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By C. Sunderman, J. Johnson, S. Signer

Researchers at the National Institute for Occupational Safety and Health have developed a miniature data acquisition system (MIDAS) that can measure resistance changes and temperature, store data for later retrieval, and illuminate LED lights. This instrument can be used with strain-gaged bolts, cable bolts, CSIRO stress-measuring gages, string pots, and any other instrument that uses single-ended, resistance-type gages. MIDAS has the capability to measure up to 16 gages at preset time intervals and store more than 2000 scans, yet is small enough to fit in a 35-mm hole. Because the MIDAS consumes little power, a 9-V alkaline battery will operate the system for 6 months. Data from the MIDAS can be sent to a PC via an RS232/RS485/IRdA port. A software program was written to set operation parameters, graph data, and store all information directly to a spreadsheet. Three LED lights change from green to yellow then red based on reading levels and/or rates of change. This feature can be used with different types of gages to warn miners of possible rock instabilities. The MIDAS has received MSHA experimental permissibility approval and is currently being tested at several mines.

Reduce the time, complexity and expense of dissolving metal and mineral samples in solution in preparation for chemical analysis. Approach In earlier research, the Bureau of Mines developed a rapid and inexpensive method for the dissolution of mineral and metal samples in plastic pressure bottles heated in a boiling water bath. Using this technique, samples could be prepared for chemical analysis in less than one hour compared with several hours by traditional dissolution methods (see Technology News No. 85, December 1980 for further details). By heating in a microwave oven, sample dissolution time can be reduced to approximately 5 minutes.

Jan 1, 1983

Permit visual inspection of underground cavities dam the surface. Approach A closed circuit TV camera and a 35mm still camera are lowered down a borehole, and remotely operated. How It Works A platform holding the cameras, and other equipment is lowered on a graduated cable until the depth of interest is reached. Then a quartz lamp and the TV camera are turned on. The television picture is monitored at the surface and recorded on video tape. Areas of special interest are photographed with a 35mm still camera. These photographs contain more detail than TV images because photographic film is capable of higher resolution than a TV transmission.

Jan 1, 1979

By R. V. Ramani, V. T. Burgos, J. A. McClay

The data for Test I1 describes an underground bituminous coal mine operating in a 72 inch seam, with an estimated production rate of 4,257,000 tons per year. The system includes 15 continuous mining sections, conveyor belt haulage, and a rail network for supply and personnel transportation. The following section includes the input data sequence, annual cost report, and cash flow analysis "report for this data set.

Jan 1, 1975

By P. R. Bremner

The United States is more than 90 pct dependent on imported bauxite a source for aluminum, but it has vast nonbauxitic aluminum resources, such as kaolinite, anorthosite, alunite, etc. As part of a program to devise processes for treating these resources, the Bureau of Mines investigated a bench-scale leaching process using hydrochloric acid (HC1) and fluoride to extract aluminum from Wyoming anorthosite. HC1 and fluoride-to-aluminum (F/Al) mole ratios were studied with respect to aluminum extraction for single-stage, cocurrent, and countercurrent leaching modes. Using 95 pct stoichiometric HC1 and a F/Al mole ratio of 0.27, 90 pct of the aluminum was extracted by countercurrent leaching. Single-stage leaching with the same amount of acid and fluoride extracted 48 pct of the aluminum. Three fluoride sources, CaF2, Na2SiF6, and H2SiF6, were used and gave similar results on aluminum extractions.

Jan 1, 1982

Predict the cumulative hydrologic impact of mining on the environment. Approach A comprehensive set of computer models has been developed to predict the impact of mining on ground water. Mine inflows, drawdowns in aquifers, and ground water quality can be predicted. How It Works The Prickett-Lonnquist finite-difference groundwater model was specially modified for the hydrologic problems of mining. This model, developed at the Illinois Water Survey in the 1960's,

Jan 1, 1982

By Sathit Tandanand

Geological differences among various coalfields restrain the applicability of subsidence prediction using empirical approaches previously developed. The Bureau of Mines assessed data collected from 16 longwall panels in the Northern Appalachian basin. Attention was focused on the effects of rock lithology, excavation width, and panel depth on the subsidence factor. The results show that the subsidence factor can be expressed in terms of the width-to-depth ratio by a simple exponential equation, which has a coefficient tentatively considered as the subsidence index. This index varies with the lithology of a particular site, and can be expressed in terms of percent distribution of weak and strong rocks in the overburden.

Jan 1, 1982

By Fred N. Kissell

Methane-flow and pressure data taken from a mine in the Pocahontas No. 3 coalbed are compared with flow rates from lump coal obtained in laboratory experiments. From this, it is concluded that the main source of gas is the intact coalbed rather than a "crushed zone" near the working face. The permeability and sorption capacity of the intact coalbed are calculated and gas emission rates are theoretically accounted for.

Jan 1, 1972

By C. M. Mason

Mechanical mining produces large quantities of very fine coal dust called float dust. The associated increase in hazard requires a reexamination of the Bureau of Mines method of evaluating the incendivity of explosives in coal dust-gas-air mixtures. A technique recently developed by Bureau of Mines laboratories for evaluating the incendivity of explosives in coal dust-air mixtures was applied, with modifications, to coal dust-air-natural gas mixtures. A series of permissible explosives were evaluated by this modified technique. Results indicate that the modified technique could be the basis of a more discriminatory procedure than that presently in use.

Jan 1, 1968

By P. D. Laverty

The U.S. Bureau of Mines treated mixed and contaminated super alloy scrap by pyrometallurgical and hydrometallurgical methods to separate and recover metal values. Best results were obtained by leaching Zn-treated or atomized scrap with HCI-02 at 9SO C and 50 psig 02' This resulted in dissolving approxi-mately 98 pet of the AI, Co, Cr, Cu, Fe, Mn, Ni, and Zn while rejecting over 98 pct of the Mo, Nb, Ta, Ti, W, and Zr as an insoluble refractory residue. Chlorine was successfully substituted for HCI to leach Zn-treated scrap but was unsuccessful for leaching atomized scrap. The leaching solution was treated by pH adjustment and hydrothermal precipitation at 2000 C for 4 h to remove AI, Cr, Fe, and other contaminants as a filterable precipitate. Recovery of Co and Ni would be accomplished by solvent extraction and e1ectrowinning. Chromium recovery as a ferroalloy was demonstrated.

Jan 1, 1989

By Larry J. Nicks

The Bureau of Mines is investigating the catalytic activity of rare-earth compounds to develop a catalyst for the cathode reaction of a hydrogen-oxygen fuel cell. This report presents the results of studies of the catalytic activities of lanthanide oxides for the oxidation of hydrogen at 150° to 250° C. Preliminary activity tests were made with approximately stoichiometric mixtures of hydrogen and oxygen diluted with helium. A series of tests was also run under oxygen-rich conditions in which specific rate constants and activation energies were determined. Variations in rate constants up to 2,000 times were observed for the various lanthanide oxides. The three most active catalysts were oxides of Ce, Pr, and Eu, having specific activities of 6.93 X 10-7, 4.88 X 10-7, and 4.06 X 10-7 moles H2.sec-1.m-2, respectively, at 200° C.

Jan 1, 1973

By Zachary J. Fink

A continuous-monitoring system has been developed for analyses of mine gas concentrations associated with spontaneous combustion, mine fires, and explosive and toxic levels. The analysis center, which is linked to sample locations by polyethylene tubes in bundles, has been successfully field tested by the Federal Bureau of Mines for analyzing carbon monoxide and oxygen; a computational scheme has been developed to process the data at the site. This report contains information on the design, purchase, installation, and maintenance of the tube-bundle system. A brief comparison of the tube-bundle system with the underground-analysis system and plans for future research are also included.

Jan 1, 1975

By M. MacLaughlin, J. Whyatt

A case study is presented that relates statistical descriptions of joint sets to the distribution of local wedge failures along the crest of a catch bench at the Yellowstone Talc Mine. The fracture sets and bench width were mapped by teams of geological engineering students from Montana Tech under the direction of Dr. Mary MacLaughlin. The students analyzed the fracture data, conducted physical property tests, and used a beta version of a NIOSH program “Bwedge” to predict the distribution of surviving bench widths. In the course of this analysis the students developed evidence of software performance issues that, unfortunately, frustrated their analysis. These have now been addressed and a full analysis completed. The analysis confirms the validity of the student mapping program and provides insight into the effects of blasting and excavation practices on the bench. It also provides a tool for exploring the pattern of bench crest failure that would result from variations in both bench geometry and blasting practices.

By Sabri Ergun

The method of constant compositions involves the determination of the time required for the attainment of a given conversion at various temperatures. Heretofore, it has been used in evaluating the energy of activation only. A development of the method, made in the present study, makes possible the evaluation of the functional dependence upon composition and the frequency factor in addition to the energy of activation. INTRODUCTION Kinetics of reactions are best analyzed in the light of the mechanism, energy requirements, and forces involved in the reaction. Such physico-chemical information is not often available in solid state phase transformations. The reaction rates are followed by changes in a physical property during the course of the reaction, and repeating the experiment at different temperatures permits the determination of activation energy only. The possibility of a complete kinetic analysis by such a purely "phenomenological" approach has been questioned.4/ In this report a method is developed making possible the evaluation of the functional dependence upon composition and frequency factor in addition to the energy of activation. The application of the method to a study of solid state order-disorder changes is demonstrated.

Jan 1, 1960

By D. J. Bauer

Solvent extraction separation of light group rare-earth elements in a quaternary ammonium compound-chelating agent system was demonstrated in single-stage studies, Typical separation factor values obtained were 93 for lanthanum-praseodymium, 5.4 for praseodymium-neodymium, and 11.6 for neodymium-samarium. These values are significantly higher than those obtained using organophosphate extractants. Further studies in a 20-stage countercurrent mixer-settler resulted in the production of 99 percent lanthanum (oxide basis) at 96-percent recovery. Subsequently, 88 percent of the neodymium with a purity of 92 percent was recovered in the raffinate.

Jan 1, 1971

By Gordon H. Dechman

This Bureau of Mines report presents an iterative approximation method for microseismic source location that was developed to adapt microseismic techniques for rock structure analysis to investigations of surface problems, such as slope failure in an open pit mine. The source location method and two derivative location algorithms are described in detail, and the speed and accuracy of the two algorithms are compared.

Jan 1, 1977

By Jeffrey Johnson, Thomas Brady, Radford Langston, Mary MacLaughlin, Hendrik Kirsten

The magnitudes and directions of in situ stresses affect the stability of mine openings, as well as the type and amount of ground support needed to maintain a safe working environment for miners. Using hollow inclusion stress cells, researchers from the Spokane Research Laboratory of the National Institute for Occupational Safety and Health obtained two in situ stress measurements from the face of two footwall lateral drifts at the Stillwater Mine near Nye, MT. The first measurement, obtained in 1997, was collected under the valley beneath the Stillwater River. The second measurement was obtained in 2002 under the main frontal massif of the Bear tooth Mountains in the western sector of the mine. Although few data are available, the major principal stress under the valley has been recorded as nearly horizontal in a north-south direction perpendicular to the ore body, while beneath the mountains, stress runs east-west parallel to the ore body. This paper documents the measurements, describes the in situ stress state, and discusses a finite-difference analysis of the biaxial test.

By Stephen Krickovic

A methane emission rate study was conducted in 1969 on a longwall section of a Lower Kittanning coalbed mine in central Pennsylvania. The longwall face was mined with a drum shearer between developed headings on the head end and headings on the tail end that were driven with a ripper-type continuous miner as needed. The study was conducted over 22 consecutive shifts (7-1/3 days). The average methane emission rate from the Lower Kittanning coalbed during mining at the face and developing the headings at the tail end of the face was 34 Am. Caving of the gassy overlying strata as the result of mining at the face increased the methane emission to rates ranging from 702 to 1,049 cfm.

Jan 1, 1971

Provide the U.S. mining industry with the means to measure and control exhaust emissions of diesel engines used in underground mines. Approach Diesel research is divided into four primary areas: exhaust aerosol measurement, particulate control, gaseous emission control, and chemical and biological characterizition of particulate matter. Diesel research is frequently cosponsored by industry; collaborative research ventures between industry, academia, other government agencies, and the Bureau arc common. Diesel research at the Bureau is conducted in the diesel engine research facility at the Bureau?s Twin Cities Research Center (TCRC). This facility is a state-of-the-art laboratory capable of performing emissions testing, exhaust control evaluations, and safety tests. Background Exposure of mine workers to airborne contaminants from diesel engine exhaust is potentially harmful. The National Institute for Occupational Safety and Health has recommended that whole diesel exhaust be regarded as "a potential occupational carcinogen" and that ?reductions in exposure to diesel exhaust in the workplace would reduce the risk." The U.S. Mine Safely and Health Administration (MSHA) convened an Advisory Committee on Standards and Regulations for Diesel-Powered Equipment and is beginning to implement its recommendations, which cover health, safety, and certification and approval issues surrounding the use of diesels underground. In January 1992, MSHA published an advance notice of proposed rulemaking to regulate diesel particulate matter in underground mines.

Jan 1, 1992

To monitor the quantity and quality of air in underground mines to assure safe working conditions. Approach Several mine air monitoring systems, consisting of sensing stations in the return airways and control stations on the surface, have been Installed and tested. How It Works Sensor stations are located at strategic places in the underground mine. At each station, the sensors measure air velocity, air temperature, methane concentration, and carbon monoxide concentration. In one system, differential air pressure between intake air and return air, is also measured. Output voltages of the sensors are converted to digital signals at the sensor stat ion; these signals are multiplexed so that data from all sensors can be trans-phone wire to a central station. There the data are displayed and alarms are triggered when the sensed values exceed (or in the case of air velocity, fall below) a preset value. In addition to receiving data automatically, the central station can poll individual sensors at any time.

Jan 1, 1978