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By J. H. Starkey

SAGDesignTM Testing for grinding mill design was introduced commercially in 2004. Up to January 2008, 18 projects have been completed and 99 samples have been tested using this method. Two papers have been published describing the patented test procedure and one of these shows how the results compare with other grinding test methods. This paper will briefly discuss the theory on which this technology is based, and explain the procedures used to develop the calibration equation. Case studies are also included to demonstrate the effectiveness of the test work being done. These case studies show how the SAGDesign test is being used today: to design new grinding circuits for commercial full scale use; to calculate throughput in existing mills for production planning; and to accurately define grinding mill requirements at the scoping, pre-feasibility or feasibility study stage of project development, in order to economically identify the size and cost of the grinding mills that will be needed for the project. This is important because if the full rec-ommended SAGDesign testing program is done at an early stage in the project, the definitive cost for a guaranteed throughput, grinding mill design (by Outotec if their mills are purchased) is available. New grinding mill design for final engineering will be represented by the test work done on the Climax Molybdenum Project for Phelps Dodge (now FMI) in Colorado, USA. The SAG mill and ball mill for Climax are now in fabrication with project start up in late 2009. Next, the sizing of grinding mills at the scoping, pre-feasibility or feasibility study stage of mine development will be represented by a large metal mining property in Russia. Finally, calculation of the throughput for existing mills will be represented by work done at a base metal mine, in eastern Canada. Test work for designing SAG mills is now done in four laboratories at the time this paper was written. One in the USA at Dawson Metallurgical Laboratories, Inc. in Salt Lake City, two in Russia at the TOMS Research and Design Institute and at the Irgiredmet Research Institute, both in Irkutsk, and a fourth mill has been installed in Australia at AMMTEC Limited?s lab in Perth. A fifth SAGDesign test mill for radioactive ores has been built by Starkey & Associates, specifically for testing uranium ores and can be moved to any licensed lab in the world on a project basis.

Jan 1, 2014

By W. Krieglstein

Due to the natural variability of ores, it is necessary to carefully test flotation behavior of flotation cells before designing flotation circuits. For performing quick and versatile tests in the laboratory, Siemens developed a laboratory-size Hybrid Flotation Cell, which has been down-scaled from the 300 m³/h production cell to a 0.6 m³/h flotation cell. This small cell is being used as a test bed for technical and chemical concepts, the improvement of decisive components and the characterization of customer ores. In this study the evaluation results for Andean porphyry copper ores are shown. Total recovery rates of the order of 45 to 50 % have routinely been achieved in a single flotation cycle over a wide range of feed grades. In addition, the Hybrid Flotation Cell has proven to be particularly well suited for the flotation of fine particles below 20 µm down to below 1 µm, at high recovery rates and concentrate grades.

Sep 1, 2012

By L. Li

Chemical composition, mineral composition, and iron occurrence state of main mineral are studied, Research of mineral processing technology is carried out according to ore features. The test results indicate, that through staged grinding-staged concentration process, the better separation index is up to 65.54%, iron preparation concentrate grade and 85.66% recovery with the fineness (-200 mesh) 45.88% in the primary grinding ore and the fineness (-200 mesh) 75.50%, in secondary grinding ore in the situation of best magnetic field intensity (roughing 0.2T and cleaning 0.15T).

Sep 1, 2012

By Yuhua Wang, Haitao Zheng, Guangli Zhu, Yuehao Zhao, Fushun Yu, Dongfang Lu

"Spodumene, feldspar and quartz possess similar surface properties, which make the difficult to separate spodumene from other silicate minerals by flotation. The differences of crystal structure, surface property and floatability of three minerals were studied by various technical means. The results show that Li-O and Al-O bonds in spodumene structure are not strong and easy to be broken. However, Al-O and Si-O bonds in feldspar and Si-O bond in quartz are very strong and not easy to be broken. High contents of Al and Li on spodumene surface were found by XPS measurements, which is benefit for the adsorption of anionic collector. The surface energies of main cleavage planes of spodumene (110), feldspar (001) and quartz (001) are 1.88 J/m2, 2.97J/m2 and 2.68J/m2, respectively. Hence, the exposed surfaces of feldspar and quartz are not saturated and easy to adsorb OH- ions from solution and cause the lower IEP than spodumene. The contact angles of three minerals in water are lower than 16º, suggesting that the hydrophilicity of three minerals is high, and the order of hydrophilicity is quartz > feldspar >spodumene. Correspondingly, contact angles and flotation recoveries of spodumene are bigger than that of feldspar and quartz in presence of a combined anionic and cationic collector named YOA.INTRODUCTION Flotation technology plays most important role for the recovery of spodumene from pegmatite ore. Generally, spodumene with fresh surface is easy to be floated using soap and oleic acid as collector, and the best flotation pH range is 4.0 to 9.0. However, the flotability of spodumene will become worse when its surface was polluted by slime which produced by the weathering of spodumene and other silicates (Dresler et al. 1998; Moon and Fuerstenau 2003; Menéndez et al. 2004; Yu et al. 2015). In addition, the species of Ca2+, Fe3+, Mg2+ and other metal ions in pulp can not only activate the flotation of spodumene, but also the activation of gangue minerals, and then the flotation selectivity of spodumene from gangue minerals became wores (Wang and Yu 2007; Yu et al. 2014). In order to eliminate the negative effects of slime and metal ions on the flotation of spoddumene, the desliming and long time scrubbing with the addition of NaOH and Na2CO3 were adopted. Usually, NaOH shows the activation for spodumene flotation, and the recovery of spodumene increases with the increase of NaOH dosage. Na2CO3 can eliminate the non selective activation of Ca2+, Fe3+, Mg2+ ions in the pulp, and the concentrate grade of spodumene increases with the increase of Na2CO3 dosage. Anionic collectors such as chelants, hydroxamic acid, oxidized paraffin soap, naphthenic acid and oleic acid were widely used for the flotation of spodumene (Dresler et al. 1998; Moon and Fuerstenau 2003; Menéndez et al. 2004; Yu et al. 2015)."

Jan 1, 2018

By Chuansheng Luo

If lead-zinc ores have high oxidation rate, separation of lead and zinc is very difficult. This paper studied the technology of preferential flotation by the coarse grinding and re-grinding. The lead concentrate grade is 51.40% and the lead recovery is 62.83% when feed grades Pb 1.74% and Zn 6.46% with oxidation rate being 13.75%. At same time, the zinc concentrate grade is 50.07% and its recovery is 90.01%.

Sep 1, 2012

By D. J. Hallbom

The ?yield plastic? rheological model describes the flow behaviour of a variety of non-settling suspensions, including many types of mineral slurry. The current paper presents the laminar flow relationship (pressure gradient vs. flow rate) for a yield plastic fluid flowing through a pipe or cylinder. Simplified algebraic equations, suitable for engineering purposes, are presented for yield plastic fluids with values of the scaling factor in the range that includes most industrially important slurries. The laminar pipe flow relationship is one of the most important fluids engineering calculations. It may be used to determine the rheological parameters of a material in a capillary rheometer or flow loop. If the rheology is known, these relationships may be used to determine the laminar flow pressure gradient in pipelines of various sizes.

Jan 1, 2014

By P. Braga, A. Chaves, S. França, A. Luz

"In Brazil, there are no official reserves of molybdenum, and the unofficial reserves are modest. Therefore, the molybdenum ore (molybdenite) produced as a co-product or by-product of emerald mining in the region of Campo Formoso, BA, has arisen as the only economic option. The flotation process is commonly used in Brazil for the recovery of molybdenite from emerald mining tailings, but it produces low-content molybdenite concentrates, thereby resulting in a product with low economic value. The molybdenite concentrate produced in Campo Formoso contains 83.5% MoS2 (50% Mo), which is less than the international standard product that contains > 90% MoS2 (54% Mo).This low value is due to the presence of talc, which is a naturally hydrophobic mineral that is also floated with the molybdenite during the flotation process. Separability studies were done in a Partridge-Smith cell using dextrin and quebracho as a molybdenite depressor in solution at different concentrations and pH values to produce a technical-grade concentrate (i.e., 90% MoS2). These basic studies were accompanied by measurements of the zeta potential and contact angle, which was determined by the capillary rise method. The results of these floatability studies were used in bench flotation tests, which were performed in a Denver laboratory flotation cell. A molybdenite concentrate of 93.4% MoS2 was obtained when dextrin was used at a concentration of 100 g/t."

Jan 1, 2014

By A. V. Neretin

This paper is a continuation and extention of the previous paper on energy-efficient placer mining methods which was presented in 2007 at the World Gold Conference in Cairns, Australia (Nere-tin, 2007a). The paper reports the results only on gravel processing as they were not fully discussed in the previous paper. It is common knowledge that placer gold mining requires processing of large tonnages of gold-bearing gravels by wash plants of different types. In Russia, gold-bearing gravels are mostly disintegrated and screened by the following types of wash plants: a water canon, a derocker or a scrubber trommel. Gold-bearing gravel processing is regarded as highly energy-intensive due to high energy consumption for transportation of large tonnage of material and high pressure water flow rate. The industries requiring a significant expenditure of energy normally estimate the process efficiency by energy consumption per product unit. In order to obtain quantitative data on energy consumption for gravel processing and to estimate placer mining costs, in 2003~2006 four placer gold mines located in the Irkutsk Region were thoroughly investigated through time and motion studies. At all these placer mines gravels were processed by a water canon, a derocker or a scrubber trommel. The objective of the study was to investigate the following parameters: ? wash plant throughput rate per hour; ? hourly diesel fuel and power consumption per cubic meter of gravel processed; ? volume per cent and shape of oversize material; ? different combinations of gravel processing methods. The results from this study were as follows: ? specific energy consumption per cubic metre of gravel processed for different combinations of gravel processing methods was estimated; ? a correlation between energy consumption and unit cost of gravel processing was determined; ? effect of yield and shape of oversize material on wash plant throughput rate per hour was de-fined; ? energy-efficient gravel processing methods were developed. Based on these results, an improved method of gold-bearing gravel processing was proposed. Implementation of this method at a placer mine saved US$ 123 000 in operating expenses only during a short-time Siberian placer mining season. At the same time, this method improved gravel disintegration, screening and processing operations used at the mine. Another advantage of the pro-posed method was higher gold recovery due to reduced yield of undersize material. In order to improve efficiency of gravel processing, a wash system including a derocker for primary gravel processing and a lightweight scrubber trommel was developed. There are two economic benefits of replacing water cannons with the proposed wash system. The first benefit includes lower operating costs for gravel processing due to lower specific energy consumption, while the second benefit is lower gold losses during slurrifying (disintegration and screening) and sluicing of the undersize material.

Jan 1, 2014

By C. Dorfling, C. A. Snyders

South Africa has extensive mineral processing and extractive metallurgy capacity and infrastructure for metal production from natural resources. Decreasing ore grades, increasing labor costs, and more stringent legislation have made economic metal production from primary resources challenging. Opportunities exist for metal production from secondary resources such as mining wastes and end-of-life consumer goods. The objectives of this study were to evaluate the current status of metal production from secondary resources in South Africa and to identify potential opportunities for further development. Two main classes of secondary resources, namely mining waste and electronic waste, were considered. Primary metal producers are dominating metal production from mining wastes; several of the gold, platinum and chrome producers operate low risk and low cost tailings retreatment facilities that contribute significantly to their overall production. Further opportunities exist in, for example, the treatment of more than 450 estimated gold tailings dumps in Gauteng, as well as metal recovery from slags and furnace dust. The majority of companies involved with electronic waste recycling in South Africa focus on collecting and disassembling; only a few perform preliminary physical processing, with the recovered fractions then being sent overseas for metal recovery. Projections are that the rate of waste generation will increase significantly and that treatment will become critical to comply with more stringent environmental legislation. Projects related to process development, techno-economic evaluations and environmental impact studies for metal recovery from batteries, printed circuit boards, and fluorescent lamps are underway. South Africa is ideally positioned to further explore opportunities for synergistic relations between metal recyclers and primary metal producers. Processing of electronic waste for production of technology metals, for which limited natural resources exist in South Africa, would be a key enabler for local manufacturing industries and expansion of the value chain.

Jan 1, 2018

In the present work, the flotation behaviours of zircon, rutile and ilmenite using sodium oleate as collector in absence and presence of depressants were thoroughly investigated. The maximum in the flotation recovery of any of the above minerals falls within similar pH ranges. A range of inorganic and polymer depressants were examined in order to improve the separation of zircon from rutile and ilmenite. Optimum values of conditioning pH and depressant concentration to achieve maximum recovery and best selective floatability of zircon were obtained. Selective flotation of zircon from Ti-bearing minerals was anticipated from single mineral experiments under different pH values, depressant and collector conditions.

Jan 1, 2014

By Alok Tripathy

A simulation code called SIMJIG and the user interfaces have been developed using discrete element method (DEM) and the .NET platform respectively for the jigging process. DEM platform is used for tracking of particles in the jigging operation. DEM uses the net force balance on the particles to track the trajectory of the particle. Simulation results are compared with experimental results obtained by jigging of low grade iron ore lumps. Two different iron ore samples one from Chatishgarh and one from Odisha were used for the experimental studies. The Alljig? stratification test rig meant for batch laboratory experimental studies has been used in the present work. The behavior of different sizes of material on jigging has been examined. Later, the particle size behavior during jigging at different layers of the jig bed has been studied. Further stratification profile across the jig bed has also been studied. It was observed that simulation results are matching quite nicely with the experimental results. The SIMJIG simulator developed in the present study could be used for predicting the performance of the jigging operation effectively. Keywords: DEM, gravity concentration, jigging, iron ore, simulation

Sep 1, 2012

By F. v. d. Meer, G. Kretschmar, T. Mütze, T. Leißner

"Dynamic air classifiers separate particles in a gas flow due to different particle trajectories utilizing differences in the settling velocity of particles as characteristic property for separation. The present contribution takes a close look at the separation of heterogeneous mixtures, in which valuables and gangue minerals show significant differences in density. The focus was on a moist iron ore sample, which was characterized in terms of mineralogy, grain size distribution, and particle size distribution. The material was classified at a cut size of 45 µm and at feed moistures between 0 and 6 wt.-%. Additionally to standard characterization techniques, the moisture of both products was measured as well as the yield of fines as product fraction in a corresponding processing plant. In addition, an automated mineral liberation analysis (MLA) provided information of the enrichment and segregation of individual mineral phases in the products. The MLA of the classification products reveals a selective comminution of the mineral phases and especially on overmilling of the valuables. For the first time, the separation of individual mineral phases has been assessed and compared to the classic assessment of classification processes by means of particle size analyses. KEYWORDS Dynamic classifier, segregation, MLA, selective comminution INTRODUCTION Dynamic air classifiers separate particles in a gas flow due to the different trajectories of the particles. The result of such a separation process depends on the gas throughput of the classifier, the dimensions, design and rotational speed of the deflector wheel, as well as the state of dispersion and thus the geometry of as well as the turbulence and interparticle interactions in the separation zone. Air classification of moist feed materials can be divided into several sub-process (Leschonski, 1977; Mütze et al., 2016): - dosage of the feed material, - dispersing the solid feed material into a gas stream, - feeding the dispersed material into the classification zone by pneumatic conveying, - drying of moist particles during pneumatic conveying, - separation of coarse and fine particles, and - separation of fine particles from gas."

Jan 1, 2018

By A. Muhammad, A. Abdelaal, M. EL Salmawy

"Energy is vital for economic growth and sustainable development. Greater efforts are being devoted to developing unconventional energy resources such as oil shale as an alternative promising source of oil or solid fuel supplement. The main object of this contribution is to determine the upgrade potential of El-Nakheil oil shale using froth flotation. Samples were prepared by comminution followed by sieving into different size fractions. The flotation behavior of the material and extent of cleaning was studied with respect to nonionic and ionic collectors of anionic and cationic types. It was found that the organic rich portions could not be rendered sufficiently hydrophobic by the used collectors and selectivity towards surfactant was very low."

Jan 1, 2014

By Bharat Garg

The coking coal or clean coal from raw material division, Tata Steel Ltd. is a prime source of energy for inhouse steel making. Coal reserves of semi soft coking coal at West Bokaro is beneficiated by dense media cyclone and froth flotation processes to produce clean coal. In dense media cyclone process two byproducts-middling and rejects are also produced along with clean coal. With the growing demand for clean coal, it becomes imperative to maximize the recovery of clean coal in beneficiation processes. This will help, not only in reduction in cost of production, but also in raw resource conservation, and proper utilization. In this context, a case study was conducted at West Bokaro to identify opportunities for clean coal recovery from by-products. This paper mainly discusses the process for recovery of clean coal from byproducts and study of further liberation of clean coal from byproducts for economic consideration.

Sep 1, 2012

By Herman D. Mendoza

A rapid recovery/recycling process was introduced utilizing the surface-chemical properties of finely dispersed mercury and alumina (Al2O3) fibers in aqueous environment. The conventional method of amalgamation or .ball milling. involves the mixing of a substantial amount of mercury to collect free gold during the grinding stage. In effect, a portion of the mercury is transformed into minute droplets that readily float and disperse in the amalgamation effluent. The fine droplets of mercury in the dispersion readily attached onto the positively charged macroscopic alumina fibers (i.e. = pH 9.8) at conditions pH 3 to 10. When an effluent from settling procedure after an amalgamation-grinding stage is passed through a column-bed packed with alumina fibers, maximum collection of negatively charged finely dispersed mercury occurred at pH 3 to 6. The collection/attachment efficiency was 99.5%. The collected droplets of mercury, which are left in the column-bed of alumina fibers, were subsequently rinsed with alkaline solution at pH 10 to 11.5. At these conditions, both mercury and alumina fibers carry negative surface potentials and resulted in the partial detachment of mercury from the alumina fibers. The detachment efficiency was only 30-35%. The attachment/detachment mechanisms in this study were analyzed using the DLVO theory.

Jan 1, 2003

By L. X. Yu

As is known, the oxidized antimony and antimonate are hard to treat. A new combined mineral processing flowsheet which is controlled in grinding and classification ?bulk floatation?gravity separation is adopted to dispose of gravity-separated tailings (antimony content: 1.48%; oxidization rate: 68.92%) in Muli Antimony Mine, the grade of floatation antimony concentrates is 32.64%; the grade of gravity-separated antimony concentrates is 26.99%; the combined grade of floatation and gravity-separated antimony concentrates is 30.85%, and the total recovery of antimony is 70.64%. Adopting the new mineral processing technique have solved the problem of over grinding of antimony ore by controlling grinding and classification, recovering effectively the sulfide antimony and the easy floatable oxidized antimony of fine size by bulk floatation, recovering effectively the oxidized antimony which is hard to float by classified gravity separation. This is a great breakthrough in the mineral processing technique of the recovery of the oxidized antimony. At present, favorable economic benefit has been obtained from the application of this processing technique in Muli Antimony Mine.

Jan 1, 2014

By Bisweswar Das, Barada Mishra, Hrushikesh Sahoo, Swagat Rath

Banded hematite jasper (BHJ) containing 45.2% Fe, 32.64% SiO2, 0.63 % Al2O3 and 1.25 % LOI is found difficult to beneficiate either by magnetic or flotation techniques due to fine intergrowth of jasper with hematite. Phase transformation by reduction roasting with activated charcoal followed by low intensity magnetic separation to achieve a suitable iron concentrate has been attempted in this study. The mineralogy of the ore and different roasted products has been studied by X-ray powder diffraction (XRD) and scanning electron microscope (SEM) to understand the reduction mechanism. The magnetite formation is observed at 850ºC while metallic iron appeared at a higher temperature. The effects of reduction variables such as reduction time (30-270 min), temperature (750-1050ºC), and reductant (1-12 %) using activated charcoal are studied. An iron concentrate with 64.65% Fe and 55.8% recovery could be obtained under optimum conditions of temperature: 850ºC, time: 1.5 h, and reductant: 6% by weight.

Jan 1, 2014

By Walter W. Focke, Zola Kwela, Willem van der Merwe, Arao Manhique

"The advantages of the de Wet zirconium process for the manufacture of AZST from zircon sand include: Fewer processing steps; removal of radioactivity by leaching rather than by precipitation; alkali reagent recovery in the form of a sodium silicate solution that is essentially free of radioactivity; fewer waste streams and less waste to discard.Here we report on our efforts at maximizing the alkali recovery in the sodium silicate product stream: Milled zircon, d50 ˜ 9 µm, was fused with caustic soda pearls in open reaction vessels at temperatures between 650°C and 850°C. Fusion times of 1, 2, 4, 24 and 336 hours (with intermittent milling) were investigated.For prolonged fusion times the fusion products approached equilibrium compositions. However, the phases Na2ZrSiO5 and Na4Zr2Si3O12 observed at 850°C did not form at 650°C. Since they do not hydrolyse in water they limit the recovery of alkali. For 2-hour fusions a broad spectrum of non-equilibrium reaction-products, that are rich in sodium silicates, is formed. Optimum process conditions, with respect to NaOH recovery, correspond to a 2:1 stoichiometry and fusing for 2-hour at 850°C. At these conditions the alkali recovery is ca. 78% and the zirconia yield is ca. 57%."

Jan 1, 2003

By Haragobinda Srichandan

The present study aimed to investigate the bioleaching efficiency of moderate thermophilic microorganism in a growth medium without Fe supplement on three different size fractions of spent catalyst obtained from petroleum refinery. All the experiments were conducted on shake flasks at a temperature of 65 °C and a pulp density of 10% (w/v) on three size fractions viz. 45-106 µm, 106-212 µm and >212 µm and a working volume of 100 ml comprising of 10 ml of microbial inoculums and 90 ml of Modified Kelly medium. The parameters like pH, redox potential, viable planktonic cell count and the amount of acid addition was measured and quantified on regular basis to follow the progress of the bioleaching. The pH varied much in the lag and logarithmic phase of the experiments but stabilized toward the stationary phase. The total acid additions in each batch experiment were determined the amount of Conc. H2SO4 requirement, which ranged between 683-757 kg/ton of spent catalyst. The redox potential values ranged between 625-650 mV, Ag/AgCl, but were very low ranging between 350-450 mV during initial period. The planktonic viable cell count ranged between 108-109 cells/ml active in the bioleaching system, without any toxic influence of the spent catalyst, but initially due to fall in redox potential and new environment for the microbes, their population was low. The leaching yield of Ni was found to be promising with very high leaching yield of 92-96% followed by Al as 61-62%, which means both Ni and Al leaching were favored by the moderate thermophilic bioleaching compared to the mesophilic bioleaching. There was very little difference in the leaching yield, when compared with different size fractions and hence grinding can be avoided prior to leaching. This process seems to be economical as no Fe source is supplemented together with no requirement of grinding and over all a biological process resulting for an eco-friendly process for future optimization of the metal recovery from petroleum refinery spent catalysts. Keywords: bioleaching, spent catalyst, thermophile, 9K medium

Sep 1, 2012

By Miguel Becerra, Daniel Jordán, Jorge Soto, Luis Torres

"Most SAG grinding operations currently use ball sizes between 5.5 and 6 inch maximum size. However, in most cases the use of this ball sizes hasn’t been justified by a phenomenological analysis of the real effect on the grinding process, but rather by trial and error. The analysis of the influence of ball sizes in SAG grinding hasn’t been developed in detail by considering the effect on process parameters inside the mill, grinding efficiency or internal classification. Historically a conventional grinding reference has been made on the empirical procedure developed by Azzaroni (1980). Further to Azzaroni’s methodology, Sepulveda (Sepúlveda, 2007) developed the SPEC methodology, incorporating the ball size effect on the grinding efficiency parameters using a population balance model included on Molycop tools spreadsheets.This paper demonstrates a detailed analysis at pilot scale of the ball size employed in SAG grinding and scaling that exists between the different levels. This analysis includes assessing the effect of balls sizes on parameters associated with grinding efficiency and its effect on the total fill level, product size distribution and specific energy consumption, among others. In a complementary way it develops a technical - economical evaluation from industrial data comparing two different ball sizes and its effect on the grinding process analysed integrally."

Jan 1, 2014