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By Zhisong Chai, Wei Xu

Q&P steels undergo continuous multiple processes, including hot rolling, intermediate heat treatment, cold rolling and continuous annealing etc. The inheritant effect of initial microstructure could affect the final microstructure and mechanical properties of Q&P steels. In this work, effects of different hot rolled microstructure/texture on the final microstructure and properties subjected to Q&P process were investigated in Fe-0.38C-1.58Mn-1.6Si system. Different initial microstructures were generated combing different TMCP and cooling strategies. The microstructure and texture of hot rolled materials were characterized in detail. The hot rolled material was subsequently processed by intermediate annealing, cold rolling and continuous annealing. The comparison reveals great effects of the initial hot rolled microstructures, i.e. inheritance effect. The faster reverse transformation would lead to more sufficient austenitization and it would greatly weaken the inheritant effect of the initial microstructure. Although the difference of final phase fraction for different initial microstructures was not significant, the inheritance effect was mainly reflected in the effect on austenite morphology. For the mechanical properties, no obvious difference in strength was shown for the samples with different initial microstructures after Q&P heat treatment, but there was fluctuation in elongation.

Oct 1, 2019

By Jorge Alberto Soares Tenório, Denise Crocce Romano Espinosa, Beatriz Peralta Oruê

Manganese, a toxic mineral, related to manganism may have high added value for the steel industry. The difficulty in obtaining manganese encourages the exploration of new secondary sources such as the lateritic nickel effluent. In Brazil, nickel reserves are predominantly lateritic, making the country a potential producer. For the tests, a synthetic solution was used which simulates the lateritic nickel effluent from leaching. The oxidative precipitation with ozone occurred at the oxygen flow rates: 0.5; 1.0 and 2.5L/min, at the original pH 1.5 at 21°C in a 500 mL bubble column reactor. O3 was produced in the benchtop generator feed by 99% oxygen. The ozonation time was determined by the oxidation potential1.55V. The ozonated solution was centrifuged and filtered. The filtrate and collected samples were characterized in ICP-OES. Optimization tests with ultracentrifuge were performed. The best precipitation reached 97% at 0.5L/min O2 at 6.07 ± 0.045mg/min of O3 dosage and resulted in a solution 10-15mg/L Mn+2, above 1mg/L, maximum value acceptable by Conama 2011, to be retreated before being discharged into the water body or being reused as a manganese source.

Oct 3, 2019

By Günther Staudinge

Aperam is a global player in producing of stainless, electrical and special steel qualities. The steelmaking plant in Timoteo Brasil is equipped with one AODconverter for stainless steel and one MRPL-converter for special steel production. After almost 20 years of operation Aperam decided to exchange the existing 80 t MRP-L converter by a new one including a new trunnion ring and a state of the art suspension system. Due to an optimized design the inner volume of the new converter could be increased which comes along with improved production. A special feature is a flange connection in the barrel section of the converter. This allowed to avoid any critical site welding and the time between shut down of the old and cold commissioning of the new converter could be done with 17 days only.

Aug 17, 2017

By Ananda Moreira Vaz Ourique de Avila

Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells (SOFC) interconnects, replacing the ceramic materials. However, at high temperatures, on the order of 700-850 0C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the SOFC. Thus, the knowledge on kinetics of oxidation/corrosion of these steels and their relationship with the microstructural transformations are of great importance. In this study, samples of ferritic stainless steels AISI 430, AISI 441 and Crofer22APU® were tested for oxidation at high temperature (800 0C) for long periods of time (up to 3,600 hours) and mass gains were monitored allowing the determination of the oxidation behaviors of these steels. Additionally, the microstructural characteristics of the samples before aging (corrosion-oxidation test) and after various oxidation times were evaluated by optical (OM) and scanning electron microscopy (SEM), as well as by micro chemical elemental analysis (EDS) and X-ray diffraction (XRD) phase analysis. Electrical characterization allowed determination of electrical area-specific resistances (ASR) characteristics of the systems studied, thus relating the electrical and oxidative behaviors of steels evaluated.

Aug 7, 2018

By Luke A. Balzan

Access to information is a key component for making improvements to any process. This is particularly true for all aspects of the iron mining and steelmaking process. The ability to make rapid control decisions can significantly influence process outcomes, including ensuring product specification, mining quality, transportation limits, upgrade factors, waste bypass and direct shipping, among many others. While traditional laboratory methods provide feedback for such processes, having access to analysis results in real-time can lead to positive reactive and predictive control decisions to be made rapidly, leading to significant improvements throughout the process. Scantech has been designing, manufacturing and supplying technological products to the minerals industry since 2002 to enable the availability of such realtime information to a mine or plant, with the benefits being enjoyed by a wide range of operators. This paper provides a summary of the available technologies used in the iron ore and steel industries, as well as providing a case study of their use at an Australian site, and a description of the potential benefits of a range of analysis equipment.

Aug 17, 2017

By Geovane Viturino da Silva, Jeziel de Melo Canedo, André Wulff Hirano, Maxwell Pereira Cangani, Luiz Henrique Curado Ribeiro

With the deterioration of the quality of the iron ore, the new conditions of quality of the raw materials (mainly sinter feed) were adapted to their processes, resulting in the need for changes in the chemical quality of the sinter for blast furnaces in the Ternium Brazil, without changing the parameters of chemical, physical and metallurgical quality. Due to the change in this scenario, there was a great impact on the quality of the fine iron ore this year in 2019, due to which the work ranges of sinter MgO and B2 were currently modified to minimize these impacts in the blast furnaces of Ternium Brazil. This work aims to minimize the effects of the sinter worsening, with the reduction of the sinter MgO and B2 bands, with an increase of 2% in the mixture yield and FeT elevation in the range of 1.6% in the sinter product.

Oct 1, 2019

By Washington Martins da Silva Júnior

In stamping process, sliding between metal sheet and forming tool leads to wear of tool surface. Maintenance of stamping tools involves polishing the tool edge, or, in case of severe damage, replacement of the tool. Hard coatings have been applied on the stamping tool surfaces in order to reduce the maintenance cost causing a great economic impact in metal work industry. In this work, CrAlSiN coatings were applied by PVD onto SRV2W tool steel. The coating toughness was avaliated by the critical load in scratch tests. The following coating parameters were analyzed: 1- substrate surface finishing process; 2- coating architecture (multilayer or gradient); 3- chemical composition of the coating. AlSi concentration varied from the substrate/coating interface to the surface. Coatings were 3 µm thick. Scratch tests were carried out using a Vickers indenter. The applied normal load was varied from 0 to 13 N for a scratch length of 5 mm. In order to study the effect in the toughness, the substrate roughness was controlled by the finishing process before PVD coating. Samples subjected to polishing presented highest critical loads. Gradient coatings presented higher critical loads than those with a multilayer architecture. Coatings with higher concentration of AlSi near the surface supported higher loads before failure.

Jul 31, 2018

By Qingwen Dai

The Marangoni effect is an important phenomenon where a surface tension gradient drives liquid towards high surface tension regions. Temperature gradient, evaporation, disparity of viscosity, and surface roughness and topography are all significant factors that can affect this thermo-capillary migration. The purpose of this study was to investigate the influence of micro-groove patterns on the migration of paraffin oil, and obtain a well-designed texture of micro-grooves to prevent the thermo-capillary migration. Patterns of micro-grooves with differing orientations and geometric parameters were fabricated on the surface of SUS 316 stainless steel substrates. Experiments on the migration behavior with different viscosities of paraffin oils were carried out various temperature gradients. The experimental phenomena indicated that the surface with the micro-grooves perpendicular or parallel to the temperature gradient have a strong impact on the migration performance of paraffin oil. Micro-grooves perpendicular to the temperature gradient exhibited extraordinary slower migration velocity than that of the parallel one. Width and depth of micro-grooves had an obvious influence on the behavior of temperature-driven migration and detail discussions on the effects of these geometric parameters were carried out.

Jul 31, 2018

By Gajraj Rathore

With the advent of modern HRM ( Hot rolling mills) with capacities beyond 5 Million tons with corresponding enriched CRM (Cold Rolling Mill) capacities, the throughput per hour exceeds invariably beyond 50 coils per hour making it possible to manage, track, handle, transport, store and dispatch inevitably with an automation system supplemented by corresponding software and hardware. This is true with respect to the production of Cold rolled Annealed, Galvanized, Continuously Annealed, Galvalume, CRGO, CRNGO and Colour coated coils which need total care in handling, tracking and dispatch. Understanding the above needs precisely JSW, Vijayanagar, India, has rightly gone in for a total automatic Yard management system and ASRS wherein the coils are handled as much as possible automatically in cradles without any damage insuring the receipt of coils to the customer as was produced. This CRM 2 has been commissioned and is operating with maximum automation with least manpower and max productivity with assured quality and safety. Pesmel OY Finland had the opportunity to Design, Supply and Commission this system which is first in the country and this technical paper analyses the above project as a case study enlisting the sound technical aspects as well as emphasis on the techno economics with assured ROI (Return on investment) and enhanced efficiency.

Aug 16, 2017

By Afonso Cardoso da Silva, Romeu Thomaz Viana Jr, Emanuelle Garcia Reis, José Herbert Dolabela da Silveira

The Gerdau Ouro Branco Mill, three years after the implementation of its new plate mill, has started to develop high complexity products. The plate mill’s learning curve has been increasingly challenging since products are being developed to their highest grades. This work aims to present the first results of the development of steels of the strength class of 510 MPa produced by TMCP (Thermomechanical Controlled Processing) followed by accelerated cooling. These results show the potential and advantage of the accelerated cooling process regarding to obtain products of high mechanical strength and high toughness, associated with a low equivalent carbon.

Oct 1, 2019

By Fernando Henrique Gomes de Souza

Techniques which use a spring to supply the bias force to actuator are well adopted since they are inexpensive and simple to construct. In this work it was design an actuator concept using bias-type device technique, which comprises two coils that mutually push against each other to supply the stroke. For the coils springs, it was used a wire of NiTi shape memory alloys (SMA) and a wire of 400 grade maraging steel as construction materials.

Aug 8, 2018

By Christoph Aichinger

The optimization and improvement of a modern integral iron and steel works gets more and more difficult as each individual plant is already operated at its best efficiency and at the lowest operational expenditures. However very often the individual plants are considered as stand-alone units and there are losses and inconsistencies on interfaces and take over points, which could be avoided and by that improving the overall performance of the iron and steel works as a holistic unit. Primetals Technologies looked into this subject extensively in the recent years and is now ready to offer new tools and services in order to assist operators to find further potential for improvement in processes, which seem to be fully developed at first sight.

Aug 17, 2017

By Márcia Maria da Silva Monteiro Pereira

Durante o lingotamento contínuo de aço, partículas de ZrO2 adicionadas na escória de molde facilitam a nucleação heterogênea de cristais devido à sua limitada solubilidade. A adição de ZrO2 promove a cristalização da fase cuspidina, o que auxilia na redução da transferência horizontal de calor no molde, amenizando desta forma o problema das trincas longitudinais. Outro benefício da adição de ZrO2 em pós fluxantes é reduzir a taxa de desgaste da válvula submersa (SEN) na interface metal/escória; a erosão da SEN é um problema sério. Através de testes de laboratório e de testes industriais concluiu-se que a adição de ZrO2 em pós fluxantes reduz a taxa de transferência de calor horizontal no molde durante o lingotamento contínuo de aço, considerando os dois tipos de pós fluxantes que foram analisados no presente trabalho. Além disso, observou-se que a adição de ZrO2 reduz a taxa de desgaste da válvula submersa na interface metal/escória.

Aug 16, 2017

By Gilberto Álvares da Silva

New elements have been inserted in NiTi lately, resulting in ternary alloys with specific characteristics beyond Shape Memory Effect and Superelasticity. Among all others alloying elements, the Ag additions itself gives potential antibacterial activity to that smart material. So on, the elaboration procedures of ternary NiTiAg alloys was studied in order to obtain a melting procedure to ensure further studies on this alloy. Microstructural and thermal analyses were used to evaluate the VAR-remelting production of NiTiAg with 4.0% wt silver content. The microstructure is composed by a NiTi matrix, pure Ag precipitates, and, scarcely, TiC inclusions. Heat treatments at high temperature could not dilute those Ag particles, but could lead to the precipitation of new ones. The silver element reduces the temperature of the martensitic transformation, yielding a material with superelastic behavior, beyond induces the R-phase on cooling stage of this alloy.

Aug 8, 2018

By Alessandro Martinis

The performance requirements for modern steelmaking facilities are ever more stringent, as customers and markets are continuously pushing for technologies which allow having high quality steel produced in an economic and sustainable way. In the details, this paper has the aim to present the excellent results obtained by integrated steel plant where an EAF is fed with high quality hot ENERGIRON DRI. The recent technology developments, combined with the affirmed basic process design, contributed to further maximize the energy of the DRI, reaching the EAF at temperatures above 600°C with a carbon content up to 3.5%, as confirmed by plant data. These improved input material characteristics resulted in reduced electrical energy consumption and increased liquid steel production.

Aug 16, 2017

By Eduardo Cabral

A nova política de resíduos sólidos, imagem positiva da empresa, utilização consciente de recursos com a consequente redução de custos e preservação do meio ambiente têm levado as minerações e siderúrgicas a adotar uma gestão responsável com relação aos seus coprodutos. Em consequência, esses coprodutos (escorias e lamas da mineração, lamas de aciaria, pós da sinterização, calcinação, coqueria, carepas e outros resíduos da siderúrgica) estão sendo economicamente reintroduzidos no processo produtivo. Esse trabalho pretende fazer um resumo de possíveis tratamentos que esses materiais podem sofrer, como umectação, aglomeração, briquetagem, granulação, pelotização ou extrusão.

Aug 16, 2017

By Xiaowei Du, Xitao Wang, Xuekun Shang

The deformation behaviors under both tensile and compressive forces and microstructure evolutions of cast SA508-4N steel were investigated at elevated temperatures. True stress-strain data were obtained from hot deformation experiments performed on a Gleeble-3500 thermal-simulator under different temperatures (750-1200C) and strain rates (0.001-10 s-1). The reduction of area decreases as a function of temperature from 750C to 900C and then increases. At 1200C, the reduction of area reaches more than 99% with the strain rates of 0.5 s-1 and 1.0 s-1. The dynamic recrystallization under compressive stress occurs at 800C under low strain rate and a complete dynamic recrystallization can be observed when the temperature reaches above 1100C. A “two-stage” flow stress constitutive model concerned with dynamic recovery and dynamic recrystallization was established based on the true stress-strain data. This model shows good agreement with experiment results. Moreover, we developed a dynamic recrystallized grain size model to describe the average grain size after complete dynamic recrystallization.

Oct 1, 2019

By Ismael Nogueira Rabelo de Melo

A adição de Fe-Nb em ligas com alto teor de carbono apresenta baixas taxas de dissolução devido à formação de uma camada carburada na superfície, exigindo longos tempos para dissolução dos carbonetos NbC no banho. Foi avaliada a eficiência da dissolução de Fe-Nb em pó pelo processo de simples adição em uma liga de Ferro Fundido Branco com Alto Teor de Cromo. No processo foram obtidas eficiências de dissolução em torno de 90% e os carbonetos NbC apresentaram em formas finas e em aglomerados.

Oct 30, 2017

By Alberto Pesamosca

The paper presents the results obtained by the AC EAF supplied by Danieli at Kroman Çelik (Gebze-Turkey) after the planned upgrade to 150 ton. The EAF – 7,4 m diameter, based on the full platform standard design - is able to handle a maximum power of 114 MW and is equipped with the most advanced and reliable technology, including module injection system and the Hireg electrodes regulation system. Excellent results were already obtained with 120 heat size in terms of fast start-up and excellent performance figures. After the upgrade, productivity was increased up to 212 t/h, maintaining high process efficiency (365 kWh/t with 32,1 Nm3/t O2).

Jul 30, 2018

By Charles Sóstenes Assunção

A mathematical model of heat transfer and solidification for a continuous casting of round billets was developed. The water flux density of the secondary cooling zone was experimentally measured, using an apparatus in industrial scale with two types of nozzles, flat jet and full cone jet. The profiles of water distribution were applied on the mathematical model. The results showed that the water distribution is not uniform in both longitudinal and angular directions owing to the unevenness of the spray and to the curvature effect of the round billet. This non-uniformity causes important variation of the heat transfer coefficients and superficial temperature of the billet, especially in the first cooling zones, where the temperature is higher. The mathematical model was used to simulate a change of nozzle type in the first cooling zone. The results showed that the heat flux and superficial temperature variations were reduced with a full cone jet nozzle in comparison with the flat jet nozzles.

Aug 16, 2017