Search Documents

By Osamu Takeda

A decomposition process for PCBs by using basic molten salts as a reaction field was investigated in order to establish a safe, simple and highly efficient decomposition process for polychlorobiphenyls (PCBs). PCB containing chlorine (e.g. 2, 2?, 4, 4?-tetrachlorobiphenyl) dissolved in n-nonane solution was supplied into basic molten salts (NaOH-Na2CO3 or KOH-K2CO3) maintained at 500-700 ?C together with the carrier gas (N2-21% O2) through an injection tube. The injected PCBs in a bubble are decomposed by the reaction with the molten salts and oxygen during rise in the molten salts. The decomposition efficiency of PCBs increased with increasing temperature and was achieved to be higher than 99.995% in a certain condition. From a series of systematic study, the effectiveness of the decomposition process for PCBs by using molten salts was demonstrated.

Jan 1, 2008

By Thomas F. Nederpel

The production of zinc and zinc-aluminum coated strip can be reasonably accomplished on a single operating unit. However, if the hot dip coating line is equip d with only one mo 7 ten metal holding furnace, it is necessary to transfer liquid metal of different chemistries and reintroduce virgin material to obtain the 18" necessary balance of elements in the bath. Dofasco produces Galvanize and Galvalume on a coating line with a sin le liquid metal furnace and has developed not only an efficient liquid metal trans& system but also an effective means of reutilizing the zinc-aluminum mixtures without detrimental quality affects.

Jan 1, 1992

By Migen Dibra

Antitrust and competition laws are designed to protect the free markets and promote competition in order to assure a dynamic and efficient economy and to provide competitive prices for quality products and services. They apply to mergers and acquisitions as well as to joint ventures especially among competitor companies who possess market power and these include collaborations on research and development. If it is determined that these actions are likely to substantially prevent or lessen competition the courts might dissolve, stop, alternate them, etc. Two new factors affect this process today: The role of new technologies and the markets globalization. They both have a considerable effect on the way these laws are interpreted by the courts and on their eventual amendments in order to reflect the new reality. A new applied technology and the globalization separately or together may change the factors that determine how anticompetitive a merger or acquisition between competitors may be and may also serve as a basis for amending the antitrust and competition laws. In this paper, a short review of the recent mergers and acquisitions of various companies has been carried out along with an abridged analysis of the current antitrust and competition laws in USA, Canada and European Union in the view of their capacity to handle the new reality. Some related court decisions are also examined and several examples are given in order to illustrate the influence of new technologies and globalization in interpreting the existing laws and on their amendment possibilities.

Jan 1, 2006

By Yamei Han, Jiang Du, Jinhui Peng, Mengbi Fu, Libo Zhang, Zhengfu Zhang

"A continuously pilot synthesis by microwave-heating was used in preparing the cathode material LiNi113Co113Mn11302 for Li-ion battery, which used Ni1/3Co1/3Mn1/3(0H)2 and LizC03 as raw materials. Decomposition of the raw materials and synthesis of LixNi113Co113Mn11302 would be fmished in single roasting process. In addition, using microwave-heating would reduce the reacting time largely. Furthermore, the yield of LixNi1/3Co1/3Mn1/302 synthetized in single roasting process was 50 kg. Meanwhile, the effects of Li:(Ni+Co+Mn) molar radio (Li:(Ni+Co+Mn)=l.06, 1.075, 1.09, 1.15) was studied in this paper. XRD, SEM and EIS were used in characterizing the cathode material. The results showed that the best Li:(Ni+Co+Mn) molar radio was 1.075. It was found that the LiNi113Co113Mn11302 synthetized with Li:(Ni+Co+Mn)=l.075 had homogenous distribution of particles and ideal layered structure. The galvanostatic charge-discharge(O. l C, 2. 75-4.3V, vs. Lt /Li) tests showed that the initial discharge capacity of the LixNi113Co113Mn11302 was 159.5mAh·g-1, and the discharge capacity was 157.6mAh·g·1after10 cycles.IntroductionRecently, as the cobalt was expensive and the restriction of dynamic power, the commercial cathode Li2Co02 which was expensive, toxic, and high pollution had exposed its defects[1·2l. Since T.Ohzuku[3l first reported the layered LiNi113Co113Mn11302, this material had high reversible capacity and caused the attentions of researchers[4l. Its reversible capacity was l 60mAh/g and 200mAh/g in the voltage range of 2.75-4.3V[5-61. But for the present, preparing LiNiwCowMnw02 by traditional had lots of disadvantages, such as the long heating time, the high cost and the volatizing of lithium and so on[7-9l. According to these, traditional prepatation wasn't good for sustainable development and energy conservation."

Jan 1, 2013

By K. Twite, K. Mujinga, J-M. Dereydt, P. Louis

"GECAMINES is a large mining concern and the world's leading cobalt producer having some of the richest cobalt deposits in the world. Cobalt is associated in the ore with copper as sulphides and oxides and in some locations with nickel too. Specific hydrometallurgical processes have been developed by GECAMINES which had done an important contribution to the development of the cobalt hydrometallurgy.In the Shituru plant, cobalt is obtained from an unique in-pulp electrolysis process, while in Lullu, cobalt is electrolyzed in a clear acidic solution giving a purer deposit. In the beginning of 1996 Shituru started the treatment of mixed Cu-Co-Ni Shinkolobwe hydrates obtained as by-product of an uranium solvent extraction plant. A typical analysis of this feedstock is: 2% Cu, 8% Co and 4% Ni.The nickel sulfide depolarized cementation process developed previously by GECAMINES was inefficient to treat such a high level of nickel contamination and it was decided to produce alloyed Cobalt-Nickel cathodes in the Shituru tankhouse.As anticipated from laboratory tests as previous studies and publications, a lower Ni/Co in the deposit was obtained compared to the Ni/Co ratio solution, despite the nickel reversible electrochemical potential is somewhat higher than the one of cobalt (-0.25 V vs -0.28 V).In this paper, the process flow-sheet and production data are given. Cobalt alloy with 5 - 20 % Ni was obtained at a production level of 300 t per month. The process developed is a new contribution to cobalt hydrometallurgy."

Jan 1, 1997

By Peter Olubambi, Babatunde Obadele, Oluwagbenga Johnson

"The microstructure and corrosion behaviour of titanium carbide (TiC) reinforced duplex stainless steel matrix surface composites synthesized by laser melt injection technique was investigated. The surface melting operation was conducted using a 4.4 kW CW Nd:YAG laser with laser power of 1.5 kW, scanning speed of 0.4 to 1.0 m/min, beam size of 3 mm and argon shield gas flow rate of 4 L/min. The morphologies and microstructures of the coatings examined using field emission gun scanning electron microscope (FEGSEM) revealed homogeneous distribution of fine precipitates of TiC in the matrix, while X-ray diffraction (XRD) analysis confirm no phase change. TiC addition to the steels significantly increased hardness value to about 547 Hv0.1 but slightly decreased the corrosion resistance of the steels in 3.5% NaCl possibly due to the intergranular carbide coating that prevented chromium from forming continuous passive oxide layers.IntroductionComposite materials evolve from the idea of combining two basically dissimilar materials with different physical and mechanical properties to arrive at a product whose final properties are superior to those of the individual components [1]. Metal matrix composites (MMCs) are receiving much attention and are the focus of intense research and development worldwide for aerospace, automotive and other applications because of their excellent combination of ductility and toughness of the metallic matrix with high hardness and strength of carbides reinforced in the matrix [2]. Surface modification techniques such as laser, thermal spray, plasma spray, chemical vapour deposition have been use to fabricate MMCs. Laser melt injection (LMI) is a surface modification technique known since the 1980s [3] has been used to improve surface properties of metallic alloys such as aluminium, titanium and steels [4-6]. It involves the lateral injection of carbides, ceramics and cermets blown by a gas stream into a liquid metallic pool, created by laser irradiation of the top surface of the base material."

Jan 1, 2012

The presence of clay adversely affects the floatability of copper and molybdenum during processing porphyry copper/molybdenum ores. In addition, reagent consumptions are much higher than when treating clay-free ores. Ores containing kaoline, brammollite, illite and montmorillonite were examined in the laboratory to determine how clay minerals affect the floatability of copper and molybdenum, and to find a possible solution to alleviate the harmful effect of clay slimes. It was demonstrated that the presence of clay mostly affects floatability of coarse and middling particles, and reduces selectivity. The results of the research work showed that there may be several possible ways of reducing the detrimental affects of clay slimes on flotation, some of which include a) use of alternative flowsheets, b) flotation at reduced pulp density, and c) the use of special frothers. The applicability of the findings in plant practice are discussed.

Jan 1, 1999

By L. Katgerman, E. N. Straatsma, Suyitno

"Single-roll strip casting process is studied using computational fluid dynamics which takes into account fluid flow, heat transfer and solidification. The computational model is based on the conservation Jaws of momentum, energy and continuity. Correlation of strip thickness, solidification zone length, and puddle shape on single-roll strip casting of Al-1 %Mn is explored. Feeding pressure and roll speed are investigated. The results show that the··strip thickness slightly increases with pressure, similarly the length of solidification zone. The variations of strip thickness and solidification zone length with roll speed show a sharp decline for strip thickness and slight decline for the length of solidification zone with increasing roll speed. The constraint and free-jet flow have different feature in term of flow field. Severe turbulence is observed on the free-jet flow.IntroductionThe near-net shape casting of strip metals is a demand nowadays. The demand is particularly stimulated by the challenge to become more competitive through enhanced performance. The improvement in the existing processes and new innovative technologies are introduced by the metal industry to gain better product quality, more efficiency in energy consumption, low throughput, yield and operating costs [1-3].There are many advantages that can be obtained by the direct casting of strip. The most prominence is the elimination of hot rolling. Beside that the high rate of heat extraction associated with strip casting offers the possibility of a finer, Jess segregated cast structure. The microstructure will result in the improvement of mechanical properties compared to conventional material, or alternatively the opportunity of using grades of metal outside the normal range for continuous casting.The concept of single-roll strip casting has been difficult to commercialize, because of the complex interactions between fluid flow, solidification, shrinkage, and stress, which lead to serious quality problems. Besides that, the quality and the thickness of the strip are affected by the thermal properties of the strip, roll cooling conditions, roll geometry, and other process parameters. To understand how these parameters affect the strip formation, some researchers have modeled the process [4]."

Jan 1, 2004

By Zhang Jianliang, Zuo Haibin, Gao Bing, Wang Zhe

"As a result of the shortage of coking coal and the quality decrease of coke, it is important to know how to make better use of highly reactive cokes. The co-gasification behavior of highly and lowly reactive coke for blast furnace is investigated. The results show that: In the middle stage of reaction, the weight loss ratio of highly reactive coke reacted together with lowly reactive coke is higher than that of it reacted individually. However, the weight loss ratio of lowly reactive coke is lower. The weight loss ratio of highly and lowly reactive coke is almost the same as that of the weighted average. The scanning electron microscope analysis indicated that the reaction degree of surface and interior of lowly reactive coke is relatively uniform with the reaction time increased. And the reaction degree of surface of highly reactive coke is obviously higher than that of interior.IntroductionIn blast furnace iron making process, coke functions as heat supplier, reducing agent, carburizer and skeleton. With development of blast furnace iron making technology, the skeleton function of coke is becoming more and more important in requirements of large scale furnace and high pulverized coal injection. High reactivity coke is usually produced by cheap coal with bad quality, and is not good for blast furnace process. The reactivity of coke is mainly determined by the coals used, and the resource of good quality coking coal is limited and is non-renewable. In order to fulfill the need of blast furnace, a lot of research have been done to improve coal matching using new kinds of coal to enlarge resource, in which coking coal and fat coal are reduced, whereas low price coal with bad caking property are used to lower the cost, and this would inevitably increase the reactivity of coke [1-4] Blast furnace iron making would still be the main stream for a predicted future, and high reactivity coke would correspondingly be used more and more, so it has great importance to study how to use high reactivity coke in blast furnace."

Jan 1, 2013

By Ronald J. McGregor

An overview or precious metals project development and start-up, which emphasizes the process decision. Logic which determines process flowsheet, project economics, and training required to train new operators for start-up. The process decision required to successfully develop a precious metals project requires a blending of test data, environmental considerations and operations experience. Decisions to use Merrill-Crowe or carbon adsorption/ electrowinning/replating, fixed pad or multi-use pad {in heap leach) are dependent not only on technology but also on ability to train new operators. The market for experienced operators is acutely depleted and almost all new operators will have to be "home grown". Experience from the Brewer project in South Carolina as well as other projects put together in the West will be discussed.

Jan 1, 1989

By Nagahiro Saito, Takashi Nishimura, Takamichi Ichikawa, Akio Fuwa

"Yttria-stabilized zircohia (YSZ) has high potential to be used as solid-oxide fuel cell (SOFC) electrolyte. However, the high efficiency of SOFC has not been yet achieved due to the high internal resistance of bulk electrolyte. The resistance becomes lower with the decrease in the electrolyte thickness. Thus, the decrease in electrolyte thickness leads to lower internal resistance. . The aim of this study is as follows: (a) to prepare the thin films of YSZ by inductively-coupled RF plasma-enhanced metal organic chemical vapor deposition (PEMOCVD) process using Zr(t-OC4H9)4,Y(DPMh and oxygeil, and (b) to reveal the relationship between the structural characterizations and the process parameters.1. IntroductionYttia-stabilized zirconia (YSZ) has, been widely used as not only heat-resistant materials but also the components in automotive oxygen sensors, electrolytes of solid-oxide fuel cell (SOFC)(1)(2) and the buffer layers for the high-temperature superconductor because of its low thermal conductivity, good mechanical properties and high ionic conductivity. However, it is said that the internal resistance of the bulk electrolyte is too high to be appropriate as a solid electrolyte for high-efficient SOFC. The authors believe that the thin YSZ electrolyte can give a high performance to characteristics SOFC, since the internal resistance becomes lower with the decrease of electrolyte thickness. Thus the process technology to prepare YSZ thin films is desirable and must be established.In recent years, the YSZ thin films have been reported by chemical vapor deposition (CVD), thermal CVD using metal chlorides (MC) of ZrCl4 and YC(3)(4), thermal CVD using metal organic compounds (MO)(5)(10) Zr(t-OC4H9)4 and Y(C11H19O2)(11) and plasma-enhanced (PE) CVD using MO. Here, these methods are called MCCVD, MOCVD and PEMOCVD. MCCVD has two disadvantages; a large quantity of chlorinated impurities in deposited films and high processing temperature (> 1273K). This high processing temperature leads to damage of substrates in particular, so the application of this technology is limited. On the other hands, the processing temperature by MOCVD becomes and is lower. Unfortunately, the accurate vapor pressures of these metal organic compounds have not been, known so: that it is difficult to control the composition and the film thickness by MOCVD method well. Moreover, the large amount of carbonic compounds in the films prepared by MOCVD method is produced. However, plasma-effect has been reported to decrease large amount of the carbonic impurities by PEMOCVD. However, PEMOCVD has many reaction parameters in plasma processing; the geometry of experimental apparatus, radio frequency, electronic power input and so on. Thus, the general understanding about the relationship among reaction parameters, the composition and crystal structure of thin deposit film by this method has not yet been established."

Jan 1, 2000

By Merete Tangstad, Lars Klemet Jakobsson

"Slag refining is a promising refining method for boron removal from silicon as a part of a metallurgical route for production of silicon for solar cells. There is, however, limited data on the distribution of impurity elements between silicon and different types of slags. In the present study, the distribution of boron and calcium between silicon and slag were determined at 1600 °C for calcium silicate slags with a CaO/SiC>2 ratio between 0.65 and 1.3. An almost horizontal linear trend was found for the distribution of boron between silicon and slag, and the borate capacity was found to follow the relationln(CB0, ) = 30.8 + 2.96-V (1)where V\s the CaO/SiCh mass ratio within the range of the experiments.IntroductionSolar grade silicon feedstock contributes significantly to the total cost and energy required to make crystalline silicon solar cells. A less expensive and less energy requiring method of solar grade silicon production is therefore needed in order to make crystalline silicon solar cells more viable as an energy source. Silicon is an abundant element and the manufacturing cost of solar grade silicon is therefore mainly determined by costs related to purification of metallurgical grade silicon. The Siemens process is the most common process today, but it is an expensive and highly energy requiring process that gives silicon with a higher purity than is needed for crystalline silicon solar cells. A cheaper and less energy requiring method for production of solar grade silicon can either be achieved by modifying the Siemens process or by using a new production method. Purification of metallurgical grade silicon through a metallurgical route is a promising method that is already in use industrially. It has however proven to be hard to lower the boron content to 0.3 mg/kg or less, which is the requirement for most p-type crystalline silicon solar cell manufacturers. Slag refining is seen as one of the most promising approaches that can be used to bring down the boron content to the required level, but there is not much data on how boron is distributed between silicon and binary calcium silicate slags [1-4]. The distribution of boron between silicon and calcium silicate slags at 1600 °C has been studied in this work, and the obtained data has been used to calculate the borate capacity of binary calcium silicate slags."

Jan 1, 2012

By Zongliang Zhang

Electrowinning is a significant step in metal extraction processes. Because the nature of electrowinning is to reduce metal from its oxidized state, substantial energy consumption accompanies it. Electrowinning processes of different metals have much in common—the deposition of the metal on the cathode and the counter-reaction on the anode. An advanced model was developed that can be applied to a variety of metal electrowinning processes. A model for specific metals can be readily obtained by modifying parameters such as potential, kinetics, and side reactions in the model. The model incorporates mass transfer, gas-liquid flow, electrochemistry, and deposition, making it a comprehensive electrowinning model. The model is applied to copper, nickel, and zinc and verified with the experimental results. In addition, the parameter settings and results of different metals were compared, showing that this model has great versatility and accuracy, thereby making it an efficient and effective research tool.

By Carlos Schvezov, Eliana Agaliotis, Alicia E. Ares, Mario Rosenberger

"The interaction between a solidification front and a spherical particle was modeled and simulated in order to study the phenomenon of ""pushing"". Finite element methods were employed in axisymetric domains. The drag force is calculated from the calculated fluid flow field and the repulsion force is the Lifshitz-Van der Waal force. The thermal field is decoupled from the force field. The model is applied to a metallic matrix containing particles with similar, lower or higher thermal conductivities than the matrix, resulting in planar, convex and concave interface shapes, respectively.The results show that the critical velocities for pushing for concave and convex interfaces are about one order of magnitude larger and one order of magnitude lower than the critical velocity for flat interfaces, respectively. The simulated results were in very good agreement with reported experimental results.IntroductionThe solidification interface of materials containing spherical particles in some cases can push the particle ahead the interface. This phenomenon generally occurs during the solidification of different materials such as, metallic alloys containing native particles, metal matrix composites containing particles or fibers as reinforcements and crystallization of semiconductor, optical, optoelectronic or biological materials. In all cases the interaction strongly determines the distribution of particles and the resulting physical and physic-chemical properties of the resulting material. The phenomenon has been investigated for many years both experimentally and by mathematical modeling [1-21]. The process is complex due to the variety of phenomena involved during pushing. In all cases, the physical problem depends on the properties, nature, and morphology of the interacting media; the particle, melt and solid; and external fields such as gravity, thermal and electromagnetic fields."

Jan 1, 2012

By Michael G. Mayer

Since its invention in 1859 various designs of lead batteries have evolved to meet commercial needs for traction applications and standby power. In recent years major developments have taken place in lead alloys and the chemistry and mechanical design of industrial lead batteries. These are reviewed in relation to their commercial application together with the new type of maintenance free gas re-combination lead-acid batteries which are opening so many new markets for lead.

Jan 1, 1990

By M. C. Flemings, S. B. Brown

"Metallurgy, as all of material science and engineering, rests on the intellectual foundations of processing-structure-property-performance relationships. Today it is widely recognized that processing has been too long neglected and presents exciting opportunities for exploitation. New processes, many of them already in the laboratory, will be exploited in the year 2000 and beyond, for near net shape forming and for achieving-new metallurgical structures and composite structures. Process modelling will alter the way we think about process and product design. Processes themselves will increasingly be automated and controlled by computers, altering the nature of the workplace and the tasks of the metallurgical engineer of the future. IntroductionInnovations in metal processing is hardly a new phenomenon, with the field thousands of years old. Nonetheless, the next few decades offer particularly important opportunities to improve our ability to process these materials. We appreciate today the variety of processing paths available to us, including vapor-, plasma- and electro-deposition, multiple phase and casting technologies, and non-equilibrium processes, and how these affect structure at the atomic level and at higher levels of aggregation. We understand the basic physical mechanisms involved far better than even before and have remarkable new abilities to predict, control, and simulate the kinetics underlying processes, and the processes themselves.The following sections describe these new opportunities in greater detail. First, we examine developments in the modelling of metal processing. We then consider some implications associated with process control and automation. Finally we present what we consider to be particularly promising metal processing technologies, and conclude with a few summary comments."

Jan 1, 1988

By Jiang Fan, Wang Haigang

"The three-dimensional complex multiphase turbulent flow in U-beam separators was simulated using the Reynolds stress equation models (RSM). To account for the effect of the stochastic characteristic of the instantaneous gas velocity on the particles, the improved Lagrangian stochastic model based on the Reynolds stress model for gas phase was adopted, which attributed to the successful prediction of the turbulence anisotropy and particle crossing trajectories effects. The interaction between the particles was also considered using the HardSphere model. To treat the particle-wall collision, the influence of the roughness of the wall on the motion of the solid particles was taken into consideration by imposing random collision angles. The result from this study not only shows the dynamic characteristics of the multiphase flow- in the separators, but also gives the relationship among the efficiency, structure and pressure losses of the separator.IntroductionCirculating fluidized bed (CFB) combustion is one of the most promising clean coal techniques. A main feature of CFB boilers is the un-delayed recycle of solid, coal and sorbant particulate, in an external loop. Separator, which is required to separate the solid particle from the flue-gas leaving the reactor of CFB, plays an importance role in the external solids recycle loop. It affects the combustion of CFB system greatly. Presently cyclone is the most commonly used as separators for CFB system and other chemical industrial processes. It provides high level of separation for CFB system for fine particles. However it suffers from some inherent disadvantages. It's volume and size is huge. Moreover, it is difficult to design and install when the CFB workload rises. The application of U-beam separators instead of hot cyclone separators in CFB boilers has many advantages. Publications indicate proposals or successful use of Ubeam separators in Swedenr11, USA 21, Russia r3land China [4]• But it is not possible to find results in the literature of detailed investigations of this new. type of separators or recommendations on the choice and calculation of an optimal design. For this reason, numerical simulation for the three-dimensional gas-particle two-phase flows with several rows of vertical U-beam elements, local in the chess order and blocking a way of outgoing from a CFB boilers dusted gases was carried out in this study."

Jan 1, 2004

By De-qing Zhu, Zi-fu Gao, Jian Pan

"In order to produce high quality metalized products and prevent from burden cohesion during pre-reduction, self-fluxed pellets were made for COREX process in the paper. The effects of reduction temperature and reducing gas composition on pre-reduction behaviors of self-fluxed pellets are studied. The results show that the prereduced pellets have poor quality and deposited carbon appears when the reduction temperature is between 600°C and 700°C. The metallization rate, reduction degree and compressive strength of prereduced pellets are promoted by the elevating reduction temperature and mole fraction of H2. Pellets reduced by pure H2 at 800°C have high metallization rate (96.2%), reduction degree (99.4%) and compressive strength (960N/pellet). In all tests, self-fluxed pellets display normal swelling (RSI<l5%) behavior which reveals that self-fluxed pellets are suitable for COREX process. Increasing reduction temperature and mole fraction ofH2 in reducing gas is benefit for pre-reduction of pellets.IntroductionCompared with Blast Furnace, the COREX process has advantages of short flow sheet, using non-coke coal and high-energy utilization. Acidic pellets and lump ores are the chief iron- bearing burden for COREX process which could lead to low melting point substance appearing in per-reduction process. In addition, the acidic hematite pellets tend to swell during the reduction [1-3]. This will result in decreasing compressive strength of pellets, burden cohesion, bad air permeability and poor work status in shaft furnace. Adding carbonate flux could restrain burden bonding to some extent in actual production, but decomposition of carbonate flux increases energy consumption. Worse still, weak reduction potential is unfavorable to iron material reduction [ 4, 5]."

Jan 1, 2013

By Toshihiko Emi

The quest for cleaner steel is driven by increasingly stringent requirements from the manufacturing and construction industries. Key issues are the occurrence and removal of inclusions; These are discussed in the context of the unit processes of deoxidation, refining, transfer and casting of molten steel. Process thermodynamics and kinetics are also discussed. Recent progresses achieved and problems yet to be solved are elaborated, and an integration of the unit processes into a system to produce extra clean, steels with better performance is presented.

Jan 1, 1999

By Ping Long, Bin Yang, Jian Wu, Xiumin Chen, Wenli Zhang

In this study, the analysis method of trace element in pure indium using glow discharge mass spectrometry (GD-MS) has been established by correcting the analysis result, which was obtained from non-standard quantitative method of GD-MS. The effect of instrument operating parameters, the resolution and isotopes and the pre-sputtering time on the determination results were investigated respectively. The optimized operating parameters of the instrument were obtained as follows: the discharge current was 37.5mA and discharge airflow was 475ml/min. Mass spectral interferences have been eliminated using selected resolution and isotope. The pre-sputtering time was 30 min. 4 trace elements in two pure samples were determined for 6 times. The RSD were less than 20%. The content of trace elements in indium samples was determined by GD-MS and Chemical Analysis Method of Indium which is tested by inductively coupled plasma atomic emission spectrometry, respectively. The results were consistent with each other.

Jan 1, 2016