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By L. W. Kelly

The primary purpose of this paper is to show the appreciable savings that were made by roof-bolting the main west entry of the Kings mine, which was to be the permanent, main haulage road, as compared to the cost of supporting the same roof with peg timbering as first planned. Additional items that might prove valuable to other mine operators are contained in this paper and detailed below. 1. A detailed cost of the system of roof support known locally as the peg-timbering method is given. It consists fundamentally of supporting steel cross bars on pegs inserted into holes drilled in the ribs close to the roof. 2. A method of supporting the roof in caved entries is shown, where such support must endure for an extended period in haulageways and air courses.

Jan 1, 1952

By R. W. Holliday

To determine the copper and nickel content of reported ore occurrences in the Chippewa mine near Rockmont, Douglas County, Wis., the Bureau of Mines reopened and sampled the old shaft and workings during the summer and fall of 1953. Occurrences of native copper near Rockmont and others near Gordon, also in Douglas County, Wis., are in lava flows, which extend from the Keweenaw Peninsula of Upper Michigan southwest across Wisconsin and into Minnesota. Sporadic attempts have been made to find additional economic copper deposits in these flows since profitable mines were developed in Upper Michigan nearly 100 years ago. The Rockmont and Gordon areas were explored extensively more than 50 years ago. More recently, from August 1944 to duly 1945, an occurrence near Gordon was investigated by the Bureau.2/

Jan 1, 1955

By B. J. Scheiner

The Federal Bureau of Mines investigated an electrolytic oxidation procedure for extracting lead, zinc, copper, and silver from lead-zinc concentrates. Concentrates slurried in brine were pumped through the anode compartment of electrolytic cells equipped with selective ion diaphragms. Hydrochloric and hypochlorous acids generated in the anode compartment converted the metal sulfides in the concentrates to soluble metal chlorides, sulfate ion, and elemental sulfur. Metal extractions of 92 to 100 pct were obtained from lead-zinc concentrates at an energy consumption ranging from 1.5 to 5.0 kW-hr/lb metal extracted. Sodium hydroxide was formed in the cathode compartment at a current efficiency of >99 pet. Silver and copper were extracted from refractory tetrahedrite minerals, but the process entailed a relatively high energy consumption. Sealing the top of the diaphragm cell utilized the chlorine more effectively, thereby reducing energy consumption 10 to 50 pct.

Jan 1, 1975

By Roy H. Poston

This paper sets forth the mode of ore occurrence, characteristics of ore and country rocks, methods of exploration, development, and. ore extraction, and the costs of underground operation at No. 8 mine of the St. Louis Smelting and Refining Works of the National Lead Co. located near the southern extremity of the Southeast Missouri lead district. The author acknowledges the assistance of E. T. Campbell, geologist, in the preparation of the paragraphs on the geology of the ores. HISTORY The first record of mining in St. Francois County, Mo., concerns more or less shallow semisurface "diggings" which were worked about the year 174-2. In 1864, however, the discovery of the disseminated deposits, the present source of lead, was made on property near the town of Bone Terre. Winslow has estimated the lead-ore production in this county prior to 1869 to be 59,526 tons.3

Jan 1, 1929

By H. C. Ko

Calorimetric determinations of low-temperature heat capacities and the standard enthalpy of formation were made by the Bureau of Mines for aluminum sulfide, A12S3. The standard entropy (S°), enthalpy of formation (?Hf°), and calculated Gibbs energy of formation (?Gf°) at 298.15 K are 27.93±0.05 call deg-mole, -155.6±0.9 kcal/mole, and -153.0±1.0 kcal/mole, respectively.

Jan 1, 1976

By Will H. Coghill, G. Dale Cole

"INTRODUCTION This paper describes a method for the rational sorting of particles by means of a laboratory batch jig. Its purpose is to show that a material can be reliably appraised for gravity concentration without the drudgery of sink-float fractionations.Development of the batch- jig method of testing was incidental to a study of the Birmingham, Ala., red-iron ores now being conducted by the Bureau of Mines in cooperation with the University of Alabama and the ore-producing companies.APPLICATIONOres and coal are commonly tested for their gravity-concentration characteristics by specific-gravity dissections in heavy liquids. The heavy liquid most commonly used for coal is zinc chloride and for ores they are benzene, carbon tetrachloride, acetylene tetrabromide, methylene iodide, and thallium malonate formate. The last is poisonous and corrosive to the skin but is essential for separations in the 3.3 to 4.4 specific gravity range. The last two of these liquids are expensive, and several of them are hard to obtain now.Although it is not suggested that heavy-liquid dissections be eliminated entirely, sometimes a more reliable evaluation of coal and ore can be obtained by other and more simple means. For example, sink-float data were unsatisfactory as a guide to commercial gravity concentration of a red-iron ore because they did not take into account the difference in particle shape of the hematite and gangue and the differences in true and apparent specific gravity of the hematite grains, some of which were porous. For this ore, the batch-jig method of testing herein discussed proved advantageous. Not Only did the batch-jig data give a truer picture of the concentration problem, but only about one-tenth the time of the conventional sink-float tests was required."

Jul 1, 1944

By Ann G. Kim

The Bureau of Mines investigated factors that influence the formation of methane and other hydrocarbon gases in coal, which is an integral part of the coalification process. Coalification begins with a biogenetic stage in which plant debris decomposes and peat is formed; methane and CO2 are the predominant gases produced during this stage. During the diagenetic stage of coalification hydrogen and the hydrocarbon gases methane, ethane, ethylene, propane, propylene, butene, iso- and normal butane, and pentane are formed by dissociation of the organic material. Methane may also be produced by a secondary reaction of hydrogen with unsaturates or by the reduction of CO2. The gas contained in coalbeds is a mixture of methane, C2 through C5 alkanes, CO2, 02, N2, H2, and H2; its heating value is equivalent to that of natural gas. The gas content of coal depends on many variables, but an empirical relationship between adsorptive capacity, rank, and depth has been observed.

Jan 1, 1978

By R. B. Moore

The story of helium is one of the romances of science . Probably nothing , except perhaps radium , compares with it in human interest . Helium is one of the best examples of a discovery in pure science that has wide commercial application . In 1868 , an eclipse of the sun was visible in India , several scientific men who were in India making observations of the eclipse turned a spectroscope for the first time on the solar chromosphere - that part of the atmosphere of the sun , about 10,000 miles deep , which merges into the corona . A bright yellow line was observed and was thought at first to be due to sodium . Janssen showed , however , that this line was not just the same as either the D or D₂ line of sodium, although it was extremely close to these lines , hence he suggested that the new line have the designation D₂ . Frankland and Lockyer decided that Dz was due to an element in the sun not previously discovered on the earth , and suggested for it the name "Helium" from the Greek work " Helios " the sun . For several years nothing more was done in connection with this element . In 1894 , Sir William Ransay , in conjunction with Lord Rayleigh , made his memorable discovery of argon in the atmosphere , which was announced at the British Association meeting in the same year . After this discovery , Ramsay looked for other sources of the element . Through Sir Henry Miers , he learned that Dr. W. F. Hillebrand , of the United States Geological Survey , had obtained an inert gas from certain uranium minerals , which gas he had decided was nitrogen . Ramsay believed that part of it might be argon ; he obtained from Hillebrand for experimentation , a sample of the mineral , cleveite , one of the uranium minerals , and after extracting gas from the mineral and purifying it , he ran it into a spectrum tube . The lines obtained ' were , however , different from those of argon; among them was the bright yellow line noted by Janssen . Thus was terrestrial heliun discovered .

Jun 1, 1922

By Sol Weller

The Fischer-Tropsch synthesis consists of the formation of long-chain hydrocarbons by passage of carbon monoxide-hydrogen mixtures over metal catalysts, usually based on iron, cobalt, nickel, or ruthenium, at temperatures in the range 180°-300° C., and at pressures of 1-15 atmospheres. Although the reaction has been known and studied for more than 20 years, the mechanism by which it occurs is still poorly understood. One approach to understanding is to consider the effect upon the course of the synthesis of variations in each of the important operating variables. Consideration of the experimental data pertaining to these variables may suggest an over-all picture describing the synthesis - a picture which, in turn, would have to be consistent with all the known facts. The first part of this paper will be concerned with such a consideration of operating variables; the second portion will discuss recent work pertaining to the role of metal carbides as intermediates in the synthesis.

Jan 1, 1949

By K. K. Kelley

This report contains heat-content values for hexagonal crystalline germanium dioxide between 298.15° and 1,350° K., and for germanium dioxide glass between 298.15° and 1,800° K. experimentally determined by the Federal Bureau of Mines. No similar data for these substances are to be found in the literature. The heat-content and corresponding entropy-increment data are presented both in tabular form and by equations. Free energy of formation values are estimated for germanium dioxide glass at 298.15° and 1,800° K.

Jan 1, 1961

The latest Active List of Permissible Explosives and Blasting Devices was published in July, 1929, as Bureau of Mines Report of Investigations 2947, 2 under the title or "Active List of Permissible Explosives and Blasting Devices Approved Prior to June 30, 1929.' Subsequent Reports of Investigations 2253, 2958, 2962, 2972, 2988, 2992 and 3000, were issued to record the official actions taken during July, August, September, October, 1929, and January, February, and March, 1930. No changes were made during November and December, 1929, and April, 1930. The following additional changes in the list recording the actions taken during May, 1930, are now authorized. [ ]

Jan 1, 1930

By H. O. Poppleton, F. E. Block

This investigation was made to develop a method of preparing high - purity thorium metal in quantities up to 20 kilograms per batch . Several methods for the preparation , purification , and reduction of thorium tetrachloride are discussed . Thorium tetrachloride was prepared by chlorination of decomposed thorium nitrate or oxalate with carbon tetrachloride or phosgene . tion of the crude tetrachloride was achieved by multiple distillations or by filtration of the molten chloride . It was found that high - purity thorium metal could be prepared by sodium reduction of thorium tetrachloride if chloride of sufficient purity were available . Byproduct salts and excess reductant were removed by vacuum distillation , and the resultant thorium metal sponge was consolidated by consumable - electrode or fixed - electrode arc melting . It was demonstrated that metal prepared by this method could be fabricated into bar , rod , or sheet , at room temperature .

Jan 1, 1964

By W. W. Odell

The results of the 1921 cooperative experiments conducted by the U. S. Bureau of Mines and the University of North Dakota at the University mining substation plent at Hebron , North Dakota , pointed clearly to certain definite dep ficiencies in the schemes hitherto developed for benefiting and utilizing lignite . First The apparatus used in the carbonizing process or used to produce carbonized lignite suitable for briquetting is too costly , that is , the cost per ton day of residue made is too high . Second - The depreciation of the carbonizing appara tus is too high . Third The carbonizing apparatus can not be operated intermittently without seriously damaging it and impairing its efficiency of performance . Fourth Too little attention has been given to the possibility of using at least a certain percentage of the carbonized lignite directly in suitable stoves and furnaces without briquetting or other treatment . Accordingly , consideration was given to the design of an oven that could be built at a mine without the importation of highly skilled and specially trained construction men , erected at a low first cost , readily kept in a state of repair , operated at a rela tively high capacity and put into operation or shut down at will without seriously damaging the brickwork . The need of such an oven was appreciated also by the University of North Dakota and a cooperative agreement was made to build and operate such an oven during the summer of 1921.

Feb 1, 1923

By Leonard Obert

A triaxial procedure is described for measuring the modulus of elasticity and Possion's ratio of stress relief cores , that is , the concentric hole cores obtained by the overcoring technique . The elastic constant determinations can be made at stress levels comparable with those encountered in underground mining . The results from tests on an aluminum alloy calibration specimen and four rock specimens are included .

Jan 1, 1964

By Charles L. Kimbell

In 1990, the aggregate value of world international export trade in mineral commodities was estimated at more than $64 billion in current (1990) dollars, about 8.4% higher than that in 1989, but still 8.7% below the record high set in 1980. Table 8 provides a data series for the estimated value of world export trade in all mineral commodities from 1979 through 1990, as well as a breakdown of this total into fuel and nonfuel commodities. It is noteworthy that for this 1990 edition, trade data for the year of review were available in time for inclusion, whereas in previous editions, the latest available global trade data were for the year prior to the year of review. Hence, as regards trade, this edition of Minerals in the World Economy updates the 1989 edition by 2 years rather than by only 1. For this reason, it is appropriate to note that the 1989 global total value for inter-national export trade in mineral commodities was almost $596 billion, 11.1 % above the revised 1988 level of more than $536 billion, both figures expressed in current dollars for the appropriate year. Despite the considerable increase in the dollar value of mineral commodity exports, their share of total export merchandise trade declined to 19.1 % in 1990 from 19.7% in 1989. At 19.1%, this share was very near the recent year record low of 19.0% reached in 1988. The year 1990 was the fourth in a row in which the total value of world mineral commodity export trade increased.

Jan 1, 1993

By Gwendolyn D. Hood

The U.S. Bureau of Mines developed a dewatering technique for treating wastewater that was tested on waste slurry from a commercial tile company in Alabama. Raw wastewater samples were pretreated with 10 Ib calcium chloride and 10 lb Wyoming bentonite per 1,000 gal of slurry. After pretreatment, polyethylene oxide (PEO) at dosages varying from 0.05 to 0.20 lb per 1,000 gal was mixed with the waste slurry, forming strong, tough floes that were separated from the clarified water using a trammel. The flocculated slurry was dewatered to a consistency that could be handled for subsequent disposal in a landfill. The clarified water quality was equivalent to that of the company's present treatment system.

Jan 1, 2010

By T. J. Ballard

The Conrad Hill mine vas first opened as a gold mine about 182 and has been operated at various times since then. The Bureau of Mines, as part of the strategic minerals program, mapped and sampled the accessible mine workings. The work failed to reveal appreciable copper values or evidence of additional ore deposits.

Jan 1, 1948

By Fredrick L. Johnson

In 1986, at the request of the U.S. Bureau of Land Management, the U.S. Bureau of Mines studied 25,640 acres of the 29,680-acre Devil?s Garden Lava Bed, 21,040 acres of the 28,660-acre Squaw Ridge Lava Bed, and 9,100 acres of the 12,600-acre Four Craters Lava Bed Wilderness Study Areas (OR-D01-D02, OR-001-003, and OR-001-022, respectively) in order to evaluate their identified mineral resources. The study areas are located in Lake County, OR, about 50 air miles southeast of Bend. No mineral resources were identified in the three study areas. The areas are almost entirely underlain by recent lava flows. Cinder cones occur in each of the areas; however, the best cinder occurrences are in the Four Craters Lava Bed study area. Slab lava, of facing stone quality, is scattered throughout the Devil?s Garden Lava Bed study area, and to a lesser extent, in the Squaw Ridge Lava Bed study area.

Jan 1, 1987

The Bureau of Mines has long been active in promoting the purchase of coal for Government use under specifications that define the requirements in terms of heating value of the coal, expressed in British thermal units, and the composition as shown by proximate analyses. To these, when required, are added the ash-softening temperature, the free-swelling index, and the Hardgrove grindability index. Under most of these specification contracts, the bidders guarantee the quality of the coal, and that guaranteed by the successful bidder becomes the standard of his contract. The deliveries are sampled in accordance with instructions1 issued by the Bureau of Mines, and the samples are analyzed in the Bureau laboratory to determine whether the coal is of the quality guaranteed by the contractor; if it is not, a price adjustment is made. The Government, with the exception of the Tennessee Valley Authority, purchased approximately 5.5 million tons of coal in fiscal year 1971. In connection with these purchases, the Bureau analyzed 4,366 samples. These are published (table 1) for the use of Government officials and the public. Such analyses of delivered coal and tipple samples (samples collected at mine tipples as coal is being loaded into railroad cars or trucks) provide valuable data for use in evaluating future bids. In addition, the continuous sampling of coal as delivered is a check on the practical results obtained in burning the coal.

Jan 1, 1972

By Causey J. Douglas

In 1988, at the request of the Bureau of land Management, the U.S. Bureau of Mines studied part of the 13,460-acre Owyhee Breaks Wilderness Study Area (OR-003-059) in order to evaluate its identified mineral resources. The study area is in Malheur County, OR, about 27 miles northwest of Jordan Valley. No mineral resources were identified in the study area during this investigation. There is an occurrence of jasper along Birch Creek and an associated occurrence of zeolite in some tuffs. In the northern part of the study area is an occurrence of bentonitic clay containing less than 40,000 tons. Much of the area is covered by landslide blocks, colluvium, earthflow deposits, and talus, composed of Tertiary-age volcanic rocks. The upper plateaus are capped by Tertiary-age basalt.

Jan 1, 1989