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By T. Badrujaman

In September 2005, after 30 years experiencing in operating an ESF using a falling water film shell cooling system, Antam entered the new era in operating an ESF, after completely modernized its ESF No. 2 from a falling water film shell cooling system to a copper cooling system. Further, in the beginning of 2007, Ferronickel plant No. 3, where its ESF also uses copper coolers, was successfully commissioned. By operating an ESF using a copper cooling technology, Antam has to face some challenges to establish the operation stability. Besides that, the chances to maximize the furnace efficiency are greatly opened. The shielded-arc mode of electrode tip is selected to operate an ESF under relatively high furnace power to produce metal having tap temperature below 1500? and slag having tap temperature below 1600?. It leads to electric current unbalance. Further, operating an ESF using a copper cooler system under high voltage as consequence of the furnace power raise increases metal and slag tap temperature. This condition damages furnace integrity fast. Besides that, relatively high metal temperature increases its pressure during metal tapping. It leads to failure in closing the metal tap hole. The main different ways in operating an ESF using a falling water film shell cooling system and a copper cooling system lie in the electrode tip mode, the water specification used for cooler, metal tap block maintenance and allowed metal & slag level in furnace. Since a copper cooler system allows an ESF to be operated by consuming nickel ore having ratio Fe / Ni up to eight and producing slag having relatively high Fe content in slag, an undesirable silicon reversion phenomenon becomes an obstacle in reaching the operation stability. A copper cooler technology lets Antam to take a chance to increase its capacity. Modernizing the ESF No.2 had increased its furnace power from 17 MWh to 25 MWh. Meanwhile the ESF No. 3 can be operated up to 42 MWh. This technology allows an ESF to be operated under relatively high furnace power above 25 MWh safely as well as prolong the campaign life of ESF brick. Further, lowering ESF power consumption, extending the limitation of ratio S/M in nickel ore consumed and adjusting Ni grade in ferronickel product can be gained by applying this technology.

Jan 1, 2014

By X. W. Zhang

Mica plate is broadly used in electric industry, production of man-made mica paper plate is in-creasing. The problem coming with is that large quantities of leftover materials unable to be re-cycled are produced during cutting and molding of mica plate productions. The leftover materials are always abandoned as crabs, which not only pollute the environment but also waste our resources. The study intends to find a new measure to decompose and to reuse the mica plate leftover materials so as to create a new production process of mica plate, which is clean and does not produce crabs.

Jan 1, 2014

By C. Knobbs

Contrary to the way it is often portrayed, the average organization or company is far from being a cold, calculating machine. It is actually a highly emotive place where interaction with people is a fundamental part of its ability to perform satisfactorily. The company, through its employers, expects employees, including new graduates, to have the ability to cope adequately with this emotive environment. The graduate is frequently unable to meet this expectation because he/she has not been developed to do so. Technical knowledge is his only asset. This deficiency manifests itself in leadership shortcomings, both intrapersonal and interpersonal. Further analysis reveals a deficiency in three elements of leadership ? self-awareness, oral communication, and an ability to work cooperatively in teams. To address these three elements of leadership, Sasol Coal, a subsidiary of the big petrochemical company in South Africa, sponsored a leadership programme at the University of Pretoria for their final-year bursary students in the faculty of Engineering. This programme, the Sasol Engineering and Leadership Academy (SELA), consisted of a number of interventions designed to address the three areas of self-awareness, oral communication, and cooperative behaviour in teams. These interventions varied from an intrapersonal nature to interpersonal aspects. Psychometric assessments were followed by experiential modules dealing with the three constructs. SELA was evaluated at the end of the year. The results showed a positive shift in the main constructs of self-awareness, communications, and cooperation. This was measured quantitatively and qualitatively. Conclusions were drawn and recommendations for improving the programme were proposed.

Jan 1, 2014

By Jianhong Xu, Hailong Hou, Yu Jing, Yundong Wang

Microcapsules containing extractants have been applied to the extraction of metal ions, organic acid, pesticide, and herbicide. The difficulties of conventional liquid-liquid extraction in phase mixing and phase separation (e.g. high energy consumption, emulsification phenomenon, and large equipment requiring housing) could be overcome in a liquid-solid system by using microcapsules. Even some extractants with high viscosity and poison can be encapsulated conveniently into microcapsules. In the work described in this paper, polysulfone microcapsules containing 2-ethylhexylphosphonic acid mono-2-ethylhexyl ester (P507) were successfully prepared. Then, the extraction rate of lanthanum, samarium, and erbium in dilute solution into the microcapsules containing P507 was studied. An extraction kinetic model is proposed based on the interfacial reaction model accompanied by intraparticle diffusion expressed by Fick’s law. The extraction efficiency was obtained by using the kinetic model with the separately determined complex formation rate constant and the intraparticle diffusion coefficient. From the results, it was confirmed that the kinetic model could predict the experiment in a microcapsule system over a wide concentration range of lanthanide solution. In the future, the model could provide good guidance for the design and application in extraction of lanthanides.

Jan 1, 2014

By Y. L. Tian

Low-grade bauxite with A/S of 4.4 from Henan province was used as raw material and the selec-tive grinding of bauxite, grinding efficiency, particle size and Al2O3 and SiO2distributions of ground products were investigated using ball and vibration mills. The results show that the selective grinding can be used to realize the separation of aluminum from silicon within a certain particle size. The optimal grinding conditions of the ball mill with bauxite are as follows: grinding material to charge ratio, 1.2, charge volume ratio, 40%, pulp con-centration, 70wt%, medium size distribution, F30mm:F20mm:F15mm=20%:50%:30%. Under the conditions, the weight rate of ground product with A/S over 7.5 is 27% and the recovery of Al 2O3is 30%. The optimal grinding condition of the vibration mill with bauxite are as follows: grinding material to charge ratio, 0.9; charge volume ratio, 70%; concentration, 70%; medium size distribution, F40mm:F30mm:F20mm=20%:30%:50%. Under the conditions, the weight ratio of ground product with A/S over 7.5 is 25% and the recovery of Al 2O3is 27%. The research is significant for the rational and economical utilization of the low-grade bauxite.

Jan 1, 2014

By Shuji Owada, Yang Geng, Natsuko Kuroki

Micro-bubble flotation is considered to be an ideal method for the separation of fine or ultra-fine particles, which are difficult to be separated with conventional flotation and other solid separation technologies. Micro-bubble flotation can increase the probability of bubble-particle collision more than conventional milli-bubble flotation. However, there are also some problems. For example, it is known that the rising velocity of micro-bubble is quite low; therefore, the flotation rate reduces. And also, the bubble-particle adhesion probability becomes lower than that of milli-bubble flotation, which is proved in our prior research. In this paper, we applied ultrasonic irradiation to the micro-bubble flotation system in order to solve the above problems and focused on the bubble-bubble and bubble-particle interactions. For clarifying the behavior of bubble-bubble interaction, bubbles behavior was recorded by high-speed camera under irradiation of various ultrasonic frequencies. As a result, in the case of bubble-bubble interaction, it is proved that bubbles are highly coalesced by ultrasonic irradiation especially in the lower frequency and it can enhance more precise separation. In the case of bubble-particle behavior, it is found that the floatability become higher with the ultrasonic irradiation of higher frequency, and it is indicated that ultrasonic irradiation might improve the bubble-particle adhesion probability. Additionally, it is also found that the apparent CMC of the micro-bubble flotation under the ultrasonic field become much lower with higher frequency than with lower frequency, and it is suggested that the dramatic improvement of hydrophobization is achieved.

Jan 1, 2014

By Ö. Genç

In this paper, full-scale mill data collected from three different circuit configurations in cement plants demonstrated the size reduction performance of dry ball mills in relation with the ball size classification achieved by the classifying liners used in the grinding compartments. Findings indicated that, breakage rates at the last 2 ~ 4 meters of the mill are not sufficient to give reasonable size reduction ratios for the production of fines. Application of only damming rings without classifying liners resulted in inverse ball size classification which lead to reduction in size reduction performance thus specific breakage rates.

Jan 1, 2014

By K. S. McClure, S. B. Chitralekha, R. B. Gopaluni, Chmylek. T., S. L. Shah

This is a tutorial paper on industrially successful approaches for nonlinear process monitoring. Online process monitoring is essential to continuous operation of plants at high efficiency. The problem of process monitoring is one where an impending but undesirable process condition has to be identified and used to alert process engineers. This problem has traditionally been solved by practicing engineers using statistical techniques that detect a change in the underlying correlation structure of process variables. For linear correlation structures, algorithms such as principal components analysis, independent component analysis and partial least squares have been proposed. However, many industrial processes exhibit nonlinear correlation structure between the process variables. In this tutorial we describe various nonlinear monitoring techniques and elaborate on two recently developed methods, namely Support Vector Machine and Local Linear Embedding. The two methods are evaluated by application on two experimental case studies, a SAG mill and a polymer extruder.

Jan 1, 2014

By J. A. Marts, R. C. Gilmore, S. Saki, J. F. Brune

Computational fluid dynamics (CFD) modeling involves the creation of a computation domain called a mesh or grid to solve the equations defining the physics of fluid flow. This process often comprises the majority of time spent in modeling efforts. In a project sponsored by the U.S. National Institute for Occupational Safety and Health (NIOSH), researchers at the Colorado School of Mines used an innovative meshing approach, allowing easy adaptation of the CFD model to adjust to a variety of longwall bleeder-ventilated and progressively sealed (often referred to as bleederless in the United States) mining geometries, with gob porosity and permeability scalable over a wide range. This paper presents the methodology of the meshing and scaling approach along with recommendations for using CFD modeling in longwall gob ventilation applications. The new meshing technique was utilized to evaluate the function of a back return in a progressively sealed gob and a bleeder-ventilated gob.

Jan 1, 2014

By Anjan Kumari, B. K. Soni, Manis Kumar Jha, A. Vidyadhar, Vinod Kumar

"In the present paper, recovery of valuable metals from the poly-cracked ash obtained by pyrolysis of discarded PCBs has been studied following physical beneficiation and a hydrometallurgical process alternate to smelting. The ash is subjected to comminution for the separation of metallic components from non-metallic fractions by scrubbing, tabling and froth flotation which enriched the metal in the concentrate -97% which was further screened to separate high and low metal concentrate. The finer fraction containing -12% metallic value was leached in acidic solution. Almost all (Cu, Pb, Fe, etc) were leached in 4M HN03 at 90°C in 75 min at a pulp density 100 g/L. The characterization of both ash and residues were made by XRD, EPMA, EDS, etc. to validate the experimental results. The metals from the leach liquor could be recovered/separated using solvent extraction techniques which can further be processed to get pure metal salts/ sheets.IntroductionPrinted circuit boards (PCBs) are an essential component of electrical and electronic equipments (EEEs) as it plays an important role during operation of these devices. The world market of PCBs has reached nearly $60 billion in 2012, with 1.7 percent real growth over 2011 [1]. The diverse technology-driven global market is expected to grow at an average annual rate of 5% by 2014 [2]. The waste EEEs are generated due to replacement of obsolete equipments with modem ones and thus their demand is also increasing rapidly [3]. The discarded e-wastes are being piled up as landfills which affect the environment and cause health threats to living organisms, if not disposed of properly. These e-wastes contain metals some of which are precious, few are hazardous and others as valuable."

Jan 1, 2014

By Alex Heath, Andrew Barycki, Baladron. Javier

"Efficient flocculation is important to thickener performance, affecting the overflow clarity, solids settling flux, underflow density and operability. Many factors affect flocculation; from the material/flocculant type, dilution of the feed and flocculant solution, mixing, to the shear rate and shear history. The flocculant addition point (or points) can be used as a tuning method to alter the effective flocculation time in a feedwell, with addition further up the feed pipe increasing the residence time but making the aggregates more prone to breakup if they experience high shear later in the process. Conversely, adding the flocculant later, eg under the feedwell shelf decreases the mixing time but allows some free (unadsorbed) flocculant to be available at the feedwell exit. An extensive trial has been performed on an operating thickener comparing seven individual different flocculant dosing positions through a Vane feedwell, and some combinations of two dosing points simultaneously. Measurements of the velocity, solids concentration and aggregate size were made throughout the feedwell at the different positions, with the dosing points significantly changing the aggregate size and clarity, and also affecting the solids concentration at some positions. The results are accessed in terms of flocculation kinetics and used as CFD validation data."

Jan 1, 2014

In this paper High Pressure Grinding Rolls(HPGR) was utilized to pretreat CVRD southern specular hematite for enhancing the pelletization of the refractory hematite. The process parameters of HPGR, balling and firing were optimized, and the mechanism of HPGR was demonstrated by determining the surface activity by means of Blaine specific surface area tester, laser size analysis, scanning electron microscopy (SEM),X-ray diffraction (XRD), micro calorimeter and pelletability index. It is shown that the pelletization of the refractory hematite was greatly improved. The drop strength of green balls increases from 3.4 times to 13.6 times from 0.5m height while the bentonite dosage decreases from 2.2% to 1.3%.The compressive strength of roasted pellets also reaches 2500N/pellet. The mechanism of the pretreatment of CVRD southern specular hematite concentrates by HPGR is revealed that the surface activity is improved by an increases in specific surface area and the amount of micron size fractions, and higher lattice deformation and defects due to the fractures occurring inside particles during static pressure comminution, resulting in more wetting enthalpy, higher pelletability index and good property of roasting.

Jan 1, 2014

By S. J. Baumgartner

The ferromanganese industry is under pressure to deal with the slag arising from the production of ferromanganese, which is discarded in landfills or slag heaps. This material poses an environmental and health risk to surrounding ecosystems and communities, and disposal costs are increasing. Ferromanganese slag contains an appreciable amount of residual manganese metal, which can be exploited. Previous work has shown that the slag can be leached fully, while rejecting the silica to a residue. The methods that were investigated to recover manganese from the leach solution included hydroxide precipitation to upgrade the leach solution followed by manganese carbonate precipitation to produce a pure manganese carbonate product or a manganese carbonate furnace feed material, which would be recycled to increase manganese recoveries in the production of ferromanganese. In addition, electrowinning of electrolytic manganese dioxide from the leach solution was studied. The methods were compared in terms of selectivity, costs, and product quality. Co-recovery of the leach residue, which is a potential cement additive, is discussed. Among the methods investigated to upgrade the pregnant leach solution, hydroxide precipitation utilizing ammonia to adjust the pH appears to be the most effective in removing major impurities such as iron, aluminium, and silica to less than 1 ppm. The manganese carbonate and impure manganese carbonate furnace feed products met quality specifications. However, although the production of these materials was technically viable, the large amounts of base reagent that were required to raise the pH, and the associated high operating costs, rendered the process uneconomic. An optimization study was therefore carried out with the primary objective to determine the ideal acid amount to be utilized in the waterstarved digestion stage, thereby decreasing acid and base consumption while optimizing the quality of the pregnant leach solution, and producing a leach residue that contained <1% Mn. The outcome was an economically viable process. Additional benefits included an increase in the manganese content of the impure manganese carbonate furnace feed material, and a substantial reduction in the dilution of the pregnant leach solution, thereby maintaining high manganese concentrations that rendered the solution viable for electrowinning of electrolytic manganese dioxide, the production of which yielded a current efficiency of 74%.

Jan 1, 2014

By Stefano Trevisani

Abstract The FIEC Sustainability Vision states that “risks should be identified and allocated in a fair manner across the project team from the early stages of the design phase. A partnering approach, where objectives and timescales are agreed in advance together with all relevant partners in the value chain, offers a useful solution to improve on site efficiency and reduce disputes”. An alliance or collaborative form of contract involving all parties is the best way to ensure fair contract conditions and proper risk allocation in construction projects. Collaborative contracts are particularly useful where there is uncertainty or undefined information or in the event of technical difficulties and other risks difficult to allocate among the parties involved in the project. Owners sometimes require even special output in terms of innovative technical solutions or special performance. In addition, this particular form of cooperation has been construed and developed with the intention of avoiding and mitigating another great risk associated with the construction industry (especially in complex projects): disputes and conflicts, which are often a major cause of delays, increased costs, loss of reputation and opportunities. In contrast, Alliances are a way to increase and strengthen business relationships, technical and economic innovation and effectiveness, in a worldwide global context where the waste of resources must be avoided in order to guarantee future recovery and growth. Of course, the total cost of a project is usually a key factor and the main driver for the Owner and the Contractors in deciding the type of relationship between them as well as the subsequent relationship with subcontractors and lower-tiers. This paper and presentation, will explain the main features and the principle benefits that the use of collaborative contracts can bring to all parties involved in the construction project, including the sustainable financial return that might be achieved if costly and time consuming disputes can be avoided.

Jan 1, 2014

By R. Bugueño, W. Calderón, G. Montes-Atenas

From the point of view of industrial performance of metal extraction, the efficiency of a column leaching operation depends strongly on the leaching agent and the ore properties such as mineral composition, mineral liberation and particle size distribution. One aspect that has become particularly important is how the leaching solution flows through the porous structure which contains the valuable minerals. It is known that the output flow rate of leaching solution depends mainly on factors of the input flow, environmental condition and porous bed properties. The latter factor is often evaluated and reported under saturated conditions but in practical leaching systems unsaturated conditions are dominant. This investigation has the purpose of determining the residence time of the leaching solution in columns with different diameters under unsaturated conditions by using experimental data and numerical simulations. Laboratory leach test were performed using isothermal jacketed columns with top cap to reduce the evaporation. The simulations were performed using the software SVFlux® which incorporates material properties such as Soil Water Characteristic Curve (SWCC) and Unsaturated Hydraulic Conductivity. Preliminary results indicate a non-linear asymptotic behavior of the saturation rate with respect to the operation time. Results from numerical simulations show the same non-linear behavior and a considerable delay between input and output flows. Further analysis concerning with the effect of transpiration and evaporation mechanisms is discussed.

Jan 1, 2014

By K. Osburn

South Deep Gold Mine, owned by Gold Fields Ltd., is situated near Westonaria in the Gauteng Province of South Africa and mines the conglomerate bands of the Upper Elsburg reefs (Mondeor Conglomerate Formation) of the Witwatersrand Supergroup and the Ventersdorp Contact Reef (VCR) of the Ventersdorp Supergroup. The stoping and underground developments are mechanized. The Upper Elsburg reefs are mined by a variety of mining methods, including mechanized drift and fill, modified drift and bench, longhole stoping, and low-profile mining. Optimal mine design and scheduling for deep-level mechanized mining are complex, and success is highly dependent on detailed, robust, and accurate geological and geostatistical models. Geological structures significantly influence the sedimentological characteristics, distribution, and preservation of the Upper Elsburg reefs and VCR. Accordingly, particular emphasis is placed on the generation of a mine-scale structural model that accommodates the relationships between the older north-trending fault systems (West Rand and Panvlakte faults) and younger east-trending dextral wrench faults. Results from underground mapping, borehole intersections, and highresolution three-dimensional seismic data have been integrated to produce coherent three-dimensional geological models. The Upper Elsburg reefs suboutcrop against the VCR and comprise an easterly diverging clastic wedge, thickening from the suboutcrop position, to approximately 130 m at the mine?s eastern boundary. The Upper Elsburg reefs are characterized by conglomerate and quartzite bands forming multiple, stacked, upward-fining unconformity-bounded couplets. Palaeocurrent directions are dominantly from west-northwest to east-southeast, indicating that the more proximal deposits are preserved close to the suboutcrop, with distal facies to the east. Sedimentological modelling is applied to individual stratigraphic units and caters for facies definition. This is achieved through channel width (CW) kriging and fitting of type sections to borehole and mapping data. Homogenous geological geozones for each stratigraphic unit are thus defined within individual structural blocks on the basis of those sedimentological parameters that have been found to have a positive spatial correlation to gold concentration. These geozones then serve as constraints to the evaluation of the orebody. This contribution presents a summary of the modelling processes that are currently applied in the development of high-confidence, timeously produced geological models that are essential input for mineral resource estimation and mechanized mine planning and scheduling.

Jan 1, 2014

By Kilian Neubert, Hermann Wotruba, Henning Knapp

Sensor-based sorting has been integrated into more and more applications in mineral processing over the past decades. Various sensor types, such as line scan cameras, near infrared sensors and X-ray transmission sensors, allow the separation of a vast variety of raw materials. Sensor-based sorting has several economic benefits which can make the difference between an uneconomic operation and a profitable mine. Sensor-based sorters can be applied to fulfill various sorting tasks, such as waste rejection, product quality improvement and ore type diversion, and have a significant impact on the layout of the processing plant. Therefore, it is important to include sensor-based sorting into the planning of a processing plant at an early stage. To evaluate the applicability of sensor-based sorting for any specific ore type, it is currently necessary to provide several hundred kilograms of material for subsequent bulk tests. In exploration, ore samples are usually rare and only available in form of drill cores. The acquisition of drill cores is time-consuming and expensive especially for deposits in great depth. Hence, it is unfavorable to spoil valuable drill cores for bulk tests. This paper describes a methodology to evaluate the applicability of sensor-based sorting based on drill core analysis. That methodology offers the possibility to calculate the achievable performances of different sensor types for various grain sizes without comminution of drill cores. The general methodology is shown on basis of an exemplary test work on drill cores from a currently conducted exploration.

Jan 1, 2014

By Brian Lindner, Lidia Auret, Niel Knoblauch

In this paper, a fault detection and identification framework based on feature extraction and topology extraction methods is proposed, and evaluated on a simulated base metals refinery high pressure leaching process. Feature extraction methods included linear and kernel principal component analysis, while process topology information was extracted with linear cross-correlation, partial cross-correlation and transfer entropy. Connectivity maps were constructed to identify possible fault propagation paths to aid root cause analysis. The results indicate that process topology can enhance the fault identification capability of data-based process monitoring methods. The study of the considered base metals refinery pressure leaching process is ongoing, with future work including the creation of a fault library which would lead to further critical evaluation of the proposed fault detection and identification framework.

Jan 1, 2014

By Stoyan Gaydardzhiev, Michel Shengo, Pierre Kalenga

Lab-scale flotation of copper and cobalt oxidized ore from the Luiswishi deposit in the Katanga province (DRC) has been done focusing on the influence of the degree of process water recycling on metals recovery. Results have shown that at 20 % recycling rate, the recovery of copper and cobalt in the cleaner stage have been respectively reduced to 23 % and 45 % in comparison to 53 % Cu and 63 % Co if process water has not been recycled. At 10 % recycling rate however, the system could still tolerate the effect from recycling, since Cu and Co recovery has remained respectively at acceptable levels of 52 % and 60 %. In order to explain the reasons for the observed worsening of flotation results if process water was recycled at rate higher than 20 %, electrochemical investigation of the pulp has been performed. It has been established that the chemical compounds formed in the pulp when process water was recycled, do influence the sulphidization of malachite and heterogenite and impact further collector adsorption. To confirm these assumptions, the effect from thiosulphate ions presence during the sulphidization of high purity malachite has been studied. It has been found, that thiosulphate ions depending on their concentration in water induce variations in pulp properties such as DO content, pH, Es and contribute to formation of undesirable chemical compounds on mineral surface as identified by DRIFT spectroscopy.

Jan 1, 2014

By J. Jacob, A. G. Guézennec, F. Savreux, S. Nanaa, M. Delclaud, P. d’Hugues

Mining wastes can contain base and precious metals, but also metalloids and rare earth elements that are nowadays considered as highly critical for the industrial development of the European Union. The development of alternative routes to conventional processing is still required in order to decrease the cost associated with the treatment of these resources, which are more complex in composition and with lower grades. An ecologically acceptable and yet economic alternative for processing of low-grade sulphidic primary ores as well as mining wastes is the extraction of metals using bioleaching processes. The purpose of this study was to test the potential of bioleaching procedures for the extraction of residual metals contained in sulphide-rich tailing wastes coming from a European copper mine. These wastes are mainly composed of pyrite (60%) and contain cobalt (0.06 %) and gold (0.95 g/t). Bioleaching experiments were performed in 2 L stirred reactors in batch mode and in pilot tanks (110L) in continuous mode, using the "BRGM-KCC" bacterial consortia. High metal extractions were obtained (cobalt dissolution > 90%), which confirm that bioleaching is an effective process for this tailings material. Experimental results were used to design a global treatment process scheme and to perform a preliminary economic evaluation, showing good profitability of a hypothetical industrial project.

Jan 1, 2014