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"I have been involved in the refractory industry for many years and at some time or another I have designed materials, tested materials, manufactured materials, installed materials, in fact I have done everything except actually chemically analyzed a refractory material.So I would not even begin to tell you how to analyse a refractory material. I'm sure everyone here knows more about chemical analysis than I do.However you could regard me as a customer with and perhaps the insights I have developed may help in putting the role of chemical analysis in the Refractories into perspective.For a start, let's take a step back and ask why we test refractories. The refractories handbook of the American Foundry Association gives four reasons:1. To determine appropriate specification.2. For quality control, to ensure conformance to specifications.3. To provide special property information not available elsewhere.4. For postmortem analysis to determine property changes in service and provideinformation that can point the way to better service.I want to discuss these points with regard to the role of chemical analysis and in particular the abuse of in house chemical analysis facilities. Let me talk first about detelmining appropriate specifications. Most refractory products are made from alumino-silicate raw materials.The phase diagram for alumino and silica is as follows:"

Jan 1, 2014

Notices Competition for Student Members of the South African Institute of Mining and Metallurgy Each year the Institute offers a prize (or prizes should the entries warrant it) of up to Rl00 for the best paper or dissertation on a topic appropriate to the interests of the Institute. The competition is open to all Student Members of the Institute. NEW PUPLICATION Bougainville-the establishment of a copper mine. St. Kilda (Australia), 'Foundations', 1973. The editors of Foundations, Australia's journal of architecture, engineering, and construction, are preparing the above book for publication late in 1973. The story of Bougainville is told and illustrated NIM REPORTS Report No. 1503 Fast-neutron-activation analysis for the determination of oxygen m rock sam ples. Report No. 1514 The determination by X-ray-fluorescence spectrometry of minor amounts of niobium and tantalum in geological materials. Report No. 1530 AUREOL - an X-ray-absorption analyser for the determination of the uranium on loaded resin in ionexchange plants. Report No. 1534 The determination, by atomicabsorption spectrophotometry, of noble metals in the presence of sodium, barium, or sulphate ions. A comparison of uranium and lanthanum as 'releasing agents.

Jan 10, 1973

By Axel Schulze

HUGO PETERSEN has developed from the traditional firm of the same name that was established in 1906 in Berlin and is an engineering company specialising in general plant engineering now based in Wiesbaden. HUGO PETERSEN has many years wide-ranging experience in process plant engineering, primarily in the field of Sulphuric Acid Processes and Gas Cleaning. Together with its main shareholder, Chemieanlagenbau Chemnitz GmbH (CAC), a company with over 40 years experience in the international plant engineering business, HUGO PETERSEN implements turnkey new plants from initial consultancy right through to commissioning. In addition, HUGO PETERSEN can offer its clients improvements and revamps of existing plant systems. Initial consulting, planning and implementation take place within the context of a lean company organisation with experienced engineers and specialists. In all respects, many years of experience guarantee expertise over a wide range of possible applications For clients from the chemicals and metallurgical industries, as well as those in metals processing, HUGO PETERSEN GmbH?s breadth of experience means not just an efficient introduction to new methods and processes, but also their full implementation. In addition, along with design and construction for individual components, the company?s range of services also covers supply of complete plants, as well as modernisation projects and revamps in line with local conditions and existing quality requirements With own technologies and patents in the field of gas cleaning and sulphuric acid, supplemented by licences and cooperation projects, HUGO PETERSEN ensures expertise over a wide range of applications. With specialists and expert knowledge in these fields of application, HUGO PETERSEN is your partner of choice, supporting you and bringing your acid, and project to a successful conclusion.

Jan 1, 2009

1. New books Specialty steels and hard materials, edited by N. R. Comins and J. B. Clark. Oxford, Pergamon, 1983.482 pp. Hardcover £55.50. Papers presented at an international conference on advances in flow measurement techniques, edited by H. S. Stephens and B. Jarvis. BHRA Fluid Engineering (Cranfield, Bedford, MK43 OAJ, England), 1982. £36. Papers presented at Fourth European Conference on Mixing, edited by H. S. Stephens and D. Goodes. BHRA Fluid Engineering (Cranfield, Bedford, MK43 OAJ, England), 1982. £36. Papers presented at an international conference on hydrocyclones, edited by H. S. Stephens and G. Priestley. BHRA Fluid Engineering (Cranfield, Bedford, MK43, OAJ, England), 1982. 248 pp. £27. Controlled atmospheres for heat treatment, by R. Nemenyi. Oxford, Pergamon, 1983. 225 pp. Hardcover 20, flexicover £7.50. Electrochemical techniques in corrosion testing and research, edited by J. S. Scully. Oxford, Pergamon, 1983. 150 pp. Flexicover £9.45 2. Book reviews Off highway truck haulage, by the Newman Combined Group. Parkvine (Victoria), Australasian Institute of Mining and Metanurgy, 1982. Reviewer: B. J. Vorster Elsevier's mineral and rock table, compiled by P. Lof. Reviewer: A. Wedepohl Field geologists' manual, by B. A. Berkman. Monograph Series No. 9, Australasian Institute of Mining and Metanurgy, 1982.295 pp. Reviewer: R. A. G. Cuipers 3. Mintek reports Report M56 A computer programme for the evaluation of process routes in the production of ferrochromium. Report M61 An atomic-absorption programme for the Apple 11 Plus computer. Report M63 A general-purpose data logger. Report M65 A preliminary survey of the corrosivity of water in gold mines. Report M66 A review of corrosion inhibitors: theory and practice. Report M67 The determination of total cyanide in solutions containing uranium and gold. Report M68 The suitability of Doppler flowmeters for use in the minerals-processing industry. Report M70 The preparation and certification of two reference materials of South African manganese ore. Report M78 A n evaluation of the Leeds laboratory-scale flotation cell. Report M79 The determination, by X-ray-fluorescence spectrometry, of gold and uranium on resin. Report M80 The installation and commissioning of a Siemens SRS200 sequential X-ray-fluorescence spectrometer. Report M81 The application of the inductively coupled plasma system to the simultaneous determination of precious metals. Open-pit and strip mines The South African Institute of Mining and Metallurgy and the Mining Alumni Society of the University of Pretoria are organizing an International Conference on The Planning and Operation of Open Pit and Strip Mines in Pretoria from 9th to 13th April, 1984. Other Institutes co-sponsoring the Conference are The Canadian Institute of Mining and Metallurgy, The Institution of Mining and Metallurgy, and The Society of Mining Engineers of AIME.

Jan 1, 1983

YEAR 1943-1944 Vol. 44 Page A major change-over in the ventilation of a deep level mine, by F. G. Hill and E. C. Ranson, 27; Discussion 56, 62, 67, 71, 72, 79, 123, 129 131 A note on the quarrying of surface limestone in the Sinai Desert, by V. L. Bosazza.. .. 59 Mining with diamond drills at the Nkana Mine of the Rhokana Corporation, Limited, Northern Rhodesia, by W. A. Odgers and A. G. Stirling, 95; Discussion 117, 121, 122 123 On silicates and dusts from the Witwatersrand gold mines (some preliminary notes), by J. J. Frankel, 169; Discussion .. 178 Presidential Address-Review of the rock pressure problem, by C. Biccard Jeppe, 3; Discussion 11,15 17 The chemistry, production and application of plastics, by P. N. Lategan, 138; Discussion 151 153 YEAR 1944-1945 Vol. 45 Page A microtechnique for the size-grading of mine dust, by S. R. Rabson, 34; Discussion 49, 50, 52 55 Activated carbon for regenerating used lubricating oil, by F. J. Tromp and J. J. Matthee 90 A contribution to the study of the production of zeolites, by C. C. le Grange and A. J. Petrick 235 A laboratory method for the determination of the suitability of South African coal and coal blends for the manufacture of metallurgical coke, by R. F. J. Teichmann .. .. 202 Copper containing cements for self-sanitising surfaces, by R. S. Young and H. L. Talbot 156 Notes on some sulphide minerals from the Far East Rand, by E. Mendelssohn, 84; Discussion, 88 89 Presidential Address-A review of underground support on the Witwatersrand with its Bearing on the Problem of ultradeep mining, by P. J. Louis Bok, 3; Discussion, 24, 25 27 Scientific management with particular application to a Witwatersrand gold mine, by J. S. Ford, 63; Discussion, 77, 80, 82 83 Some aspects of rock-drilling practice (the Witwatersrand gold field), by C. J. Irving, 163; Discussion, 185, 190 *197 Temperature measurements in a mine on the Witwatersrand with an electrical resistance thermometer, by O. Weiss, 127; Discussion, 136 137 The measurement of the geo-thermic gradient by means of the clinical thermometer, by R. A. H. Flugge-de Smidt, 105; Discussion, 136 137 The micro-chemical determination of free and combined silica in mine dust, by S. R. Rabson, 43; Discussion, 49, 50, 52 55 The oxidation of pyrites associated with South African coals, by R. F. J. Teichmann 141 YEAR 1945-1946 Vol. 46 Page Air cooling plant, No. 4 Shaft, City Deep, Limited. A review of layout and results achieved, by H. W. Unwin, A. Malcolm and R. E. Campbell Pitt, 66; Discussion, 100, 102, 103, 106, 110 115 A preliminary note on the Waterberg coal field as a possible source of coking coal, by P. E. Hall 124

By Peter N. Calder, Alan Bauer

The complexity of modem open pit load-haul-dump systems is described, and the need for realistic working models is pointed out. Both standard and probabilistic simulation procedures are discussed, probabilistic simulation being indicated as the more powerful and practical technique. Acquisition of the necessary pit operating data required for simulator construction and general modelling procedures are described. Finally, results from a typical open pit simulator are used to indicate the scope of the technique.

Jan 1, 2014

MASSMIN 92 edited by H.W. Glen. Johannesburg, The South African Institute of Mining and Metallurgy, 1992. xiii, 485pp. ill. 30 cm. (SAIMM Symposium Series S12). Includes bibliographies. ISBN 1-874832-18-8. R342 (MemberR285; Student Member R218,88. Available in Australia from the AMF Bookshop, 63 Conyngham Street, Glenside, SA 5065 at $A171.00 (approx). This volume is the twelfth in a series of symposia published by The South African Institute of Mining and Metallurgy since 1962. This particular meeting addressed the subject of the underground mining of massive ore bodies.

Jan 1, 1994

By R. L. C. Maggs

The following members of the Orange Free State Branch and visitors paid a mini-visit to the H.J. Joel Gold Mine on 23rd January, 1991: Members E.N.D. Westgate Organiser R.LC. Maggs Hon. Secretary S.V. Stander S.P. van Wyk D.S. Minnie O.W. Fourie Visitors C. Knight-Hassel J. Campos E.W. Booysen J. Steyn P.!. Masseratte C.J. Higgins S. Guven F. Scof N. Hastings R. Hays On arrival at the Mine, the visitors were welcomed by the General Manager, Mr Chris Naude, who introduced the staff who would be involved in the visit.

Jan 1, 1991

By R. T. White, A. Higginson, M. Phil

Samples of water that had been collected underground from eight gold mines in South Africa were subjected comprehensive analysis of the quality of the waters, and their corrosivity on mild steel was measured by the laboratory techniques of extrapolation from Tafel plots and of polarization resistance. The results indicate that, if such factors as pH, Langelier index, and degree of aeration are beyond certain specified limits, the corrosivity ofthe water is affected. The applicability of the corrosivity index in predictions ofthe degree corrosion is questioned. Suggestions are included for future work involving the fundamental characterization of the corrosivity of mine waters.

Jan 1, 1983

By G. Sommer, R. P. Chaix, G. T. W. Ormrod

Recent developments in the instrumentation and automation of uranium-processing plants by G. SOMMER, Ing. (Grad.) (Visitor), G. T. W. ORMROD (Visitor), and R. P. CHAIX, B.Sc. (Visitor) The paper discusses work at the National Institute for Metallurgy on the evaluation of measuring techniques for the automatic control of free acid in leaching. of the ratio of ferric to ferrous ion in leaching, of pH in liquid-liquid extraction. and of uranium in loaded solvent. Commercially available instruments. and the modifications that have been made to adapt them to South African uranium plants, are also described.

By T. G. Pedro, Q. Gonzalo, R. E. Roberto

Anionic surfactants, such as oleic acid and sodium oleate (OLE), and cationic surfactants, such as dodecyl amine-hydrochloride (DDA), are used as flotation collectors of spodumene. However, recovery is poor even if activating ions are used because gangue minerals are also activated. Some reports demonstrate that OLE/DDA mixtures act as a selective collector to enhance spodumene recovery. From mostly macroscopic tests, it has been argued that anionic OLE and cationic DDA form electroneutral complexes, which are adsorbed on the mineral surface through chemisorption; however, no molecular evidence has been presented. Therefore, the adsorption mechanisms of the collector mixtures remain mostly unknown. It seems necessary to first study the behaviour of these surfactants confined in salt solutions, to determine auto-associations when they are pure and cross-associations when mixed, the transition from monomers to micelles, and the structure of the micelles and the effects of pH, temperature and concentration. In this paper, ab initio calculations are first used to determine the surface charge distribution of OLE and DDA separately. Then molecular dynamics simulations are used to determine the conformation, aggregation, and diffusion of these pure and mixed surfactants in freshwater and saltwater with the ionic strength of seawater in a pH range. In particular, it is interesting to determine the various associations that result in mixtures of both surfactants and the impact of alkali and alkaline earth metal cations on the structures formedp. Cations influence the order of the structure and orientation of water dipoles, reducing the mobility of water, ions, and surfactant molecules. This knowledge is critical to improve the molecular understanding of the adsorption mechanisms on minerals. Keywords: Computer simulation, molecular dynamics, flotation, collectors, saltwater

Jan 1, 2020

By L. S. Linda, P. G. H Pistorius

Ferritic stainless steel is utilized to fabricate automotive exhaust systems using a ferritic weld metal. Ductility of the weld metal is higher if its microstructure contains a significant proportion of equiaxed grains. The formation of equiaxed (rather than columnar) grains is favoured by a higher titanium weld metal content. In this study, the Ti content of ferritic stainless steel weld metal was changed by using Tifree (Type 436) and Ti-containing (441) ferritic stainless steel as base metals. The metal-cored welding consumable contained 0.4% Ti. Gas–tungsten arc welding and gas–metal arc welding processes were compared. The weld metal Ti content ranged from zero to 0.5% Ti, as determined from scanning electron microscopy supplemented by inductively coupled plasma optical emission spectroscopy. Cross-sections of the weld beads were subjected to point counting (to estimate the fraction of equiaxed grains) and image analysis (to estimate the average grain size). Point counting proved to be more reliable. The fraction of equiaxed grains was sensitive to the Ti content, but not to the welding process. Below 0.4% Ti, the fraction of equiaxed grains gradually increased with an increase in the weld metal Ti content; above 0.4% Ti, the fraction of equiaxed grains rapidly increased with increasing Ti content. The transition in behaviour at 0.4% Ti corresponded to a Ti content at which Ti-rich precipitates became stable at the estimated liquidus temperature of the weld metal.

Jul 2, 2022

By F. E. Steffens

The application of kriging in assessing the area rainfall in a weather modification experiment is complicated by the presence of many zero rainfall recordings on a given day, and the fact that the variograms seem to be quite different for the rainfall on different days. Indicator variograms are shown to be directly related to two sets of conditional probabilities. Probability kriging is used in estimating the probability of rainfall amounts above any cutoff at any point

Jan 1, 1987

By S. Potgieter-Vermaak

The main mineral components of the so-called heavy sands (or black sand) are the titanium, zirconium and iron-bearing minerals, rutile, zircon and illmenite, accompanied by various minor and trace amounts of silicates or phosphates, often present together with the rare earth elements. The investigated samples originated from Richards Bay Minerals (RBM) in South Africa, which is jointly owned by BHP Billiton and Rio Tinto, the largest titanium slag producer in the world. The present study focused on the characteristics of samples originating from various points in the separation plant. The heavy-mineral fractions and concentrates of a representative suite of samples were investigated using various analytical techniques to establish the differences in morphological and elemental compositions at the different points in the plant. These techniques included: reflected light microscopy, micro-raman spectrometry (MRS), scanning electron microscopy coupled with energy dispersive X-ray analysis (SEM/EDX) and structural and chemical analyser (SCA). All samples comprised a heterogeneous population of zircon and rutile grains with diverse physico-chemical properties, expressed by large differences in colour and trace element chemistry of single grains. The elemental composition proved the presence of the rare earth elements that appeared to coexist with both Ti and Zr minerals. The percentage of grains hosting inclusions, such as anatase, monazite, quartz, spessartine, augite, epidote and actinolite, varied for each sample and could be uniquely characterized by Raman investigations. Keywords: heavy mineral sands, micro-ram an spectrometry, elemental analysis

By D. W. Horsfallt

The above paper gives a fair amount of information and is a useful addition to the literature on a subject of growing importance. I believe that more experimental results could have been given, together with more details of the modifications made to the plant that enabled it to operate with the success mentioned in the paper. One important omission is a definition of the word fines. As pointed out elsewhere!, this word is used very loosely.

Jan 1, 1980

NOTICES PROCEEDINGS OF THE SECOND INTERNATIONAL CLEAN AIR CONGRESSThis massive volume of 1,380 pages contains all the papers presented at the congress held in December 1971. INDEX TO SOUTH AFRICAN PERIODICALS This bibliographical work has been produced by the Johannesburg Public Library since 1945, and is of interest to all our readers. THE CONTROL OF GASEOUS SULPHUR COMPOUND EMISSION An international conference on this theme will be held at the Salford University from 10th to 12th April, 1973. COLLOQUIUM ON SLlMES DAMS The South African Institute of Mining and Metallurgy have great pleasure in advising members that two-day colloquium on Slimes Dams is being arranged for the 14th and 15th November, 1973. NATIONAL INSTITUTE FOR METALLURGY / NASIONALE INSTITUUT VIR METALLURGIE REPORT. VERSLAG No. 1424 REVIEW OF THE WORLD'S FLUORSPAR INDUSTRY, WITH PARTICULAR REFERENCE. TO SOUTH AFRICA Ist August, 19n Investigator: H. H. Gossling SYNOPSIS The consumption of fluorspar has increased significantly during the last three years, and a consumption of approximately 5,76 million tonnes per annum is projected for 1975. REPORT. VERSLAG No. 1432 LABORATORY METHOD No. 44/2 THE DETERMINATION OF RUTHENIUM AND OSMIUM IN THE RESIDUES RESULTING FROM THE LEACHING OF MATTES 5th July, 19n Investigators: Magdalena M. KrUger R. V. D. Robert SYNOPSIS The method described involves the sintering of the residue with barium peroxide, and the distillation of ruthenium and osmium from the sinter. REPORT. VERSLAG No. 1439 THE REACTION OF SULPHIDE MINERALS WITH THIOL COMPOUNDS 29th June, 19n Investigator: L. A. Goold SYNOPSIS A selected group of thiol reagents was reacted with a wide range of sulphide minerals, and products that were formed at the surface were extracted and identified by infrared spectrophotometry.

By S. L. Miller

The development of a pilot gold geostatistical ore reserve system proved that geostatistical methods worked well for the routine production of annual ore reserves on gold mines of the Gold Fields of South Africa (GFSA) group, and that the techniques could also be practically implemented, understood and accepted by Survey Department personnel. Many side benefits of the pilot system became apparent, and a variety of useful management information was provided by manipulating the data values that were already captured. It was decided that it was a priority computing project to develop a standard production system (GORS) for routine use by all the GFSA gold mines. Experience with the pilot system enabled detailed functional specifications for GORS to be laid down. These, together with group computing policy determined the terms of reference and constraints for the GORS development. System design could not be finalized until new and appropriate mainframe database software and graphics workstation equipment and software had been found. With these in place the basic system was structured to take best ad- vantage of the interactive features of the workstation, the number-crunching power of the mainframe and the flexibility offered by a relational database and associated 4GL tools. Application sub-systems were developed for data capture, statistical applications, geostatistical calculations, contour plotting and graphical queries. GORS is being introduced to the mines in a phased manner with suitable documentation, training and support structures to enable it to be routinely and effectively used on a day-to-day basis by all group gold mines.

Jan 1, 1987

By A. Karadogan

Decision making can be defined as the selection process of the best routes from the alternatives in order to achieve a goal, and mostly involves uncertainty. Additionally, mostly qualitative variables (weak rock, massive ore deposit, etc.) are in question. Mine planning engineers often use their intuition and experience indecision making. As fuzzy set theory has been used since 1970, these uncertainties are easily evaluated in the decision-making process. Real world study is decision making under vague constraints of different importance, involving uncertain data (qualitative variables), where compromises between antagonistic criteria are allowed. This paper presents a new approach in the selection of an underground mining method based on fuzzy set theory for the Ciftalan Lignite Site located close to Istanbul in Turkey. The physical parameters such as geology and the geotechnical properties of ore, hanging and foot wall, economic effects, environmental effects, are established with field and laboratory tests together with the determination of other qualitative variables. Meanwhile, some qualitative variables dealing with the matter was described according to the view of a number of experts. Then fuzzy set theory is applied to these parameters, considering the available underground methods in order to choose the proper method. At the end of the evaluations, the room and pillar method with filling was determined as the most suitable method for the test site. Keywords: Decision making, fuzzy set theory, underground, mining, method selection

Jan 1, 2008

By A. L. Edwards

A retrospective study was conducted on the Rand Mutual Assurance (RMA) noise-induced hearing loss (NIHL) compensation claims from 1998 to 2008 to determine if the 2008 milestone agreed at the 2003 Mine Health and Safety Summit was achieved. The number and costs of NIHL compensation claims in different commodity sectors and workplaces were collated. A secondary analysis of the ages of employees compensated after 2008 was conducted. A complementary retrospective analysis of audiogram data investigated the percentage loss of hearing (PLH) shift in different homogeneously exposed groups and occupations at two gold mines. The compensation claims analysis indicated a significant decrease in NIHL claims from 1998 to 2008, but the milestone was not achieved. The reason may be either that claims have not been submitted timeously as required by Instruction 171 and that the current submissions are a result of pre-2003 noise exposure, or that employees who were baselined are still developing NIHL owing to ineffective hearing conservation programmes in place in the mining industry. On the basis of best practice for hearing conservation, recommendations are made for leading indicators in hearing conservation programmes and for reducing the risks of NIHL in order to achieve the 2013 milestone.

Jan 1, 2012

With the advent of the First World Conference on Sampling and Blending (WCSB1) in Denmark in 2003 and the subsequent biannual meetings, together with other sampling conferences held on a regular basis, the central tenets of sound sampling practice and theory are spreading throughout the minerals industry. End-users and project houses, or groups who execute the projects, are all now better-informed about the principles of ?correct? sampling and preparation. To support this, many large mining companies now have their own in-house champion who will advise and ensure that the supply of sampling equipment is correct in terms of design and application, which further contributes to improved metallurgical accounting. The presence of a sampling champion also ensures that consistent and acceptable standards in regard to sampling practice are maintained throughout the group. This has, in turn, placed a greater degree of responsibility on the shoulders of sampling equipment suppliers, in terms of their equipment designs and product offerings, as well as applications knowledge for effective installation of equipment on client plants. This paper attempts to highlight the significant challenges that sampling equipment manufacturers often face with regard to complying with the newly understood requirements of best practice and sampling equipment design. Manufacturers invariably face issues with end-users or project houses, including project cost control, restricted headroom for samplers in plant layouts, and a lack of knowledge in certain quarters. These all have a potentially negative effect on the final outcome of a proposed sampling solution or implemented project. In reality, what is intended by all parties and what is ultimately installed are at times very different, with undesirable consequences for all concerned. Against this challenging background, there are, however, a number of instances where intent and implementation are complementary, with very satisfactory results. Keywords sampling, mechanical samplers, design, installation, sampling theory.

Jan 1, 2014