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By M. Reza Bateni, M. Zandrahimi, J. A. Szpunar

Titanium aluminides and nickel aluminides offer the potentials, as coating materials, for high temperature and aerospace applications. In this research, attempt has been made to develop Al-Ti and Ni-Al intermetallic compound coatings on the surface of Inconel 738. The coatings applied through pack cementation and simultaneous diffusion annealing processes. Scanning-electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDAX) and grazing angle X-ray diffraction were used for evaluating of coating structure. It was demonstrated that the pack cementation technique could be used to develop TiAl3 and AlNi intermetallic compounds coating on Inconel 738 substrate. When pack cementation technique is based on a halide-activated pack with aluminum and titanium powders, the coating consists of TiAl3 intermetallic compound phase. Whereas, by pack aluminization of Inconel 738, the coating consists of AlNi intermetallic compound phase.

Jan 1, 2004

By J. Bourgeault

Modem civilization is indebted to that most ancient of the skilled crafts - the art of stone working, as the one consistent means whereby the dim un-recorded past has conveyed to our modem schools of science volumns of facts, written in characters of imperishable stone. Although left, centuries ago, to ruin and decay, architectural examples of the ancient building crafts still remain to the glory of the old master-builders, whose accomplishments in that remote age continue to influence and inspire their modem successors. Present-day architects and builders will leave to posterity just as faithful a record of our modes of living and of the methods now adopted for protection, as if it had been made by written word; and our craftsmen have profited greatly, in meeting modem requirements, by taking advantage of the indurance and utility of stone. Stone in all ages and stages of the world's civilization and development has been the material chosen by the masterbuilder, the one material possessing qualities that render it most desirable in affecting the artistic ideals of each period. It perfects the science of architecture through its durability and thus renders possible the study of man's workmanship in stone throughout periods of civilization of which we have no specific written account. Other materials have been used for the construction of man's habitations, but none have withstood the test of time, nor have established the credit of designer and builder so well as stone. _All other materials fall into ruin and decay, leaving neither mark nor monument for the enlightenment of mankind.

Jan 1, 1925

By Shamia Hoque, Charles Q. Jia

Smelter slags contain valuable metals such as Co, Ni and Cu in proportions of less than 1 wt% along with about 40 wt% of Fe and 15 wt% of Si. Although aqueous SO2 is a versatile lixiviant for transition metals, dissolving the slag in aqueous SO2 produces solutions in which Co and Ni concentrations are lower than that of Fe due to the low metal/ Fe ratio in the slag. To develop the options for increasing Co and Ni concentrations the solubility of slag in aqueous SO2 was studied experimentally and theoretically using OLI, a software package for simulating electrolytes chemistry. The modeling results correlated well with experimental results. The model suggested that the species dominating the system was FeSO3, which would precipitate out as FeSO3.3H2O when the concentration of Fe+2 reached 1.22 molal and the concentration of S032- was beyond 1.4 molal. In the experiments the influence of pH and solids loading were studied. The leach solution obtained after dissolution of slag at 50% solids loading had a pH of 1.85. On raising the pH to 3, precipitation occurred. Analysis of the solution collected after the addition of alkali showed over 50% reduction of Fe, Co and Ni. XRD analysis revealed the precipitate to be of amorphous nature due to the silica present. The analysis confirmed that the precipitate was mainly FeSO3.3H2O. The paper also discusses the potential impact of the slag on the environment.

Jan 1, 2004

By T. Maruyama

Tamano Refinery started its operation in 1972 with the cathode production capacity of 84,000 tons per year. After several expansions, the production capacity increased to 228,000 tons per year in 2001. In this paper, we are introducing our next expansion projects starting October 2006. The project expands the production capacity of cathode from 228,000 tons to 260,000 tons per year. The main modification of this project is the conversion to the ISA process and the installation of additional seventy-two cells in the No.2 Tankhouse. The No.1 Tankhouse remains the same, using the conventional process. Half of our starting sheet cells are converted to commercial cells. The other expansions are to enlarge our purification plant. And the incidental facilities are enlarged, for example, circulation tanks, heat exchangers, filtration system, etc. Finally, this paper describes those improvements to our refinery performance and preparing for future expansions.

Jan 1, 2007

By M. Huang

Electrodeless conductivity was employed to investigate the feasibility of continuous on-line monitoring of the free acidity of sulphate and/or chloride solutions of Cu and other base metals from various hydrometallurgical processes. These solutions were measured with both commercial and experimental electrodeless conductivity sensors from 15 to 250°C. It was confirmed that hydrogen ion has the greatest impact on conductivity by carrying the bulk of the current because it is the most mobile ion. In combination with a solution speciation analysis the conductivity sensor can be calibrated to account for the contribution of Cu electrolytes as well other dissolved salts allowing fast and accurate on-line measurement of free acid. The sensor was tested at both lab and pilot scale with very good performance. The average difference between the measured and the titrated acid concentration was less than 5%, which is excellent for industrial applications.

Jan 1, 2007

By O. -J. Siljan

"Refractory materials are an integral part of aluminium production. One special feature of aluminium making is the prominent role of sodium in all parts of the production process. This presence of sodium inflicts stresses on the refractory materials through reactions and may cause severe damages to the refractory linings. The present paper address possible reactions between sodium and refractories in anode bake furnaces, electrolytic pots and casting furnaces. The discussions presented in the paper points to the importance of selecting materials with excellent alkali resistance in all parts of the aluminium making process, although alkali resistance is not the sole parameter to determine refractory life-time. ""Acid"", i.e. silica-rich alumino-silicate refractories are shown to be the best materials for aluminium electrolysis cell potlinings, whereas high- alumina refractories based on minerals like andalusite seems to be the preferred choice for anode bake furnaces as well as cast house furnaces."

Jan 1, 2004

By F. King, R. Sutherby, J. Been

With thousands of kilometers of buried oil and gas pipelines throughout the country, carrying flammable, high-energy hydrocarbons, the integrity and safety of this transportation and distribution network are paramount. The pipeline industry has the primary responsibility for pipeline safety and has in many ways taken the lead in dealing with safety issues. Over recent years, regulatory demands have increased, requiring operators to comprehensively evaluate their pipelines through indirect and direct inspections and to manage risk through integrity programs. Mechanistic and correlative models have been developed that assist in the prediction of pipeline integrity and the determination of reassessment intervals. These lifetime prediction models are based on decades of laboratory research as well as pipeline operating data, material data, and field monitoring data pertaining to soil conditions and CP. An overview is presented of an integrated approach towards the development of such models for the evaluation of external cracking and corrosion of transmission lines.

Jan 1, 2005

By Hani Henein

Most metals and alloys processed undergo a solidification processing step. Increasingly, there is a growing number of solidification processing routes that involve rapid solidification of the alloy. These include strip casting, high pressure die casting, 3D printing, and atomization for the production of powders or spray formed parts. By contrast, there are few experimental techniques developed to study the solidification path of alloys during rapid solidification. Amongst these laser melting and solidification, Electromagnetic Levitation (EML) and Impulse Atomization (IA) are the most prominent. Of relevance is the formulation of the solidification path of an alloy and the resultant identification and quantification of metastable phases and their relationship to processing conditions. This typically involves the understanding of the interplay between undercooling and cooling rate for the various phases that form. This presentation will outline some of the methodologies developed to quantify phase fractions and their solidification path as a function of processing conditions using EML and IA.

Jan 1, 2016

By J. E. Nesset

The past 50 years have been a golden era, not just for the CMP but also for the development and success of Canadian technologies in the field of mineral processing. The CMP has played a critical role of technology transfer agent, and the success of these technologies is also linked to the success of the CMP itself. The presentation will cover, in brief, the growth of the CMP from its origins as the Canadian Gold Metallurgists in 1964, with some 39 attendees, to the present day when the annual meeting sees 500 and more from a dozen countries. Also covered will be selected technology success stories from the 50th anniversary volume to be given to all delegates ‘Canadian Contributions to Mineral Processing Technology 1968-2018’. The volume itself highlights some 40 technologies that have been divided into five categories; process water treatment and minesite environment, technology innovations, innovations in operations, technology providers and university contributions. Some international perspectives will also be shared.

Jan 1, 2018

By Y. C. Kim

This paper discusses Air Liquide's patented SPALTM (Surface Protection Air Liquide) technology and process for the inerting of coreless induction furnaces using cryogenic liquid gas. Air Liquide Canada Inc., in collaboration with Riverside Brass and Aluminum Foundry Limited (Riverside Brass), conducted plant trials to demonstrate the applicability of the SPALTM technology for copper-based alloys. Results showed that with SPALTM, Riverside Brass benefited from a significant increase in metal yield as the level of dross formation was drastically reduced. Together with the many other benefits of this technology, SPALTM demonstrated to be a non-negligible cost-effective solution to reduce metal production costs. In an effort to optimize the argon flow, different flow rates were used and the oxygen level above the metal bath was measured to pinpoint optimal flow. The results of metal yield, charge mix, dross formation, and melt temperature are compared with and without argon. The metal yield improvements are dramatic and calculated net savings are presented hereunder.

Jan 1, 2007

By R. A. L. Drew, J. P. Immarigeon, F. Jalilian, M. Jahazi

In the present work TLP bonding of Inconel 617 is investigated. The influence of the main processing parameters i.e. time and thickness of the interlayer were studied with optical and scanning electron microscopy. Boron containing interlayers with two different thicknesses were used and the influence of various holding times from 5 min to 24 hours on the microstructure of the bond region was investigated. The results indicated that, for the testing temperature of 1065°C and holding times above 2 hours with an interlayer of 25.4 microns thick no liquid phase was observed. The same phenomenon occurred only after 6 hours for a 76.2 microns thick interlayer. Precipitate growth started at grain boundaries and continued inside the grains. The composition, size and morphology of the precipitates were studied using electron microprobe analysis. No noticeable changes were observed in the grain size of the base metal with increasing holding times.

Jan 1, 2004

By W. Beres, Li. J.

The finite element method (FEM) has been applied to investigate the stress fields and deformation of a TiN/Ti-6A1-4V coating/substrate system subjected to nanoindentation. MSC Patran and MSC Marc were used to prepare the three-dimensional finite element models and to perform the simulations of the Vickers nanoindentation experiments. Pure silicon and TiN/Ti-6A1-4V coating/substrate system were analyzed. The properties of the materials were assumed to be homogeneous and isotropic with a linear hardening behavior. The reverse method was used to extract material properties, such as the yield stress and strain hardening coefficient, from the numerical results by comparing the simulated indentation load vs. penetration depth (P-h) curves with those obtained experimentally. Both non-linear elastic and non-linear elastic-plastic analyses were carried out for the coating/substrate system. The results are given for four different coating thicknesses.

Jan 1, 2004

By B. T. Lu, J. L. Luo, H. X. Guo

This paper investigated the synergistic effect in the slurry-erosion process of carbon steel. In line with the mechanisms of material loss, the synergism due to interaction of erosion and corrosion was divided into the corrosion enhanced by erosion and erosion enhanced by corrosion. The erosion-corrosion tests were conducted with A1045 steel in slurries containing silica sand. Experimental results showed that the rotating of the sample in corrosive media raised both OCP and corrosion rate, but the impingement of solid particles did not affect the corrosion current significantly. In the quiescent solutions, the Faraday's law gave a good prediction for the weight loss caused by corrosion but for rotating samples, the weight loss experimentally measured was virtually greater than that predicted by the Faraday's law, indicating that the corrosion-enhanced erosion could occur in corrosive fluids in absence of solid particles. A half-logarithm relationship was observed between the weight loss due to corrosion-enhanced erosion and the anodic current density.

Jan 1, 2004

By R. Mohamad, J. Asfahani

Abstract - Radioactive characteristics of pits drilled in the Al-Sharquieh mine while prospecting for recent phosphatic resources have been investigated. The results indicate that phosphatic layers are characterized generally by high radioactive intensities (more than 800 c.p.s). The lithological section in the study area is very complex sedimentologically, and characterized by high faciological variation in all directions. The Schlumberger geo-electrical configuration with fine separation of AB/2 was successfully applied to determine lithological boundaries, and the resistivities of the layers of the lithological section, especially for thin layers. It was shown that the phosphatic layer resistivities increase or decrease as a function of associated material. As a result, two types of phosphatic layers have been geo-electrically distinguished. The first is characterized by high resistivity and relatively low radioactivity, which could be related to the rock phosphatic layers. The second is characterized by low resistivities and high radioactivity, which could be related to the sandy phosphatic layers.

Jan 1, 2000

By Steven Aiken

The East Boulder Mine located in Montana, U.S.A. utilizes snowmaking to assist with mine water treatment for nitrogen removal. Nitrogen species, including ammonia, are common contaminants in mine water from underground mining operations. Snowmaking provides secondary treatment of nitrogen during the winter due to the chemical and physical processes that occur during snowmaking, in the snow pack and in the snowmelt. The primary processes include atomization, evaporation, sublimation and volatilization. The snowmakers also provide secondary treatment for nitrogen removal when used as evaporators and/or land application units during the summer. In 2002, the snowmaking process was successful at reducing total nitrogen in the mine water by up to 87%. If additional losses due to soil and root zone processes are included, total nitrogen reduction would increase to between 87 and 97%. Snowmaking is an effective nitrogen reducing treatment method during the winter when other treatment methods such as land application cannot be used.

May 1, 2004

By K. Madi, E. Yeugo Fogaing, S. Forest, M. Boussuge, L. Massard, M. Huger, Gaultm C.

This study has been carried out owing to the French research program PROMETHEREF, which aims to improve the knowledge of thermal and mechanical properties of industrial refractories at high temperature. In this frame, this paper relates a collaborative study between Saint-Gobain CREE, R&D Centre for Saint-Gobain Ceramics & Plastics in Europe (Cavaillon), the Materials Center P.M. Fourt of Ecole des Mines de Paris (Evry) and the Research Group on Heterogeneous Materials (GEMH) of ENSCI (Limoges). Data collected at high temperatures by using different means (bending tests, ultrasonic measurements,...) allows the identification of the high temperature behavior of two fused cast materials, produced by Saint-Gobain group for the glass manufacturing industry. The results emphasize the importance of the transformation of zirconia and of the viscosity of the glassy intergranular phase on the mechanical behavior. Damage under the form of microcracking caused by thermal expansion mismatch between the phases is also observed during cooling down at low temperature, when the material is elastic.

Jan 1, 2004

By Steve Dismuke, Tom Diment

In December 1994, Polaris decided to investigate the use of cemented rockfill (CRF) to supplement the existing frozen rockfill system. Extraction plans for the remaining ore reserves required a backfill with superior stiffness proper-ties and capable of developing high early strengths. Although CRF has been used success-fully at several mining operations, there was the additional challenge of making a reliable cemented product in permafrost conditions. There was also the challenge of procuring and storing one year’s supply (13 000 tonnes) of bulk cement. By the spring of 1995, following three months of research, test work and process design, the decision was made to proceed with the procurement and construction of a 3000 tpd batch plant. An ambitious completion date of December 1995 was set. Team Manufacturing of Langley, British Columbia was awarded the contract, complete with the considerable task of having the batch plant fabricated and ready for sea lift shipment by August, 1995.

Jan 1, 1996

By R. Anthony Hodge

Who/what is ?community?? What are most communities interested in, what do they care about? What has happened in the past? What is happening today? What is hoped for tomorrow? What are the lessons and keys to success?

May 1, 2006

By M. A. Keogh

This paper reviews the physical properties that make low-density polyethylene the most practical and economical material for launder• fabrication in the majority of mine and mill applications. The basic design features and use of other launcher• materials are also discussed.

Jan 1, 1976

By J. Scalise

The paper covers a wide range of topics relative to filtration for continuous cast copper and aluminum. Subjects include system concepts, filtration concepts, system components, filter types, filter media selection, caster water filtration, coolant disposal, and recommended materials of construction.

Jan 1, 2007