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By J. J. Bodmer

In 1855, Franz Uchatius patented, in England, his process of manufacturing cast steel. The first experiments, on a practical scale, were made at the Ebbw Vale Iron Works, Monmouthshire. The charge consisted of a mixture of cast iron with about 20 per cent. of a pure iron ore, and with or without other ingredients. In order to obtain the cast iron in a subdivided condition, Uchatius granulated molten pig-metal by running it into water, which during the operation was kept well agitated, and found that "the finer the iron is granulated, the softer will be the resulting steel." The writer is not aware that granulated iron has been used practically, otherwise than in the above-named process; and until 1866 no other process of subdividing iron than by granulation was known. In April, 1866, an English patent was obtained by the writer for subdividing blast-furnace and other slags and metals in a molten condition, by passing the same through one or more pairs of rolls. In reference to iron the idea was, in following up the direction pointed out by the Uchatius process, to obtain better results in the puddling process by means of a thorough amalgamation (not simply a mixture) of the iron with the oxides and other ingredients in the charge itself. Experiments were made. A quantity of iron direct from the blastfurnace was subdivided (or laminated) by passing it through a pair of plain rolls. The rolls were hollow, and water was made to pass through them to keep them sufficiently cool. Without giving differential speed to the rolls, sheets were obtained about one-sixteenth inches thick, and from about one hundred square inches surface, downwards. With differential speed, the iron falls from the rolls in

By Samuel S. Wyer

The magnitude and economic importance of the problem of correctly valuing natural-gas leaseholds become evident when me consider that: (a) Natural gas is handled in 55 per cent. of the gas distributing plants in the United States. (b) Present known natural-gas acreage forms 47 per cent. of the total known mineral-land acreage in the United States. (c) Five acres of land are now required to protect and maintain continuous service to each of the 2,000,000 domestic natural-gas consumers in the United States. (d) The cost of acquiring and maintaining this acreage of an expendible resource represents a substantial part of the cost of the natural-gas service to the consumer. (e) "The right of a citizen by means of his ownership of or his mining leases on land to draw gas from beneath its surface is property and sometimes valuable property."' A large number of other court decisions have established the basic legal principle that the right to drill for gas within a given area constitutes an interest in the land itself, and is necessarily an exclusive property right. Definition of Vested Interests or Rights "Vested interests are economic interests which are legally recognized to be such that they cannot be impaired by public action, directly or indirectly, without indemnification. Vested interests are largely property interests. The recognition of an interest as a vested interest gives it some of the attributes of property, and by American courts it would be comprised in their very inclusive concept of property. Otherwise than through property, vested interests generally arise through contract."

Jan 1, 1917

By Sanford S. Cole

LABORATORY TESTS Takakuwa and Takamori' have applied the principle of phase inversion, well known in the chemistry of colloids, as a means of evaluating the wettability of minerals and to classify some frothing agents. By determining the angle of contact across the liquid phase of an emulsion, it has been possible to readily determine the wettability of a mineral. When this angle is less than 90°, the emulsion is of the oil-water type, and if it is greater than 90a, then the emulsion is of the water-oil type. The authors replaced oil with benzene in their recommended operation. They studied this method with the influence of ethyl xanthene on galena, on activated or unactivated zinc blend and of sodium cyanide on chalcopyrite and zinc blend. Raffinot and Formanek" described a pilot flotation plant with a capacity of 33 to 66 lb per hr of ore which is at the Laboratory of the Sociktk Minerais et Metaux in Paris. The plant will handle about 440 lb of ore per 8-hr shift and a regular series of tests can be undertaken with two to three tons of ore. Ore is ground to 0.1 in. and blended in advance. The plant includes two mills used either as rod mills or ball mills, conditioners, four groups of three cells for rougher circuits, eight cleaner cells and two small mills for regrinding middlings. Automatic controls for the pulp level in the cells, automatic sampling and addition of flotation reagents by electric valves facilitate plant operation and help to produce regular runs in spite of small throughputs.

Jan 8, 1963

By G. S. Hume

IN. THE autumn of 1922, British Petroleums Ltd. found oil of 14° Baumé in a sand 17 ft. thick in its. No. 2 well at Wainwright, 120 miles southeast of Edmonton. This greatly encouraged drilling in the Wainwright-Irma area and this past summer several wells were started, three of which are now completed and the others still being drilled. Of the three completed, No. 4 British Petroleums contains oil; No. 3 British Petroleums gave a show of oil but so far has not given much hope, of becoming a commercial producer; and No. 1 Maple Leaf Co., as now finished, is a. gas well with a daily flow of gas of about 2,500,000 cu. ft. at a closed pressure of 700 lb. An oil sand is reported to have been encountered below the producing gas horizon in the Maple Leaf well but has not been tested. Operations on this well have been suspended for the winter. The Geological Survey of Canada this past summer undertook a geological investigation of this area with the object of defining the structures with which the oil and gas are associated. The structure underlying this portion of the plains was supposed to be a terrace with the western edge dipping into the Alberta syncline and with a monoclinal structure to the east. By accurate leveling on known geological horizons on this terrace, a number of gentle folds were located and -it is in these folds that the oil and gas are found. At the British Petroleums Nos. 2 and 4 oil wells, the western flank of the fold has a gentle dip of only a few feet to the mile to the southwest whereas the strata on the eastern flank dip to the northeast about 40 ft. in ½ mile, the strike of the fold being northwest and southeast. How far oil will be found down the gentle southwest dip is unknown but probably the productive part of the fold will not exceed 1 mile in width, and possibly less. No. 3 British Petroleums well is on the strike of the fold 1 mile southeast of the two oil wells. The sand that was productive in Nos. 2 and 4 wells was not present in this well or, if present, was very thin and unproductive. Two other sand horizons, however, were encountered. The upper of these

Jan 3, 1925

By Frank T. Sisco

DURING the past year the iron and steel industry of the world as a whole operated on a satisfactory basis. No discoveries nor new processes of outstanding importance were announced either here or abroad, although rumors of such were persistent. In general, the efforts of operating and research men in the iron and steel industry seemed to be confined to improving quality and reducing cost, not a new aim, for the same efforts have been noted in nearly all of the annual reviews of the industry for at least fifty years. Most published papers on blast furnace or steel-making practice were of minor importance, at least when judged by the criterion of radical change in process or product. If the number of reports in the technical journals, or articles in the trade press, is used as a basis for comparison, continuous-mill sheet is still the most important single product of the industry; papers were published detailing the results of the investigation of various phases of the

Jan 1, 1938

By J. S. Bowles

DISCUSSION, M. Cohen presiding J. W. Christian (The Inorganic Chemistry Laboratory, oxford, Englandl)—I was very interested in Dr. Bowles' results on the suppression of the transformation by solid films of alcohol or propane. The transformation in cobalt, which is also martensitic, can be explained by a mechanism involving the reflection of "half dislocations" down a series of atomic planes.* This reflection process is similar to that considered by Frank13 for plastic deformation on a single slip plane and, as he pointed out, reflection would be impossible if the metal were immersed in a liquid of higher density. It seems possible that solid films of alcohol have a similar effect on the lithium transformation. Reflection should also be possible at a grain boundary, though a higher kinetic energy of the dislocation, and hence a lower temperature would be required. As Dr. Bowles used coarse grained polycrystalline speci- mens, transformation on cooling should still have occurred in grains which did not form part of the outside (free surface) of the metal. This may account for the X-ray lines of the low temperature phase which were found. There is thus the interesting possibility that in a polycrystalline specimen a liquid, or in some cases a solid, film of material of or or higher density will lower M,, while in a single crystal it should suppress the transformation completely. In the case of cobalt it is necessary to find a dense liquid which will not react with the metal at the transformation temperature. The most promising liquid appears to be pure lead, but it is very difficult to devise a method of investigating whether or not this does suppress the transformation.

Jan 1, 1952

By J. S. Marsh

JOSEPH PRIESTLEY prepared oxygen on Aug. 1, 1774, and noted with great surprise "that a candle burned in this air with a remarkable brilliant flame." On Aug. 2, 1774, some ironmaker possibly began to wonder if this substance could be used to increase his rate of production; at any rate, there is no disputing the fact that the notion of using oxygen for steelmaking in concentrations greater than that available in great abundance-as air-has been in existence for years. Action was delayed by the lack of enough oxygen at a cost within reach of the steelmaker. Within the last several years enough has been available to permit large-scale tests of its use for both combustion, with which this paper is concerned, and for decarburization. The literature is now enormous and easily available; it is sufficient here to cite three items of historic- importance in that all are about 25 years old and in that all are remarkably consistent as far as they go, with what is known today.1,2,3 SIGNIFICANCE OF HIGH-TEMPERATURE HEAT The principal 'function of the open-hearth furnace is to supply sufficient, high-temperature heat to melt the charge and then to increase its temperature to a range suitable for tapping, ordinarily in the neighborhood of 2900°F. That heat is required to make steel everybody; however, there seems to be some confusion now and then about the significance of high-temperature heat. Transfer of energy-and heat is energy is always from a point of higher potential to a point of lower potential and, other things being equal, the greater the potential difference, the greater is the rate of transfer of energy. In the open hearth the flame, of course, is the high-potential source. Perhaps the most satisfactory approach is through the notion of theoretical flame temperature; which is the ratio of heat input to the heat content of the combustion products,* the former is composed mainly of heat of combustion of the fuel plus sensible heat of the fuel plus sensible heat of the combustion air. Thus, flame temperature can be increased by increasing the value of the numerator, by decreasing the value of the denominator, or both. The first method is as old as the open-hearth process and, of course, makes use of preheated air; its possibilities have been by no means exhausted. The second method can be put into effect only by changing the composition of the combustion air, since the combustion of a given quantity of fuel produces a definite quantity of product, and since the denominator includes the non-reactive fraction of the air, principally nitrogen. In other words, the denominator consists of the volume of exit gas multiplied by its heat capacity and that volume consists of carbon l is understood by dioxide and water vapor as reaction

Jan 1, 1948

By J. S. Browning

The pegmatites of the Kings Mountain-Lincolnton, N. C., area constitute the largest known domestic reserve of beryl and spodumene. The reserve is estimated to contain 90 million tons of pegmatic material with 1,280,000 tons of recoverable Li2O (lithia) as spodumene.1 The pegmatites also contain 0.4 to 0.5 pct beryl disseminated throughout the orebodies. The pegmatites may contain a potential reserve of 240,000 tons beryl, equivalent to approximately 34,000 tons of BeO. Different flotation methods for separating beryl from feldspar or quartz, or both, have been developed by various investigators.2,3,4,5,6,7 On the other hand, published information is limited on concentration of spodumene-beryl ores. As the response of beryl and spodumene to flotation is essentially the same, a successful separation of the two minerals depends upon use of a selective depressant or a selective collector for one of the minerals.

Jan 7, 1961

By David S. Butts

There are many solution mining operations that use solar ponds as a mineral recovery step. Other locations in the world are now under investigation to recover minerals by solution mining but require the cheap energy of solar ponds to make the recovery viable. This paper shows a step-by-step material balance system that can be used in both simple and complex solar ponds. Use of this system will help the engineer determine if solar ponding efficiency can be improved or if solar ponding will work at all with a given set of conditions. Even the most complicated solar pond can be reduced to six flow streams. These are (1) feed, (2) exit, (3) leakage, (4) entrainment, (5) salts, and (6) evaporation. The equations developed in this paper will allow the solar pond engineer to easily evaluate the effect of each of the flow streams on the mineral production of a pond or pond complex.

Jan 1, 1985

By G. S. Hume

IN THE autumn of 1922, British Petroleums Ltd. found oil of 14° Baume in a sand 17 ft. thick in its No. 2 well at Wainwright, 120 miles southeast of Edmonton. This greatly encouraged drilling in the Wainwright-Irma area and this past summer several wells were started, three of which are now completed' and the others still being drilled. Of the three completed, No. 4 British Petroleums contains oil; No. 3 British Petroleums gave a show of oil but so far has not given much hope of becoming a commercial producer; and No. 1 Maple Leaf Co., as now finished, is a gas well with a daily flow of gas of about 2,500,000 cu. ft. at a closed pressure of 700 lb. An oil sand is reported . to have been encountered below the producing gas horizon, in the Maple Leaf well but has not been tested. Operations on this well have been suspended for the winter. The Geological Survey of Canada this past summer undertook a geological investigation of this area with the object of defining the structures with which the oil and gas are associated. The 'structure underlying this portion of the plains was supposed to-be a terrace with the western edge dipping into the Alberta syncline and with a monoclinal structure to the east. By accurate leveling on known geological horizons on this terrace, a number of gentle folds were located and it is in these folds that the oil land gas are found. At the British Petroleums Nos. 2-and- 4 oil wells, the western flank of the fold has a gentle dip of only a few feet to the mile to the southwest whereas the strata on the eastern flank dip to the northeast about 40 ft. in 1/2 mile, the strike of the fold being northwest and southeast. How far oil will be found down the gentle southwest dip is unknown but probably the productive part of the fold will not exceed 1 mile in width, and possibly less. No. 3 British Petroleums well is on the strike of the fold 1 mile southeast of the two oil wells. The sand that was productive in Nos. 2-and 4 wells was not present in this well or, if present, was very thin and unproductive. Two other sand horizons, however, were encountered. The upper of these

Jan 3, 1925

WILLIAM B. PRICE* and PHILIP DAVIDSON, ? Waterbury, Conn. (written discussion?).-A few months ago we became interested in deter-mining the properties of. pure nickel as a metal for certain uses and arranged, in cooperation with the International Nickel Co., a series of tests on cold-rolled so-called pure nickel and both longitudinal and transverse specimens annealed at 100° intervals from 250° to 1050° C. Since our tests confirmed; in a general way, the observation put forth by Messrs. Browne and Thompson, they are given at this time. A bar of hot-rolled nickel about 9 in. (23 cm.) wide and 1/2 in. (12.7 mm.) thick made by the International Nickel Co. -of grade A stock, analyzing nickel plus cobalt 98.48 per cent., iron 0.67 per cent., manganese 0.27 per cent., carbon 0.07 per cent., silicon 0.162 per cent., sulfur 0.033 per cent., and copper 0.22 per cent., was cold-rolled down to a final thickness of 0.134 in., malting a 73.2 per cent. reduction by rolling. Test specimens, 9 by 1 in., cut parallel (marked longitudinal) and normal (marked transverse) to the direction of rolling were milled to give a test section 2 5/8 in. long by 0.5 in. wide. Three specimens each, longitudinal and transverse, were annealed at one time in a nichrome-ribbon-wound tube furnace. The temperatures were taken with a Pt-PtRh thermo-couple in conjunction with an Engelhard millivoltmeter. An annealing period of .) 2 hr. plus 25 min. preheating was used in all cases. Sclero-scopic and Brinell hardness tests and static tensile tests were made on the rolled and annealed specimens. The tensile tests are shown in graphic form in Fig. 7. The Brinell and scleroscopic values are given herewith.

Jan 11, 1919

By H. S. Rawdon

One of the most vital problems in the manufacture of steel at present is the occurrence of the defects that have been popularly termed "snow flakes," "flakes," or "scabs." Particularly is this the problem of many manufacturers who, during the past 2 yr., have undertaken large-scale production for the first time. A study of the microstructure of such defective material throws considerable light upon the nature of these defects and is essential before measurcs may be taken for the elimination of the defects. Flakes do not appear to be found in the plain carbon steels; they have been found. however, in abundance in some of the simple alloy steels that are being used in such vast quantities; vie., nickel steel of the approximate composition, 0.40 carbon and 3.5 per cent. nickel, and in the chrome-nickel type. The present article summarizes the characteristic features of defective steel of the flaky type as they have been found by laboratory study of numerous specimens, and it aims to show the conditions within the metal that are favorable to the occurrence of this type of defect without entering into the details of mill practice (size of ingot, design of molds, rate of cooling, distribution of cooling stresses, etc.), all of which conditions appear to play a role in the production of these defects. MacrostrUctURe To one familar with flaky steel, the appearance of "snow-flakes" is unmistakable and is not to be confused with other types of defects. Figs. 1 to 6 show the appearance of fractures of steel showing this type of defect; the white silvery area, which always has the appearance of being of a very coarsely crystalline structure, in the specimen stands out in bold contrast to the darker background and readily justifies the use of the term "snow-flakes." Fig. 1 shows the appearance of the faces of the two halves of a nickel-steel forging that has been split to show the interior flakes. Fig. 2 is a nickel-steel bar (carbon 0.40 per cent.,

Jan 1, 1920

By E. P. Polushkin

The object of this paper as to show that the structural composition of an alloy may be found by the planimetric measurement of the total area occupied by each of the constituents on a few representative photomicrographs of this alloy. When the area is determined the volume and the proportional weight of the constituent may be calculated. This method has been used for the determination of the structural composition of binary eutectics and other binary alloys with known constituents; also the composition of unknown constituents in binary alloys. The accuracy of the method is. high enough to justify its application to metallographic problems instead of the chemical analysis. THIS work has for its purpose the establishment of a new method for determining the structural composition of alloys. The area occupied by a constituent on a few representative photomicrographs of the alloy is measured, by a planimeter, especially designed for metallographic work, and the volume and proportional weight of the constituent calculated. Experiments have shown that 'the results are accurate enough to justify the application of the method to many problems in metallographic research instead of chemical analysis. The advantage of the method is the possibility, of determining the amount of the constituents with-out separating them from the alloy; their composition may also be determined if the ultimate chemical analysis of the alloy is known. DESCRIPTION OF PLANIMETER Suppose Fig. 1 represents a part of a photomicro-graph on which the total area of the black figures is FIG. 1?-PART OF PHOTOMICROGRAPH ON WHICH TOTAL AREA OF BLACK FIG- URES IS TO BE FOUND. to be found. By a system of parallel lines drawn short equal distances apart all figures may be divided into trapezoids. As the area of a trapezoid is equal to its median multiplied by its altitude, the relation between the total areas of the black and the white figures comprised within each strip is equal to the relation between the sums of medians for these figures respectively.

Jan 12, 1924

By Arthur S. Wright

THE accuracy of the silver-assay depends in great measure upon a careful regulation of the heat of the muffle during the process of cupellation. At the beginning of the operation, a relatively high temperature is required to " open " the lead buttons, that is, to clear off the black film of oxide that covers the surface of the metal button immediately after fusion has taken place. The muffle is usually closed up until the buttons are uncovered. As soon as a clear, free surface of molten metal is exposed to the oxidizing action of the air, the temperature should immediately be lowered to the minimum temperature at which the formation and absorption of litharge can progress freely, and the buttons still be kept from " freezing." The process, under satisfactory conditions, will be characterized by the formation of rings of litharge crystals (" feathers," as they are styled), on the cupel, about the oxidizing globule; and the nearer these rings of litharge crystals call be made to approach the central oxidizing globule without interfering with the freedom of oxidation and absorption, the smaller will be the volatilization of silver, and consequeiltly the greater the degree of accuracy attained. This minimum heat must be maintained uniformly during the oxidation of the lead; and just as the last of the lead is disappearing, and the button is preparing to l blick," the temperature of the muffle should be allowed to rise so that the last traces of lead will be driven off. This regulation of the heat calls into play all the skill of the assayer, and requires a vigilant eye, able to distirlguish between the slightest variations of temperature of the muffle, assisted by a nice adjustment of fuel and draft. With a few cupels in the muffle at one time, the proper heat for each cupel can be maintained by roughly approximating the proper temperature, and then moving the cupels backward and forward in the muffle; but this is gene-

Jan 1, 1897

By Claus G. Goetzel

PRESSING of powdered metal parts is best done in the direction of the shortest extension of the piece, to avoid too great a loss of pressing force through internal [ ] friction. As long as curved surfaces, recesses, or offsets occur only parallel to this shortest axis of pressure, no special difficulties arise: the cross sections, perpendicular to the pressure, do not vary, nor does the shape of the parts change during compression except for a gradually reduced thickness (Fig. IA). The problem becomes more difficult, however, when the curved surfaces or recesses are perpendicular to the shortest axis of the part (Fig. IB). Two processes for molding uniformly dense parts with complicated shapes from powdered metals are described in detail in this paper. Both can be employed successfully by those trained in the art. The first refers to curved parts; the second is especially adapted to parts having one or more recesses or steps. Both methods, as set forth here, are applied under the condition that presents the more difficult problem. For clarity, before description of the two practical methods, the variable factors in molding powdered metal parts will be reviewed, then an idealized procedure will be considered briefly. VARIABLE FACTORS IN MOLDING POWDERED METAL PARTS Compression Ratio Compression ratio is defined as the proportion of the final relative density of the compact to the apparent density of the powder. For iron powder of an apparent density of 3.0, for example, a compression ratio of 2 1/2 : I would be required to produce a compressed compact of 7.5 density; whereas for another iron powder having an apparent density of only I.5, a compression ratio of 5:I would be required to produce the same density. The lower the powder's apparent density, the greater must be the compression ratio for pressing compacts of high density.

Jan 1, 1945

By Nicholas J. Grant, Rolf Nordheim, Thomas B. King

Constant-load creep-rupture tests were conducted in an argon atmosphere at temperatures of 1600 to 2200°F on two heats of iron containing about 0.06 and 0.09 pct P in solid solution. The tests were conducted in the as-cast condition. Stresses were selected to give strain rates approaching those encountered in the hot working of steel, and within the limits of the creep-rupture test apparatus, namely. from about 0.001 to 50 pct per sec. FOR generations, rolling and forging practices have been developed largely by empirical methods, based on prior experience. While largely successful, difficulties are frequently encountered when new or different alloy compositions are tried for the first time. There is need to know the relationships which exist among temperature, strain rate, composition, and other variables on the deformation and fracture characteristics of steels. It has been shown for aluminum and several high-temperature alloys that the deformation and fracture characteristics follow rather well-defined laws and patterns which are closely related to the effects of strain rate, temperature, and composition.1"3 As the melting temperature of aluminum or its alloys was approached, it was possible to study the interplay of work-hardening factors and recovery or recrystal-lization, the latter resulting in improved ductility and increased resistance to intercrystalline fracture. In particular, the effects of composition are very poorly known. Within the meaning of "composition" should be included impurity elements, such as sulfur, phosphorous, lead, copper, and many others, as well as those elements which are added for alloying purposes in iron. The role of multiphase structures, in contrast to solid solutions, should also be studied in much greater detail. high strain rate creep-rupture tests would provide information regarding the deformation and fracture characteristics of metals at hot-working temperatures. It was also desired to establish the stresses which are necessary to accomplish the desired deformation, and to relate these to the strain rate and temperature. Secondly, it was the purpose of this particular study to determine the effects of phosphorus, within solid solution limits, on the deformation and fracture characteristics of iron at hot-working temperatures. EXPERIMENTAL PROCEDURE Two phosphorus levels were selected, one corresponding to the upper limit normally found for commercial steels, and one substantially higher than this, but within the region of solid solubility at the test temperatures chosen for this investigation. Twenty-pound heats were prepared by induction melting electrolytic iron in air in a magnesia lined furnace. After deoxidation with about 0.2 pct Al, ferro-phosphorus was added, and the heats were then poured into prefired silica molds. The purpose of using silica molds was to obtain a slow cooling rate during solidification to produce a relatively coarse grain size, producing a structure subject to some segregation and therefore more nearly characteristic of ingot structures. The major part of the casting assembly provided a large shrinkage head in order to produce sound castings and to promote slow cooling of the specimens. The primary austenitic grain size varied from ASTM No. 2 to No. 00. The composition of the heats, including a low phorphorus melt, used for comparison purposes, is shown in Table I. It will be noted that the oxygen content of the phosphorus containing heats is relatively high, in spite of the deoxidation practice, a condition which is difficult to control in small melts. Creep-rupture tests were nevertheless undertaken when it was noted that this quantity of oxygen did not appear to give results any different from those from a heat containing 0.01 pct 0, low phosphorus and comparable carbon Content;4 see Table 11.

Jan 1, 1961

By Walter S. Larsh

The Ruth orebody, so far developed, is roughly oval in plan, major and minor axes about 1600 ft. (457 m.) and 1200 ft. (365 m.) respectively, average thickness about 120 ft. (36 m.), and with a general dip of about 15" to the northwest. According to the generally accepted theory, the ore is a secondary enrichment of the porphyry due to leaching in situ by meteoric waters. Copper occurs as chalcocite, chalcocite coating pyrite, and a little chalcopyrite. The leached zone, or capping, covering the ore varies in thickness from 110 to 540 ft. (33 to 164 m.), average about 410 ft. (124 m.). The ore is blue gray in color, and the capping, light yellow to brown. Ore was first discovered in quantity in the workings from the Ruth shaft, now caved. Further development work was done by churn drills, and the outline of the orebody, as stated above, determined in this manner. Drilling is still being carried on. The porphyry area is entirely surrounded by sedimentaries, limestones, and shales; and, in so far as the underground workings have shown, the porphyry itself, the sedimentaries' near the contact, and the country underlying the ore (igneous or sedimentary) is very soft, heavy, and in places swelling ground. All openings have to be carefully and stoutly timbered, and, after once driven, they have to be constantly eased off and repaired. The mine Is at present served by two shafts, the Star Pointer, the main working shaft, a vertical, and the Ingersoll, an incline used for waste and material. The two shafts are about 2600 ft. (792 m.) apart, connected on the 500 level; a connection is now being driven on the 600 level. (Dec., 1917. This connection is now completed.) The 300 level, which is finished, and the 400 level which is nearly completed, are accessible only from the Ingersoll and connections with the 500 level. The 300 level was developed for and mined by the shrinkage stope system, similar to that used successfully in the Ray Consolidated property.

Jan 1, 1918

By Howard S. Lee

In central Colorado is a great belt of intrusive porphyry nearly 100 miles long (160 km.), extending from the Clear Creek district on the north to Aspen on the south, which includes many of the well known mining camps of the state. Near the southern end of this belt, at Leadville, the occurrence of these intrusives is most marked, resulting in intensive mineralization and the formation of a great variety of large orebodies. During the past 40 years, Leadville has been a steady producer of gold, silver, lead, zinc, manganese, iron, and bismuth, in the forms of sulfide, carbonate and oxide ores. It is the purpose of this paper to discuss pyrite alone, which, under present economic conditions, is valuable chiefly for its sulfur contents. The ore-bearing formation of the Leadville district consists of two beds of limestone separated by a layer of quartzite. The upper limeatone is carbonaceous, and is known locally as the blue limestone. It varies in thickness from 50 to 300 ft. (15 to 91 m.). The lower limestone is Silurian, known locally as white limestone, and is about the same thickness as the upper bed. Underneath the Silurian limestone is a layer of Cambrian quartzite from 100 to 250 ft. (30 to 76 m.) thick resting on Archean granite, which forms the limit of ore deposition. As a rule, there is a sheet of white porphyry above the upper, or blue limestone; a sheet of gray porphyry is associated with the blue limestone, either in or below it, but the porphyries are not so regular as the quartzites and limestones and are not always found in their expected positions. Throughout the district there is an elaborate system of faults and intrusive porphyry dikes, which have an important bearing on ore deposits. The writer has seen two or three orebodies which were not closely associated with either a fault or a porphyry dike, but if the minor fractures and water courses are considered as part of the fault system it is safe to say that all orebodies are directly traceable to one or both of these causes. The distribution of pyrite in the Leadville district is quite general; but, eliminating the smaller bodies and those containing prohibitive quantities of zinc or lead, and considering only the larger deposits commercially valuable for their sulfur, we find the chief pyritic ore-bodies extending in a zone approximately 6000 ft. (1828 m.) long and several hundred feet wide, from the Yak and Moyer, on the south; through the Louisville, Greenback, Mahala, Adams, and Wolftone, on Carbonate Hill; across Yankee Hill, and into the Quadrilateral, Denver City, and Tip Top, on Fryer Hill.

Jan 1, 1920

By S. F. Emmons

Introductoy.—In view of the fact that an opportunity is to be offered to the members of the Institute present to inspect the recent developments of gold-deposits in the immediate vicinity of Washington it has seemed appropriate that some preliminary description of them should be given which may facilitate that inspection. It would have been a matter of much satisfaction to me to be able to present some general description of the gold-deposits of the Appalachian system ; but I have as yet had no opportunity of personally examining any others than those of Montgomery county, and these are still in their infancy. It is, moreover, a slower and more difficult operation to make geological observations in this region than in the more northern States; for whereas in the latter region the

Jan 1, 1890

By S. B. Lement

THE nature of the carbides that form during the tempering of martensite is a subject of continuing controversy. The only direct methods of identification available are X-ray and electron diffraction. These methods are subject to several difficulties. Only a relatively few diffraction lines of appreciable intensity emanate from carbide phases that are formed at low tempering temperatures. Furthermore, some overlapping of carbide and matrix lines occurs. There is also the problem that numerous lines in the patterns of possible carbide phases that may be present have about the same d-spacings. Increasing the number of carbide lines and eliminating the matrix lines can be accomplished by extraction techniques. However, there is always the possibility that a change in carbide structure will occur as a result of removal from the parent matrix. Therefore, such techniques as electrolytic extraction and making extraction replicas should be checked by other methods. For identifying small amounts of carbide in a tempered martensitic matrix, electron diffraction carried out in reflection is more advantageous than X-ray diffraction. To properly prepare a specimen for reflection electron diffraction, an etchant that will selectively attack the matrix and thereby cause the carbide particles to stand in relief should be used. With an electron beam directed at a grazing angle to the specimen surface, the major contribution

Jan 1, 1960