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By Rodrigo Fina Ferreira, Jacek Kolacz, Luciana Gois, Neymayer Pereira Lima

The recent developments on the sensor detectors together with the higher capacity of the machines, due the high-speed computing recent advances, have made possible extending the application in the mining industry. The use of x-ray fluorescence, x-ray transmission and radiometric sensor based sorting can selectively remove gangue minerals in different size fractions for different minerals. This paper summarizes the potential application of SBS for an iron ore in three size fractions aiming to increase the %Fe after the removal of particles with main gangue minerals associated. Pilot plant tests were carried out with samples of iron ore in different size fractions and different content of hematite and gangues. The use of x-ray transmission sensor showed the possibility to increase the %Fe from about 63% to above 68% for particles below 80mm and 45mm, after the removal of low density particles. The presence of fines on the feed affected the performance of the SBS X-rays transmission machine, especially for the fine fraction feed. The mineralogical determination, carried out to know the association between hematite and gangue minerals, and the density of the particles on the feed, can be used to preview the quality of products of the x-transmission sorting process.

Oct 3, 2019

By Hui-bin Wu, Rui Yuan, Yang Gu, Peng-cheng Zhang, Zheng-zhi Zhao

The corrosion behavior of three kinds of medium-Cr rolled steel pipeline steels in carbon dioxide collecting and transporting environment at different temperatures was studied. The results shew that the 5Cr sample was most affected by temperature. When the temperature rised from 30 °C to 90 °C, the corrosion rate increased from 0.12 mm/a to 1.87 mm/a, which was increased 15.6 times. The corrosion rate of 7Cr steel at 30 °C was similar to that of 5Cr steel. However, as the temperature increased, the corrosion rate rised slowly, increasing by 2.4 times at 90 °C. The corrosion rate of 9Cr steel was not obvious with temperature, and it was always below 0.06 mm/a. The thickness of the corrosion product film of the three samples gradually increased below 70 °C, and suddenly increased above 70 °C. This was related to the negative temperature coefficient of the solubility of FeCO3, and the thickening of the product film also affected the ion exchange of the cathodic reaction. An increase in the Cr content contributed to grain refinement and increased the proportion of the small-angle grain boundaries. More fine grains mean an increase in the total length of the grain boundaries, which could provide a diffusion channel for the free Cr element; on the other hand, the low-angle grain boundary structure was more orderly, with a lower free volume and lower interface energy. Under the combined effect of both, 9Cr steel and 7Cr steel had high volta potential and better corrosion

Oct 1, 2019

By Nelson SOUTO, Nicolas LEGRAND, Sami ABDELKHALEK, Zafer KOONT

A work roll thermal crown model has been developed for a wide range of hot and cold rolling mill applications. The model is extremely fast, robust and accurate to determine the evolution of thermal crown all along the rolling campaigns. It has also ability to consider work roll shifting, multiple segmented cooling zones along the length and circumference of the roll as well as composite rolls properties (e.g. different thermal properties between mandrel and core of the roll). Moreover, the model includes simultaneously fast and slow temperature evolution calculations, respectively near roll surface (skin area) and at a certain distance below the roll surface (bulk area). This gives to thermal crown predictions a higher accuracy than conventional thermal crown models from literature that consider only the slow temperature evolution regime. An optimization procedure together with roll surface temperature and roll thermal profile measurements have been used to tune the model. The tuned model applied to hot rolling conditions has shown a significant influence of roll shifting and composite rolls properties on the prediction of roll temperature distribution and thermal crown during rolling. The tuned model applied to cold rolling conditions highlights the importance of mill operators practices to modify cooling distribution across roll barrel length with the segmented cooling zones to adjust the thermal crown and to get better strip shape control.

Oct 1, 2019

By Verônica Scarpini Candido

O uso cada vez mais frequente do poli metacrilato de metila (PMMA), muitas vezes em substituição ao vidro temperado, se deve a sua alta rigidez, praticidade, leveza e transparência. No entanto, as normas de fabricação atuais na indústria de polímeros recomendam testes específicos nesses materiais. O presente estudo tem o objetivo de testar mecanicamente as propriedades do material Polimetacrilato de Metila (PMMA) em condições que simulem um ambiente muito mais agressivo do que o usual. Para tanto foram realizados testes de espectroscopia na região do infravermelho (FTIR), análise termogravimétrica (TGA), testes de tração e impacto Izod, e análise por Microscopia Eletrônica de Varredura (MEV). Os resultados revelaram que o Polimetacrilato de metila (PMMA) manteve suas propriedades mecânicas em tração até a temperatura de 105°C. No que se refere à resistência ao impacto, a temperatura influenciou negativamente no desempenho desse polímero.

Oct 30, 2017

By Ronaldo Câmara Cozza

Iron aluminide alloy; Ball-cratering wear testing; Rolling abrasion; Wear volume; Coefficient of friction

Jul 31, 2018

By Flavia de Paula Vitoretti

Pelletizing of iron ore fines is an important process used to produce high quality of raw materials for the subsequent reduction processes in the ironmaking industries. The process involves the production of green pellets and subsequent induration on a traveling grate furnace to promote inner partial melt and agglomeration which confer physical and metallurgical proprieties appropriated to the subsequent reduction processes. The pellets are produced with addition of charcoal to improve efficiency in the reduction processes. The lignin coal from sugarcane straw is an alternative source to replace the charcoal or coke in the self reduction of pellets. This work focused on the influence of biomass on the chemical kinetics parameters inner agglomerate pellet structure under industrial process conditions of the travelling grate furnace due hot gas flows within the pellets.

Aug 1, 2018

By Henry Chumienski

Next to the paper industry, the steel industry is a major user of water. Without an adequate and reliable source of “good” water, steel cannot be produced. The use of water has a direct impact on steel quality and on our environment. Used improperly, water can also add unnecessary costs. Used properly, water can maintain and improve steel quality, enhance our environment and control or reduce the “total cost of operation”. Water needs to be more than just “wet and not lumpy”. Water quality needs to be based on the end use. This paper discusses ways to manage many of the water systems. With little or no capital investment it is possible to develop operating practices that protect your initial investment, ensure that the water systems do not have a negative impact on quality or your production costs and also minimize your chance of having an environmental incident.

Jul 30, 2018

By Maciej Korecki

Pyrowear®Alloy 53 steel is an excellent material for the construction of drive transmission components (gears, shafts, etc.) which have to operate in difficult conditions primarily in the aviation industry (Fig. 1.). Among the properties of such items is a high case hardness and abrasion-resistance, while the core remains flexible and is capable of carrying large impact loads. They can work at elevated temperatures with limited lubrication. The thermal treatment of such materials is based on case hardening by means of carburizing. This paper presents the technology of vacuum carburizing of Pyrowear® Alloy 53 steel. It discusses the methods of establishing different profiles of carbon concentration in a layer and their influence on the hardness profile. The effects of sub-zero treatment and tempering on the properties of the hardened case are also considered. It also presents a SimVaC® simulator of vacuum carburizing, designed especially for Pyrowear® Alloy 53 steel, which provides highly accurate predictions of the outcome of the process as the profile of carbon concentration in the layer, or vice versa: establishes the process parameters which will guarantee the required profile.

Aug 16, 2017

By Constantino Capurro

For certain applications, coarse titanium nitride (TiN) precipitates can be deleterious for the final properties of the material. Hence, in order to better understand the mechanisms involved in the generation of these precipitates, a thorough characterization of the particles observed in steels with different titanium and nitrogen content was carried out. Samples from liquid steel (tundish), continuous casting billets and final product were evaluated using an Automatic Particle Analyzer (APA) coupled to a Scanning Electronic Microscope (SEM). The location, frequency, size distribution and composition of the different particles observed were assessed. While only few TiN precipitates were observed in liquid steel samples, the density of this type of particle significantly increased in the continuous casting billets samples. Particles ranging from 1 to 10 µm were mainly found in the interdendritic zones of the as-cast structure. The density of TiN particles observed in these samples did not change after re-heating and rolling operations. A model to predict TiN precipitation during solidification was developed. A reasonable agreement was found between model results and measured data. Results of this analysis confirmed that the precipitated fraction of TiN increases as the product of steel Ti and N contents rises.

Oct 30, 2017

By Osmar Roberto Bagnato

Este trabalho apresenta um estudo do desgaste de insertos e tensões residuais em diferentes estratégias de entrada de ferramenta no fresamento da liga Ti-6Al-4V. Esta liga possui propriedades mecânicas que a torna ideal para aplicações onde é necessária uma ótima relação resistência-peso. O objetivo é reduzir o desgaste dos insertos no processo de fresamento e analisar as tensões residuais na usinagem da liga Ti-6Al-4V. A integridade superficial do material após a usinagem deve ser conhecida já que esta liga é utilizada em aplicações criticas. Quatro estratégias de entrada foram estudadas, sendo que no faceamento foi utilizada a entrada por rolagem e a frontal reta e no fresamento de cavidade foi utilizado mergulho reto e em rampa. Em todos os ensaios foram utilizados os mesmos parâmetros de usinagem. As tensões residuais foram medidas por difração de raios-X (Luz Sincrotron), pelo método sin²?, utilizando um difratômetro de raios-X instalado no LNLS. No faceamento a estratégia por rolagem mostrou uma importante redução do desgaste e uma pequena redução da tensão residual quando comparada com a estratégia frontal reta. No fresamento de cavidades a estratégia de mergulho reto mostrou um inesperado aumento do desgaste e uma significativa redução da tensão residual quando comparada com o mergulho em rampa. Todas as tensões residuais encontradas foram compressivas. As tensões residuais encontradas em todos os experimentos se mostraram favoráveis a aplicações sujeitas à fadiga.

Aug 8, 2018

By Jackson de Brito Simões

As Ligas com efeito de Memória de Forma (LMF) são metais funcionais que podem recuperar grandes deformações, superiores a 5%, quando submetidos a carregamento mecânico e/ou aquecidos. Este fenômeno ainda surpreende pesquisadores e engenheiros de projetos, materiais e processos. Esses metais possibilitam o desenvolvimento de atuadores termomecânicos capazes de gerar esforço mecânico com o bloqueio da recuperação de forma. Inúmeros são os processos para obtenção dessas LMF, cada um com sua particularidade e limitação específica. Nesse contexto, este trabalho avalia o efeito do reprocessamento pela técnica Plasma Skul Push-Pull (PSPP) e do tratamento térmico de solubilização nas propriedades térmicas de transformação de fase de uma LMF 55,1Ni-44,9Ti (% em peso) obtida originalmente pelo processo de fusão por indução a vácuo (VIM). Para isso, a LMF foi refundida com uma tocha de plasma e vazada sob pressão em quatro moldes metálicos distintos (aço, bronze, alumínio e cobre). As técnicas de caracterização térmica Calorimetria Diferencial de Varredura (DSC) e Resistência Elétrica em função da Temperatura (RET) foram utilizadas para avaliar o efeito desse reprocessamento e do subsequente tratamento térmico de solubilização a 850°C em diferentes tempos. Verificou-se que a injeção em molde metálico proporciona uma significativa redução nas temperaturas de transformação de fase, da ordem de 30°C em relação ao material bruto obtido por VIM. Por fim, foi possível concluir que a LMF NiTi reprocessada mantém a transformação de fase mesmo após tratamentos de solubilização a 850°C em tempos mais longos (8 h), contrariamente ao material originalmente obtido por VIM.

Aug 16, 2017

By Claude Bodeving

The present steel economy drastically increases the financial strain on blast furnace operators. As a consequence, the importance of reliable cast floor operations is increasing drastically, which has a direct influence on the required clay mass and tapping equipment performances. When using modern high performance clay masses, pneumatic taphole drilling machines quickly reach their performance limits, which has made fully hydraulic drill hammers a standard in modern cast house operation. Besides the well-established hydraulic TMT hammers with high impact energy, an alternative version with lower impact energy, but high impact frequency was developed by TMT in the past, in order to achieve improved taphole protection. TMT’s recent research has shown that the drilling requirements inflicted by the taphole condition change over the taphole length, which has triggered the development of a new hammer, capable of switching between a high impact frequency mode and a high impact energy mode.

Aug 17, 2017

By Luiza Esteves

Corrosion testing was performed in white liquor from a Brazilian Kraft mill. Specimens of duplex stainless steel (DSS) and lean duplex (LDSS) were exposed at 170 °C for 30 days to simulate conditions of the digester. Corrosion rates were determined from weight loss measurements. After this exposure, the corrosion products formed on the steel surface was characterized by using scanning electron microscope (SEM) equipped with EDS, X-Ray Diffraction (XRD), and X-ray photoelectron spectrometer (XPS). EBSD can be used to quantify of basis balance phases in DSS and LDSS. General corrosion rates for UNS S32304 LDSS were higher than the UNS 31803 DSS in industrial white liquor at 170 °C for 30 days. XPS and XRD analyses indicated that the film formed after the immersion test may be consisted by Fe and Cr oxides and sulphides.

Oct 30, 2017

By Thinnie Hahn dos Santos

O aço API 5L X60 é empregado na fabricação de dutos submarinos para a produção de óleo e gás. Com a ajuda de métodos de inspeção e estudos de mecânica da fratura é possível avaliar a severidade dos defeitos existentes, prever a falha dos componentes e tomar as devidas providências para evitar acidentes que podem levar a danos ambientais, perda de vidas e prejuízos financeiros. Com foco na redução do efeito do histórico de carregamento, avalia-se uma técnica alternativa de pré-trincamento por fadiga para a obtenção das curvas de crescimento de trinca por fadiga. Esta técnica permite a nucleação de trincas em carregamento cíclico compressivo, isentas de tensões residuais compressivas, que mascaram os resultados na determinação do limiar de propagação de trincas. Neste trabalho, foram utilizados corpos de prova do tipo C(T) para a nucleação das pré-trincas de fadiga. Foi avaliada a influência das características do carregamento, como o nível da força aplicada e a razão de carregamento no comprimento de saturação das trincas produzidas, a fim de se obter avanços no estabelecimento dessa metodologia. Com um carregamento mais intenso, o comprimento de saturação de trinca foi maior. Além disso, a diferença de comprimento entre o centro e as superfícies do corpo de prova se torna mais acentuada. O comprimento de saturação de trinca é menor que o raio da zona plástica e maior que a região máxima governada por tensões residuais trativas. Para carregamentos menos severos, a trinca cresce de maneira mais uniforme e alcança comprimentos de saturação de trinca menores. A razão de carregamento não interfere significativamente no comprimento de saturação de trinca.

Oct 30, 2017

By Diogo Tenório dos Santos

This property has been studied to characterize the strength a metallic material exhibits when it is machined so it can be regarded as its typical behaviour. As such, it may even be considered as an intrinsic material property. It is usually measured by an index called Coppini index, which is expressed by the ratio between the removed mass of a cutting tool caused by wear when it is used for machining and its initial one for a certain set of machining parameters. In this investigation, the tests were therefore conducted by an established set of parameters, namely feed rate, cutting and depth rates, in which the same wear mechanism took place in both ferrous alloys: AISI 4140 and AISI 316 steels. They were chosen based upon their increasing ordinary machinability indexes. The initial and final mass of the cutting tool were measured by an analytical scale with 0.01 mg precision. Cylindrical rods of 50-mm diameter were machined and the CI indexes showed a remarkable difference between them: 0.080 for the first steel and 0.049 for the second one, i.e., AISI 316 steel presented better machinability than the first one. It was then possible to conclude that this method presents good results in terms of both reproducibility and adequacy for machine shop conditions and it may be applied in a foreseeable future, mainly for metallic materials that have rather low machinability indices.

Jul 31, 2018

By Bruna Brito Freitas

O processo de soldagem por fricção é uma técnica recente que vem sendo desenvolvida a fim de melhorar a qualidade das estruturas offshore. Com a finalidade de aperfeiçoar essa técnica é importante estudar as propriedades metalúrgicas do material soldado. Este trabalho tem como objetivo avaliar a tenacidade ao impacto de um aço C-Mn soldado por fricção com pino consumível, conhecido como FHPP (Friction Hydro Pillar Process). Desta forma, no presente estudo o material foi soldado, tratado termicamente, e após avaliado através de análises metalográficas, de microdurezas e ensaios de impacto Charpy. Como resultados foram geradas microestruturas para as diferentes regiões da solda e foram obtidos valores de energia, segundo a norma ASTM E-23. Por fim, conclui-se que o material não processado apresentou uma tenacidade superior a região de interface soldada, devido as diferentes microestruturas geradas no processo.

Aug 16, 2017

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By J. Bas A. F. Smeulders

Traditional laboratory lubrication tests, including those for cold rolling lubricants often involve measurement of neat oils. To achieve increased levels of test severity, such tests are often carried out at high temperatures and prolonged durations. However, we found that the levels of lubricant degradation and wear in these tests can be much higher than in the field. Moreover, steel rolling is not done with neat oils, but with emulsions, where the presence of water influences film formation, surface chemistry and oil composition in the roll bite. To better approach the situation in the field, and thus to be able to develop rolling oils with improved lubrication performance, several lubrication tests were developed for emulsions: direct measurement of film formation and measurement of Stribeck curves, in which the emulsions can be assessed in terms of their boundary lubrication and elastohydrodynamic behaviour. The key innovation is that also another test method was developed, which focuses on boundary lubrication and wear, and the role of extreme pressure and anti-wear additives. Realistic levels of test severity are achieved in the tribometer by mimicking frictional power intensities and flash temperatures for typical cold rolling or tinplate mills. Test conditions can be adapted according to the mill stand or pass number and other cold rolling process parameters. The emulsions are kept at normal operational temperature. Clear differences could be observed between emulsions of various concentration and composition. The viability of the method is illustrated by a number of field cases, in which a good correlation is demonstrated between the laboratory tests and the performance in a pilot or production mill.

Jul 30, 2018

By Matheus Soares Siman

A soldagem GTAW tem importância fundamental para a indústria não só pelo excelente controle do aporte térmico, como também ao fato de proporcionar, repetitividade e reprodutibilidade. No entanto, este apresenta uma série de desafios, principalmente em relação à determinação de algumas variáveis e como essas podem afetar a resistência das juntas soldadas. Neste trabalho, investigou-se a influência de diferentes procedimentos de soldagem em tubos de aço SAE 4130 sem costura com e sem a deposição e com a aplicação ou não de pré-aquecimento. Após procedimentos de soldagem, as propriedades mecânicas e a microestrutura da junta soldada, zona fundida, zona termicamente afetada e metal base, foram avaliadas por meio de ensaios de microdureza, de dobramento e análise metalográfica. Foi possível avaliar a influência da aplicação do pré-aquecimento e analisar as propriedades mecânicas e microestrutura das juntas soldadas. Os perfis de microdureza revelaram a importância do pré-aquecimento. O ensaio de dobramento possibilitou a avaliação das juntas de maneira qualitativa. Porém, um ensaio quantitativo, como o de tração, possibilitaria mais informações.

Oct 30, 2017

By Priscilla Pessin Coppo

The prevention of dental enamel wear has particular relevance for preventive and restorative purposes in dentistry. The wear damage can increase due to salivary disorders and/or parafunction (bruxism); antagonists incisal surfaces become flat and coincident. This study aims to investigate the wear behavior and the related mechanisms in sliding pairs of conformal incisal enamel, with similar values of hardness and fracture toughness, with different applied normal loads and lubricated conditions. Bovine incisors, under pin on flat configuration, were tested in two lubrication condition (dry or with natural saliva) and two applied normal loads (8 and 16 N). The worn surfaces were investigated by 3D profilometry and SEM. The analysis of worn surfaces indicated mechanisms of brittle fracture, but with different severities. Under a normal load of 16 N and dry condition, wear is controlled by a brittle process: microcracking with flake-like wear particles, which results in high friction coefficient (> 0.85), wear rate and wear volume. On the other hand, under a normal load of 8 N and natural saliva, wear took place in the interprismatic region, with consequent exposure of prisms and fracture in localized regions. In this case, the friction coefficient was 16% lower and the wear volume was one order of magnitude lower. Under 8 N and natural saliva, the wear was greater than in the dry condition, probably due to tribochemical reactions.

Jul 31, 2018