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By J. M. Seward, W. D. Dietzman, M. E. Hawkins

Analytical studies of formation waters are widely used by the petroleum industry as an aid in solving problems such as identifying intrusive waters , corrosion studies , treating injection water , and choosing open or closed water- injection systems . The solution of a problem is often simplified when reliable analyses of the waters under consideration have been made previously . Chemical analyses and electrical resistivity measurements are presented on 267 samples from 74 fields in south Arkansas , and 199 samples from 80 fields in north Louisiana .

Jul 1, 1960

By B. E. Davis

Over 80 pct of domestic phosphate rock, which is the starting material for phosphorus-containing fertilizers, comes from central Florida deposits. As K-her grade deposits are depleted, lower grade phosphate ores containing 'Mg0 in the form of dolomite are encountered. Treating high MgO ores with present beneficiation technology will not yield a concentrate meeting specifications for acidulation. The Bureau of Mines conducted research on three high-MgO phosphate samples from south Florida. The sales contained, in percent, 5.4 to 10.2 P205, 1.9 to 7.6 MgO, and 35.3 to 60.1 acid insolubles. A technique of sizing, grinding, desliming, scrubbing, and redesliming was used to produce a feed suitable for continuous flotation studies, A conventional fatty acid-fuel oil rougher flotation followed by two to three cleaner stages resulted in concentrates containing, in percent, 30.7 to 31.3 P205, 0.6 to 1.3 MgO, and 2.5 to 4.8 acid insolubles. The P205 recovery from the flotation feed ranged from 55.1 to 89.7 pct.

Jan 1, 1984

By C. A. Pearson, W. D. Dietzman, M. E. Hawkins

Results of chemical analyses and electrical resistivity measurements of 422 samples of oilfield brines from 120 east Texas fields in Railroad Commission of Texas Districts 5 and 6 are presented in tabular form . These samples represent water from all of the major petroleum- productive formations in the area . Water analyses and electrical resistivity data , when fully utilized by proper study techniques , are useful tools in the solution of many engineering problems such as detection of well leaks , identification of water sources , and interpretation of electrical well logs . In the area included in this study , these representative data should facilitate the solution of problems in which water analysis and water resistivity are factors .

Jan 1, 1964

By J. S. McNabb

"A search for manganese ore by core-drill exploration was carried out by the Bureau of Mines in the Philipsburg mining district in Granite County, Mont., in 1939 and 1940. This work was based on detailed studies of the manganese ore bodies of the district previously made by the Geological Survey.In 1949 further search for manganese in the district was deemed advisable. Diamond drilling was begun the following year as a joint program by the Geological Survey and the Bureau of Mines with the primary purposes of probing ore-leasing structures and extending the limits of known ore bodies. A secondary objective was to test a geologic theory based on a new conception of manganese-ore localization. The exploration targets were designated and the drilling results interpreted by the Geological Survey, and the Bureau of Mines was responsible for the drilling, sampling, and core handling. Improved drilling equipment and methods were utilized in an effort to obtain better core recoveries than resulted from the earlier drilling campaign.The Philipsburg mining district, Granite County, Mont., is 27 miles south of Drurrnnond, about 45 miles airline northwest of Butte, and 1 mile east of Philipsburg. During the course of the investigation patented lode-mining claims owned by the American Machine & Metals, Inc., the Contact Mines, Inc., and the Moorlight Mining Co. were diamond drilled.The district has been an important source of domestic manganese dioxide ore since local recognition of the mineral's importance during World War I. Peak annual output in 1918 of about 127,000 tons of manganese ore was utilized principally by the steel industry. A small but relatively steady output has persisted to the present to satisfy demands by battery manufacturers for battery-grade manganese dioxide.The known manganese deposits of the district are in sedimentary rocks of Paleozoic age. These rocks lie along a north-trending anticline traversed by a series of east-west tension veins. The east flank of the anticline terminates at a steep-dipping fault contact against a small granodiorite batholith.Replacement deposits of manganese oxides and carbonates occur locally in or closely associated with tension veins cutting calcareous rocks, or adjacent to the intrusive. Rhodochrosite has been a common accessory mineral in deposits valuable chiefly for lead, zinc, and silver. Some of the replacement deposits characteristically are irr2gular in outline, whereas others have fairly regular walls marking the limits of favorable beds."

Dec 1, 1955

By Robert L. Jones

The Boston Consolidated mine is situated in the Bingham mining district, Salt Lake County; Utah (fig. 1). The property has had a noteworthy production of cupriferous, gold-bearing, pyritic ore in addition to lead ore. The Bureau of Mines established a diamond-drilling development project on the property in September 1943 with the primary objective of determining the continuity of a mineralized zone in the Commercial limestone below and to the northeast of the 800-foot level (fig.2). Examination of the geologic feature at the property previous to drilling indicated that the mineralized limestone horizon would continue belay the 800-foot level, but with a flatter dip than disclosed above this level. During the project period, 36 holes totaling 4,001 feet were drilled from underground stations outlining the zone below the 800-foot level (figs. 2 and 3).

Jan 1, 1949

By Robert W. Smith

[In a certain application it was necessary to compute the incomplete beta function, ß(1/2, p, q), for a certain set of values of p and q. Since the set of p and q values was much more finely spaced than those in any published tables, the authors have decided to make their results available in this report. In connection with this application, the function ß(1/2, p, q) was needed at various points in the p, q plane at intervals of 0.05, 0.05 p = 2q < 10.00. Fletcher, Miller, and Rosenhead3/ state that the only tables available in the desired range are those of Pearson.4/ However, the interval used by Pearson was not small enough for the present application. For this reason, it was decided to calculate the function ß(1/2, p, q) for p = q = 0.05 (0.05) 10.00. This table is published because of the fundamental importance in mathematical analysis of the incomplete beta function.]

Jan 1, 1953

By Robert S. Warfield

The Bureau of Mines investigated a geologically favorable area in the Beluga River coalfield in south-central Alaska to determine if there were sufficient minable coal reserves for onsite utilization to meet the projected thermal power needs of the Anchorage area. A program of diamond core drilling and sampling delimited a shallow saucerlike structure estimated to contain indicated reserves of more than 20 million tons of subbitminous coal in a seam over 50 feet thick that could be mined by opencut methods. A large sample of fresh coal was taken across the full width of the seam for washability studies. This sample, with 4 volume-percent of clay partings eliminated, contained 24.4 percent moisture and 16.8 percent ash and had a calorific value of 7,162 Btu per pound. The studies indicated that mechanical cleaning would be of doubtful value.

Jan 1, 1963

By William A. Beck

Since bauxite mining began in the Irwinton District, Wilkinson County, Ga., in 1912, it has been on a small scale, as most of the deposits of high-grade ore are small. The bauxite has a high silica content, and its use has been largely limited to the chemical industry. Drilling under this project did not disclose any bauxite deposits of commercial value: However, numerous holes penetrated high-alumina clay deposits, but no attempt was made to delimit them, as the project was solely an exploration for bauxite. Bauxite was first discovered near Irwinton in 1907. The district covers virtually all of Wilkinson County and extends into the adjoining counties of Washington, Baldwin, and Twiggs. Mining was begun in 1912 by the Republic Mining & Manufacturing Co. on the Honeycutt, Parker, and Daniel properties, which are 1.5 miles from Wriley on the old Irwinton to Milledgeville Road.

Jan 1, 1949

By Manuel Gomez

This report presents experimental work conducted on a number of coals found within the boundaries of the Missouri River Basin, which were, to an extent, a selection of coals typical of that region. In the min, the laboratory work falls into three general classifications: (1) Laboratory distillation assay of coal to establish yields on carbonization; (2) chemical analyses of the coal samples before drying or carbonization; and (3) chemical analyses of the products of carbonization. It will be seen in the following discussion that these data derived from the small-scale laboratory apparatus are useful in predicting yields from pilot plants or industrial units. Coal is produced in about 48 general areas or mining fields in the Western States, of which approximately 18 fall within the limits of the Missouri Basin.3/ Beginning with the Northern Colorado field, through the Central and Western Wyoming fields, the coal is principally bituminous and subbituminous rank. The western Montana coals are also of these ranks. Progressing northeast from central Wyoming the coal decreases in rank, as shown by the subbituminous C coals of the Gillette field in northern Wyoming and the lignites of eastern Montana and North Dakota.

Jan 1, 1953

By W. D. Musgrove, B. W. Gandrud, A. C. Richardson

"INTRODUCTION The Cahaba coal field is the second largest coal—producing area in Alabama. This field underlies parts of Shelby, Jefferson, St. Clair, and Bibb Counties and has an area of about 270 square miles. The Cahaba formations contain a number of coal beds, about 8 of which are mined at present. Although the area contains many folds and faults, samples from various mines and beds indicate that, except for the variation in ash content, the coal from this field is very uniform in character and quality. It is a high-volatile bituminous coal used chiefly for steam-raising purposes and domestic fuel. The coal as mined usually contains too high a percentage of impurities to be marketed without some preparation. The majority of the mines have washing plants in which jigs are the favorite type of equipment, although at some mines tables are used for cleaning the slack sizes. The washing characteristics of the coal from the Cahaba field are very uniform and differ from those of the near-by Warrior field, in that the coarser sizes contain a much lower percentage of bony material than the finer sizes. In general, the bone increases with decrease in size. It breaks into thin flakes, making difficult its elimination in the cleaning process, and gives rise to what is known among the washery operators of the Cahaba field as the ""rash problem.""A previous publication 5 referred to rash from the standpoint of jig operation and suggested some means of handling it with jigs. This report presents the results of table tests on two samples of fine coal from the Thompson and Woodstock beds, respectively, of the Cahaba field to determine the influence of rash on table efficiency.This investigation has been made in connection with the study of coal-washing problems now being conducted by the U.S. Bureau of Mines and the University of Alabama, with the cooperation of the different coal operators of Alabama."

May 1, 1934

By Gary A. Kingston

Domestic nickel resources are costed to develop a contingency supply curve of U.S. nickel availability at various costs. It is estimated that 4.3 billion pounds of nickel is potentially recoverable from 698 million tons of ore at prices ranging up to $6.36 per pound of nickel. Over 95 percent of the total is estimated to be available at a price of less than $4.00 per pound.

Jan 1, 1970

By S. J. Aresco

The Bureau of Mines has been active in promoting the purchase of coal for Government use under specifications that define the requirements in terms of heating value of the coal, expressed in British thermal units, and the composition as shown by proximate analyses. To these, when required, are added the ash-softening temperature, the free-swelling index, and the Hardgrove grind-ability index. Under most of these specification contracts the bidders guarantee the quality of the coal, and that guaranteed by the successful bidder becomes the standard of his contract. The deliveries are sampled in accordance with instructions4 issued by the Bureau of Mines; the samples are analyzed in the Bureau laboratory to determine whether the coal is of the quality guaranteed by the contractor; if it is not, a price adjustment is made. Analyses of the delivered coal and tipple samples (samples collected at mine tipples as coal is being loaded into railroad cars or trucks) provide valuable data for use in evaluating future bids. In addition, the continuous sampling of coal as delivered is a check on the practical results obtained in burning the coal.

Jan 1, 1965

By O. M. Bishop

The Douglas fluorite property is in the Empire district of eastern Pope County, Ill., which lies near the west boundary of the productive Southern Illinois fluorspar field in Hardin and Pope Countios. Production from mines on the Douglas property accounts for about one-half of the 72,000 tons of fluorspar with which the Empire district is credited. This output was from the Sycamore, Pierce, Slapout, and Empire veins, which are normal fissure veins of little displacement along which there has been local wall-rock replacement by fluorite.

Jan 1, 1949

By R. E. Campbell

Uranium metal of improved purity was prepared by electrorefining commercial magnesium-reduced uranium in a molten sodium chloride-uranium trichloride electrolyte. The best operating conditions for the preparation of refined metal were established as follows: an electrolyte containing 8.7 to 13.3 weight-percent uranium; initial cathode current densities from 300 to 1,500 amp/sq ft; and a molten salt temperature of 860° C. Ingots produced from electrorefined uranium crystals prepared with these operating conditions were substantially free of metallic impurities. The only impurities in the refined and consolidated metal were present in low or undetectable amounts.

Jan 1, 1965

By Mark I. Copeland

Bureau of Mines researchers investigated the combined effect of copper and tin additions on the mechanical properties of hot-rolled steels. Wrought steels containing 0.2 wt-pct C and up to 0.2 and 1.0 wt-pct Sn and Cu, respectively, were made and evaluated by conducting tensile and impact tests and electron-beam microprobe and electron microscopy examination. Tin additions did not significantly affect the tensile properties of steel at different copper contents in the hot-rolled condition. Tin lowered the copper content at which strengthening by copper precipitation normally starts, 0.8 wt-pct, and decreased the strength of steel aged at 1,022° F (550° C). The most adverse effect of tin was lowering the notch toughness of steels at most copper contents.

Jan 1, 1976

By L. T. MCELVENNY, Robert B. McElwaine, M. Clair Smith

Production of mercury from the cinnabar deposits of the southwestern Arkansas mercury district began in 1931 , reached its peak in 1942 , and ended in 1944. The mines are now idle . Virtually all the cinnabar was obtained from deposits in a belt , about a mile wide , of steeply dipping sandstone beds in the overriding blocks of three thrust faults . The belt was productive for a length of about 27 miles eastward from eastern Howard County, through Pike County, into Clark County . During the early life of the district, Federal agencies watched and recorded its progress as a contributor of a strategic metal, and later, during the war, conducted investigations designed to advance its development . In 1941 , the Bureau of Mines and the U. S. Geological Survey cooperated in investigations on eight mineralized areas in the western part of the district , to wit : Hales mine , U. S. mine , Lulu Bell property, Hopkins Hill , East Gap Ridge , Gap Ridge , Parnell Hill , and Section 17 mine area . U. S. Geological Survey prepared both surface and mine maps and designated the areas to be investigated ; the Bureau did the drilling , trenching, and sampling involved in the investigations . Twelve holes , aggregating 3,539 feet of bore , were diamond drilled on six properties ; 5,309 linear feet of surface trenches were bulldozed in six areas and 19 samples taken from them ; and 86 underground channel samples were cut in two adits on one property . In 1944 , the Bureau of Mines measured mine dumps and calcine dumps in the district in an investigation of their mercury content . Two mine dumps and one calcine dump were sampled . The data pertinent to the work done by the Bureau are included in this report .

Oct 1, 1950

By Jerry T. McLendon

The proper disposition of phosphatic clays has been the subject of research and debated for years by phosphate producers, State and Federal research agencies, regulatory authorities, and environmentalists. To date, no "universal" solution exists for the ultimate disposl of phosphatic clays. This Bureau of Mines report examines the state of conventional clay disposal technology and reviews the technical progress of innovative alternatives. Twenty impoundment sites were investigated by the Bureau of Mines using geotechnical methods and laboratory analysis of cored samples. In addition, quasi-static cone penetrometer soundings were conducted to define clay and/or sand-clay interfaces en masse. Samples of the top, middle, and bottom hole segments were obtained at each station for laboratory studies of clay densities, pore fluids, plasticity, and mineralogical properties. The results of this study support the continued use of initial clay settling impoundments but emphasize the need for "in-line" systems to reduce the initial volumes of plant-generated phosphatic clays. The effective use of sand tailings is also encouraged to promote further consolidation of clays via self-weight stressing, sand-clay admixtures, and/or surcharging sand caps.

Jan 1, 1984

By F. B. Tough

"INTRODUCTION Organizations formed for the purpose of conducting conservation work in oil fields, in order to conserve and prolong the supply of crude petroleum are rare and novel. Such an organization is the Rocky Mountain Petroleum Association, Denver, Colo, As our production of petroleum can no longer keep with the consumption, the plan of organization, character of work, and results obtained by this association are well worth considering. It is hoped that the results achieved in the Wyoming fields will serve to stimulate similar organizations among operators in the state or other oil fields of the United States, The Rocky Mountain Petroleum Association, Danvers Colo., was formed in May, 1919. It comprises the Midwest Refining Co,. The Ohio Oil Co., and the Continental Oil Co. These three companies entered into a cooperative agree¬ment with the Federal Bureau of Mines whereby $30,000 would be spent under the direction of the bureau, which agreed to furnish competent men, and to furnish the work and expenditure of funds. Although the financial burden for the first year's work, now drawing o a close, was carried by only three companies, they stipulated their desire that the benefit of the work should accrue to the industry, and that the personnel employed should be as zealous to assist one operator as another, without regard to whether ha was contributing to the support of the work or not."

Apr 1, 1920

By J. B. Clemmer

Fluorspar is one of the most important nonmetallic minerals and is used extensively in the metallurgical, ceramic, cement, and chemical industries. The steel industry consumes most of it, but as the Mineral is the chief source of fluorine, it is becoming increasingly valuable to the chemical industry in the production of fluorine compounds The development of nontoxic organic fluorides for use as refrigerants in mechanical refrigeration and air-conditioning units illustrates the increasing use of fluorspar in the chemical industry. Most domestic flurospar comes from deposits in the Illinois-Kentucky district, which centers around Rosiclare, Ill. About a dozen companies operate in the district, which comprises parts of Pope and Hardin Counties in southern Illinois and Crittenden, Livingston, and Caldwell Counties in western Kentucky. According to the latest available statistics, this district supplied 1/5,960 short tons of fluorspar in 1937, compared with the total domestic production of 181,230 tons. Imports totaled 37,063 tons.

Jan 1, 1939

By O. C. Blade

This report on the properties of aviation gasolines and aviation jet fuels produced in the United States during 1956 was made under a cooperative agreement between the American Petroleum Institute and the Bureau of Mines of the United States Department of the Interior. Analytical data are presented for 120 samples of aviation gasoline and for 38 samples of aviation jet fuel. The analyses were made on samples typical of the manufacturers&apos; 1956 production in their laboratories and the results submitted to the Bureau of Mines for compilation. The products of 20 manufacturers of aviation gasolines and of 17 producers of aviation jet fuels are represented.

Jan 1, 1957