The present report presents analytical data for 1,381 samples, representing the products of approximately 75 companies. Most of the samples represented in this report were secured during July and the first half of August, 1945. As in previous surveys, the companies covered by the survey include both large and small suppliers. Conforming to former reports, the data cover three groups of samples – regular-price, premium-price, and third-grade gasolines.As the number of analyses submitted for samples of third-grade gasoline are not considered adequate to represent this type of motor fuel, data for the analyses have not been averaged, but the individual items are tabulated. The number of samples, items and brands comprising each group is as follows: Regular-price, 733 samples, 229 items, and 57 brands; premium-price, 504 samples, 197 items, and 56 brands; third-grade, 84 samples, 28 items and 12 brands. The meanings of these terms as sued in the surveys are as follows:"

Jan 1, 1946

By C. J. Wilhelm

The disposal of brines produced with crude petroleum and natural gas has been a long-continuing problem to oil and gas operators as well as to farmers and stock-raisers in the vicinity of producing fields. .An impartial appraisal of conditions pertaining to the problem of brine disposal lead to the conclusion that study of the technical considerations, with proper weight given to the economic and social factors, is the most desirable approach to this problem . Brine disposal is a problem of such magnitude 1n certain areas in the State of Kansas that in August 1934 a cooperative agreement w s made between the Kansas State Board of Health and the U. S. Bureau of Mines for a cooperative technical study of methods of brine disposal.

Jan 1, 1935

The objectives of this research were to examine and to laboratory performance of several brands of rigid urethane een brands, produced by 13 manufacturers, were examined. was performed in a laboratory under controlled conditions. document the foam. Eight-All testing Preliminary laboratory tests included flame spread evaluations, flame penetration, ignition temperatures, air permeability, and adhesion. Having established arbitrary cutoff values, the original 18 candidates were narrowed to 8. More specialized tests followed. The effects of water immersion and dry aging on flame spread performance and other physical properties were then examined. This Bureau of Mines report was written to provide information for those concerned with using rigid urethane foam as a sealant. Its intent is to describe the various laboratory evaluations performed and to delineate the performance of each candidate. This report neither promotes nor discourages the use of rigid urethane foams. It presents results that will enable those responsible for using or enforcing the use of rigid urethane foams in underground mines to make informed decisions.

Jan 1, 1985

By H. Kenworthy

The objective of this research was to develop methods and determine conditions under which metallic sulfides with lower boiling points than sphalerite may be removed from zinc sulfide concentrates by volatilization. A higher percentage of extraction of lead, cadmium, and germanium than is common in current practice was sought. The investigation, conducted by the Metallurgical Branch of the Minerals Technology Division, Region VI, showed that, under proper conditions, it is possible to remove over 90 percent of the lead, cadmium and germanium as an enriched sublimate. The uses of lead, and cadmium to a lesser extent, are well-known. Although germanium was discovered in 1886 by C. Winkler, commercial use has been achieved only in recent years. The amount consumed per manufacturer unit is so small that the price of germanium may still be quoted by the gram. The electronic industries have been the chief consumer of this semiconductor. Germanium is sold largely to the fabricator as a dioxide for reduction to metal and subsequent processing into wafers for use in diode and triode electronic tubes. Extensive research at Purdue University during World War II led to the first practical use of germanium.

Jan 1, 1952

By H. G. Miller

The success of any project in which gas is injected into oil-producing sands to increase the current rate or the economic ultimate production of oil or in which surplus gas from oil-producing operations is stored temporarily in reservoir sands that have been wholly or partly depleted of their producible oil depends mainly upon an understanding of the underground movements of oil, water, and injected gas and the ability to control their speed and direction of migration through the reservoir sends. Many operators believe that injected gas always travels up the structure and drives oil to wells structurally higher than the injection wells, because the specific gravity of the injected gas is less than that of the fluid substances in the formation. Consequently, many injection wells are located on the flanks of oil-bearing structures with the idea of utilizing the energy of the injected gas to drive the oil to producing wells higher on the structure. It is true, under certain conditions of pressure and fluid depletion of the reservoir sands that injected gas will move in an up-structure direction, but the theory that injected gas always moves up the structure is based on an erroneous conception of the laws that pertain to the expansion of gases. By definition, "a gas is distinguished by its property of infinite expansion and is limited in volume only by the walls of the vessel which contains it." The expansion of gas that is injected into reservoir sands also is limited by "walls" that surround the space influenced by the injected gas. The walls of the majority of undrilled or virgin oil-bearing reservoirs in California are the impervious shales overlying and underlying the productive strata and the "dams" or effective barriers of edge water around the rims of the reservoirs. When gas is injected into the sands of a producing reservoir, regardless of the location of the injection well on the structure or the degree of depletion of oil from the sands, one of the walls which confine the gas in the structure about the injection well is fluid. This wall will be edge water in a nearly depleted reservoir, where the drainage cones or regions of reduced pressure about injection and producing wells intersect; and, where there is no interference of drainage cones and the injection well is structurally above the edge water, the wall will be oil. In some producing reservoirs bottom water may be the lower wall of the space that confines the gas about injection wells, but the effect of bottom water on limiting the expansion of gas is the same as if the water was not present and impervious formation separated the producing from the underlying nonproducing strata. Therefore, since compressed gas always seeks regions of reduced pressure and its final volume is limited only by formation and fluid barriers and since the force exerted by the gas under pressure is equal in all directions, the course of migration of injected gas in reservoir sands in California and the effect of the gas pressure on fluid movement does not depend necessarily upon the up-structure location of low-pressure regions.

Jan 1, 1932

The Florida phosphate industry, which supplies about three-quarters of the domestic phosphate fertilizer, produces tremendous volumes of phosphatic clay wastes (slimes). These clays retain a high percentage of water for extended periods of time. The clays also pose an environmental hazard because the disposal technique involves aboveground storage behind earthen dams. Although much research has been undertaken by numerous organizations to dewater slime, no completely satisfactory solution has been developed. In June 1972, a cooperative effort by the Federal Bureau of Mines and the Florida phosphate mining industry was initiated to develop a solution for dewatering the Florida phosphatic slimes. This report discusses various aspects of the slimes problem, reviews past research, makes recommendations for future research, and includes a bibliography of references and patents dealing with the subject.

Jan 1, 1975

By J. Kruttschnitt

This paper, describing milling practice at Mount Ira Minis, is one of a series covering milling methods and cost that is being published by the Bureau of Mines, United States Department of the Interior. The Mount Isa concentrator began operations in day 1931 by treating a mixture of oxidized and sulfide ores. Since March 1935 only sulfide ores have been milled; this change involved major alterations to the flow sheet. The maximum capacity on mixed oxide and sulfide ores was 2,650 tons per day; the present capacity is approximately 1,880 tons of sulfide ore per day. The installation of additional crushing, grinding, and flotation equipment when completed early in 1939 will increase the maximum capacity of the concentrator to 2,240 tons of sulfide ore daily.

Jan 1, 1939

By A. B. Hooker

Many attempts have been made to develop methane detectors that will be safer and more accurate than the flame safety lamps used to detect methane in mines. The development has taken two general forms, namely: (1) Methane detectors, in which the evidence of methane depends entirely upon changes in the appearance of the detecting element, such as a flame or filament; (2) indicating methane detectors or those equipped with scales upon which the approximate percentage is definitely indicated. As an aid in the development of suitable detectors, the United States Bureau of Mines has assembled and published in its Schedule 8B a set of minimum requirements which tests and experience have shown desirable for methane detectors. Any manufacturer may submit his detector for inspection and tests leading to approval under this schedule.

Jan 1, 1930

By E. P. Carman

This report is the 19th in a series summarizing Bureau of Mines research and technologic work on coal and related investigations. The first 17 reports covered fiscal years; however, the 18th report3/ covered the 18 months from July 1, 1952, to December 31, 1953, to permit the publication of this and subsequent reports on a calendar-year basis. Most of the material in this report relates to publications by Bureau authors issued during the reporting period. Some work is referred to on which the results have not yet been published or may not be published for security or other reasons. In a few instances publications are mentioned that were issued before the reporting period but were not included in previous reports. Further details on the published work described herein may be found in the publications cited in the footnotes. Research and technologic work on coal by the Bureau is directed toward developing and encouraging increased conservation of coal resources through safer and more efficient mining, preparation, and utilization. Significant advances were made during the year in these fields, particularly in coal-mine safety and in preparation and utilization of the various ranks of coals.

Jan 1, 1956

By M. C. Malamphy

A general description of the activities and results of bauxite investigation by the Bureau of Mines at its bauxite project in Saline and Pulaski Counties, Ark., has been given in Report of Investigations 4251. The factual data obtained during the project are reported in a series of Reports of Investigation beginning with No. 4251, of which this is the thirteenth. The data are accompanied by maps showing the location of holes drilled and the deposits developed. Each area upon which work was done is reported by half townships. Each bauxite deposit investigated was assigned a name and a number for ready reference and identification, and its location and name are shown on the appropriate half-township map. The description of each half township is followed by a description of each deposit developed in that half township. The 14 half-township maps and 77 detail maps of the bauxite deposits in this series of reports give the locations and numbers of all the holes drilled on the project, except the deep holes drilled to test the geophysical anomalies. The locations of those holes show on figure 13 in volume 1. The description of the deposits developed is followed by complete detailed logs of the drill holes. Many of the widely spaced exploratory holes did not discover bauxite of minable thickness and grade. The pertinent information obtained from the widely spaced exploratory drill holes has been summarized and tabulated and a table for each half township is given with the discussion covering that area.

Jan 1, 1948

By Paul S. Goodman

This report examines the effectiveness of bonus plans in the coal industry. The analysis uses theoretical, literature review and empirical approaches to determine the impact of bonus plans on safety and productivity in underground coal mines. The basic finding is that the modal bonus plan in underground coal mining does not have a major impact on productivity and safety indicators. The design of the plan, or organizational factors, and the process of introducing the plan all contribute to its relative ineffectiveness. Strategies and options for designing effective plans are presented.

Jan 1, 1987

By Lloyd Williams

1. The investigation shows that the bed identified as Wilder in this report is the only bed in Overton County that has produced commercial coal and is the only bed in which coal reserves were estimated for this report. Three other coal horizons were recognized but lacked enough data for reserve estimates. 2. Known measured and indicated reserves of coal, based on a minimum bed thickness of 14 inches and on 1,800 tons per acre-foot of coal in place, are estimated to be 19 million short tons, as of January 1, 1953. Of this total, 10 million tons represents coal 28 inches and more thick. Areas of the Wilder bed were omitted from the estimate because available data relative to the bed characteristics were too meager for making an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these areas, such reserves should be added to the total estimated reserves.

Jan 1, 1955