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By Paul W. Jeran

This Bureau of Mines report has been prepared to provide a means whereby mineworkers without specific geologic training can recognize and record the existence of potentially hazardous geologic features encountered in coal mines. Each geologic feature described in this report has been implicated in roof failure. Through the recording of the observations of mineworkers, based on this report, a geologic map of mine workings and the associated ground control problems can be compiled. From such maps, the trends of changes and features can be determined and projected ahead of mining. The face crew can be alerted to a potential problem and what to look for as the face is advanced.

Jan 1, 1983

By C. M. McCulloch

A geologic study of Mines 32 and 33 in Cambria County, Pa., was conducted as part of a methane control research program. Areas of high methane emission and roof instability are encountered which are related to the structural and stratigraphic features that characterize the geologic setting of these mines. Locally the folds trend N 20° E ±2°, the direction of the butt cleat in the Lower Kittanning coal. The face cleat strikes at N 69° W ±2° and the systematic rock joint in the surface bedrock strikes N 67° W ±2°. This suggests that a directional stress oriented N 70° W produced the folds and influenced the directions of coal cleat and systematic joint sets. Analysis of SLAR indicates three directions of prominent regional lineation: N 39° E, N 31° W, and N 70° W. Little gas was encountered during development mining; large volumes of gas are encountered when roof falls. Most of the gas comes from strata above the mined coal; therefore, to control methane, roof instability must be controlled. Roof falls and high rates of methane emission are most likely where less than 30 feet of many thin layers of limestone, shale, and sandstone occurs between the Lower Kittanning coal and the next coal and in zones along the margins of a sandstone channel.

Jan 1, 1973

By C. W. Owings

"PURPOSE OF REPORTThe safety and efficacy of permissible storage—battery gathering locomotives are becoming recognized more and more in coal mines. The great mobility of this type of haulage equipment is due to the fact that no trolley wire and bonding of rails are needed; hence wherever there is track and adequate ventilation to dilute properly any dangerous gases, the storage—battery gathering locomotive may go. As coal near the outcrop or the surface is mined out, coal farther from the outcrop or deeper in the ground must be mined, and gassiness of the coal bed often increases under these conditions. The use of electrical equip¬ment capable of giving off arcs or sparks while operating near or at the coal faces constitutes a serious explosion hazard. Often, it is uneconomical or impracticable to use animal haulage, and locomotives must be employed. The operator should consider the safest and most economical unit; permissible equipment is the answer to this problem, and storage—battery locomotives are the only permissible electric haulage units.A comparison of permissible storage—battery locomotives with cable—reel locomotives of the latest enclosed ""explosion—tested"" type has been made at the Keystone No. 1 mine of the Houston Collieries Co., at Keys one, W. Va. The information and data contained in this publication were obtained by the writer during an inspection of haulage at this mine.ACKNOWLEDGMENTSThe writer is indebted to P. C. Thomas, vice president and general manager, the Koppers Coal Co., operator of the Keystone mines, who granted permission for making the study. W. A. Wilson, general superintendent, Houston Collieries Co., arranged for the investigation and for obtaining the data. C. E. Zuspan, chief electrical inspector, and J. C. Newman, division electrical inspector, accompanied the writer underground and assisted materially in obtaining information and data upon the haulage methods and performance of the locomotives. The assistance or general mine Foreman Pierman and of mine foreman White is gratefully acknowledged."

Aug 1, 1931

By W. A. Calhoun

"INTRODUCTION A letter from S. D. Strauss, vice president of Metals Reserve Company, Washington, D.C., dated May 22, 1945, to the chief of the Metallurgical Branch, Bureau of Mines, in Washington; includes the following: Because of the present critical shortage that exists in the supply of corundum required by certain industries in war production, the Reconstruction Finance Corporation, Mr. W. C. Keeley, Vice Chairman for Metals and Minerals, War Production Board, has recommended that the Reconstruction Finance Corporation though Metals Reserve Company, proceed with preliminary mill testing of the corundum ore in Gallatin County, Montana, and that the results of that testing be transmitted to the War Production Board. If the results of the testing work are considered satisfactory, Metals Reserve Company will then provide for the actual mining and milling of the ore for the production of corundum concentrates.Pursuant to the above stated recommendation by the War Production Board, Metals Reserve Company desires to make -use of the facilities of the Bureau of Mines testing plant at Rolla, Missouri, for conducting sink and float and other concentration tests on representative samples of the Montana corundum ore. Two, and possibly three samples of ore are to be tested which will have an aggregate weight of approximately 50 tons."

Dec 1, 1947

By Miles B. Royer

The experimental blast furnace has attracted increasing interest during the past decade as a practical means for investigating a broad range of blast-furnace smelting problems. Under experimental-furnace conditions, information can be obtained with less expenditure of time and raw materials and, therefore, at lower cost than comparable information could be obtained under industrial operating conditions. Furthermore, the experimental furnace may be operated beyond the range of smooth operation, even to failure, to delineate the limits of operability. Such deviation from normal operating practice would be economically intolerable in industrial operations where production and operating stability might be disrupted. The Federal Bureau of Mines experimental blast furnace at Bruceton, Pa., near Pittsburgh, has been operated and under development since 1951. However, the usefulness of this experimental data to industrial practice was somewhat nebulous in early experiments, and the correlation of the experimental blast furnace with the industrial blast furnace was not known.

Jan 1, 1961

By Cavallaro. J. A.

This report presents the results of a washability study of 455 raw coal channel samples with special emphasis on sulfur reduction. These raw coals contained on the average 14.0 percent ash, 1.91 percent pyritic sulfur, and 3.02 percent total sulfur. The complete washability data are presented for each sample processed. A statistical evaluation is included for the coalbeds from which more than 10 samples were collected and for the geographical coal producing regions. A graphical summation is presented for the coal producing regions and selected coalbeds. Finally a similar statistical evaluation is included showing composited data interpolated at Btu recovery levels of 50, 60, 70, 80, 90, and 100 percent. Graphical summations are presented for the various coal producing regions. Generally, significant sulfur reduction is achieved if the coals are crushed to a finer size and the higher specific gravity increments are removed. If a 50-percent Btu recovery was acceptable, then 32 percent of the samples tested could be upgraded to meet the current Environmental Protection Agency (EPA) standard of 1.2 pounds of S02 emission per million (MM) Btu when crushed to 14-mesh top size and separated gravimetrically.

Jan 1, 1976

By Peter L. Swanson

This investigation, which began 90 minutes after the February 3, 1995, seismic event, has benefitted from the assistance of a large number of individuals. These individuals provided information, data, analysis, brainstorming opportunities, field equipment, assistance with communication, conducted rock mechanics tests, and provided insight into mining in the southwestern Wyoming trona district. They include Rich Hodgson, Ron Hughes, Larry Refsdal. Mike Weller, John Kolesar, Joe Vendetti, and Rick Casey (Solvay Minerals), Dave Delling (Solvay consultant - former Solvay President), Karl Zipf (formerly with USBM, now with MSHA), Bob Friend, Bob Ferriter, Dave Ropchan, Jerry Davidson (MSHA Tech Support), Don Stauffenberg, Ben Hohler (Wyoming State Mine Inspector's office), Bruce Presgrave (USGS/NEIC), Chris Wood, Dan O'Connell (Bureau of Reclamation), Sue Nava, Jim Pechmann (University of Utah), John Norgord and members of FMC's mine rescue team (FMC Corp.), Bill Walter (Lawrence Livermore National Laboratory), Ron Gerlick, Kevin Wood, and Mike Harmel (USBM rock mechanics lab), Jim Case (Wyoming State Geological Survey), and Solvay consultants. In addition, many individuals helped us gather information on other recent large mining-related seismic events in Germany, Russia, and Australia. and other parts of the United States. These individuals include Wolfgang Minkley (IfG Institut fur Gebirgsmechanik, Leipzig), Arnfinn Prugger (Potash Corp. of Saskatchewan), Hartmut Spetzler (University of Colorado/ University of Bayreuth), Sergei Stanchits (Ioffe Poly-technical Institute, St. Petersburg), Rocky Thompson (Cyprus-Amax) and numerous seismologists throughout the Internet.

Jan 1, 2011

By C. H. Schack, A. O. Ipsen, H. G. Poole

"INTRODUCTION In the course of the investigation of manganese mineral occurrences in continental United States, the Bureau of Mines has collected several lots of ore from properties in the vicinity of Long Valley, Ariz. The ore occurs as irregular and random pockets in a brecciated zone. As only high-grade portions of the deposits obtained by selective mining would be acceptable as commercial-grade manganese ores, an investigation was made to determine amenability of the ores to concentration by ore-dressing methods. Several types of ores, differing in grade and mineral associations, were studied.Ores from the Vaiazza property are of special interest, owing to the successful application of silica flotation for their concentration. Ores from the Shroup and Conner-Hough properties are very similar but differ somewhat in their response to ore-dressing Method's. In all instances, the man¬ganese minerals are psilomelane and pyrolusite, with minor amounts of other manganese oxides. The country rook is a brecciated limestone; the diluent in the high-grade ore pockets is chiefly silica. The low-grade manganese ores are limestone replacements, and the chief gangue material, of course, is limestone."

Nov 1, 1947

By L. C. IlsLey

"According to accident statistics, issued from time to time by the Department of the Interior, Bureau of Mines covering fatalities in coal mines, between the years 1870 and 1921 there were 4,897 deaths caused by explosives. The legislatures and safety commissions of the various mining States have Elected and formulated many excellent regulations in regard to the handling and use of explosives in an endeavor to keep this class of accidents as low as possible. An analysis or comparison of the explosive, regulations issued by over thirty States would make a very long paper, however, by subdividing according to phases and issuing several papers it is believed that the material will be more readily available. The first phase was treated in Serial No. 2405 of the Bureau of Mines (""State and Federal Electrical Shot-Firing Regulations,"" issued in October 1922) which gave a compilation of such regulations as apply strictly to electric shot-firing. The second phase under consideration is ""Who may set off blasts in coal mines.""In some States, the person who does the firing must be an ""authorized shotfirer,"" while in other States he must have proved his ability to do this work, and again in other States he is ""any person."" The present paper covers rules and regulations relating to this phase of shotfiring, and those States having similar regulations have been grouped as follows."

Jun 1, 1923

By J. G. Donaldson

Optimum conditions are given for chloridizing pyrite, marcasite, chalcopyrite, arsenopyrite, stibnite, and covellite with chlorine gas. The formation of metal chlorides is affected by the time and temperature of chloridizing, and by particle size of the sample. Chloridizing data also are given for chemically precipitated antimony (III) sulfide and copper (II) sulfide.

Jan 1, 1962

By Seth C. Schaefer

The Bureau of Mines investigated thermodynamic properties of Mn304 (manganomanganic oxide) and Mn203 (manganese sesquioxide). The standard Gibbs energies of formation (?Gf°) of Mn304 and Mn203 from their lower oxides were determined with high-temperature galvanic cells using stabilized Zr02 (zirconia) as the electrolyte. Potential measurements were obtained for the cell Pt, MnO, Mn304//Zr0 2//02(g, 0.0112 atm), Pt, with the overall cell reaction 6Mn0(c) + 02(g, 0.0112 atm) = 2Mn304(c), where- 02 refers to indicated partial pressure of oxygen at the reference electrode. Similar measurements were obtained for the cell Pt, Mn304, Mn203//ZrO2//02(g, 0.0115 atm), Pt, with the overall cell reaction 4Mn304(c) + 02(g, 0.0115 atm) = 6Mn203(c). Equilibrium oxygen pressures for the Mn0-Mn304-02 and Mn304-Mn203-02 systems were measured and may be expressed for the respective systems as [23,400 109 P02 T + 11.91 (764.9 - 1,208.6 K) and log p02 = - 11,957 + 9.66 T (968.6 - 1,208.2 K),] where pressure (p02) is in atmospheres and temperature (T) is in kelvins. Standard thermodynamic properties of Mn304 and Mn203 were derived from these measurements and auxiliary thermodynamic data from the literature.

Jan 1, 1982

Develop technology for preparing thick corrosion-resistant coatings and electroforms of iron-chromium-nickel alloys. Approach To reduce the United States' dependence upon foreign sources for supplies of strategic and critical metals such as chromium, cobalt, and nickel, new technology must be devised to conserve these valuable commodities. One approach being investigated by the Bureau of Mines is the use of a modified-aqueous-electrodeposition method to prepare thick (-25 µm), complex alloy coatings (e.g., stainless steel composition) with properties similar to the commercial alloys. An alloy coating on a low-alloy steel or carbon steel substrate would require significantly less strategic and critical metals than those contained in an equivalent mass of the commercial alloy. Coatings applied to appropriate mandrel materials make possible the preparation of intricately-shaped alloy electroforms (near-net-shape parts). As a result, the loss of valuable metals associated with machining finished products would be minimized.

Jan 1, 1986

By Philip W. Holland

This U.S. Bureau of Mines (USBM) report describes a chromatographic method that is used for rapid field determinations of carbon dioxide in natural gas streams at a USBM helium production facility. The method employs a commercially available portable gas chromatograph that is equipped with a 10-m fused-silica capillary column coated with a porous polymer. The instrument operating parameters permit determinations to be performed over a concentration range of 10 ppm to 10 pct with a frequency of 20 samples/h. The speed at which determinations can be performed is an important factor when evaluating efficiency or troubleshooting processes at the helium facility.

Jan 1, 1994

By Ronald H. Church

As part of the Bureau of Mines health and safety research program in strata control, a ground-penetrating radar (GPR) system capable of pene-trating approximately 10 ft into the mine roof has been devised to identify anomalistic conditions. The GPR system consists of a transmitter with carrier frequencies of 250, 500, and 1,000 MHz, utilizing a dipole antenna, and a receiver, consisting of a dipole antenna fed into a sampler with a time base housed in a storage oscilloscope. A computer was utilized for data acquisition and data processing. Data analysis by computer enhancement revealed recognizable return ra-dar signatures from the middle man rock and main roof of the test site. These stratigraphic anomalies can be cataloged for recognizable fea-tures, which from the past history of the mine may have been shown to create strata control problems. Early recognition of such features could lead to immediate corrective actions and result in the saving of lives.

Jan 1, 1985

By C. A. Frenzel

Extensive spectroscopic data are needed in making reliable vibrational assignments for use in calculating thermodynamic functions of polyatomic molecules. The fundamental vibrations of organic molecules may be observed at any wavelength from 2.5 to 200 microns (micron = µ = 10-4 centimeters), but most often in the region from 3µ to 50µ. Raman spectra generally cover the range in which fundamental vibrations occur, but equally important infrared spectra usually are not measured at wavelengths longer than 25µ. This limitation results because most infrared spectra are determined for analytical purposes, which seldom require information outside the region 2µ to 25µ. Measurements of infrared spectra in the range 15µ to 35µ recently were begun by the Bureau of Mines to obtain data needed in making vibrational assignments. This report presents the spectra of the following thirteen compounds: Tetrahydrofuran, 1-methylpyrrole, piperidine, 2-methylpyridine, 3-miuthylpyridine, 2-propanethiol, cyclopentanethiol, 2-methyl-2-butanethiol, 3,3-dimethyl-2-thiabutane, cyclohexanethiol, cyclopentyl-l-thiaethane, 2,4-dimethyl-3-thiapentane, and hexamethyldisiloxane.

Jan 1, 1960

By D. A. Baker

This report describes the elemental characterization of chromite and related materials at the Bureau of Mines, Albany Research Center. Analytical methods for determining the major constituents, representing extensive experience, refinement, and development, are described and fully annotated. This presentation should allow other laboratories to use these methods and obtain comparable results with a minimum of time needed for familiarization with individual methods.

Jan 1, 1990

By F. N. Kissell, R. J. Bielicki

The Bureau of Mines found sulfur hexafluoride (SF6), released from a lecture bottle, to be an ideal gaseous tracer for studying mine ventilation systems. Air samples were collected in glass syringes and analyzed by electron-capture gas chromatography. In these studies, the lower limit of detection was about 1 part per billion by volume (ppb) of SF6 per part of air. Experiments conducted in a Pennsylvania limestone mine showed this technique useful in evaluating the effectiveness of auxiliary fans, measuring low flow velocities, probing the air circulating near a working face region where ventilation appeared to be poor, and estimating volumetric flow rates in airways of large cross-sectional area and having low flow velocities. This technique was also used in a western vein-type metal mine to measure the amount of return air being recirculated into the intake air due to leakage through old stoped areas.

Jan 1, 1974

By Albert E. Long

This paper presents a description of the operational mechanics involved in block-caving a granodiorite-capped, limestone deposit. This method was used for 24 years at the Crestmore mine, near Riverside, Calif., which was operated by the Riverside Cement Co. as a source of raw material used to manufacture a portland cement. The Crestmore mine is the only place where a block-cave method has been used to mine a limestone deposit. Structurally, limestone is relatively strong, and it is not usually considered to be a substance amenable to mining by block caving. It is therefore a credit to the engineering department of the Crestmore mine that it developed a satisfactory, relatively efficient method of block-caving a structurally stable rock. In the discussion, covering the methods applied to produce about 7.9 million tons of limestone and granitic rock materials by block caving, particular emphasis has been placed on an assessment of (1) physical properties of the deposit, (2) ground pressure and support, (3) methods used to induce fragmentation and maintain cave action, (4) surface and subsurface subsidence, (5) secondary blasting of oversize, (6) production rate, (7) safety, and (8) the advantages and disadvantages of the cave method as applied to this specific limestone deposit.

Jan 1, 1958

"An active list of permissible explosives was published in September 1935 as part of United States Bureau of Mines Report of Investigations 32S6, under the title ""Active List of Permissible Explosives and. Blasting Devices Approved. Prior to July 31, 1935."" This list included 154 brand names,Changes in the list that have been authorized subsequently placed 24 addi¬tional brands of permissible explosives on the active permissible list as a re¬sult of tests, changes in brand names, or transfer from the inactive list. Eight permissible explosives were transferred from the active to the inactive list. The present active permissible list contains 170 brand names. The brand names of the permissible explosives placed on the active list are as follows:Black Diamond Nu-Gel No. 4 By test.Black Diamond Special A,do.Burton 11, L. F. By change in name,Burton G, L. F. By test.Columbia B By change in name.Columbia C Do.Columbia D Do.Columbia E Do.Columbia. F Do.Columbia G Do.Columbia 1 Do.Columbia 2 D.Columbia 3 DoColumbia 4 Do.Columbia-Gel 1 Do.Columbia-Gel 2 Do.Genite 5, Do.Genite 7, Do.Genite G Do.Lump Coal C By test.Peerless No, 1 By transfer from inactivePeerless No. 8, L. F. Do.Tri-State Special No. 1 Do.Unilite No. 2 Do."

Dec 1, 1936

After nine years of negotiations, the U.N. Conference on the Law of the Sea approved a Law of the Sea Treaty text in April. Israel, Turkey, the United States and Venezuela voted against the text and 17 other nations including Belgium, the Netherlands, Italy, the Soviet Union, the United Kingdom and West Germany abstained. These nations still have the option of joining the treaty when it is opened for signing in December. However, the Reagan Administration has stated that several provisions of the deep seabed mining portion of the text are unacceptable and it seems unlikely that the United States, at least, will change its position. ALUMINUM Reynolds Metals Co. has criticized an Oregon state plan to relax air pollution standards for aluminum plants. The company feels that relaxation of the rules does not go far enough. Reynolds officials say that they have spent about $31 million at their Troutdale plant for state-of-the-art pollution control equipment, and if they are required to make the pollution reductions called for in the 1986 rules, Reynolds would be forced to close the 40-year-old plant.

Jan 1, 1982