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By Ernt. W. D.

A membrane based mixed extractant process was developed for selective removal of copper from waste acidic cupric chloride etchant solutions found in printed wire board manufacturing. The process uses a mixture of Adogen 381 (tri-isooctylamine), MOC®-45 (ketoxime) and MOC® 55TD (aldoxime) in a kerosene diluent. The mixed extractants recover the copper from a hydrochloric acid medium and transfers it to a sulfuric acid medium. The process also utilizes unique wetted membranes to separate the aqueous and organic phases. The driving force for these membranes is not pressure but the difference in surface tension between the two phases. By using these membranes, complete phase separation results. There is no physical entrainment contamination as found in conventional systems. The only cross contamination is the solubility concentration of one phase in the other. This however is less than 10 mg/l.

Jan 1, 1998

The OK orebody comprises a steep dipping narrow quartz reef averaging 0.4 m in width hosted in basalt and gabbro with porphyry bars cross-cutting through it. The following paper tracks the mining of this orebody, challenges encountered, measures undertaken to address these challenges and changes in mining conditions and methods as the mine matured in both depth and age. The initial mining method was narrow vein hand held shrink stoping accessed by shaft, that over the period of the mines life was superseded by gallery stoping, shrink stoping and ultimately mechanised narrow vein long hole sublevel open stoping. The reasoning behind the change in mining methods is detailed, including safety and cost benefits. The transition presented many challenges that were overcome, resulting in the successful development of a narrow vein long hole stoping method. The lessons learnt during the transition period and the practices and principles developed for successful mining of narrow vein orebodies using long-hole open stoping methods are summarised in this paper. The final section of the paper takes a retrospective view of how the knowledge gained through the mining of the OK orebody would be applied to a new mine containing an orebody of this type, with consideration given to the initial excavation design, equipment selection, mining sequence, geotechnical investigations and mining method used.

Jan 1, 1998

By I. Le May

"The assessment of integrity in plants is discussed, together with the codes that are being developed for in service evaluation of engineering fitness for service. The use of Risk Based Inspection is described and some examples are provided of the evaluation of in service components in which flaws have been detected. An example of the assessment of the structure of a mine processing facility is described, and application of Risk Based Inspection and plant assessment procedures to mines is discussed. Periodic assessment of large plants and components to determine their integrity for continued safe operation is becoming a more accepted approach than formerly when regular shutdowns were the normal practice. This is on the way to becoming the preferred procedure for petrochemical plants and power generating plants, and the same philosophy is appropriate for many mining operations. Both the American Petroleum Institute (API) and the American Society of Mechanical Engineers (ASME) have committees developing codes for the continued operation of equipment as distinct from the existing design codes. The philosophy is one of risk-based inspection, which can be on a purely qualitative basis or more quantitatively based.The purpose is to reduce the inspection of unnecessary and non-critical items and to concentrate on the most critical components, reducing costs and downtime and increasing safety. The approach differs from that considered by many maintenance engineers, in that defects that are identified during an integrity evaluation do not automatically cause a component or structure to be condemned or require that repairs are made right away. The seriousness of the defect must be considered and the safe operating life can be estimated before it becomes necessary to replace or repair the unit or component. This is no different from what is done today with passenger aircraft and, to an increasing extent, with pressure vessels, reactor vessels and similar components in the petrochemical and power generating industries."

Jan 1, 1998

By W L. Lane, T R. Yanske

The Doe Run Company and its predecessors have been mining for over 130 years utilising the room and pillar mining method. This method has left approximately 20 per cent of the orebody in the remaining pillars. The original design and planning for the mines did not include extensive pillar extraction. This paper summarises the introduction of the pillar extraction and backfill techniques which have been implemented since 1991. These techniques include the use of low cost fill walls up to 20 m in height and the use of slinger trucks for topping off the fill. In conjunction with these accomplishments, much experience and confidence has been gained in the use of numerical modelling as a method of predicting pillar stability as the mining of pillars progresses. These advances have led to pillar extraction becoming a major portion of the overall production and have added to the mine life of Doe RunÆs six operating mines.

Jan 1, 1998

By Chi-Ming Chang

Alloy powders are commonly used in the purification of zinc sulfate solutions for use in standard electrowinning practice. The primary goal of this research was to study the use of zinc-lead alloys for similar reactions in the galvanic stripping of impurities from organic solutions. The effects of various parameters on the electrochemical behavior of commercially produced zinc-lead alloy powders were determined. A qualitative evaluation and summary of the influence of the more pertinent parameters on iron removal from di-(2-ethylhexyl) phosphoric acid (D2EHPA) by galvanic stripping is given. Water concentration, oxygen content and reaction temperature were the principal factors affecting the reaction rate and process efficiency. Activation energies were also calculated and indicated that the reaction changes from chemical to diffusion control .with increasing temperature in the range of 35" to 45°C. The results showed that zinc-lead alloy gave faster reaction rates with less sensitivity to process variables than SHG zinc as a reducing agent for galvanic stripping. The role of lead could be as cathodic sites for the reaction which enhances the zinc dissolution or anodic half reaction. The morphology of the zinc-lead alloy surfaces, before and after the reactions, supports this assumption.

Jan 1, 1998

By G. Ferrara

To obtain a reliable comparison between conical and cylindrical separatory vessels used in dynamic dense medium separation systems, the following studies were made: (1) study of the swirling flow in conical and cylindrical vessels using laser-Doppler velocimetry (LDV); (2) study of the behaviour of suspensions of magnetite and ferrosilicon in water in both separators. It was found that: (a) the tangential velocity profiles differ in conical and cylindrical vessels: in a conical cyclone free vortex conditions affect the largest part of the vessel, while in a cylindrical vessel, the motion approaches that of a forced vortex, i.e. that of a centrifuge; (b) the conical vessel manifests higher centrifugal acceleration and very strong densifying; the density differential, and hence the density gradient inside the vessel is large; (c) the cylindrical vessel manifests lower centrifugal acceleration and low densifying, i.e. low density differentials, and hence, the density gradient inside the vessel is small; (c) due to greater densifying, the density cut-point in cyclones is higher than the operating medium density, while in cylindrical vessels the density cut-point is closer to the medium density. The results provide an interesting description of the differing behaviour of conical and cylindrical vessels and help explain the differences in performance between the two types of separators.

Jan 1, 1998

By W. E. Lytle

Environmental permitting is a critical component for joint-venture projects located in the Commonwealth of Independent States (CIS). This paper presents the basic CIS regulatory environmental requirements for permitting of a hypothetical mining source and emphasizes air permitting. Topics which will be covered include: the Expertiza process, air pollution quantification, data requirements, and air pollution modeling protocol. A comparison will be made between permitting requirements for air pollution sources in the United States and a CIS country, Kazakstan.

Jan 1, 1998

The history of the rail and mining industry in Queensland over the past century is inseparable. Indeed it was mining that led to the construction of the line west from Townsville and that shaped its current alignment. The discovery of gold at Charters Towers started construction of the Great Northern Railway west from Townsville in 1879, with completion to Charters Towers in 1882. The line was extended to Hughenden in 1887 and to Cloncurry in 1907 - driven by copper mines both to the south west and the north west of Cloncurry. The mining industryÆs association with funding the construction of rail lines to service their individual mines began in this area when the Hampden and Mount Elliot mine companies agreed to pay 50 per cent of the cost of the line from Cloncurry. The line to Selwyn was completed in 1910. Copper mining saw the construction of many other rail lines in the Cloncurry area in the 1910 - 20 period before copper prices slumped. Included in these lines were the Malbon to Duchess line and the line to Kajabbi and beyond.

Jan 1, 1998

By Jussi Vaamol

A commercial CFD-code was used to solve isothermal flow fields of gas and liquid in a Peirce-Smith converter. The model was validated with a 1/4 scale water model, and parametric study. Limits of the modeling technique used were recognized, but calculated results indicate that the present model predicts the general flow field with reasonable accuracy. The model was used to examine general flow conditions in an industrial scale PS-converter. Typical scaling factors of physical models were also evaluated with the aid of predicted bubble distribution, patterns of the flow fields and magnitude of flow velocities. The numerical simulations were found to open new viewpoints to the fluid dynamic related phenomena in the PS-process.

Jan 1, 1998

By P. Lan

Gold is often associated with arsenopyrite in many refractory gold ores. The selective recovery of arsenopyrite by flotation is therefore necessary in order to maximize the recovery of gold. However, the complexity of arsenopyrite flotation often makes it difficult to obtain a high recovery from real lean gold ore. This paper presents the results of arsenopyrite flotation by ultrasonic pretreatment in micro flotation experiments and bench scale flotation tests. The tests showed that pure arsenopyrite exhibited low natural floatability due to the oxidation on the mineral surface under ambient conditions. Using ultrasonic pretreatment, the oxidation film was ruptured and the floatability was enhanced greatly. The presence of Fe (III) was found to inhibit the flotation of arsenopyrite and this depression was also removed by the ultrasonic pretreatment. This result explained why the arsenopyrite in real ore is often difficult to float and how ultrasonic pretreatment can effectively improve the arsenopyrite flotation in real gold ores. Guanidine (GMM) was found to be a superior collector for arsenopyrite in acidic medium and xanthate in alkaline medium.

Jan 1, 1998

By Terry McNulty

There are many potential pitfalls in the commercialization of innovative technology. The failures often are remembered longer than the successes, thereby serving as deterrents to subsequent attempts. The mineral industry's future depends on effective innovation. So it is essential that the causes of failure are understood. Innovation can be examined equally well in the context of geophysics, geology or mining. However the author's experience has been in mineral processing and chemical engineering. So the following discussion is limited to processes and/or plants for producing mineral concentrates, metals or inorganic chemicals. More of what follows has to do with underachievement or failure than success. But this article demonstrates that there is a strong element of predictability in the former. Furthermore, it is a credit to the minerals industry and to the engineering profession that a very high percentage of projects succeed in achieving design capacity and forecast operating costs. Innovation means the introduction of something new. In this article, the words "innovative technology" are used broadly. They include new processes and novel combinations of established unit operations, as well as novel types of processing equipment or largest-ever equipment models. The discussion of project outcomes is based on personal experience or on published information. Citations are given for technical publications that provide either project information or insights into the methodology used to analyze project performance. However, specific projects have not been identified due to the rather negative connotations of some of the conclusions drawn about the less favorable outcomes.

Jan 1, 1998

By M. K. Mohanty

Due to inefficiencies of the flotation process, significant effort has been recently provided to develop gravity separators for treating ultrafine particles. As a result, several enhanced gravity concentrators have been developed and commercialized. The Altair Centrifugal Jig is an enhanced gravity separator that provides relatively efficient separations on +25 µm size fractions. An experimental program conducted on -600 µm coal found that the Altair Jig reduced the ash content of the 600 x 44 µm from about 30% to 10% with an 86% combustible recovery value. The pulse water pressure, feed volumetric rate and ragging volume were found to be the key operating parameters affecting the separation performances obtained from the process. An extremely low density cut point of 1.54 and an Ep value of 0.08 were indicative of the high process efficiency values achievable by the Altair jig.

Jan 1, 1998

By Paul Miller, Rene Laprade

Does a 76 mm Ø hole drilled over 45 m deep remain straight? This is the question asked by the Engineering department at Placer Dome's Dome Mine in Timmins, Ontario before they could lay out the initiation sequence in a long-hole production stope. Everyone realized that the holes would wander over such great depths, but it was important to know where they went.

Jan 1, 1998

By J. Gallagher

Henderson Mine has been transporting molybdenum ore using a rail haulage system for the past 21 years. Due to the age of this system, limited performance, and obsolescence, a capital investment decision was imminent. Henderson used this opportunity to evaluate other transportation methods and continuously improve their mining practices. These efforts resulted in a new mine plan for Henderson, which ensures that Henderson will continue to supply high quality molybdenum into the 21st century. This paper will discuss the dramatic changes taking place at the Henderson Mine as a new production level is mined. These changes include the installation of an underground crushing, conveying, and truck haulage system, as well as increasing the scale of the panel caving process. Each of these topics will be discussed, as will their rock mechanics and material flow implications.

Jan 1, 1998

By Harvey T, Kizil M, Bride J

Hydrogen sulphide (H2S) as a seam gas has occurred in several locations in the German Creek seam at Southern Colliery. This paper overviews the techniques developed to quantify the H2S content of the seam, overviews research into controlling and reducing H2S emissions from the seam, and details the procedures used to mine through the HZS zone in 702 longwall panel. Learning points from research and mining experience are reviewed for application in the next longwall block.

Jan 1, 1998

Although anion exchange resins are widely used for gold recovery in Russia and the former CIS, accounting for almost 50 percent of gold recovery in that part of the world, the technology has not been adopted in the West, apart from one small operation in South Africa. This situation is likely to change as the gold industry heads into the twenty first century. With gold prices having declined steadily through the 1990's, mining companies are under great pressure to reduce costs and improve gold recovery. Most studies on the use of resins for gold recovery from cyanide solution or pulp have shown that this technology has the ability to achieve both these goals. Resins can also be used to recover and recycle free and complexed cyanide in gold plant tailings, which has the potential to significantly lower operating costs, and latest developments in this area of technology are discussed. Finally, recent studies on thiosulphate leaching of gold have'shown that this process is very well suited to the treatment of carbonaceous, preg-robbing ores from the Carlin trend (Nevada, USA), and elsewhere in the world, because the gold thiosulphate complex does not load on to carbon. Whilst this obviously benefits the leaching process, it means CIP and CIL are ineffective in this situation, and the use of ion-exchange resins for gold recovery from thiosulphate leach solution are discussed.

Jan 1, 1998

By Laura Bustemante, Bruce Vandenberg, Fred Huettig

Recent advances in solid-state, field portable, fast framing video camera systems and PC based frame capture hardware now allow blast imaging up to 1000 frames per second. Up to 8 seconds of data can be stored directly into the unit, downloaded to a PC or archived to a standard VCR without data compression. Since no film processing is involved, motion analysis can be performed instantly and on-site within a few minutes. This paper will describe the design features and applications of the KineView 1256P system and compare these with the analogous aspects of fii based cameras.

Jan 1, 1998

By Árpád B. Palotás, Adel F. Sarofim, John B. Vander Sande, Lenore Rainey Christian, J. Feldermann

"Interest in the fine structure of soots and carbon blacks is motivated by a variety of possible applications. The structure provides information on the origins of the particles and on their adsorptive and reactive properties. This paper describes a method for quantification of the structure of soots and carbon blacks based on direct electron microscopic observation followed by image analysis of these materials. High-resolution transmission electron microscopy (HRTEM) provides a very detailed observation of particle structure. The differences in soot structure, because of its complexity, may not be easily quantifiable with the human eye; therefore, high-level computer software has been used to manipulate HRTEM images. This technique involves the application of fast Fourier transforms (FFT) to single particles and the measurement of characteristic parameters such as interplanar spacings and crystallite sizes from these particles. The methodology and application of this characterization technique are presented here. Results are shown for dif¬ferent samples obtained from soot and carbon black particles selected to illustrate the capabilities of the methodology. Quantitative information can be obtained on structural characteristics, e.g., interplanar spacing, circularity, orientation, elongation, and length distribution of lattice fringes, as well as on the fractional coverage of the extracted pattern. c 1996 Wiley-Liss, Inc.This paper presents a combination of techniques for recognizing and classifying different carbonaceous materials, using their structural morphology. A new method to assess and quantify the parameters which define such structures is proposed and discussed. The technique is based on the use of HRTEM (high-resolution transmission electron microscopy) and computational image analysis.It is well-known that carbonaceous materials like graphite, soots, coals, cokes, chars, etc. possess characteristic structural appearances which can vary from mostly random or amorphous to a perfectly ordered graphitic crystalline structure (Buseck and Bo-Jun, 1985; Buseck et al., 1987). The carbon structure has been variously described as turbostratic (Oberlin, 1989) or as crumpled sheets (Rouzaud et al., 1991) to indicate that parallel layering, reminiscent of graphite, is observed over dimensions of nanometers, but that these planes or crystallites show disorder over larger scales. The degree of order of such structures is strongly dependent on the thermal treatment of the material as well as on the composition of the source of the carbonaceous material. The value of the electron microscope in studying the morphology of such materials has been well-established, and abundant information is available (Ishiguro et al., 1991; Lahaye and Prado, 1978; Buseck, 1992).The use of HRTEM has brought further insight into this matter. Qualitative assessment of the structural order of such materials has been attempted over a long period of time in order to differentiate between various sources or treatments. There is, to date, no successful method available for quantifying the structural characteristics of various carbonaceous materials. This paper presents a technique which is able to recognize dif-ferent materials and to quantify the structural parameters of those materials using HRTEM and computational image analysis, including pattern recognition techniques.In the case of perfectly ordered graphitic crystals, electron diffraction is widely used for obtaining details on structure. Analysis of diffraction patterns can reveal parameters such as interplanar spacing, d002, crystallite size along the c-axis, Lc, crystal size in the plane of the layers, L., mean number of crystallites, Nc, etc.Complicated electron microscopy methods such as defocusing, tilted illumination, axial illumination, etc., often have to be used in order to characterize complex materials such as randomly oriented crystals in soots and carbons. Obtaining the right fo"

Jan 1, 1998

"Minimizing Particle Contamination During Generation of Fresh Dust for Inhalation Studies J. Abraham, MS, Mechanical and Aerospace Engineering, West Virginia University, 1995Correlating Lung Crackle Using Holographic Interferometry Ali Afshari, MS, West Virginia University, 1989Effect of Bit Wear on Dust Generation Mudassar Ahmad, MS, West Virginia University, 1992 The Effect of Surfactants on Suppression of Non-Wettable Particles Ali Alaboyun, MS, Mineral Engineering, The Pennsylvania State University, 1989 Geochemical Characterization of Kerogens, Shales, and Coal Refuse Associated with Allegheny Formation of Cases of Northern West Virginia Dick Andre, MS, West Virginia University, 1987Size and Mass Characterization of Airborne Particulate Matter in Underground Coal Mines Using Diesel-Powered Equipment Indranil R. Bardhan, MEM Report, The Pennsylvania State University, 1992Size and Mass Characterization of Airborne Particulate Matter in Underground Coal Mines Using Diesel-Powered Equipment I. Bardhan, R. V. Ramani, and J.M. Mutmansky, Mining Engineering, The Pennsylvania State University, University Park, PA, Final Report to the U.S. Bureau of Mines, April, 1994Particle Concentrations in a Hazelton Inhalation Chamber Shahram Bavani, MS, West Virginia University, 1985Use and Potential of Lazer Holographic Interferometry and Subsidence Model- Study of an Underground Room and Pillar Mine Richard Begley, MS, West Virginia University, 1984Development of a Mechanistic Model for Prediction of Subsidence in a Longwall Mine Richard Begley, PhD, West Virginia University, 1990Redesign of Micro-Orifice Uniform Deposit Impactor Steve Behm, MS, University of Minnesota, 1991Evaluation of a Two-Phase Spray System for Dust Suppression B. Belle, MS, The Pennsylvania State University, 1996Evaluation of a Two-Phase Spray System for Dust Suppression B. Belle and R.-V. Ramani, The Pennsylvania State University, University Park, PA, Final Report, September 9, 1996A Fracture Mechanics Study of Crack Propagation Mechanism in Coal: The Mechanics of Fine Fragment Formation Z.T. Bieniawski and R. Karl Zipf, Jr., Mining Engineering Department, The Pennsylvania State University, University Park, PA. Final Report, October l, 1988A Mathematical Model for the Prediction of Ambient Dust Concentrations in Mine Atmospheres R. Bhaskar, MS, Mining Engineering and Operations Research, The Pennsylvania State University, 1984Spatial and Temporal Behavior of Dust in Mines-Theoretical and Experimental Studies –R. Bhaskar, PhD, Mining Engineering, The Pennsylvania State University, 1987"

Jan 1, 1998

By M. E. Rossi

Reconciliation of long-term block model reserves and mine production frequently shows significant discrepancies. This reconciliation can be done comparing the long-term block model reserves against a grade control model (generally, a model based on blast holes or production data). in this paper called an FI factor for tonnages, grade, and ounces; and also it should be done comparing the grade control model to the mill feed (or loaded to heaps) tonnages, grades and ounces (called an F2 factor). The long-term model usually contains blocks with dimensions larger than the size of the selective mining unit (SMU) of the operation. The smoothing effect of an estimator such as kriging will generally result in a grade-tonnage curve that does not match the grade-tonnage curve of the SMU's to be recovered. This problem is partly to blame for the reconciliation discrepancies found. In addition, in-pit perfect selection is impossible. and therefore the grade-tonnage predictions based on blast holes also need to be assessed, considering both unplanned dilution and the errors of estimation of the grade control model. This paper will focus on using conditional simulations to assess the uncertainty of the predicted grade-tonnage curve in terms of minable reserves, and in the framework of long-term mine planning. Quantifying the uncertainty in no uncertain terms is done in conjunction with a popular pit optimizer, which will yield not one, but several possible minable reserves, and therefore a range of possible minable tonnages and grades per pit shell or scheduled phase. This is a step further from the usual sensitivity analyses that are performed for deposit evaluation or development planning. Specifically, this approach takes into account the volume-variance relationship, the selectivity of the mining operation, planned and unplanned dilution. and carries the local uncertainty implicit in grade estimation into the mine design and mine planning phases. The motivation for the approach is discussed through an example, as well as a description of the procedures and steps involved.

Jan 1, 1998