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By M. H. Kline

The Scarlet mine, in Randolph County, N. C., was operated on a small scale at intervals from 1899 to 1915, but no records of the quantity of ore produced are available. J. I. Moore unwatered the mine in March 1948, and Bureau of Mines' engineers examined the underground workings. Several assays checked previous sampling of the mine and indicated a small but comparatively high-grade copper-zinc deposit. The high metal content of the veins and the possibility of developing additional reserves prompted the Bureau of-Mines to drill three holes, totaling 530 feet, at the deposit during March and April 1948. Drilling disclosed that the mineralized vein did not extend over 300 feet along the strike and is probably limited in depth to the contact with the granite mylonite.

Jan 1, 1949

By Ramie H. Thompson

1.1 BACKGROUND In many underground coal mining operations the use of electromagnetic field equipment, particularly communication systems, not only increases the overall efficiency of the mining operation but can be directly linked with mine safety considerations. The use of electromagnetic field producing equipment in underground coal mining operations can only be expected to grow. Several new communication systems have already been proposed. In addition, high-frequency producing equipments for many diverse uses in mining operations are under study. The use of these equipment in underground mining operations is hampered by the possibility of their electromagnetic fields interacting with the electric blasting cap operations commonly carried out in the mines. Such interactions can have at least two results bearing directly on mine safety: o premature initiation of the cap, either in its normal shot location or during hookup or transportation; o dudding of the cap so that normal firing operations do not cause irritation; thereby leaving unexploded high explosives after normal firing. Since the consequences of a premature initiation could, particularly in coal mines operations, result in catastrophe involving human life, the overall approach to prediction of possible hazard must be, as far as possible, of a "worst case" nature. The general problem of predicting possible RF hazards for any electroexplosive device (EED) is best treated by reference to Appendix A of

Jan 9, 1983

By A. Sainato, S. J. Kravits, G. L. Finfinger

This Bureau of Mines report describes and compares the procedures, capital investments, and operating costs of rotary and in-hole motor drilling techniques used to drain methane gas from the Pittsburgh Coal- bed in an underground mine located in southwestern Pennsylvania. A timestudy was conducted during the drilling of each of two boreholes, and the data were collated to serve as a base for comparing drilling procedures and operating costs. Findings indicate that drilling with an in-hole motor offers four advantages over rotary drilling; namely, an increase in drilling productivity, fewer worker-hours required, ease of maintaining vertical and horizontal bit trajectory, and less expensive drilling cost per foot of borehole.

Jan 1, 1985

By Philip C. Good

The Bureau of Mines investigated the feasibility of utilizing low-grade phosphatic shale as a feed for phosphoric acid production. Present practice in the phosphate mining operations of southeastern Idaho is to remove and either stockpile or waste low-grade phosphatic shales as the high-grade phosphate beds are selectively mined. Acid digestion studies were performed on uncalcined shale and on shale calcined to remove free carbon to determine phosphoric acid quality, yield, and amenability to filtration. The untreated shale, containing 21.4 pct P205, was digested with sulfuric acid in a single-tank reactor to yield phosporic acid and gypsum residue. Although 96 pct P205 recovery was attained in digesting uncalcined shale, only the calcined product gave satisfactory filtration rates. Calcined shale yielded phosphoric acid recovery of about 93 pct of the contained P205. It was higher in impurities than commercially prepared acid derived from high-grade western phosphate rock. An acid filtration rate of 745 lb P205/ft2/day was attained. This value is lower than the rate of 900 lb P205/ft that is generally considered to be acceptable in industrial production of phosphoric acid from high-grade phosphate rock.

Jan 1, 1981

By W. E. Webb, R. H. Church, W. G. Hopkins

The development of systems for location of miners who have become entrapped following a mine disaster has been one of the major research goals in the Bureau of Mines. This study details the preliminary development of such a system. Current technologies for locating trapped miners from the surface are either simple direction, finders or time difference pulse systems that have accuracy Limitations. Developing technologies using full vector field measurements at several receiving points are currently being studied. The necessity of measuring field strength with great accuracy can be a drawback in these systems. A system that operates with continuous wave radio signals, whose phase differences can be measured accurately even in weak signal conditions, greatly improves the location accuracy. A microcomputer would be used, in conjunction with the system, to gather and manipulate the data to automatically pinpoint the location of the trapped miner. Comparison of this system with existing technology indicates a favorable accuracy/complexity ratio for the phase difference of arrival technique.

By W. T. Culler

"The ""rate-of-preduotion curve"" described in the revised Treasury Manual* was devised by the author in May, 1920, and since that time has been use by the oil and gas valuation section of the Treasury Department in determining the rate of production of wells for purposes of taxation. This curve is most useful for estimating the future production of a well, or group of wells, of known daily settled production, where future-production curves and tables based on yearly production records are available. It also provides a means for determining the past year's production of a well of known daily settled production, or conversely, the estimated production on any day for a well of known yearly production.The rate-of-production curve is auxiliary to the production decline curve and is derived from it in estimating the future production of a tract, a production decline curve formed from the records of the tract itself should be used. If such records are not available, and there is no information which leads to the belief that the average production decline of the wells in this tract differs from the average for the pool or district, an average curve for the pool or district may be used.The accompanying chart illustrates a typical rate-of-production curve, with the yearly production decline curve from which it is derived. The production decline curve shown is for an average well in the Augusta district, Butler County, Kansas, and has been constructed from the tables given on page 128 of the revised Treasury Manual.The ordinate (vertical scale on the chart) of any point on a yearly production decline curve represents the production of the well during the year previous to the date shown by the abscissa (horizontal scale). For example, the chart shows that an average well, which produced 100,000 barrels of oil in 1915. produced 92,000 barrels in the year previous to January 19, 1916, produced 53,300 barrels in the year previous to June 1, 1916; produced 49,000 barrels in the year previous to July 1, 1916, 27,000 barrels in 1916, and 10,000 barrels in 1917."

Oct 1, 1921

By J. M. Singer

Flame propagation of lower limit hybrid coal dust-methane-air mixtures in vertical and horizontal flame ducts of 15.2 cm id and 1.8 m length has been investigated to provide information bearing on safety in mines. Fuel concentrations at lower limits of flame propagation and equivalences of coal dust and methane are much higher for continuing flame propagation than for short-span flame propagation in the vicinity of an "overdriving" ignition source. As the energy of the ignition source was increased, the flame speed and the distance of flame propagation from the ignition source increased, whereas the total fuel concentration at the lower limit decreased.

Jan 1, 1968

By Francis Church Linxoln

"This property was explored as part of a general investigation of zinc-prodccing areas of southwestern Wisconsin at a time when an effort was being made to increase the production metals important to the Nation's war program. This report describes the work that was done and presents the data obtained.ACKNOWLEDGEMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the and that they make the greatest possible contribution to national security and economy. It is the policy of the bureau to publish the facts developed by each exploratory protect as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metallurgical Branch, P., G. Knickerbocker, chief, analyzes samples and performs beneficiation tests. Both these branches are under the supervision of Dr. R. S. Dean, assistant director. Special acknowledgment is due Professor G. H. Pett, of the Wisconsin Institute of Technology at Platteville, Wis., Jack Tracy, manager of the Mifflin Mining Co., and J. M VanMatre, representative of the Defense Property, for their assistance in the work. Acknowledgment is also due to A. F. Agnew and A. V. Heyl, geologists of the Federal Geological Survey, for furnishing geologic interpretations and lithologic studies of the drill-hole sections. All drilling was done under the immediate supervision of Francis C. Lincoln and M. Howard Berliner, project engineers, Edward P. Barrett, district engineer, Minneapolis, and E. D. Gardner, regional engineer, of the Bureau of Mines."

Sep 1, 1946

By E. C. Perkins

This report describes a ferric chloride trap, based on formation of a low-melting sodium chloride-ferric chloride mixture of near-eutectic composition, and its use in chlorination of impure titaniferous materials. The trap is placed in the hot gas stream between the chlorination reactor and the condenser. Virtually all of the iron is removed by the trap. The condensed titanium tetrachloride is free of suspended solids and contains only a trace of iron. Four examples are given of the use of the ferric chloride trap in chlorination of impure titaniferous materials. INTRODUCTION In the Kroll process, ductile titanium metal is produced by reducing titanium tetrachloride with magnesium metal.4/ In commercial practice, titanium tetrachloride is produced by chlorinating titaniferous materials in the presence of carbon.2/ In 1957 most producers were using rutile, and virtually all plants were designed for its use. About four-fifths of the domestic consumption of rutile was imported from Australia. The Bureau of Mines, under provisions of contract DMP-116 with the General Services Administration, studied electrosmelting of domestic ilmenites and titaniferous magnetites to produce high-titanium slags with pig iron as a byproduct. Under the same contract, chlorination studies also were being made of these slags. Smelting was done at the Northwest Electrodevelopment Experiment Station, Albany, Oreg., and chlorination at the Electrometallurgical Experiment Station, Boulder City, Nev.

Jan 1, 1958

By R. W. Freedman

The gas chromatographic method, devised by the Bureau of Mines for analyzing routine mine air samples, was compared with the infrared method used for confirmatory determination of methane in mine air. While maintaining the specificity of the infrared method for methane determination, the gas chromatographic method is more precise, much more rapidly performed, and more convenient.

Jan 1, 1968

By B. J. Scheiner

The Federal Bureau of Mines investigated an electrolytic oxidation procedure for extracting lead, zinc, copper, and silver from lead-zinc concentrates. Concentrates slurried in brine were pumped through the anode compartment of electrolytic cells equipped with selective ion diaphragms. Hydrochloric and hypochlorous acids generated in the anode compartment converted the metal sulfides in the concentrates to soluble metal chlorides, sulfate ion, and elemental sulfur. Metal extractions of 92 to 100 pct were obtained from lead-zinc concentrates at an energy consumption ranging from 1.5 to 5.0 kW-hr/lb metal extracted. Sodium hydroxide was formed in the cathode compartment at a current efficiency of >99 pet. Silver and copper were extracted from refractory tetrahedrite minerals, but the process entailed a relatively high energy consumption. Sealing the top of the diaphragm cell utilized the chlorine more effectively, thereby reducing energy consumption 10 to 50 pct.

Jan 1, 1975

By Thomas C. Atchison

The experimental work described in this report is part of a continuing study by the Federal Bureau of Mines of the fundamental physical processes involved in breaking rock with explosives. Six explosives were tested for their strain-producing abilities in a dolomitic marble. The explosives selected for testing had a tenfold variation in detonation pressure and a fivefold variation in characteristic impedance (product of loading density and rate of detonation). Strain pulses produced by the detonation of small charges of the explosives were recorded at distances of 5 to 130 feet. Peak strain, ?, was found to decrease with distance, R, in accordance with an exponential propagation law previously determined for other rock types, namely ? = (K/R)e ?aR The absorption constant, a, did not vary significantly with the explosive and was of the same order of magnitude as that for other rock types. The different explosives produced a fivefold variation in the value of the intercept constant, K.

Jan 1, 1961

By F. E. Block, T. T. Campbell, D. Z. Hobbs

Several methods were investigated for the preparation of high- purity elemental boron in an attempt to develop a feasible process for producing boron on a large scale . In the work described in this report , the metal was prepared by metering boron trichloride gas into a crucible containing molten metal reductants . It was necessary to remove reaction byproducts by acid and aqueous leaching . Magnesium and sodium were tested as reductants , but best results were achieved using lithium or zinc as reductants . Contaminants originating from the materials of construction were the chief impurities in boron made by this method . Impurities ranged from 0.5 to 5.0 percent . Impure boron ( 85 to 90 percent ) was also prepared by the magnesium reduction of boron trioxide in a thermite - type reaction . This product contained magnesium as the chief contaminant . Impure boron made in this way could be upgraded by fusing with potassium fluoborate or potassium acid fluoride . After acid leaching the fusion cake , a product containing 95 to 97 percent boron was obtained . Analytical techniques for accurate determination of impurities in elemental boron are a major problem , requiring solution before a valid comparison can be made of the quality of boron prepared by these various methods .

Jan 1, 1964

During 1990-1999, a total of 458 fires occurred in all coal mining categories; 157 of those fires caused 164 injuries and 2 fatalities. The greatest number of fues and fire injuries occurred at surface mines, whch also had the highest risk rate values. A total of 66 fuefighting interventions were required. Of these, there were 25 mine rescue team interventions in underground mines, including 5 mobile equipment firefighting interventions, and 41 fire brigade and fire department interventions at all surface operations, including 19 mobile equipment interventions. In all, 50 fires destroyed or heavily damaged equipment (including 16 pieces of mobile equipment) because of failure of other firefighting methods, late fire detection, undetected fires, or fire size. A total of 1 14 fires were detected late by smoke, and 42 fires were not detected.

By J. W. Adams

Measurements of surface magnetic field noise were made at various locations over the Geneva Coal Mine near Price, Utah, on June 12, 1973. The locations selected were on the surface over emergency locator beacons underground at depths between 3S0 meters (1150 ft.) and 488 meters (1600 ft.). The surface terrain where these measurements were made was mountainous, and access was difficult. There were no power lines within several miles, and the weather was clear; therefore, the magnetic noise levels were about as low as will normally occur. Results of measurements of distant sferics indicate rather sharp cutoff frequencies below which broadband, impulsive noise is attenuated. The mechanism of propagation for this noise above the daytime cutoff frequency of 3500 Hz and the nighttime cutoff frequency of 1700 Hz is deduced to be a waveguide formed by the D or F layers of ionosphere as an upper plane and the earth as a lower plane.

Jan 1, 1974

By Israel Liebman

The Bureau of Mines developed three types of passive water barriers for suppressing slow-moving coal dust explosions. One type is a modification of a conventional tub barrier and depends on the dynamic pressure generated ahead of an explosion to tilt the tub to release its water and suppress the explosion. The other two barriers operate in response to an increase in static pressure developed ahead of the explosion. Tests indicate the first barrier begins to release its water at air speeds as low as 50 ft/sec, and the second and third barriers will operate at a rise in static pressure as little as 0.5 psi. All three barriers were found to be effective in suppressing coal dust explosions propagating at speeds as low as 100 ft/sec. A plan is described for installing a water barrier in a working mine on a trial basis.

Jan 1, 1976

By Arthur Metcalfe, Edward Thomas, A. J. Barry

"Early in 1947 the Bureau of Mines became interested in adapting suspension roof support to coal mining 5/ as a possible means of reducing the high rate of accidents from falls of roof. For a time the program made little progress be¬cause of the shortage of steel products after the end of World War II, but during the past 8 months this restriction has eased, and as of May 1, 1949, 114 mines had either started experimental work or had ordered materials and equip¬ment in anticipation of trial installations. It is estimated that 30 linear miles of roof in underground passageways have been secured by this method in recent months, and no lost-time roof-fall accident has been reported in these areas up to that date.Many coal-mining companies in widely separated localities have cooperated in making experimental installations. In very few instances are these companies entirely satisfied that they have arrived at the best solution in determining the most efficient adaptation to suit their particular conditions. Moreover, new ideas and modifications of the basic principle are constantly being brought to light and are being tested. Available test data is far from complete, and it is conceivable that some new idea will be developed to alter the present concept of proper technique; therefore, this progress report does not attempt to answer all questions that might arise in connection with this method of roof support; it simply recounts the experience acquired to date. Consequently, few references to costs are made. Up-to-date quotations on material and equipment used in suspension roof-support installations may be obtained from numerous mine-supply companies.The authors gratefully acknowledge the cooperation of mining companies whose personnel made possible collection of the information contained in this circular: Bethlehem Collieries Corp., Barrackville, W. Va.; Berwind-White Coal Mining Co., Windber, Pa.; Consolidation Coal Co., (Ky.); Jenkins, Ky.; Consolidation Coal Co. (W. Va.), Fairmont, W.Va.; Clinchfield Coal Corp., Dante, Va.; Consolidated Coal Co., St. Louis, Mo.; Hanna Coal Co., St. Clairsville, Ohio; Missouri Portland Cement Co., Sugar Creek, Mo.; Pocahontas Fuel Corp., Pocahontas, Va.; Reppert Coal Co., Dola, W. Va.; St. Joseph Lead Co., Bonne Terre, Mo.; and Tennessee Coal, Iron, & Railroad Co., Birmingham, Ala.The fundamental theory of suspension roof supports is not new; in fact, its application in the construction of beams predates mining itself. The basic principle involved is the reinforcement of roof rock with steel rods inserted in the roof and anchored therein at points where the rock is least likely to be affected by stresses resulting from mining. Such roof supports have been used in mines for many years in widely separated localities. The St. Joseph Lead Co., operating in southeastern Missouri, apparently was the first large mining company to prove the practicability of the principle by applying it in a systematic manner for securing roof for more than 20 years (fig. 1)."

Sep 1, 1949

By Oliver Bowles

The exingencies of a world war have brought home to the American public, especially the people of the. Eastern States, the urgent need for conserving fuel. Transportation problems in the East have created an unprecedented situation wherein fuel-oil supplies are greatly restricted, and the consequent increase in demand for coal further complicates the problem of transporting and storing that commodity. People should awaken to the need for utilizing every possibly means of conserving to fuel, even to the extent of reducing the temperature in their homes.

Jan 1, 1942

By Foster Fraas

The response of minerals in magnetic separators is in accordance to dynamic rather than static magnetic susceptibility values . The dynamic value varies with respect to both passage speed through the separating field and time of exposure in a preliminary treatment field . Tests on 16 minerals and solids have demonstrated that both of these factors affect different minerals in different ways .

Jan 1, 1964

By Russell E. Griffin

Dielectric constants and dissipation factors were measured for six rocks over the 20-to 100-megahertz frequency range by means of the susceptance-variation method. Results for both dry and moist specimens are presented and compared with data reported by others. Loss factors calculated from the data presented are important to the Bureau's study of rock fragmentation by means of dielectric heating.

Jan 1, 1967