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By Leandro Rigo Ramos, Marcelo Lucas Pereira Machado, Lumena Gloria de Souza Nunes, Mariana Valinhos Barcelos

The aim of this work was to study the influence of temperature on the grain refining process from severe plastic deformations through the simulation of Accumulative Roll Bonding (ARB) by torsion tests. The assays were performed to simulate the ARB at three different temperatures of 550 ° C, 625 ° C and 700 ° C with 5 torsion cycles with equivalent strain of 0.8 per cycle at a rate of 0.1−1 , totalizing an accumulated deformation of 4.0. Grain refining was obtained with an average size of 2μm, 5μm and 6μm for the temperatures of 550 ° C, 625 ° C and 700 ° C respectively. There was a rise in Vickers hardness by 68%, from 119HV in the annealed sample to 175HV in the deformed sample at 550 ° C. In the deformations at 625 ° C and 700 ° C the value of 130HV E and 150HV respectively was obtained. Based on the obtained results, it can be stated that the severe plastic deformations in microliged steel, carried out at temperatures lower than the end of the austenite-ferrite transformation, produce refined grains of the order of 2μm and, consequently, increase the mechanical strength of the material.

Oct 1, 2019

By François DUMORTIER

Due to the increasingly stringent requirements and the needs of the automotive industry, galvanizing lines for automotive products have to be modernized and improved. Beginning of 2017, SEGAL, a Tata Steel CGL located in BELGIUM and fully dedicated to automotive market, placed an order to increase the line capacity from 550kt/year to 600kt/year to process a wider range of steel grades and improve the product quality according to automotive requirements. To improve quality, a major revamping of the skin pass was necessary. The objectives were first to increase the work roll diameter from Φ560mm to Φ650mm to be able to transfer the required roughness with low elongation on soft material and second to increase the rolling force and tension to reach higher elongation on high strength steels. The result was the adaptation of the whole skin pass mechanics. Old mechanical elongation system has been replaced by a completely new single AC motor with helical gearbox at each bridle roll. John Cockerill achieved such complicated revamping in a very short time since the shutdown started only 6 month after the contract signature. The shutdown down schedule has been optimized with pre-erection works and the teams working 24/7 to implement all the changes. The complete project (skin pass, furnace, loopers) have been adapted during the three weeks shutdown. Today the customer can use both 560mm and 650mm work roll diameters. Thanks to the use of the new 650mm work roll diameter, the customer is able to make the same elongation using a bigger roll force (average 20% more), which has strongly improved the roughness transfer to the strip and the removal of the defects. SEGAL is really satisfied able to produce and supply higher quality automotive products to his customers.

Oct 1, 2019

By Renan Tavares Ruy

Esse trabalho tem como objetivo buscar um melhor entendimento dos fatores que influenciam de forma significativa nas propriedades mecânicas do vergalhão 1350AA, avaliando especificamente a influência da temperatura de bobinamento. Foram retiradas amostras de seis bobinas e então submetidas à diferentes temperaturas de recozimento por um período específico e analisadas mecanicamente e microscopicamente. Os ensaios de tração mostraram que o alumínio 1350 AA sofre uma influência significativa da temperatura, cujo comportamento foi muito similar ao apresentado na literatura. Constatou-se que o fenômeno de recuperação ocorreu de forma mais significativa a temperaturas elevadas. O trabalho permitiu concluir que é necessário um resfriamento mais eficiente no vergalhão para que a variação de LRT seja minimizada.

Aug 16, 2017

By Piezanowski Ludivine

With the aim to reduce the hot metal production cost, ArcelorMittal Gent decided to integrate more ores with finer particle size distribution in the raw material mix for the production of blast furnace sinter. As a consequence of such an increase of finer material in the sinter raw mix, the sinter machine productivity and the quality of the sinter are affected. In order to compensate this impact, modern granulation technology can be employed. Within this context, ArcelorMittal Gent has invested in a vertical intensive mixer. The equipment was placed before the existing drums, with a function of “mixer”, whereas the drums are fully optimised for the nodulizing process. The paper presents the results of the industrial operation during the commissioning phase of the new equipment. Gradually increasing the proportion of fine material in the sinter raw mix has made it possible to compare the performances of the old system using drums for mixing and pelletizing with the new system using an intensive mixer combined with a nodulizing.

Aug 1, 2018

By Anna Carolina Cerqueira Neves

Synthetic fibers have been gradually replaced by lignocellulosic fibers. Compared to the synthetic fiber, natural fiber showed economic and environmental advantages presenting interfacial characteristics with polymer matrices that favor the impact energy absorption by the composite structure. However, so far little has been reported about the hemp fiber embedded in polymer matrices, such as tensile properties. This study aims to evaluate the resistance in tensile tests of epoxies composites reinforced with different percentages of hemp fiber. Tensile tests were submitted with percentage of 0%, 10%, 20% and 30% incorporated hemp fiber in epoxy matrix. The tensile strength and deformation substantially increased the relative amount of hemp fibers incorporated into the polymeric matrix.

Aug 16, 2017

By Paulo Masiero

Sintered titanium carbide has been extensively used since the early 1980s for demanding wear-resistant applications and, in particular, in environments characterized by high temperature and oxidation. Thanks to its physical characteristics, especially its low density, titanium carbide (TiC) has been successfully applied in the manufacture of cassette guide rollers for hot steel rolling. However, the peculiar characteristics of the sintered Ti carbides make it difficult their redressing and hence this has always represented the limit for a more extensive application. Very often iron based alloys are preferred even if, in general, they are less cost effective just because they are easier to be redressed by turning. The availability of a simple, compact, fully automatic and reasonably priced CNC machine; specialized in the grinding of guide rollers and able to operate accurately and efficiently -both in contour and in plunge- can definitively solve TiC’s redressing problems and render its use even more widespread and attractive.

Oct 30, 2017

By Péricles Bosquetti

Estudou-se o comportamento dos aços inoxidáveis AISI 304 e 316, quanto à corrosão causada pelo caldo da cana-de-açúcar nos processos que simulam a sua extração. Devido a inviabilidade de realização dos ensaios de imersão utilizando o próprio caldo da cana-deaçúcar de pH médio de 5,5, pela deterioração do caldo e da variedade da concentração devido a variedade da cana, do tempo de maturação e das condições ambientais expostas, foi utilizado o ácido cítrico, que é o precursor do ácido transaconítico, sendo este o ácido encontrado em maior concentração no caldo da cana, utilizando-se uma solução de 10% em massa, apresentando pH em torno de 5,0 [1]. As amostras permaneceram imersas por vários períodos de tempo, sendo que para tornar o ensaio acelerado, a solução foi submetida à ebulição durante todo período que as amostras ficaram imersas. Ao final de cada um dos períodos, os corpos de prova foram limpos, pesados e avaliados na relação de perda de massa por área, tendo-se medido a massa inicial bem como a área superficial inicial das mesmas. Foram obtidos resultados interessantes que mostram o ataque diferenciado da solução ácida a estes dois aços inoxidáveis, onde se observou a presença de “pites”, cujo tamanho e quantidade dos mesmos foram diferentes, sendo que o AISI 304 foi o que sofreu maior ataque.

Aug 16, 2017

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Peter Hodnik, Gabriele Paulon, Herbert Moser, Thierry Gautreau, Loris Busolini

At voestalpine Stahl, Linz a new conventional slab caster has been installed to produce mainly automotive and electrical applications grades, implementing the latest design solutions: tight pitch roll geometry, mould and strand stirring and braking devices, SEN water modelling validation, enhanced roll cooling design to allow dry casting conditions, finely defined slab cooling system layout to control slab surface temperature across the width. To control these design solutions the latest generation of technological packages has been implemented like detailed solidification model based on meshless computational algorithm and a fully dynamic application of soft reduction to achieve sound internal quality results.

Oct 1, 2019

By Rafael Abreu Fraga, Carlos Noberto Paula da Silva, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Since 2016 Gerdau Ouro Branco has been producing steel plates of various qualities and grades. However, it was not until 2018 that the first plates produced by accelerated cooling process were made available for external testing, in this case for large diameter UOE pipes manufacturing. Recent line pipe and OCTG specifications are showing that the oil and gas market still consumes regular API grades, such as X60, X65 and X70, however with increasing wall thicknesses, reaching values up to 1.5 inches. These specifications also demand longitudinal and transverse tensile guarantees and drop weight tear tests in temperatures as low as -40°C. Projects with these types of mechanical properties present process requirements as challenging as those necessary for higher API grades in lower thicknesses. This paper shows the steel design concepts and rolling routes for achieving the necessary properties for X70 steel plates in 28.15 mm. The microstructural features were also investigated and associated with the production process and the tensile and toughness results. Finally, challenges such as tensile anisotropy and DWTT abnormal fracture are presented.

Oct 1, 2019

By Lidong Teng

ArcSaveTM is a new generation of electromagnetic stirrer (EMS) from ABB for electric arc furnace (EAF) operation. Its goal is to improve the safety, increase the productivity and reduce costs. Electromagnetic stirring in the melt bath during arc furnace operation will affect the scrap smelting, bath temperature distribution, refining reactions, and also the tapping practice. This paper has summarized the investigation results obtained from the first ArcSaveTM system installed in a 90 ton EBT arc furnace in USA. The hot test results show that ArcSaveTM has enhanced the heat and mass transfer in the arc furnace process. This results in a faster scrap melting rate, lower slag superheat during arcing, more homogenous melt bath, higher decarburization rate and higher EBT free opening frequency. ArcSaveTM has also reduced the tapping temperature and tapping oxygen in the steel. This brings a higher scrap yield and saves ferroalloy consumption in the downstream ladle furnace operation. The lower energy consumption, short tap-to-tap time, and consistent furnace operation bring increased productivity and safety.

Aug 16, 2017

By Juarez Linhares

A mini sinterização processo JL patenteada sob o número PI-9202973-6, é caracterizada por soprar o ar pelo fundo da panela, dispensando o uso de grelhas, caixa de ignição além de proporcionar um baixo consumo de energia elétrica, o que se traduz em vantagens técnicas e econômicas ao processo de sinterização.

Aug 16, 2017

By Diego Berti Salvaro

The morphology, dimensions and chemical composition of tribolayers strongly depend on the pressures and temperatures acting on the contact. They are formed by reactions between the surfaces in contact with each other as well as with the atmosphere, lubricants and possible contaminants. In this paper the influence of test time (180, 500, 1000 and 2500 h) into the formation and characteristics of tribolayers in pairs DLC-stainless steel tested under refrigerant gas R134a atmosphere without presence of lubricating oil was analyzed. The characterization was performed using scanning electron microscopy, energy dispersive spectroscopy (SEM-EDS) (morphology and chemical composition) and white light interferometry (dimensions). The tribolayers thicknesses ranged from 100 to 500 nm and they were composed by elements originated from mutual transfers between the tribological pairs as well as oxides, being more pronounced on the stainless steel surface. The results show that the tribolayers are chemically stable (maintained the same composition over time) and the thickness remained stable after a thousand hours of testing.

Jul 31, 2018

By Allana Cristina Pires Ferreira

O endurecimento secundário de aço rápido AISI M3:2 nome comercial Sinter 23 obtido por uma técnica de metalurgia do pó de sinterização por compactação isostática a quente é objeto desse trabalho de pesquisa. O aço rápido em questão foi austenitizado em banho de sal a 1.140°C, 1.160°C, 1.180°C e 1.200°C, temperado ao ar e revenimento a 540°C, 560°C e 580°C. Amostras do aço rápido foram fabricadas e submetidas ao tratamento térmico acima descrito e submetida a ensaios de dureza Vickers e Rockwell C para a determinação das suas respostas ao tratamento térmico de endurecimento e avaliação do pico de endurecimento secundário através dos resultados de dureza.

Aug 16, 2017

By Eduardo Vitral

The present study focuses in the simulation of pattern formation by ion beam sputtering on a material surface. This process is responsible for the appearance of unexpectedly organized patterns, such as ripples, nanodots and hexagonal arrays of nanoholes. A numerical analysis of preexisting patterns is proposed to investigate surface dynamics, based on a model derived from a Kuramoto-Sivashinsky anisotropic equation, in a two dimensional surface with periodic boundary conditions. While deterministic, its highly nonlinear character gives a rich range of results, making it possible to describe accurately different patterns. A finite-difference semi-implicit splitting scheme is employed on the discretization of the governing equation. Simulations were conducted with realistic coefficients related to physical parameters (anisotropies, beam orientation, diffusion). The study dealt with a random and a monomode 1D structure initial condition in order to understand how the shape and wavelength of the initial pattern evolve with time. Ripples and hexagonal patterns were observed in the results, being physically consistent with the phenomenon. Moreover, the Method of Manufactured Solution has been used as verification of the developed numerical scheme.

Aug 16, 2017

By Jan Lückhoff

The introduction of the EAF Quantum furnace by Primetals Technologies represents an important milestone in the field of electric steelmaking during the last 15 years. In this process the latent and chemical heat of the off-gas generated during a melting process in an EAF is used to pre-heat scrap in an integrated shaft prior the melting of the scrap in the vessel. Combining proven own technologies, Primetals EAF Quantum enables nearly continuous process, cutting down idle times and enhancing availability for production. The essential benefits will be shown in this Paper.

Aug 16, 2017

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Vagner Machado Costa

O presente trabalho tem por objetivo analisar parafusos Classe 8.8 produzidos por 4 fabricantes nacionais. Para tanto, realizou-se caracterização mecânico-metalúrgica, baseando se nas normas ABNT NBR ISO 724: 2004 [3] e DIN EN ISO 898-1: 1999 [2]. O estudo de caracterização mecânica consistiu na realização de perfis de microdureza, ensaio de tração, MEV da superfície fraturada e medição dos perfis dos parafusos. A caracterização metalúrgica seguiu através de análise química e caracterização metalográfica (macrografias e micrografias). Está caracterização é de fundamental importância para verificar as variabilidades devido aos diferentes fabricantes as quais este componente está sujeito e compreender como elas podem vir a influenciar no desempenho deste produto.

Aug 16, 2017

By Eric Yoshimitsu Sako

One of the main difficulties in the operation of trough and runners at Arcelor Mittal Tubarão (AMT) Blast-furnace no.02 is the reduced amount of time available for repair procedures. The consequence is that the castable installation must often be performed during hot conditions and the installed castable could easily detach from the base material during the early stage of operation, exposing the previously oxidized base material to molten iron and corrosive slag attack. When events like this happen, emergency repairs must be executed, resulting in increased refractory unit consumption and an unplanned shutdown of unit operation. Considering these targets, Nippon Crucible Co. and Saint-Gobain HPR Brazil have developed a high-performance Al2O3-SiC-C composition based on an entirely novel anti-oxidation technology. Oxidizing reactions could be attenuated by adding an oxidant inhibitor and a water reducing agent. As a result, the open porosity was significantly reduced, resulting in an improvement of campaign life in terms of pig iron throughput when compared with the regular castable. An analysis of this life improvement showed successful results for the material after 250 days of campaign. The main reason for such successful results was that the deterioration caused by the oxidation was significantly less and that this change made on the high cohesive structure of the base material was maintained for a long time. The attained results allowed Arcelor Mittal Tubarão to achieve longer trough campaigns, and avoid any unplanned stoppages with zero breakdown risks.

Oct 30, 2017

By Renan Oss Giacomelli

The adhesion of multifunctional coatings on soft substrates is of paramount importance in the tribological behavior of this important class of surface treatment. In particular, scratch and indentation tests have been extensively used in order to assess this property. In this paper, the adhesion of a-C:H diamond-like carbon films deposited on nitrided low carbon steel was evaluated by indentation and scratch tests. The coatings were produced by PECVD onto 1020 steel substrates with two different surface finishing: ground (Sq = 0.184 µm) and polished (Sq = 0.002 µm). Indentation tests using a Rockwell diamond indenter were conducted and the adhesion evaluated by measuring the spalling region on images obtained by using optical microscopy. The analysis of the spalling regions produced semi-quantitative results, eliminating the subjective qualitative analysis proposed by the standard method VDI 3198. In addition, scratch tests were performed using the same indenter and a comparison between the two techniques was established.

Jul 31, 2018