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By R. L. Hopkins

The work described was performed to determine whether sulfur compounds of the thienothiophene class occur in crude oil. The presence or absence of various classes of sulfur compounds in crude oils is of interest and value to petroleum science. The Bureau of Mines, for the first time, identified hydro-carbon products of desulfurization that point directly to the identity of two individual thienothiophenes, namely 3-methylthieno[2,3-b]thiophene and 2-meth-ylthieno[3,2-b]thiophene, in Wasson, Texas, crude oil. These identifications, described in detail, were accomplished using microdesulfurization, mass spectrometry, and gas-liquid chromatography.

Jan 1, 1966

By M. G., Corson

1. In addition to the alloys of copper with iron previously found by Hanson and Ford to show an increase in the concentration of the alpha range with increase in temperature the following binary and ternary systems have been found by the author to exhibit: the same feature: (a) Copper-chromium. (b) Copper-cobalt. (c) Copper-silicon. (d) Copper-nickel-silicon and its pseudo-binary section Cu-Ni2Si (formula of compound definitely established). (e) Copper-cobalt-silicon and its pseudo-binary section Cu-Co2Si (formula of compound established with some probability but not as definitely as for Ni2Si). (f) Copper-chromium-silicon; formation of a compound definitely established (compare Figs. 1 and 2). The formula of this compound may be either Cr2Si or Cr3Si. (g) Copper-iron-silicon; presence of a phase containing both iron and silicon established in an indirect way only. No definite microconstituents observed. 2. RANGES OF SOLID SOLUBILITY (percentage at various tempera¬tures). (a) For copper-chromium: 0.8 at 1000° C.; 0.5 at 900° C.; 0.25 at 800° C.; 0.05 to 0.1 at 500° C. (b) For copper-cobalt: 3.4 at 1000'C.; 2.4 at 900'C.; 1.7 at 800'C.; 0.9 at 600°C.; 0.35 at room temperature. (c) For copper-silicon (Fig. 3) : 6.8 ± 0.1. per cent. at 800° C.; 3 per cent. at 400° C. and probably below 2 per cent. at room temperature if sufficiently long annealed. (d) For copper-cobalt silicide: 3.3 at 1000° C.; 2.4 at 900° C.; 1.6 at 800° C.; 0.7 at 600° C.; 0.3 at 300° C. (e) For copper-nickel silicide (Fig. 4): 8.2 at 1000° C.; 5.5 at 900° C.; 3.6 at 800° C.; 1.6 at 600° C.; 0.7 at 300° C.

Jan 1, 1927

By T. A. Lazier, C. S. Longley

"Paymaster Consolidated Mines, Limited, owns several groups of claims in various parts of the Porcupine district. The area in which mining has been carried on includes parts of lots 5, 6, and 7, con. 1, Tisdale township, and twelve adjoining claims in Deloro township to the south. Highway No. 67A between South Porcupine and Timmins crosses the property.The discovery of the Dome mine in 1909 caused a rush of prospectors to the district and in a few weeks practically all territory adjacent to the Dome was staked. At that time work was started on the West Dome, West Dome Lake, Apex, and Standard properties. These were consolidated in 1930 to form the present Company. Gold was produced from the West Dome Lake from 1915 to 1930, and from the Standard-Paymaster from 1922 to 1928. The total production of the previous and present companies from 1915 to November 30, 1946, has been 487,170 oz. gold and 149,342 oz. silver from 2,337,554 tons of ore."

Jan 1, 1954

By José Bellina E

"El propósito del siguiente estudio es mostrar el análisis comparativo de los reactivos de flotación de las distintas nacionalidades (americana, alemán, japonés)-en tanto herramienta de conocimiento y difusión- para el manejo de plantas metalúrgicas del país. Los factores a considerar en dicho estudio fueron: igualdad en factor molienda, densidad de pulpa, pH en el circuito, tiempo de flotación y prueba de paladas. Los reactivos utlizados son Xantato(Z-3), Xantato,(Z-4), Xantato(Z-5),Aeroflat 15, Aeroflat 25 y aceite de pino,respectivamente. Concluyendo que de cada reactivo estudiado, se compara su calidad como promotor y factor precio. Así para el XANTATO Z-3, el Xantato americano y alemán son de calidad semejante, con la variante que el alemán es un 22% más económico en su precio de compra. En cuanto al xantato japonés es de menor fuerza que los anteriores, siendo su precio más o menos igual al alemán. En el XANTATO Z-4, el xantato americano es de mejor calidad que los otros dos, aunque estos son también un 22% más económicos. Para el XANTATO Z-5, no hay casi diferencia entre el xantato alemán y el americano en cuanto a su calidad como promotor. El precio del xantato alemán es un 30% menor que el americano. En cuanto al xantato japonés es de menor fuerza que los anteriores, siendo su precio mayor que el xantato alemán. En el AEROFLOAT 15, es evidente que el aerofloat americano es mejor en calidad como promotor que los otros dos y su precio es casi similar al alemán. El japonés es inferior en calidad y su precio es similar a los otros. De otro lado, en el AEROFLOAT 25, el Aerofloat alemán da mejores resultados para esta flotación de cobre oxidado, donde su precio es similar al norteamericano. El japonés es inferior en calidad y su precio es también similar a los otros. Finalmente en el Aceite de pino, es indiscutible que el americano sea de mejor calidad que el alemán y japonés, sin diferencias destacables."

Jul 20, 1956

By J P. Bolduc, P. E. Pelletier

Preceded by brief general considerations such as the development of the mining industry in. the Province of Quebec, the choice of plant location, the types of problems studied etc., the paper gives a complete description of this new research and treatment center for metallic, non-metallic and asbestos ores. Facilities for carrying out operations in the three sections of the plant -the sampling section, the ore treatment section and the asbestos section -are fully discussed as well as laboratory facilities for (a) the preliminary testing of ores prior to pilot plant treatment and (b) the grading and testing of asbestos fibre. AT THE beginning of the century, the annual value of the mineral production of the Province of Quebec stood at the $2,500,000 level. Twenty-five years later, it was just under $24,000,000. In 1950, half a century later, it was slightly in excess of $200,000,000. But in 1959, in the span of only nine years, it

Jan 1, 1962

By I. Garba

The Bin Yauri deposit in the Zuru schist belt of northwestern Nigeria is a vein-type quartz-sulphide-carbonate gold mineralisation hosted by a brittle fault zone. The occurrence of the mineralisation in a contact zone of a Pan-African granitoid was believed to be sufficient evidence of deposition from magmatic fluids. However, studies may now indicate a metamorphic source for the mineralising fluids. A study of rare earth element geochemsitry was used to investigate the nature of the fluid-rock processes involved and identify the sources of the auriferous mineralising fluids.

Jan 12, 1992

By James T. Kemp

AN historical society of particular interest to mining engineers all over the world was born in Cornwall in 1935. A hundred-year-old winding engine then finished its long labors at the Levant mine on the cliffs near Lands End, England. The engine was to be dismantled and scrapped. A few men living near-by, appreciating that this event was one of the final acts in closing a long century of extraordinary mining and engineering evolution. armed a committee to prevent the destruction of the old mine hoist and succeeded in purchasing the engine. They restored the engine house and in time arranged with the Manor of Trewellard, owners of the land, for a 99-year ground lease on a peppercorn rental.

Jan 1, 1947

By Eduardo Amado Marconato

Na usina siderúrgica de Cubatão da Usiminas, o forno de reaquecimento de placas do LTQ2 utilizava como gás combustível a composição de gases de coqueria, alto forno e natural. A partir da interrupção da produção das áreas primárias (Redução e Aciaria) em Cubatão, o equipamento precisou ser adaptado para uso exclusivo do gás natural como gás combustível. Além das adequações feitas nos sistemas de controle de combustão foram adotadas ações para redução do consumo de combustível como desenvolvimento de novos procedimentos de acendimento do forno, reduzindo o número de queimadores ligados visando aproveitar melhor o calor gerado pela combustão do gás natural. O sistema de combustão foi reconfigurado, permitindo reduzir a temperatura da zona de pré-aquecimento e o tempo de permanência no forno, com isso a economia alcançada no consumo térmico superior a 7%.

Oct 30, 2017

By Juan Enrique Alvarez Ogusko

Rotas hidrometalúrgicas para o beneficiamento do minério de cobre vem sendo estudadas a fim de substituir o processo tradicional por pirometalurgia. No entanto, o uso de soluções lixiviantes como o ácido sulfúrico e a amônia são considerados ambientalmente desfavoráveis ao processo e descarte. Além disso, durante a lixiviação do cobre também ocorre a lixiviação do ferro. O uso de glicina como agente lixiviante é uma alternativa de baixo impacto ambiental já que é um aminoácido capaz de ser metabolizado por organismos vivos. Na lixiviação, a glicina apresenta a capacidade de formar um complexo quelante apenas com o íon Cu2+. Esse trabalho buscou avaliar a capacidade de lixiviação de um minério de cobre concentrado proveniente do Peru. Para isso, três concentrações de glicina em meio aquoso foram avaliadas nas temperaturas de 25ºC (48 horas de contato) e 60ºC (duas horas de contato). O pH da solução foi mantido entre 10,5 e 11 com adição de hidróxido de sódio. Foi possível lixiviar acima de 30% do cobre usando 0,8M de glicina na solução e em ambas as temperaturas de estudo. Além disso, a lixiviação do ferro ficou abaixo de 0,6% mostrando a seletividade da glicina para o cobre durante a lixiviação.

Oct 30, 2017

By Jörg Schwelberger

Government regulations around the world concerning environmental care are becoming more stringent, also including regulations and restrictions of depositing and use of dust, sludge and slag generated in the iron and steelmaking process. With this scenario, by-products such as iron containing dust, sludge, oxide fines, mill scales and slag, become a valuable resource and recycling may be a profitable activity within a plant. Up to ten percent in mass of the total steel output of dust, sludge and mill scale by-product materials and more than 40% of slag by product are generated within an integrated steel plant with an iron content ranging from 50% to 65% for fines and up to 25% for BOF-slag. Slags are being widely recycled and used in the cement industry, as is the case for BF slag, and in the construction industry in the case of BOF slags and EAF slags. However, value of BOF unmodified slag is typically low and environmental regulations limit the usage of the unmodified BOF slag. This paper describes innovative solutions for recycling of fines using cold briquetting technology and the modification and granulation of slag from steelmaking that increase the value of the by-product and yield a marketable product.

Aug 16, 2017

By Jerin Russell

This paper presents a new instrument for real-time detection of excessively coarse material in the overflow pipes of individual hydrocyclones using a non-invasive acoustic measurement technique. The hydrocyclone is an important device used in mineral processing beneficiation circuits for classification of mineral slurries by particle size. It separates a single input stream into two output streams; an underflow of coarse particles that undergo additional grinding for further size reduction, and an overflow stream of finer particles that typically goes directly into a flotation circuit for recovery of the desired mineral. However the hydrocyclone is a major piece of equipment in the beneficiation process that has no instrumentation for directly measuring its performance. The parameters currently measured – inlet pressure, feed flow rate, feed flow density – are common to the entire hydrocyclone cluster which typically has three to twelve hydrocyclones. Thus no information is available to detect individual hydrocyclones that are operating poorly. The system described in this paper detects the presence of unwanted excessively coarse material in the overflow stream of a hydrocyclone using sensors mounted to the exterior pipe surface. It provides real-time monitoring, trending and alarming of the coarse material level. This enables operators to identify poorly performing hydrocyclones, and enables corrective action to reduce or eliminate the coarse material discharge. Improving the classification efficiency of individual hydrocyclones will improve the overall classification efficiency of a hydrocyclone cluster. This leads to less variation in the particle size distribution and slurry density in the flotation feed, which will in turn improve overall mineral recovery. The reduction of unwanted coarse material in the flotation feed reduces the accumulation of that material in flotation cells. This can lead to equipment damage, and unplanned shutdowns due to events such as blocked dart valves.

Aug 16, 2017

By Janaina Gonçalves Maria da Silva Machado, Carlos Mateus Braga de Almeidar, Leandro Miranda Nascimento

Knowing the reduction of the concentration of iron in the mineral load extracted in the last decades and, therefore, greater need for comminution processes, there is no denying that iron ores tend to get increasingly thin for steelmakers. In Reactors such as Blast Furnace and others of fusion-reduction, where the reduction of the iron ore for the metallic iron for the steel production occurs, we observed that one of the alternatives is to agglomerate the raw materials in the form of briquettes, improving the kinetics of the chemical reactions, since ores in the form of fines impair factors such as the permeability required for reduction. These agglomerates are composed of a reducer, fines of ferrous materials and a binder material, and require, in addition to satisfactory Metallization, mechanical resistance, avoiding losses when the compound is fragmented during transport or during its deposition in the Steel Reactor. In the following work, Briquettes were produced with Charcoal, Pellet Feed, Molasses Cane and Hydrated Lime. The mixtures were pressed under different conditions of Pressure (1, 2 and 3 tons-force), and pressing time (20 , 60 and 100 seconds), aiming to analyze the influence of these two variables on the drop tests, mechanical resistance of the briquettes generated.

Oct 1, 2019

By G R. Power

A useful way to assess potential productivity of SLC mines is by quantifying tonnes/drawpoint/day to be extracted from the mine. However limited industry information has been published to help mines benchmark this number. This paper assesses industry data which can be used to support estimates of potential productivity from new mines based on tonnes/drawpoint/day. The information used has been extracted from historical production schedules which indicate what was achieved, rather than what was planned. It has been assessed using an algorithm created for the purpose and is presented with discussion of varying definitions of active drawpoints, analysis of the data and inquiry into some of the underlying contributing factors.

Mar 15, 2021

By Ameir Altaee

Unconventional means and methods were utilized to install over 650 contractor-designed micro-piles for the replacement of the Bronx approach to the Bronx-Whitestone Bridge in New York City. The method utilized reverse circulation (RC) drill rods and down-hole-hammers (DHH) along with grouting through the DHH bit. The overall construction sequence of drill-down, grout-up, place reinforcing is similar to auger-grout piling. The extremely tough drilling conditions required the use of a percussive DHH. The piling subcontractor refers to this pile as a hammer-grout pile. Project background, constraints and subsurface conditions are given. The proposed means and methods as well as the collaboration between stakeholders are detailed. Results of load testing and production installation are summarized.

Jan 1, 2010

By George F. Weaton

Although an almost continuous campaign had been carried on by various experimenters since 1885 to find a commercial process of smelting zinc by electrothermic means, no commercial success was attained in the United States. The St. Joseph Lead Co., appreciating the theoretical possibilities of such a process, such as the ability to construct units of large capacity, quality control, and the possibility of treating complex and refractory ores, decided in 1926 that the process was worthy of further investigation, and in that year, at one of its southeast Missouri plants, began the development of the electrothermic zinc-smelting process according to the invention of the late Earl C. Gaskill. Late in 1929 the process reached a stage of commercial significance, and in 1930 the erection of a modern electrothermic zinc smelter was begun, at Josephtown, Beaver County, Pa. The site is 3 miles from Monaca, which is on the main line of the Pittsburgh & Lake Erie Railroad, and a spur of the railroad has been constructed to the plant site. The site borders upon the Ohio River, which is navigable for 600 to 800-ton barges. This district was selected for the plant after an economic survey involving such questions as cost and availability of electric power, reduction fuel, transportation facilities, and the transportation charges on raw and finished materials, labor conditions, and taxes. The initial unit of the plant was designed to treat daily 120 tons of 58 per cent zinc sulphide concentrates from the company's mines in St. Lawrence County, New York. The plant equipment is housed in seven modern steel-frame buildings, and includes: Roasting and Acid Plants 3000-ton concentrate storage. Two Nichols-Herreshoff 21 ft. 6-in. diameter, 12-hearth roasters with usual cast-iron airshaft supporting chromium-alloy rabble arms and rabbles. SO2 gas purification system consisting of: One double-compartment hot-dust Cottrell precipitator. Cast-iron sinuous air-contact gas cooler.

Jan 1, 1937

By I. S. Parrish

As noted by McKinstry (1948), "How to deal with erratic high samples is one of the knottiest problems in ore estimation." He described a variety of approaches and methods to alleviate the problem through the averaging and weighing of assay data and by "cutting" or "clipping" of the erratic assays. Bird (1991) elaborated on ways of dealing with the nugget effect (erratics). He listed several procedures for cutting. Bird's list has been reproduced and/or added to by several authors including Vallee (1992) and Stone and Dunn (1993). Missing from each of these otherwise excellent reviews is a definition, description or guideline to recognition of an "erratic," or just where or when cutting is warranted or justified.

Jan 1, 1997

By Dimitrios Polantzas P. E., Collin E. Sweeney E. I. T., Franklin M. Grynkiewicz P. E., Leili Javidanian P. E.

In the latest AASHTO design specifications, the Load and Resistance Factor Design (LRFD) method is prescribed for the design of retaining walls. However, inconsistencies arise when LRFD is used for retaining wall design versus the traditional Allowable Stress Design (ASD). Required toe embedment and wall loading demand vary greatly when the two design approaches are compared, all else being equal. This is due to application of linear load factors to properties that vary non-linearly in the design. These inherent inconsistencies are further intensified when introducing factors such as layered soil profiles, different wall types, groundwater elevation, and surcharge requirements. When applied correctly, these two design approaches, in theory, should lead the designer to the same result with little discrepancy, as they do with steel structure design. However, the use of the current AASHTO LRFD method for various geostructural retaining wall designs yields contradictory results that suggest existing retaining walls that have been successfully designed and constructed are unstable. Fundamentally, LRFD should be built on reliability-based calibrations; the successful past performance of existing retaining structures designed using ASD suggests that the LRFD approach requires considerable modification. The authors of this paper recommend that the current LRFD load factors be reviewed and revised based on more comprehensive wall performance data and wall type such that the difference between retaining structures designed using LRFD and those designed using ASD is eliminated.

Oct 1, 2022

By Alastair Torrance, Gary Cavanough

Over the past two years a research project has been performed on reactive and hot ground. A key finding is that host materials including carbonates and coal are inhibitors to the reaction of sulphide and nitrates. The mechanism of this inhibition is pH buffering and isolating the surface of sulphide from reactants. It has been identified that acidity is a key driver of the reaction with a pH of 2 required for a reactivity event. A series of decomposition experiments confirmed that reactive and hot ground are essentially the same phenomenon with the heating produced either by the reaction of sulphide with nitrates or an external heat source. The results indicate that the key driver of detonation in reactive ground is energy and heat released from the acid induced reaction of sulphide and nitrate with no indications of sulphide being a catalyst or contributor to detonation apart from being a heat source. There must be sufficient sulphide and thermal insulation to provide and retain enough heat for detonation to occur. A pathway to detonation is postulated whereby the heat travels upwards and results in evaporation of water in the explosive. When the temperature reaches approximately 200°C (400°F) the ammonium nitrate starts to decompose, decreasing the mass of the reacting species. The material in the top layers has reduced density and specific heat hence the temperature of the top region rapidly increases up to >1000°C (1800°F) and may initiate detonation. Field tests on loaded blast holes support this proposed mechanism. Case studies are presented whereby the research findings are used to provide an analysis of historical reactive ground events.

Jan 21, 2025

By Dyego Monteiro de Souza

This study compares the wear resistance of specimens lubricated with biofluids or mineral oil. Tribological studies were performed by ball-cratering test. In these tests were used as lubricants epoxidized soybean oil, castor oil and mineral oil. The specimens used were untreated and nitrided AISI 4140, while a steel ball AISI 52100 was used as a counterbody. In order to analyze the results obtained, the worn volume was calculated and the characterization of the crater, after the test, was made using optical microscopy and SEM. Wettability was also measured for the different surface condition and lubricants. As expected both specimens showed a smaller volume worn when lubricated with mineral oil due to inherent properties of this type of lubricant. Among the vegetable oils studied, the castor oil showed a better performance in the lubrication of the specimens untreated while on the nitrided specimen have shown less wear when lubricated with epoxidized soybean oil, indicating a difference in the efficiency of oils, as lubricants, depending on the surface conditions of the mechanical components.

Jul 31, 2018

By R. T. DeWoody, W. C. Miller, W. Chester

Studies were made to determine the effect of the shape of a pneumaticrock- drill exhaust muffler on its efficiency, and the origin and reduction of exit noise from the mufflers. Tests of mufflers of three different shapes proved that the shape is not critical and that a muffler could be incorporated into the shell of the drill. Petal diffusers are beneficial in reducing exit noise but add another projection to the machine. Increasing the number of exit openings while maintaining the same area of exit opening has a markedly beneficial effect on the exit noise and appears to be the most satisfactory treatment.

Jan 1, 1964