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By Leszek Maldzinski

The present concept assumes carrying out the process of controlled nitriding with NH3 alone. This is a simpler process than that using two-component mixes of ammonia diluted with N2 or NH3diss. The regulation of the chemical composition of the atmosphere in the retort, and therefore the regulation of the nitriding potential KN, is obtained through the variation of the inflow rate of NH3 into the retort. What is a completely new things in a relevant process, the inflow of NH3 into the furnace is at times reduced to zero, which widens the range of the gas composition in the retort (and by the same token, of KN). The amount of NH3 introduced into the furnace is regulated (controlled) with the aid of a gas analyzer (for example an infrared analyzer). The gas analyzer opens and closes periodically the NH3 inlet valve with a frequency maintaining a desired gas composition (a desired KN) in the retort. The concept was based on experimental and theoretical investigations in term of thermodynamic and kinetic of gas nitriding. Investigations were carried out in a laboratory furnace with a quartz tube and also in an industrial furnace with a steel retort and a circulating fan. Nitriding was performed using NH3, NH3+H2, NH3+NH3diss. mixtures. In an industrial furnace the supply of NH3 into the retort was periodically closed, though with an operating circulation fan. The studies demonstrated that the growth rate of nitrided layer depends only on the composition of the atmosphere, (or KN), in the retort. It depends neither on a type of atmosphere introduced into furnace (NH3, NH3+NH3diss. or NH3+H2) nor a type of furnace (laboratory with a quartz tube or industrial with steel retort and fan). The results proved also that entirely closing of NH3 supply to the retort does not affect the growth rate of nitrided layer. A detailed analyses of the results was performed in a paper.

Aug 16, 2017

By André Alexandrino Lotto

A demanda global por energia renovável vem aumentando ao longo dos últimos anos. A energia solar é uma energia limpa e abundante, mas seu uso ainda é limitado por causa dos preços altos e baixa eficiência das células fotovoltaicas. O silício bruto, também chamado de silício de grau metalúrgico, tem sido alvo de muitos estudos visando sua purificação a um nível suficiente para aplicações de energia solar por processos mais baratos do que o processo convencional, chamado Processo Siemens. Neste trabalho, 3 kg de silício de grau metalúrgico foram fundidos por plasma térmico numa atmosfera de vapor de água, hidrogênio e argônio. O teor de boro foi reduzido de 10 ppm para 0,09 ppm em 18.000s (5 horas), mostrando que o processo poderia ser uma alternativa viável ao processo tradicional por via química

Aug 8, 2018

By Samara Sâmid Aguiar Correia

A crescente necessidade por resultados de análises laboratoriais dentro das indústrias são cada vez mais exigentes em termos de tempo de resposta e precisão. Aliado a isso, a elevação do volume de minério de ferro exportado e o aumento da variabilidade desses produtos requerem processos cada vez mais rigorosos e tomados de decisões mais rápidas. Nesse contexto, os analisadores on-line têm um papel fundamental, pois atendem tais exigências, além de preservarem a segurança operacional. Este trabalho tem por objetivo mostrar o desenvolvimento da implantação de analisadores de umidade on line na descarga dos vagões da Vale no Terminal Ponta da Madeira. A metodologia utilizada na medição de umidade dos analisadores usa o princípio de transmissão de micro-ondas, que é a melhor tecnologia disponível no mercado para este fim. Dentre as etapas de implantação, que abrange desde a aquisição dos equipamentos até a avaliação dos controles e ajustes operacionais, é mostrado o período de cada etapa, os problemas encontrados e as soluções adotadas. Em suma, atualmente há medição de umidade on line na descarga deste site e está em fase de implantação a análise durante o carregamento do embarque para controle de processo.

Aug 1, 2018

By Flanelson Maciel Monteiro, Yago Lutz Castro Pinto, Marcondes Mendes de Souza, Mauro Froes Meyer

This article is based on a bibliographical review of a field work that was done in the Salina São Camilo in the region of Mossoró - RN. The general objective of this research is to present the main exploratory and beneficiation aspects of salt production. Among the aspects of salt is the properties of salt, history and mining, besides the aspects of environment and work safety. However, this research resulted in preliminary data, but it would be interesting to be more thorough so that the extraction of salt in the academic world is disclosed

Oct 3, 2019

By Eric Yoshimitsu Sako

One of the main difficulties in the operation of trough and runners at Arcelor Mittal Tubarão (AMT) Blast-furnace no.02 is the reduced amount of time available for repair procedures. The consequence is that the castable installation must often be performed during hot conditions and the installed castable could easily detach from the base material during the early stage of operation, exposing the previously oxidized base material to molten iron and corrosive slag attack. When events like this happen, emergency repairs must be executed, resulting in increased refractory unit consumption and an unplanned shutdown of unit operation. Considering these targets, Nippon Crucible Co. and Saint-Gobain HPR Brazil have developed a high-performance Al2O3-SiC-C composition based on an entirely novel anti-oxidation technology. Oxidizing reactions could be attenuated by adding an oxidant inhibitor and a water reducing agent. As a result, the open porosity was significantly reduced, resulting in an improvement of campaign life in terms of pig iron throughput when compared with the regular castable. An analysis of this life improvement showed successful results for the material after 250 days of campaign. The main reason for such successful results was that the deterioration caused by the oxidation was significantly less and that this change made on the high cohesive structure of the base material was maintained for a long time. The attained results allowed Arcelor Mittal Tubarão to achieve longer trough campaigns, and avoid any unplanned stoppages with zero breakdown risks.

Oct 30, 2017

By Flávio Beneduce Neto

As trincas a quente ou de solidificação em peças micro-fundidas em superligas a base de níquel podem ser um item importante no índice de perdas em componentes específicos. O aparecimento desse defeito está ligado fundamentalmente à quantidade de líquido interdentrítico nos últimos estágios da solidificação e, principalmente, ligado à composição química desse líquido. Há duas ligas amplamente utilizadas na produção de rotores para turbo-compressores ou turbinas para a geração de energia: o Inconel 713C e o Inconel 713LC. A diferença entre estas duas ligas é essencialmente o teor de carbono. Curiosamente, a liga LC tem uma maior tendência ao aparecimento de trincas de solidificação. O presente trabalho procura identificar as diferenças de comportamento na solidificação dessas duas ligas através da termodinâmica computacional e ligar essas diferenças no aparecimento das trincas. Os resultados indicaram que os teores de Zr e Nb do líquido remanescente da solidificação são muito superiores na liga LC causados pelo atraso na precipitação dos carbonetos tipo MC nessa região que deve ser a fase que aumenta a resistência mecânica da área. O correto balanceamento da composição química da liga em relação aos elementos citados permitiu que o índice de perdas por trincas de solidificação caísse para níveis próximos a zero.

Aug 8, 2018

By Fábio Heiji Yamada, Marcelo Koiti Fugihara, Ruano Fonseca Araujo

Conception the simulation and optimization technologies for industrial processes applied in the mining environment: tools and methodologies. Clarifications provided about the differences of these techniques when compared with static analysis (intuition, use of static spreadsheets, etc.). Presentation of practical cases at several big mining companies in Brazil. These projects will be presented and illustrated through dynamic simulation models developed at those companies, each one with its set of objectives, scope and results (for example: sizing the number of equipment, silo, piles related to the mining processing, logistics, ROM transportation, mine operations plan, etc.).

Oct 3, 2019

By Samuel Vasconcellos

É comum um sistema de resfriamento de água por meio de torres de resfriamento perder performance ao longo de sua vida útil e começar a se tornar um limitante de capacidade para o processo. Nestes casos, o mesmo pode sofrer manutenção e até retomar sua capacidade original. Entretanto, ocasionalmente esta manutenção se torna inviável, pelo impacto gerado na disponibilidade das operações ligadas a este sistema. Este foi o caso deste projeto, onde a solução adotada foi a adição de uma célula às duas existentes na torre de refrigeração, atingindo uma performance melhor que a nominal no sistema como um todo.

Jul 31, 2018

By Denise Freire Duarte

Desclassificações de corridas por elementos fora da faixa de especificação do tipo do aço que está sendo produzido impactam negativamente nos indicadores da empresa. É esforço contínuo os projetos de melhoria e ações implantadas para a redução dessas desclassificações. Quando uma corrida é desclassificada, há um custo para refazer a corrida perdida, ocorre um processo de reclassificação que fica em estoque aguardando aplicação, perde-se tempo e pontualidade na produção entre outros impactos. Portanto identificar a causa raiz do problema e atuar em ações efetivas e bem implantadas são as chaves para a resolução do problema e melhoramento do processo. O fósforo é um elemento que deve ser controlado pois é item de norma para atendimento às especificações pois impactam na fragilização do material. Este trabalho mostra a análise realizada na busca da causa raiz das ocorrências das desclassificações de fósforo.

Oct 30, 2017

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019

By Juliano Braz Possatti, Arnaldo Carneiro Salles, Cleudson dos Santos Rego, Leandro de Lucas Mendes

The increase in customer demand for steels with higher surface requirements, associated with the need to increase ArcelorMittal Tubarão's HSM productivity, it was necessary the development of controls and actions to reduce scale losses within the scenario of high productivity. This article describes the path followed by the hot strip mill team in order to reduce the occurrence and severity of scales.

Oct 10, 2019

By Diego Berti Salvaro

The morphology, dimensions and chemical composition of tribolayers strongly depend on the pressures and temperatures acting on the contact. They are formed by reactions between the surfaces in contact with each other as well as with the atmosphere, lubricants and possible contaminants. In this paper the influence of test time (180, 500, 1000 and 2500 h) into the formation and characteristics of tribolayers in pairs DLC-stainless steel tested under refrigerant gas R134a atmosphere without presence of lubricating oil was analyzed. The characterization was performed using scanning electron microscopy, energy dispersive spectroscopy (SEM-EDS) (morphology and chemical composition) and white light interferometry (dimensions). The tribolayers thicknesses ranged from 100 to 500 nm and they were composed by elements originated from mutual transfers between the tribological pairs as well as oxides, being more pronounced on the stainless steel surface. The results show that the tribolayers are chemically stable (maintained the same composition over time) and the thickness remained stable after a thousand hours of testing.

Jul 31, 2018

By Peter Grawenhof

Universal joint shafts and slipper spindles are commonly used in rolling mills to compensate the design- and process-related offset between the motors and work rolls. Although both types of shafts exhibit on the same kinematic principle, there are basic differences regarding the design concepts. These differences become noticeable on many levels and may become very distinct in terms of Life-Cycle-Costs (LCC). In this respect, a critical comparison between universal joint shafts and slipper spindles can be made.

Aug 16, 2017

By Michel Rodrigo Luiz, Glaudistoni da Silva Félix, Osmar Duarte Junior

This article deals with a project to reduce the preparation time and threading the coils in the input section of a pickling line coupled to the cold strip mill (PLTCM) at ArcelorMittal Vega. The project developed serves for the detection and elimination of bottlenecks in the input section. The project was conceived by the philosophy of the Theory of Constraints (TOC) and Lean Six Sigma (6 sigma), here seen as sequencing serial / parallel in the preparation and threading the coils. In this context, a proposal to modify the automatic sequencing and reduction of interruptions due to failure of the automation / equipment confirmed its effectiveness reducing the total time preparation time and threading the coils in the entry section by 15%. This project was developed without investment costs, bringing gains on the order of US$613,769.00.

Oct 1, 2019

By Andrelio Marcos Ribeiro, Lucio Ribeiro Camisao, Antonio Carlos Ataíde, Alan de Sousa Pereira, Renato Siqueira Campos

The annealing and pickling line n. 1, responsible for the production of stainless steel 3xx, 4xx and 430a in thicknesses from 4 to 0.4 mm, has two vertical strip accumulators. These are intended not to let the material exceed the determined time in the furnace and in the pickling, and consequently do not cause defects like burning and excessive pickling. Strip accumulator n. 1 avoids the line from stopping during welding execution of the coils in the welding machine. In sequence, the strip accumulator n. 2 avoids the line from stopping at the end cutting of the tips, and in the coils removal from the pickling. The strip accumulators have a roller table that during the strip accumulation moves vertically downwards while its counterweight moves vertically upwards, and do the inverse movement when the material is released. On December 12th 2018, the failure occurred in the strip accumulator n. 1, where it was verified that the shaft of one of the pulleys had been fractured by high-cycle mechanical fatigue, which was characterized by alternating bending. With the fracture of the shaft, occurred the unevenness of the counterweight that damaged the guides. Failure analysis of this occurrence was based on the PDCA methodology, when was verified a weld between the shaft and the pulley. The analysis of the microstructure transformation in the molten zone, in the heat affected zone and in the base metal was carried out in an optical microscope, and no abnormality was observed. It was also carried out the end test by penetrating liquid, finding an inadequate weld in its geometry, as well as longitudinal trunks along the center of the weld bead. However, after a huge investigation of the causes, it was found that the failure was triggered by an inadequate design of the pulley shaft. It was also verified that the shaft had an open measure, inadequate for the operational context. After the analysis, action plans were drawn up based on the FMEA methodology to inhibit the failure recurrence.

Oct 7, 2019

By Breno Totti Maia

In these hard days for Brazil steel market, all steel shops want to achieve the same goal, work with: productivity, low costs and high performance. In this scenario the Slagless® technology (which is applied into BOF converter) was important to reach these targets. After use has been reduced the number of times of tip exchange in more than 04 times. Was reduced too, the time to remove lance skulls. Lance keeps clean during all his life with record number of the life 1255 .Blow keep stable due strong measure control at the nozzles and more improvements are planning.

Oct 30, 2017

By Rainer Fackert

3D-Measurements for slabs and heavy plate are now available and close the gap in the production chain. The measuring systems described in this presentation must be seen as high-tech solutions in the field of casting and rolling technology. The measuring systems were developed taking into consideration the harsh casting and rolling mill environment in which they are to be used, with the aim of achieving high operational reliability and eliminating disturbances. Interconnected quality management systems enable optimization across the complete production process. New limits are being defined constantly for all these developments. What is technically feasible today becomes normal practice tomorrow, and will probably be replaced by completely new technologies the day after.

Aug 16, 2017

By Marcelo Rebellato, Beatriz Pereda, Beatriz Lopez, Pello Uranga

The classical application of Nb microalloying in the development of thermomechanical processes for flat products has been related to its suitability to enhance strain-induced precipitation and get a pancaked austenite prior to transformation. As new steel grades or new lay-outs are being developed, more complex metallurgical conditions need to be evaluated. In this context, Nb microalloying, alone or combined with other microadditions, needs to intervene in a more controlled way in additional steps of the thermomechanical process, besides its conventional strain-induced precipitation role. For example, the hardenability enhancement associated with Nb to properly achieve lower temperature transformation products, demands a proper balance of the Nb amount precipitated during rolling and the one remaining in solid solution. Similar effects are also sought when the final available Nb is used to increase strength through precipitation hardening. This manuscript evaluates how changes in the rolling strategies affect the interaction between Nb(C,N) precipitation and austenite recrystallization at different steps of the rolling process. As the possible interactions between parameters intervening simultaneously are quite complex, the application of microstructural models helps to properly define the best austenite conditioning combined with the convenient amount of Nb in solution, as a function of the final property requirements. Along the manuscript, several strategies will be discussed for the case of hot rolling of flat products comparing both normal and coarse initial austenite grain sizes.

Oct 1, 2019

By Beatriz Dogliani, Elisabeth Williams, Maria Berenice Sandobal, Carina Bertino

The environmental management of steel mill slag should be understood as a management philosophy, observing technical, economic and environmental criteria associated with their generation, storage and final destination. The slag can be considered as a synthetic mineral resource and become a very useful co-product in different areas. The Argentinean steel industry prioritizes the efficient environmental management of its waste, thus contributing to its own survival taking into account the sustainable development. In the world, the slag produced by the steel industry has been used as steel aggregate for road bases, railway ballast and filling material among others. Any factor that influences the economy of the country affects all branches of society, mainly public agencies, whose financial resources are increasingly scarce to deal with all public works. It is necessary to join efforts of private and public initiative in the adoption of alternative materials that replace the use of finite natural resources. This presentation aims to show the work done by private companies together with public bodies and universities to obtain a regulatory document for the management of slag as steel aggregates for three different uses, namely: road use, railway use and general use.

Nov 5, 2019

By José Fagundes Junior, Cleudson dos Santos Rego, Bruno Bastos da Silva Murad, Vitor Borlot Borba

Since the startup in 2002, the Hot Strip Mill at ArcelorMittal Tubarão has increased gradually the coil output as the customers demand new and more resistant dimensionally challenging (thinner and/or wider) steel grades. As a critical feature for customer applications, improvements have been carried out aiming a higher thickness performance and reduction of internal losses while still meeting the more restrict tolerances booked by the customers. This paper presents the recent thickness performance evolution since 2017 and the main actions deployed to improve it.

Oct 1, 2019