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By Renata Cristina Teixeira

The lubricant oil is a complex mixture of different basestocks and additives. Engine oils evolved from the use of pure mineral basestocks back in the early years of automotive industry to the advent of synthetic, fully formulated, low ash lubricants. This evolution was driven by a number of factors, such as new engine designs, extended durability needs, increased fuel economy needs, environmental concerns, feedstock prices and availability and legal issues. This paper uses technology prospecting on literature and patents databases to allow an investigation on the historical evolution of engine oils. Main basestocks (mineral, hydrotreated, polyalphaolefins, esters) and additives (antioxidants, antiwear, friction modifiers, detergents and dispersants) are characterized according to their research effort. Technology prospecting data is crosschecked against the evolution of engine oil classes, allowing an analysis of how the main drivers push the development of lubricant oil quality. A research effort was identified in late 1990’s until mid-2000’s and related to the adoption of chemical limits for lubricants. Different patterns for the articles and patents publication account for the high value technological knowledge has in this industry. Technology prospecting is seen as a useful methodology for the understanding and forecast of lubricant technology movements.

Jul 31, 2018

By Samuel Filgueiras Rodrigues, Clodualdo Aranas Jr., Gedeon Silva Reis, Eden Santos Silva, Fulvio Siciliano

When austenite is deformed above the Ae3 temperature, partial amount of it transforms dynamically into ferrite by a displacive mechanism. After unloading, it retransforms back into the stable austenite by a diffusional process. This influences the rolling load which decreases under isothermal condition or does not increase with decreasing temperature as rapidly as expected under cooling. Plate rolling simulations under isothermal and continuous cooling conditions were carried out on a 0.09 wt.% Nb X-70 steel. Pass strains of 0.2 were employed together with interpass times of 10 s, and 30 s for the cooling conditions and 0.3 with interval of 10 s at 900 °C for the isothermal experiments; strain rate of 1 s-1 was used during the simulations. The mean-flow-stress (MFS`s) behavior of both conditions indicates that dynamic transformation and dynamic recrystallization were taking place during straining. The critical strains for the initiation of dynamic transformation fell around 0.06 while the critical strain for DRX was 0.12. It has been shown that ferrite is formed due to the applied deformation of roughing passes and increases its volume fraction throughout the finishing rolling stage. Under cooling conditions, the ferrite formation is also favored as the temperature approaches the Ae3 line. Such ferrite forms when the driving force for dynamic transformation is higher than the total free energy barrier preventing its formation. This obstacle consists of the free energy difference between austenite and ferrite as well as the lattice dilatation work and shear accommodation work. The addition of Nb retards the retransformation of the ferrite into austenite. Moreover, holding times after rolling increases the amount of austenite available for microstructure control on subsequent stages. The dynamic transformation (DT) mechanism can be used to design improved rolling schedules

Oct 1, 2019

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Marcel Antonio Arcari Bassani

In the mining industry, it is common to have data collected in various formats. In an open pit mining operation, at the early stages of exploration samples are obtained from diamond drillholes. During the production stage, samples are collected from blastholes. The last is more numerous but less precise. From a geostatistical view, this dissimilarity has to be considered to integrate the two sources of information. To combine this different data, three methodologies were investigated: simple kriging with local varying mean, cokriging and ordinary kriging. The exhaustive Walker Lake data set was used and it is considered the source to obtain the true grades. Initially, samples were obtained from the exhaustive data set at a regular spacing grid of 20 x 20 meters. Next, samples were obtained again from the exhaustive dataset at a regular spacing of 5 x 5 meters and a relative error of 25% was added. Then, both data were used to estimate blocks using the three methods mentioned. The grade tonnage curves were compared with the true block grade distribution. Moreover, the block misclassification was evaluated. The results showed that ordinary kriging produced estimates closer to the true block grade distribution and reduced the block misclassification.

Aug 8, 2018

By Aitor Elorriaga Fernandez de Arroyabe

The purpose of Sinter plants is to heat iron ore fines along with fluxes and coke fines or coal, to produce a semi-molten mass that solidifies into porous pieces of sinter with the needed size and strength. Fluxes used in the sintering process need to have an appropriate size distribution and TI to avoid generation of fines, which could reduce the productivity of the Sinter. Besides, a homogeneous chemical composition and high absorption characteristics are necessary to control the basicity and to combine the flux with P, S, Si, etc, respectively. PASEK Dunite is an ultramaphic rock exploited in the north of Spain with a basic chemical classification, being olivine and serpentine its principal minerals. It is a very homogeneous and hard stone and its main characteristics are: high hot and cold resistance to mechanical stresses, softening and melting points of a flux not of a refractory material. In addition, due to its mechanical and chemical properties, less fines are generated in the sintering process and during the handling and transportation to the blast furnace, improving the productivity of these processes. In this way, the use of PASEK Dunite allows increasing the homogeneity structure of sinter, reducing the percentage of return fines and improving the Sinter productivity.

Oct 30, 2017

By Detlef Ehlert

Energy efficiency is coming to the center of attention in the metallurgical and rolling mill industry due to increasing energy costs, limited resources and political requirements. Also, a green image and energy efficient production is a clear competitive advantage. SMS Siemag, being familiar with automation and measurement equipment, provides an energy data management system which gives transparency over the energy consumptions. All energy relevant media including electricity, gas, water, compressed air and further more can be recorded. The system is manufacturer-independent and allows the use of already installed measuring technology with the possibility of subsequent extension. So potentials for improvement can be recognized and energy savings can be estimated and proven after the implementation of the measures. Being familiar with the processes in the metallurgical and rolling plants, the system by SMS Siemag allows the assignment of the energy data to the production and plant data. Only by this connection, the data can be reduced to key performance indicators allowing authoritative evaluation of energy efficiency. The results are clearly represented on dashboards and support the continuous improvement process. The system also supports the energy controlling with an automatic reporting system, cost center assignment and in support with certification according to ISO 50001.

Jul 30, 2018

By Hongshuang Di, Tianyu Zhang, Huiqiang Huang

A CMnSiAl transformation induced plasticity (TRIP) steel was used to study the effect of retained austenite on room-temperature mechanical properties. The steel plates with retained austenite were obtained by hot rolling, cold rolling and subsequent continuous annealing. The starting and finishing temperature of hot rolling are between Ac1 and Ac3. Reduction ratio of cold rolling is 75%. The continuous annealing is carried out at different intercritical temperatures. The relationship between work hardening exponent and retained austenite was discussed. The results show that, the Ac1 and Ac3 were much high because of the alloy elements, and the temperature range between them was wide. Due to the high hot rolling temperature, the grains was hereditarily refined as a result of dynamic recrystallization. Annealing at intercritical temperature of 930 ºC, retained austenite with relatively high stability reached a maximum volume fraction of 25%, a maximum total elongation of 30.2% and a best ultimate tensile strength × total elongation of 20.1 GPa·%. Instantaneous work hardening exponent reflects strengthening mechanisms at different strain stages. The TRIP effect of retained austenite is the main mechanism during deformation. With retained austenite of sufficient amount and high stability, continuous work hardening was observed in the tensile specimen of 930 ºC.

Oct 1, 2019

By José Aparecido Pereira

The customer asked for a 5” angle roll pass design. For this angle, in a normal pass design, a 160mm billet is required. For the production of this billet would be necessary a new 160mm mold for the Continuous Casting Machine, which produces 150mm billets, increasing the complexity of the melt shop. The rolling mill is designed to produce angles up to 4", technical information recommended the replacement of a gearbox because this process would generate torque up to 15% above nominal. An innovative roll pass design was done using 150mm billet using the Aparecido-W Method that cause a higher spread in the first three passes, thus reaching the desired leg length. As this method is not used in any other known rolling mill, a FES (Finite Element Simulation) and FEM (Finite Element Modeling) was done by a Research & Development center which demonstrated that the design was viable. From July, 2018, three tests were done being produced around 700 t of good quality products without difficulty of set up. The rolling mill team carried out this project at a very low cost and in record time of five months. The average torque of the motors was 36%, without overload for the equipment.

Oct 1, 2019

By Andrea Pezza

The paper describes the recent new installation and start-up of the second RH (Recirculation Degasser) in Rio de Janeiro plant of thyssenkrupp CSA Siderúrgica do Atlântico. The new plant is installed as part of the existing RH, the twin solution increases the overall melt shop production in the area of quality plates especially for deep drawing grades. With this new equipment, CSA is able to increase degassed grades production with a state of art asset that has the ultimate technology in operation, safety and automation. The description of the main components parts and the operational concept gives an overview of the latest experience in RH plant engineering combined with best operational practice of world class steel producer.

Oct 30, 2017

By Alberto Pesamosca

The paper presents the results obtained by the AC EAF supplied by Danieli at Kroman Çelik (Gebze-Turkey) after the planned upgrade to 150 ton. The EAF – 7,4 m diameter, based on the full platform standard design - is able to handle a maximum power of 114 MW and is equipped with the most advanced and reliable technology, including module injection system and the Hireg electrodes regulation system. Excellent results were already obtained with 120 heat size in terms of fast start-up and excellent performance figures. After the upgrade, productivity was increased up to 212 t/h, maintaining high process efficiency (365 kWh/t with 32,1 Nm3/t O2).

Jul 30, 2018

By Filippo Verlezza

Conventional wire rod blocks have some limitations. They can only roll with fixed reduction ratios which always require the same rolling diameters within the block. With MEERdrive® SMS, as a pioneer, has introduced an innovative drive concept for wire rod blocks that can overcome the limitations of conventional solutions. The clue: the concept is based on individual drives for each stand position. The exigent wire rod market demand and the available technology melt in a new variant of MEERdrive®, the MEERdrive®PLUS, which represents a sizing block solution for finished size rolling and allows conventional as well as thermomechanical rolling. Further “one family rolling” is also possible, since all roll / size changes will occur in this block.

Oct 30, 2017

By Ivan César Lopes Diniz, César Romero Afonso Goulart Júnior

Mandrels are tools applied to manufacturing seamless tubes. In VSB plants (Vallourec Soluções Tubulares do Brasil), it is used in two mills. Mandrel and PQF Mills. This is an expensive tool due its alloy (hot work tool steel – AISI H13) and lengh (between 12 meters and 22,5 meters). An opportunity to apply mandrels from PQF in Mandrel Mill has been identified. However, mechanical properties of PQF mandrels must be improved. This work presents the heat treatment process of Quenching and Tempering developed internally at VSB to improve PQF mandrel properties aiming to achieve Mandrel Mill requirements. Hardness and metallography tests were performed before and after some steps of the heat treatment to characterize and validate the process.

Oct 5, 2019

By Francisco Morganti

Weight reduction is the main target of all carmakers, which results in a continuous development of new steel grades. Latest 3rdgeneration advanced high-strength steel grades (AHSS) are complex materials with special chemical compositions and multiphase microstructures. The pickling, annealing and galvanizing processes of these grades aresomewhatdifferent due to the changed chemical compositions and microstructures. Therefore, these innovative steel grades place new demands on the plant technology of pickling, annealing and galvanizing lines. The most significant challenges for the pickling process are sludge occurrence during pickling, varying pickling times, weld ability of the materials, changed visual appearance and required high surface qualities. The most important topic concerning annealing line is a precisely controlled and very flexible heating and cooling process in the furnace.One of the new requirements in galvanizing linesis the prevention of surface faults caused by bare spots, which can occur since these materials feature a higher content of alloying elements like silicon or manganese. Prevention is possible with the special pre-oxidation technologies.Due to the higher strength of the material also the mechanical equipment has to be designed differently in these lines. This paper describes the influences of the changed chemical composition and material characteristics of modern steel grades on the pickling, annealing and galvanizing process and gives an overview about the technical solutions.

Oct 30, 2017

By Vitor Orlando Ferreira

The efficiency of an apparatus which uses a forced lubrication system, as well as the useful life of its components, is strongly related to the degree of contamination of lubricating oil. The presence of contaminants and the degradation of the oil itself cause it to release substances that fouling of the wall of the pipes. The cleaning and dialysis of the oil pipes, besides prolonging the life of the lubricant reduces wear of the components. There are several methods of cleaning in pipes, the problem is that some have abrasive characteristics, which could damage some types pipes. Among the non-abrasive methods stand the Flushing and Air scouring. Flushing uses the lubricating oil which circulates in temperatures alternating and high speeds, for generating turbulence to perform washing. The Air scouring method uses oil and filtered compressed air, injected into pipe, to generating higher flow, causing the power supply unit with fluid can work with lower power consumption and higher speeds, removing fouling of the pipe. The objective of this research is to evaluate the Reynolds number to correlate with the efficiency of cleaning the pipe. The method applied was the Air scouring and it was verified that the qualitative effects may occur when compared to Flushing. After testing, it was found that the chosen method brings significant changes in flow, and this flow regime varies considerably increasing the Reynolds number.

Jul 31, 2018

By Christoph Sedivy

Industrie 4.0 is slowly but surely arriving in the melt shops. Furnaces are being equipped with more and more sensors, digital models are increasing the degree of automation, and information is being shared between different aggregates within the plant. Because the electrode control system plays a key role in electric steelmaking, it naturally assumes an important position in the melt shop’s Industrie 4.0 strategy. In addition to reliable, state-of-the-art core regulation functionality, monitoring and reporting tools and the ability to communicate with other equipment are also required. Therefore, the latest generation of our electrode control system, the Melt Expert, was developed based on Industrie 4.0 design principles. Intelligent plant condition diagnostics, performance monitoring, and user-defined reporting are essential modules in this new system. With these functionalities, electrode control systems are developing into the information and control center of the furnace. A newly developed software app brings most relevant process information to mobile devices. This feature allows steelmakers to keep an eye on the performance of their equipment anytime and anywhere. This paper describes the new features of the electrode control system and shares our customers’ operational experience. Our focus is on the practical aspects of plant status monitoring, KPI reporting, and diagnostic functionality as well as the improvements achieved.

Oct 30, 2017

By Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Antônio Cezar Faria Vilela

A minor change in the chemical composition and temperature affects the slag viscosity, which has a great extent of the physical properties in regarding refining slags. Optimizing those parameters may affect the steel cleanliness. The viscosity measurement process is considered expensive, so the cost-effectiveness does not favor the measures at high-temperatures. Alternatively, it is possible to apply mathematical models or thermodynamic softwares to obtain viscosities for a given range of chemical composition and temperature of slags. The present work contemplates a validation of the experimental data, collected in the literature, with a calculated data and proposes an accurate representation of iso-viscosity curves applied for secondary steelmaking slags, covering the composition ranges: 0–100 wt.% CaO, 0–80 wt.% SiO2, 0–77 wt.% Al2O3 and 0–15 wt.% MgO (CSAM) system at 1500ºC. The viscosity representation fields include fully liquid and a partially liquid slags in the CSAM system and the viscosities were calculated using the FactSage 7.2 (for Liquid Phase) and the Roscoe-Einstein equation (for Phase mixture) for a total of 5976 slags. The preliminary results indicated that there is a great convergence between the calculated and experimental viscosities data, promoting an efficient approximation of the iso-viscosity curves for the CSAM slag system in the high-temperatures.

Nov 1, 2019

By Georg Keintzel

The origin and elimination of 3rd octave mill chatter is a frequently investigated topic since tandem cold mills are in operation. So far only chatter monitoring systems have been successfully deployed, but this implies speed reductions and therefore a significant loss in mill output. Primetals Technologies has developed a new system using active injection of damping in order to eliminate 3rd octave mill chatter. The new hydraulics-based ChatterBlock® Control has now been proven successfully in mill operation. 3rd octave mill chatter, typically occurring in a frequency range between 90 and 150Hz, is a self-excited vibration phenomena typically occurring in the rear stands of tandem cold mills. It can produce significant gauge variations and even cause strip breaks. 3rd octave mill chatter is characterized by a quickly diverging vertical vibration of the rolls for specific rolling conditions (material, mill speed, forces, gauge etc.). Its occurrence requires immediate speed reduction of the mill in order to avoid strip breakage and/or strip quality degradation. This phenomenon thus severely limits mill productivity. The first step to proof the industrial feasibility of the new system was its installation on stand no. 4 of a 5-stand tandem mill. The development process and first results of the industrial implementation will be presented in this paper.

Aug 16, 2017

By Marco Castenetto

Some of the most significant Danieli innovations in the field of long products are the: i) The EWR® system, through automatic continuous head-to-tail flash welding of billets at reheating furnace exit side, enables uninterrupted production of the mill for endless rolling of straight bars, wire rod and bar in coils. The process is particularly beneficial to wire rod and bar-in-coil mills as it enables production of “customized-size coils” (any coil weight according to specific Customer request) and with extra-high final coil weight, even starting from low-weight billets; ii) The Spooler process is based on twistfree winding of hot-rolled rebars into highly-compact/ultra-heavy coils featuring a unique cobble-free un-coiling capability. This enables high-speed feeding of the downstream cold-processing lines with hot-rolled spooled coils coming directly from the rolling mill without the need of any traditional off-line operation (such as de-coiling, stretching & re-winding). The system results highly beneficial both to bar-in-coil producers and to the downstream lines operators. The latest step forward is the combined application of these two systems that has made it possible for endless rolling of spooled bar in coils, enabling to cumulate the benefits of the two processes, particularly as far as transformation costs are concerned.

Aug 16, 2017

By Alberto Tremea

The eddy current system is universally recognized as a most suitable method to point out discontinuities or modifications on the roll surface. The automation of the controls through the implementation of sophisticated equipments on the grinding machine has favoured its employment in the roll shop. A big effort is still going on to clarify the best way to promptly identify situations that could be really unsafe for the roll life. The results presented in this paper have been obtained through an intensive activity conducted in field by Innse Cilindri on work rolls of finishing stands of hot strip mills. The correct interpretation of the eddy current signals and a good calibration of the automatic system have allowed, in many cases, a substantial optimisation of regrinding practices.

Aug 16, 2017

By Paul Riches

LR Process Expert is a cost-efficient process automation system for all types of long rolling mills, including, rod, bar, section, rail, reversing mills, and flat blocks. The system performs a wide range of tasks for optimized operation – from suggesting pass schedules to calculating and downloading optimized mill settings according to the availability of rolls. LR Process Expert also monitors and collects data from the raw material stage through to the finished product. It delivers valuable mill reports to the operator staff and management so they can easily assess a plant’s performance and optimize production. Defined Key Performance Indicators (KPIs) help to assess a plant’s performance; this system is not limited to one plant but can enable plant-toplant performance at corporate level.

Aug 16, 2017