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By Alain Denis, Marcelo Curtes Martins, Jeferson Rocio de Oliveira

In this work we present a study of optimization of a new inhibitor for turbulence pickling line. The efficiency of inhibition was measured and the weight of loss was evaluated in four different materials to optimize the dosage of the inhibitor. In seven months we had 8.7% of reduction in pickling losses.

Oct 1, 2019

By M. A. Mekicha, M. B. de Rooij, C. Pelletier, D. T. A. Matthews

One of the main factors that reduce strip cleanliness are iron fines, which are formed due to the abrasive interactions of the roll surface and the strip in the roll bite during cold rolling. They can cause a problem in fouling of the cold rolling mill as well as downstream processes. It has been repeatedly observed that chrome plating the work roll improves strip cleanliness. In the present work, scratch tests and reciprocating sliding tests were carried out under lubricated conditions to explore the influence of chrome plating on iron fines formation. Scratch tests were conducted to study the influence of chrome plating on iron fines formation at single asperity scale due to its intrinsic property. Reciprocating sliding tests were performed to study the influence of chrome plating a rough surface on iron fines formation, taking into account the initial roughness. The scratches made using chrome plated pins showed lower friction, generated less iron fines and exhibited lower material transfer. Reciprocating sliding tests done using the uncoated pins showed galling at different sliding distances depending on the roughness of the pin. On the contrary, reciprocating sliding tests with the chrome plated pins exhibited no galling irrespective of the roughness.

Oct 1, 2019

By Amauri Garcia, Noé Cheung, André dos Santos Barros, Clarissa Barros da Cruz, Thiago Soares Lima, Rafael Kakitani

Materiais de interface térmica (Thermal Interface Materials - TIMs) são responsáveis pela troca térmica entre a fonte geradora de calor do processador integrado e o dissipador de calor. Devido ao seu baixo ponto de fusão, boa fluidez e cumprimento com as exigências de regulamentação (Restriction of Hazardous Substances - RoHS), ligas à base de bismuto têm sido investigadas para aplicação como TIMs de alta performance. Neste contexto, a análise das propriedades dessas ligas em função de parâmetros microestruturais torna-se, portanto, de elevado interesse científico e tecnológico para o setor eletrônico. Assim, este trabalho tem como objetivo desenvolver correlações entre propriedades de resistência à tração e a microestrutura da liga Bi-0,28%Ni solidificada sob um intervalo de taxas de resfriamento usualmente obtido em processos industriais. Por meio de microscopias óptica e eletrônica de varredura foi observada uma morfologia tipicamente eutética lamelar, composta por lamelas ricas em bismuto com o intermetálico Bi3Ni nos contornos. Os espaçamentos lamelares (λL) foram, então, correlacionados com os parâmetros térmicos de solidificação, sendo propostas leis experimentais de crescimento microestrutural. Ao fim, observou-se que, para λL < 101 μm, equações do tipo Hall-Petch caracterizam a variação do limite de resistência à tração e do limite de escoamento.

Oct 1, 2019

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Martin Chabicovsky, Milan Hnizdil

Emulsions are frequently used for the cooling and lubrication of working rolls during the cold rolling. The fact that the lubrication and cooling are not separable makes the optimization of both functionalities difficult. The higher emulsion temperature decreases the cooling efficiency compared to cold water. Heat transfer and fluid flow laboratory (Czech Republic), CRM (Belgium), Tata steel (Netherlands) and Henkel (Germany) cooperated on the increasing of a cooling efficiency during cold rolling. Part of this research was focused on an influence of the emulsion composition on a cooling intensity. The cooling efficiency was laboratory investigated. The stainless steel sample with thermocouple was heated and then it was cooled by a nozzle. Tests were performed with various emulsions and pure water. The heat transfer coefficient was computed from measured temperatures. The cooling intensity (heat transfer coefficient) of all tested emulsions was similar but an increase of the cooling intensity was found with water. Further various emulsions concentrations were tested. Results showed decreasing cooling intensity with increasing oil concentration. Adding additives therefore is thought to cause a noticeable decrease of the cooling intensity.

Oct 1, 2019

By Jean Viana Bahia, Antônio Adel dos Santos, Vicente Tadeu Lopes Buono

During cold rolling of Cr-Mo alloyed DP steel, considerable oscillation of thickness may occur. The literature points out that such occurrence is due to non-uniform cooling of the coil after the hot rolling process. Since the austenite transformation in this steel continues after coiling, the microstructure and, consequently, mechanical properties are very susceptible to natural variations in cooling rates associated with distinct positions of the coil. The influence of coil cooling conditions on thickness oscillation during cold rolling was evaluated in this work by using both industrial experiments and dilatometer tests. It was verified that an industrial coil presented large variation of mechanical properties associated with its heterogeneous microstructure. Consequently, thickness oscillation occurred during cold rolling. Dilatometer tests simulating hot run-out table and coil cooling showed that the austenite transformation is very slow under small cooling rates that occur after coiling. Thus, the slow transformation rate makes the coil very susceptible to environmental conditions around it during its natural cooling and is responsible for variation in mechanical properties of the coil. To ensure the formation of a more homogeneous microstructure in the whole coil, it is necessary either to make use of technologies that improves the cooling uniformity or to adjust the steel alloy design. The latter alternative has been done with relative success by using conceptions with lower amounts of Cr and Mo.

Oct 1, 2019

By Luis Acainas Caballero, Karl Hoen, Stephan Krämer, Christoph Klein

The situation of the steel industry is still challenging. Worldwide overcapacities have an impact on profitability. More than ever, the point at SMS group is to provide the steel industry with flexible and profitable technologies and systems over the whole process chain. One example for that is the thin slab casting and rolling technology and, in particular the CSP® technology (Compact Strip Production), being well established for hot coil production. From its introduction in 1989, CSP® technology has been continuously further developed. Today, on a CSP® plant, the full range of high-quality steel grades can be produced with tightest geometrical and metallurgical tolerances under optimal economic conditions. With the introduction of semi-endless rolling and, as a further step, the endless rolling process, the product range for thin and ultra-thin products has been further enlarged, allowing for the production of hot rolled coils with a thickness of 0.8 mm for low carbon steel grades. Also high-strength steel grades may be produced with gauges below the minimum product thickness that can be achieved in a conventional-type hot rolling mill. Another step in the further development of CSP® technology is digitalization. In December 2016, the CSP® plant of Big River Steel (BRS), located in Arkansas, USA was put into operation. It is the first learning steel mill in the world. The CSP® plant of BRS comes with innovative technologies, providing impressive operational results right from the beginning.

Oct 1, 2019

By Edilson Alves Maranhão, Willi Anton Buehler, Andrea Pezza

O processo de vácuo é a solução típica aplicada quando é hora de atualizar o nível de qualidade do aço de uma aciaria existente. A instalação do novo Tanque de Desgaseificação à Vácuo (VD) de 135t no Canadá e do novo RH de 150t na planta integrada no México para a produção de tubos de alta qualidade na América do Norte é um exemplo típico disso. A nova instalação inclui o mais recente conceito de design para este tipo de equipamento: operações totalmente automatizadas e menor impacto ambiental são os principais aspectos do projeto. A solução de bomba mecânica a seco continua sendo a melhor abordagem de investimento e custo operacional para a tecnologia de vácuo. Os principais aspectos do design da planta são descritos neste documento. O desgaseificador a vácuo VD é responsável pela melhoria das performances metalúrgicas, especialmente em termos de nitrogênio, remoção de hidrogênio e nível de pureza do aço. O processo a jusante e os resultados estão estritamente ligados aos desempenhos do desgaseificador a vácuo. O monitoramento de processos através da linha completa é uma prática padrão para obter uma melhoria efetiva da qualidade do produto. Os desempenhos metalúrgicos do desgaseificador a vácuo VD são analisados e comentados neste trabalho.

Oct 1, 2019

By Antônio Augusto Gorni, Fabio Adriano da Silva, Emanuelle Garcia Reis, Afrânio Márcio Costa

Gerdau Ouro Branco´s plate mill started the operation in 2016 with high level technology. Stands out the capacity to produce different thicknesses in a same plate, therefore allowing special service for sectors such as building structures, bridges, shipbuilding and mechanical applications. The purpose of this study is to present the first results obtained in this innovative product in Brazil. Some slabs of EN10025-2 S355JR+AR steel were rolled and were evaluated the dimensional tolerances, mechanical properties uniformity, grain size, surface and internal qualities. In addition, a correlation was observed between slab and plate thickness reduction and internal plate quality. The results show that this technology can be used with adequate performance for these steel grades in the current market.

Oct 1, 2019

By Roberto Gomes da Silveira Junior, Marcos Cordeiro Fonseca, Geraldo da Conceição Morais, Manoel Gomes de Souza Neto

Sinter maximization in the blast furnaces charge has proven to be the most economically viable way to produce pig iron at Usiminas. This fact has led the company to develop projects aimed at increasing the production of sintering. In this context, the present work shows the recent experience of Sintering Machines 1 and 2 drum mixer exchanging contributing to the increase of operational productivity due to the optimization of the original design. For 13 days was the replacement of the original drum installed in 1974 by a new drum with improvements in the design of the internal and the sprinkling water system. The improvements contributed to the effective formation of micro-pellets and, as a result, increased productivity of Sinter Machines. Several aspects of the project are presented: engineering, planning, safety, manufacturing, technical quality, schedule and a comparison between the parameters of the equipment operation before and after the implantation

Oct 1, 2019

By Eduardo Poltronieri Trés, Francisco de Assis Dutra Macedo, Gilvandro Bueno, Anderson Denadai Thomzini

The first industrial applications of roller presses at the comminution were in 1984 in the cement industry. Since then, the equipment has taken more space in the mineral industry. However, many challenges are still present in this equipment, more specifically regarding to ore breakage predictability. The application of this equipment in the pellet feed preparation is fundamental to increase the surface area (blaine index) of the mineral using reduced energy consumption. However, even after several pressing steps, it is still challenging to achieve granulometry in percentages required for the pelletizing process. Currently these levels are reached in wet milling processes, typically carried out in wet ball mills. For the of pellets formation in pelletizing plants, both pelletizing and the firing processes requires finer granulometry. The motivation of this work is to study the pelletizing process, comparing the physical quality of the pellets produced only through comminuted ore in roller press the pellets produced in conventional comminution using circuit with ball mill.

Oct 1, 2019

By Denisio Miranda Custódio, Rodrigo Boyer, Josiane Lira Batista Haagensen, Raquel Teixeira Pereira, Felipe Viana Pimenta, Rossano Augusto Pilon Nunes

In the Tubarão Pelletizing Plants, anthracite is used as solid fuel, which has fixed carbon content of 72%. This paper will present the pilot scale results and industrial scale tests of an alternative fuel to anthracite, named Blast Furnace Dust. All the work was developed using samples from Arcelor Mittal Tubarão, due to it has a large source of production and is near to Vale/SA, which reduces significantly the cost for the material’s transportation. There was an impact on the variability in fixed carbon results of the slurry, mainly at the beginning of the test, reaching very high levels and put on risk the pellets physical’s quality. This variation can be explained by some operational disturbances and, mainly, by the low predictability of Blast Furnace Dust quality and lack of an adequate system for material preparation and dosage.

Oct 1, 2019

By Ismael Vemdrame Flores, Lindaura de Souza Cândido D’ Avila, Maurício Covcevich Bagatini, Arthur Felipe Lino Oliveira, Rafael Adriano Lopes Júnior

The use of pellet feed to adjust the chemical quality of the sinter is an alternative to the depletion of iron ore reserves. However, the addition of ultrafine in the sintering process can cause decrease of permeability and consequent drop in machine productivity. In this context, the present work investigated the addition of natural and ground pellet feed, evaluating its effects on cold agglomeration for sintering and quality of quasi-particles produced. Eight typical mixtures with industrial composition were produced in the laboratory, replacing Sinter Feed with different percentages of Natural Pellet Feed (NPF, 91% <150 μm) and Ground Pellet Feed (GPF, 83% <44 μm). The mixtures were subjected to cold agglomeration tests and the quasi-particles produced were evaluated by screening, shatter test, permeability test and disintegration into primary particles analysis. There was a decrease in the mean particle size of quasi-particles and reduce in permeability with addition of the ultrafines. The addition of NPF favored the layering mechanism in larger quasi-particles. The coalescence mechanism occurred for larger additions of NPF and GPF, being more expressive for GPF additions.

Oct 1, 2019

By Lilian Silva Costa, Laila Bonzi Ramos, Marcela Lessa de Freitas, Igor Quaresma Vianna

The eighth pelletizing plant, located at the Tubarão complex Industrial Unit of Vale S/A in Vitória-Espirito Santo-ES, processes a pellet feed primarily composed of compact and friable itabirite from Itabira and Brucutu concentration plants, located in the iron quadrangle in Minas Gerais-MG. The use of hydrated ores in the composition of the fine piles, such as Brucutu's common fines amphibolite itabirite (FABR), and Fábrica Nova pellet feed (PEFN), contributed to increase the energy efficiency of comminution, increasing the production of tumbling ball mills, minimizing the impacts during a mill preventive maintenance.

Oct 1, 2019

By Thiago Pinto Silva, Leandro Rocha Lemos, Luiz Fernando Andrade de Castro

This paper shows an evaluation about effect of dispersant sodium silicate along to limestone, in the form of pulp, on the cold agglomeration process for iron ore sintering. Before that, it was verified the effect of pH, solids content and amount of dispersant on the stability of the system (limestone, water and sodium silicate). It was found that the lower the solids content, the more alkaline pH and the amount of sodium silicate equal to 20 l for each 1t of limestone, was the level of dispersion of the system. The influence of the limestone pulp with dispersant depended on the granulometry of the ore mixture and the type of technological route. For the thinner type (42,8% <0.15mm), the limestone pulp with dispersant reduced the resistance of the adherent layer of the cold agglomerates, regardless of the technological route. However, for the coarser type (24,7% <0.15mm), the limestone pulp with dispersant increased the average size of the aggregates, preserving the resistance of the adherent layer when manufacturing with two intensive mixers in series.

Oct 1, 2019

By Walter Luiz Castro dos Santos, Leandro Resinentti Zanon

In the production of iron ore pellets, one of the factors that strongly influence the cost of ore-pellet processing is the specific consumption of natural gas that occurs during the thermal processing stage of the pellets. The filtration process is the step where the adequacy of the moisture percentage of the retained pulp occurs, so that subsequently there is the processing in the subsequent stages of the pellet formation and hardening of pellets. The water contained in the raw pellet is withdrawn at the stage of thermal processing. For this purpose, the literature indicates the demand of 600 Kcal/kg of water for the heating and vaporization of the moisture of raw pellets. The statistical analysis of the performance data of a pelletizing plant showed that for each decrement of 0.1% of water in the retained pulp is equivalent to the reduction of 0.091 Nm3 in the consumption of natural gas per tonne of pellets produced. Thus, the proper performance of the filtration stage is essential to reduce the percentage of pulp moisture retained and consequently to increase the energy efficiency of the pelletizing furnaces. The aim of this article is to present the main steps in conducting a work to increase the filtration performance to reduce the percentage of retained pulp moisture and the positive impacts on the specific natural gas consumption of a plant Pelletizing.

Oct 1, 2019

By Paula Maria Gomes Cunha Leão, Flávio de Castro Dutra, Fabrício Vilela Parreira, Silvio Maranha

In the iron ore beneficiation, tailings are inherent in the concentration processes to which the ores are subjected for the production of commercial products. The large generation of tailings has been motivating the study of technological alternatives for its reuse, with the development of processes that contemplate the concentration of fine ore particles present in the tailings, such as the reintroduction of these particles in the process of manufacture of the iron and steel itself, through the agglomeration techniques such as briquetting. The aim of this article is to study the technical feasibility of the production of iron ore tailings and coking coal briquettes for use in reduction reactors, through a systematic review of the literature on agglomeration, briquetting and self-reduction processes, covering the main variables that influence the production of high quality briquettes, such as binders use, binder behavior of coking coal, coal granulometry, iron ore and coal proportion, compacting pressure and temperature of thermal treatment and the effects of these variables on briquettes final properties.

Oct 1, 2019

By Davi Silva Braga, Alexssander Lopes Sampaio, Rodrigo Carneiro de Oliveira

Vallourec was world pioneer in the deployment, development and consolidation of technology for the use of pulverized charcoal as the main energy source on the first Grate-kiln pelletizing plant in Brazil. The objective of this work was to delve into the subject and to bring more information about this innovative practice of Vallourec that has been attracting the attention of other companies in the steel industry. Industrial tests confirmed the technical feasibility, taking Vallourec ahead in the project of adaptation and investment. With consolidated data of two years and five months from the beginning of the implementation, the main benefits are the average reduction of CO₂e emissions by 50%, cost reduction higher than expected and return on investment in just 19 months.

Oct 1, 2019

By Artur Frederico Fonseca da Cruz, Jael Moutinho dos Santos

The problem of iron ore sticking and premature wear on screening rolls on balling systems is recurrent. The importance of the "screening" function of the roller classifier is fundamental, since in perfect conservation state and operation it is possible to ensure the performance improvement of the most expensive phase in the pelletizing production chain, the thermal processing. The present works target is the identification of possible causes of iron ore adhesion in classifier rollers and develop a methodology to evaluate and quantify the iron ore sticking mechanism on the classifier surface. For this purpose, iron ore and additives were collected at four different pelletizing plants in terms of iron ore origins and process flows, three different rollers were chosen for testing around the adhesive energy at the iron ore mixture/rolls surface interface. As results, it was possible to construct methodologies to evaluate the aggregability, it was observed the importance of "specific moisture" definition and knowledge on the adhesive energy increase, besides presenting the better performance of rolls with tungsten carbide coating than other evaluated.

Oct 1, 2019

By Luís Marcelo Marques Tavares, Gilvandro Bueno, Túlio MoreiraCampos

The HPGR development and application in the minerals industry resulted in an important increase in its application in iron ore pellet feed processing in the last decades. Vale SA was one of the pioneers in application of the HPGR in integrated plants, currently operating with six HPGRs in the pelletizing plants of Complexo de Tubarão (Vitória, ES). The work uses the mathematical model of the HPGR, proposed by Torres & Casali and modified by the present authors, to predict the performance of two industrial pellet feed HPGR units of the Complexo de Tubarão. Besides model validation, results of process simulations are shown in order to optimize the pellet feed pressing according to industrial demands, presenting different scenarios that are more attractive to HPGR operation. Simulations showed that it is feasible to reduce the specific surface area of the HPGR feed from 1770 cm²/g to 1570 cm²/g, allowing to produce a pellet feed of the same quality in its product (1911 cm²/g) and therefore reduce the work done by upstream ball milling.

Oct 1, 2019