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By C. B. Thwing

IT is likely that among most races, owing to the ease of finding and working clay, the making of clay utensils was learned earlier than the molding of metal implements. The ancients made good pottery and durable brick in kilns that wasted fully one-half the heat and spoiled fully one-fourth of the ware; and, taking the clayworking industry as a whole, we are doing the same today. The chemical and physical changes involved in the burning of clay are so many and vary so much with the composition of the clay that it is not surprising that the rule-of-thumb methods so commonly employed fail to give uniform results. In its passage from plastic clay to the vitreous or stonelike character the mingled minerals and accidental organic impurities of which the clay is blended must pass through four stages, the second and third usually overlapping, and the fourth often beginning before the third is complete. These stages in their order with the rising temperature are drying, dehydration, oxidation, vitrification. In the first part of the drying stage, usually accomplished in part outside the kiln, the water mixed with clay is dried out at temperatures not much exceeding the boiling point of water. In the later part of this stage, within the kiln, the hygroscopic water, absorbed from the air is expelled at somewhat higher temperatures, this stage being known as watersmoking. Some clays are very sensitive to temperature during the drying stage and if the temperature exceeds 100°, the ware becomes checked. Other clays may be dried more rapidly without danger. In down-draft kilns, the draft is slight during the watersmoking stage and the water driven off from the top rows condenses on the ware in the bottom of the kiln, with the result that high temperatures are likely to be reached at the top of the kiln before the bottom is fully dry. The lag in temperature of the bottom persists to the second stage in spite of the better draft then prevailing.

Jan 9, 1919

By Kirtland Marsh

THE manufacture of gas masks by the Chemical Warfare Service, U. S. A., required preparation of the carbon used in the canisters. The largest plant for the production of this carbon was situated at the works of the Astoria Light, Heat and Power Co., at Astoria, N. Y.; this paper will deal1 with the pyrometry equipment at that plant. Commercial charcoal was found unsuitable for use in gas masks because of its low power of absorption and its poor resistance to abrasion. The best raw material for the production of carbon was found to be coconut shells, but any kind of nut shells or fruit pits were used when sufficient quantities of coconut shells could not be obtained. The shells were first carbonized in retorts, the carbon was then crushed and screened between 8 and 16 mesh, and finally submitted to a special heat-treatment in air; steam treatment was later substituted for treatment in air. The production of gas-mask carbon on a commercial scale was begun at Astoria about Aug. 1, 1917. Temperature control was essential during the initial carbonization of the shells, as well as during the air or steam treatment, and pyrometers were installed for this purpose. The installation and maintenance of all pyrometry equipment was done by the pyrometry department, consisting of an officer in charge, an assistant, and two men. A special pyrometry laboratory was maintained in which all repairs were made.

Jan 9, 1919

R. W. NEWCOMB, New York, N. Y. (written discussion *).-This paper is particularly interesting to me, because it gives data on a much mooted question, viz., the serviceability of Le Chatelier (platinum-platinum-rhodium) thermocouples under severe industrial conditions. It has always been supposed that platinum-platinum-rhodium thermo-couples, used at high temperatures under strong reducing conditions, would not give long service and were subject to rapid volatilization. The fact, however, that the carefully kept records indicate that a little more than 3 gm. out of more than 830 gm. was lost over this considerable period, shows what kind of service can -be obtained from platinum-platinum-rhodium thermocouples,, when properly installed, and well cared for. While the writer has no actual figures on the loss of weight, etc. of platinum-platinum-rhodium thermocouples under service, he was told, by the man in charge of pyrometers at a large industrial plant in which over 400 platinum-platinum-rhodium thermocouples were installed in furnaces doing various kinds of heat-treating work, that the average maintenance cost, for materials alone, including platinum-platinum-rhodium wires and protecting tubes, was 27 c. per furnace, per month:

Jan 12, 1919

By Kenneth L. Reid

The Mineral Resources Research Center at the University of Minnesota has recently installed a QEM*SEM system (Quantitative E.valuation of Materials using Scanning Electron Microscopy) to aid in detailed mineralogical evaluation of potential mineral resource developments in Minnesota and to provide services to the North American mineral industry. A primary application for the unit is to serve the Minnesota taconite industry by providing mineralogical analysis of ores and concentrator products. Minnesota taconite ores contain fine-grained magnetite in a quartz matrix. The ores undergo several size-reduction/magnetic-separation steps to produce a final concentrate with approximately 75% passing 325 mesh and containing about 5% gangue. The paper describes a typical taconite concentrator flowsheet and reports some preliminary results of the applications of QEM*SEM particle image maps and cumulative yield liberation data to samples from selected points in the concentrator circuit.

Jan 1, 1988

By John W. Ahlrichs

Microscope, electron microprobe and x-ray diffraction have been used to provide quantitative evaluation of products from the mill, smelter, refinery and other metallurgical processes. Phase compositions and their quantities are necessary for an adequate understanding of the various products obtained throughout an operation and in laboratory testing. By careful evaluation, important information can be gained in improving recoveries and increasing grades at various stages of processing. Four case histories are discussed in this paper. Quantitative microscopic counting techniques are applied to mill products to determine degrees of locking and liberation of the economic minerals. Rapid, but accurate evaluation aids the metallurgist to develop or improve the grinding and flotation circuits. In the smelter, the identification and quantification of the phases are important for predicting reaction mechanisms and kinetic trends. Mineralogic techniques have been applied to conventional smelter products, and to those obtained in laboratory tests for newly developed innovations to smelting. Small, but important, values of gold occurrences in ore are difficult to determine. Evaluation of gold usually requires special separations into various mineral concentrates, followed by assays and mineralogic determinations of the products. Numerous occurrences of solid solution constituents can be treated as by-products, but often they are deleterious to metallurgical treatment. Most solid solution problems can be unraveled by the mineralogist's tools.

Jan 1, 1981

By Yuanming Pan, Brett Rogers, Baoquan Hu, Gary Yeo, Christine Austman

The nature and distribution of radiation-induced defects (RIDs) in quartz from the Maw Zone, a yttrium- and rare-earth-element-enriched sandstone breccia complex exhibiting intense hydrothermal alteration, have been investigated by electron paramagnetic resonance (EPR) spectroscopy. EPR spectra show that detrital quartz in sandstone, from five diamond drill holes intersecting the Maw Zone and one above the crest of the so-called Quartzite Ridge, contain only background-level RIDs, indicating that Ubearing fluids were absent in this area. However, close to the sandstone-basement unconformity, in hole WR-194 immediately west of the Quartzite Ridge, the concentration of RIDs in detrital quartz is significantly above background but at least an order of magnitude lower than those at the Key Lake and McArthur River deposits. Widespread drusy quartz at the Maw Zone, which signifies intense hydrothermal alteration, is associated with hematite-, sulfide- and carbonate-bearing mineral assemblages, which exhibit complex crosscutting relationships. EPR spectra of drusy quartz in all three types of mineral assemblages are low in RIDs as well, supporting the EPR evidence that fluids at the Maw Zone did not carry significant U. These EPR results suggest that, in spite of intense hydrothermal alteration and favorable structural geology, the Maw Zone is unlikely to host any significant U mineralization. Moreover, this study shows that the EPR technique is potentially a useful exploration tool, capable of determining whether individual alteration zones in the Athabasca Basin were associated with U-bearing fluids or not.

Jan 1, 2013

By Robert G. Ditchburn, Cornel E. J. de Ronde, Bernard J. Barry

The age of mineralization, its mode of formation, the time elapsed to amass an economic deposit, its capacity for sustainable extraction and, ultimately, its grade and tonnage, are key aspects in the economic viability of volcanic massive sulphide (VMS) deposits (Ditchburn et al, 2004). Radiometric dating methods applied at GNS Science have been recently refined with the purpose of efficiently determining the ages of seafloor VMS mineralization along active intraoceanic arcs. These developments include: determining the longevity of seafloor hydrothermal systems, details of individual chimney and massive sulfide mound growth, and insights into deep-seated processes, such as the transfer of elements from magmas to their overlying hydrothermal systems. In our pursuit to better understand seafloor hydrothermal systems along intraoceanic arcs, we have thus far compiled age information for three volcanic centres of the Kermadec arc (South Pacific) and one of the Mariana arc (NW Pacific).

By Sheng Dai, Yuan Lee, Haiming Xiao, J. P. Young

"There are numerous analytical applications of scatter-emission and/or absorption spectroscopy applied to liquids and solids in the temperature range of 0 to 350°C. In this paper an all-silica fiberoptic probe is described which is useful for spectral analyses from 0 to 1600 K and can be used in harsh chemical environments. The probe has been used for Raman spectral analyses of many molten salt and solid material systems to 1000°C. It has applications for such studies at higher temperature ranges. The instrumentation required along with the demonstrated and proposed applications of the all-silica probe are presented and discussed.IntroductionThere are many kinds of scatter-emission spectroscopies that are of value for analytical measurements. Fluorescence, reflectance, arc or spark emission are descriptors for some of these. Raman scatter spectroscopy is also quite a useful technique for analytical measurements.In Figure 1, we give a simplified explanation of the Raman effect. If one shines monochromatic light into a sample, light may be absorbed, exciting the sample to some virtual state. We know from experience that almost all of the light is re-emitted in the same wavelength range. This is called Rayleigh or Mei scattering and is designated in the figure by the arrows in both examples that point up and down from the same lower energy state. A very small percentage (the order of 10-4%) of the monochromatic light is re-emitted leaving the sample at a vibrationally-excited state. Thus, this light is at a distinctly lower energy compared to the exciting radiation. This is called a Stokes shift and is represented in the left-hand example by an arrow descending to a more energetic vibrational state. If the sample is not at a temperature of absolute zero, some of this vibrationally excited state will be thermally populated. That portion of the sample still absorbs and re-emits exciting radiation as Rayleigh scattered light, but a small percentage of the exciting light is re-emitted as the sample relaxes to the lower vibrational state. The energy of this light is of higher energy and is called an anti-Stokes shift, depicted in the example to the right. Notice that the energy separation of the Stokes or anti-Stokes shifted emission from that of the exciting radiation is the same, and expressed in ~cm-I. The intensity of either shifted emission is a function of the population of the vibrational energy states; therefore, the ratio of the intensity of Stokes to anti-Stokes signal varies with absolute temperature. We will come back to this point later."

Jan 1, 1997

By Gifford White

CONSIDERABLE attention has been directed in recent years to methods of electric prospecting other than the conventional direct-current tech-niques. It has been extensively recognized that electrical data of a more general nature than that possible by direct-current methods might be useful in geophysical studies. To this end, a number of different types of electric currents have been employed, such as single-frequency alter-nating currents, square-topped periodic current waves,4 periodic surges of a less specific nature,8 and suddenly applied direct current.1,2 Yet, to the author's knowledge, little analysis of these different types of driving currents has been made from the standpoint of network theory to determine just what type of currents would give the most useful data, and, most important of all, to determine the relation of the data taken by one method to those of another. Without touching on the actual theoretical problem of how currents flow in the earth under specified boundary conditions, some very useful information can be obtained from the study of the fundamental integral equations of electrical networks, throwing light on the problem not ordinarily appreciated by the field worker. Some manipulation of the standard network equations will be made, with the sole purpose in mind of developing expressions leading to practical results. Suppose that four points in the earth have been located and it is wished to obtain the most useful type of electrical data by inserting current into two of them and measuring the potential developed between the other two. The first problem that arises is that of which pair of the four shall be chosen as current grounds. In the direct-current case, where only steady potentials are measured, the selection is of little consequence, but as soon as currents varying with time are used at the current grounds, a new effect arises. The fact that a varying current is flowing in the current-carrying conductor between the current grounds means that magnetic and electric fields varying with time will be produced

Jan 1, 1940

By L. Lafrenière

A trend in mining exploration is to increase the number of geophysical parameters collected and interpreted for geological features in a given area. Airborne technology now allows us to simultaneously combine electromagnetic, gravity, aeromagnetic and radiometric surveys. We report the results of a multiparameter survey conducted in the area of Kamiskotia, Ontario. This area is located near and on the West side of the multi-metalliferous Kidd Creek deposit. Various metallic occurrences are reported in the studied area. Integrating multiple parameters in the interpretation produces a more detailed pseudogeological map than what has already been published. 3D interpretation has been undertaken using some of these parameters and suggests that future work is required in 3D earth model solutions in order to fully use all parameters.

Aug 1, 2013

By C. F. Gleeson

"Geochemical stream-sediment reconnaissance can be a useful exploration tool from the point of view of rapidly and cheaply evaluating the mineral potential of an area. This is particularly true of rugged and mountainous areas such as are found in Gaspé. For the past two years, SOQUEM has been carrying out such surveys over favorable geological regions in the Appalachians of northern New Brunswick and Gaspe. To date, about 4,000 square miles of terrain has been systematically covered by reconnaissance geochemistry. Jeeps have been used as a means of transportation in the easily accessible areas and a helicopter equipped with a winch has been used to lower crews into the more difficult-to-reach regions. Such surveys have been successful in finding metallic mineralization which otherwise might not have been detected.Electronic computation of analytical information has been used to construct regional metal maps, rolling mean maps and residual metal maps. These maps have helped in evaluating anomalies, in relating the regional geo-chemistry to the regional geology and in comparing the distribution patterns of metals. To date, some 30,000 stream-sediment samples have been collected from the Gaspe region and analyzed for Cu, Pb, Zn and Mn. These analyses are being subjected to computer analysis."

Jan 1, 1969

By O. Bazhko

Regular analysis of different streams is important for the control of hydrometallurgical processes. Various physical and physical-chemical methods are applied for this purpose. Many modern methods require costly equipment and are subject to interferences. Therefore, redoxtitration methods remain of interest. The use of different types of oxidizing and reducing agents as well as redox indicators enables many cations and anions to be rapidly and accurately analysed. Sometimes redox titrations require the prior preparation and addition of masking agents. Selective, sensitive and low-cost methods of redoxtitration of copper and SO2 in plant conditions are described.

Jan 1, 2009

By Rolph Linder

It is generally known and accepted that the efficiency of the blast furnace process, expressed by the symbols specific production and coke consumption, is influenced by a large number of variables connected to the type of burden, the alloy contents of the produced iron and the conditions of production as composition and preheating of the blast, the furnace heat losses and the possible use of fuels added on the tuyere level. It is furthermore obvious, that the coke consumption of the process will be influenced by specific production which could be said to be the result of two counter-acting influences. With high production, realized through intensive blowing, the passage time of the ore through the furnace is shortened leading to a decrease of the indirect reduction taking place in the upper part of the shaft within the temperature range of 300 to 1000°C. Simultaneously the external heat losses (constant in time) will be smaller calculated on each ton of iron and the resulting change in coke consumption will be the effect of both those influences. It is certainly of interest to be able to predetermine the effect of those variables before a change in the production practice is carried out.

Jan 1, 1964

By Keith D. Koper, Kris L. Pankow, Derrick J. A. Chambers, Michael K. McCarter

"In a mining environment, high quality seismic event catalogs are often useful in interpreting local stress states and identifying areas with elevated ground control risk. Installation, operation, and maintenance of local/in-mine seismic networks, however, may be prohibitively expensive, and mine operators may not anticipate the need for seismic data until unusual mining conditions arise. If regional, generally public, seismic instrumentation could be used to reproduce the results generated by local/in-mine instrumentation to an acceptable degree of fidelity, it would be a valuable and inexpensive tool for mine planners and ground control engineers.In this study we apply subspace detection—a non-traditional seismic event detection technique—to data from a sparse, regional network. The process is employed to identify mining induced seismicity (MIS) from an underground coal district. The results are compared to a seismic event catalog produced by a local seismic array operating within the permit boundaries. Additionally, we analyze the performance of two different stations of the same sparse, regional network in identifying blasts at a surface coal mine for which we have a detailed blasting log. In both cases data from stations between 10 and 60 km away from mining activity are used. We also explore the trade-offs between the number of detections and the number of false positives, which is influenced heavily by detection thresholds and the number of stations used in the process.For the surface mine we are able to identify more than 90% of the production blasts documented in the blasting log. We also find that the detected blasts from each of the four active pits produce waveforms similar to one another. The results are not dependent on source-receiver distance, and by requiring detections to occur on both stations the number of sure false positives is reduced to zero. In the underground mining district we identify between 30% and 75% of the events detected by the local array, depending on the acceptable number of false positives and the source-receiver distance. We also find many events that were missed by the local array, showing that regional subspace detection can usefully augment traditional local catalogs. Moreover, subspace detection can provide an estimate on event location and classification using data from as little as one seismic station."

Jan 1, 2015

By Richard J. Lewandowski

Corrosion and product contamination have been difficult problems for extractive metallurgy industries in the U.S. because of the highly active chemicals used. During the past twelve years, other industries, particularly the chemical and paper segments, began to combat this problem with some degree of success using newer materials of construction, including reinforced plastics. These materials are made by combining a corrosion resistant thermosetting resin with a glass fiber reinforcing material and are used to con¬struct hoods, stacks, blowers, tanks, towers, pipe, and equipment of the most complex configurations. For service in contact with aggressive chemicals, the equipment is most often fabricated with the bisphenol-A fumarate polyester resins because of their resistance to corrosive attack. Data from both laboratory work and case histories of field applications are presented-for many common chemicals found in extractive processes. Information is also presented concerning design standards and recommended construction procedures

Jan 1, 1970

By Arkady Senchenko, Yury Kulikov

"Basic theoretical grounds of the methods applied for crushing and grinding parameters determination according to international standards are given in this paper. Statistical data about crushability and grindability research are shown. The potential relationship between the values of Fred Bond Work indices and John Starkey indices (Crushing index, Ball mill index, Rod mill index and AG/SAG index) are discussed in this paper. In order to establish correlation between the crushability and grindability indices the analysis of over 2 500 tests for 165 deposits located in different parts of the world was performed. The relationships among different types of energy consumed for crushing and grinding were determined. A method for preliminary estimation of energy consumption in semiautogenous + ball mill grinding circuit is suggested for its application in preliminary technological solutions development and technical-and-economic assessment."

Jan 1, 2014

The Yilgarn Block of Western Australia presents (figure 1) a number of problems for conventional diamond exploration based on heavy indicator mineral sampling. These problems are due to the geology and unique geomorphological development of the Yilgarn Block.Essentially the Yilgarn Block is a pene- plain developed on a craton composed of Archaean intrusive granitoid rocks with meta- morphosed greenstone; which, apart from regional uplift, has not been tectonically disturbed since planation by glaciation in the Permian. Therefore since the early Plesozoic the Yilgarn Block has been subjected to terres- trial weathering conditions. Bettany et al., (1984) identify two phases of particular importance in the development of the present landforms: 1. Periods of lateritization during the Tertiary which result in the ~lassi~al laterite profile (figure 2). Duricrust indurated : Fe and Al oxides Mottled zone : Clay and Fe oxides Saprolite or pallid zone : leached clay grading into fresh rock. 2. Subsequent periods of aridity and semi- aridity during which laterite development was truncated and reworking of laterite Occurred.

Jan 1, 1988

By S. W. Hurlbut

12.4 Application of Research Findings. After the findings of research have been evaluated and approved, there remains the problem of translating them into practical usage. It frequently happens that this is the more difficult phase of the research project. Hitherto, the problems have been largely associated with material objects and scientific laws. When the findings of research are implemented in the field, the human factor becomes the most important element bearing on success or failure. From this point on, the attitudes and reactions of people of all kinds are involved, and just how they are involved and their relation to successful implementation is the subject of the remainder of this section. 12.41. Management Attitudes. To engage in research at all implies management backing to a degree. But this could be dictated by overall company policy or by just some executives in the hierarchy of management. The existence of research per se does not necessarily mean that there is a solid, unanimous echelon of management executives who sincerely believe in the fruits of research, who have an earnest desire to make breakthroughs, and who have a willingness to take calculated risks. Under the ideal condition of complete management backing, translating the results of research into practice is greatly facilitated. If management accepts the results of research as valid, the order is given, or it has been established by precedent that those results will be implemented. The rest of the organization will have grown to accept the fact that this is so, and that the results must be given a fair trial in the field. However, this ideal condition probably exists but rarely, and it is against a background of incomplete, or partial, management backing that most results of research must be implemented. At the present time, the climate for research in the mining field is less than perfect but is improving rapidly as the realization grows within the industry that the way toward taking its proper place in the Space Age is by applying to mining the philosophy and techniques of research that made the Space Age possible.

Jan 1, 1968

By N Clarke, G R. Ballantyne, M S. Powell, P Elms, A Anyimadu

AngloGold Ashanti Ltd nominated Sunrise Dam Gold Mine as a case study via their involvement with the long-running Australian Mineral Industry Research Association (AMIRA) International P9P research program (AMIRA, 2015) . A group of researchers from the Global Comminution Collaborative (GCC) conducted a comminution circuit survey and review together with a large group of graduate metallurgists, senior metallurgists and operators. Fundamental and applied research understanding was used to identify productivity and efficiency improvements around the crushing and grinding circuits. The limitations of current scientific knowledge were identified through this process and this will allow future research to be more focussed on what is required by industry.The comminution circuit at Sunrise Dam comprises three stages of crushing followed by two stages of ball milling. The secondary crusher and primary ball mill classification were identified as the primary limitations of the circuit. The secondary crusher was found to be underperforming through overall equipment efficiency (OEE) analysis and an improved chamber design was identified by Chalmers University. This improved design will promote higher power utilisation, choke feeding and a finer crushed product for the milling circuit. The primary ball mill product is classified by a combination of a trommel, 3 sieve bends and a hydrocyclone. The combination of poor classification and coarse, competent feed led to a situation where the primary mill was overfilled with rocks, reducing grinding rate due to cushioning of impact. Size specific energy (SSE) benchmarking methodology was used to identify that a 10% increase in throughput could be achieved with improved primary classification.CITATION:Ballantyne, G R, Clarke, N, Elms, P, Anyimadu, A and Powell, M S, 2015. Application of research principles to identify process improvement at Sunrise Dam Gold Mine, in Proceedings MetPlant 2015, pp 221–229 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 7, 2015

By R. H. Hawkins

AN investigation of the applicability of geophysical methods to north-ern Ontario lignite deposits was undertaken early in 1930 by the Ontario Research Foundation at the request of the Ontario Department of Mines TABLE 1.-Formations Associated with Moose River Basin Maximum System Formation Lithology Observed Correlation Thickness, Ft. Pleistocene Marine clays 150 Glacial till (Minimum Interglacial 30) clay and peat Glacial till Lower Cretaceous or Mattagami Fireclay, sand 138 Kootenay (?) Upper Jurassic. and lignite Devonian (Upper) Long Rapids Petroliferous, 50 Portage and black and gray Genesee shale Williams Limestone and 87 Tully (?) Island calcareous shale Devonian (Middle).... Abitibi River Gray fossiliferous 65 Onondaga limestone Devonian (Lower) ?... Moose Rive- Limestone and 50 gypsum Devonian (Loner) Sextant Arkose, clay, etc. 50 Pre-Cambrian Syenite, granite gneiss, etc. Igneous intrusives. . Lamprophyre dikes cut the Abitibi River and lower formations. (Permission of Ontario Dept. of Mines) and was financed in part from a research grant made by the latter organ-ization. The work to date has included gravitational, magnetic and electrical resistivity studies. The gravitational and magnetic measure-

Jan 1, 1933