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By R. H. Sprute

The Bureau of Mines conducted a feasibility study and designed an operational system for consolidating waste coal sludge in a 110-acre pond by applying direct current between buried and floating electrodes. Consolidation would reduce the sludge to half its present volume, there-by extending the working life of the pond as well as creating a safe, stable impoundment. The project was conducted by the Bureau under an agreement with the Washington Irrigation and Development Co. (WIDCO), located near Centralia, WA. Part 1 of this report, published as Report of Investigation 8666 in 1982, covers the results of laboratory tests at the Bureau's Spokane Research Center and of a small-scale field test at WIDeO's coal preparation plant. Test results show the process is efficient and cost-effective when power is applied at low current density. Part 2 (this paper) describes a detailed design for an electrokinetic system to dewater WIDCO's 110-acre pond with a 27.4-acre electrode array. Densification of the inactive sludge pond will require 3.6 yr of treatment for a total cost of $1,450,000. The study and design are site specific, but design procedures and analyses are sufficiently detailed to serve as a guide for applying the process to any sludge pond.

Jan 1, 1988

By J. A. Baicker

A prototype borehole probe for ore grade determinations by means of in-situ neutron activation analysis was designed, built, and tested in a two-phase program. Phase I dealt with the design and fabrication of a borehole logging system for operation in 7.6 cm (3 in.) diameter or larger boreholes. It consisted of a 5.06 cm (2 in.) diameter borehole probe containing an intrinsic germanium detector, a canister-type solid cryogen cooling system, cooled FET preamplifier, linear amplifier, high voltage supply, analog-to-digital converter, microprocessor-based multichannel analyzer, buffer memory, bi-directional cable link, power supplies, and a Californium-252 neutron source. A surface support vehicle was designed and outfitted. A minicomputer system was constructed and software developed and tested. In Phase II the system was field tested at several mine sites. The system was calibrated, tested, improved, and demonstrated in a variety of applications. Tests were performed at sites pertinent to uranium, iron, coal, copper, silver and gold. Technical feasibility was demonstrated for all these applications except gold; the gold results were inconclusive. In-situ neutron activation analysis using high resolution gamma ray spectrometry was found to be a potentially viable logging method for are grade analysis under certain conditions.

Jan 1, 1984

By Wendell R. Peters

Shallow underground voids resulting from early coal mining and other resource recovery activities over the past several decades are now being recognized as a significant cause of ground subsidence problems in developing urban areas. Uncertain knowledge of abandoned coal mines also imposes potential hazards in coal excavation operations since water inundation or the release of methane gas is a pricnipal hazard when mine excavation operations break into an abandoned mine. U.S. Army requirements for an effective method for detecting and mapping subversive man-made tunnels have resulted in a surface-operated automatic earth resistivity survey system with a digital computer data processing system. Field tests aimed at demonstrating the system performance resulted in successful detection of tunnels having depth-to-diameter ratios up to 15 to 1. Under the sponsorship of the Bureau of Mines, a similar system was designed and constructed for use in the detection of coal mine workings. This report discusses the hardware and software aspects of the system and the application of the high-resolution earth resistivity method to the survey and mapping of abandoned coal mine workings. In the field tests reported, the targets of interest were both air-filled and water-filled workings.

Jan 1, 1980

By P. T. Brooks

This Bureau of Mines study describes a process for recovering nickel, cobalt, molybdenum, and chromium contained in complex waste superalloy grindings that, for lack of an economical domestic recovery process, are being largely marketed abroad. The process, devised by laboratory scale operations, includes scrap preparation, dissolution of metallics in hot chlorinated acidic liquor, carbon adsorption, three successive solvent extraction separations, and selective chemical precipitations. Nearly 90 percent of the nickel, cobalt, molybdenum, and chromium were separated and recovered as oxides, carbonates, and basic sulfate products.

Jan 1, 1969

By Madan M. Singh

Hydraulic mining has been practiced in the United States since 1852 and many mineral commodities, such as gilsonite, phosphates, lead-zinc, silver ores and St. Peter Sandstone can be mined in this manner. In 1958, the U. S. Bureau of Mines initiated research into the mining of coal using these techniques.1-4 These early investigations were conducted in the 5000 psi pressure range. The large nozzle diameters used in this pressure range produced extremely high flow rates which created visibility problems at the coal face, and required removal of large amounts of water from the mining area. Besides, the production rates were not much better than with mechanical methods. This indicated that with higher pressures the water quantities might be reduced using the same or higher horsepowers but enhanced breakage. For this reason intensive investigation in material removal using fine water jets at extremely high pressures (50,000 psi to 100,000 psi) has been undertaken. This was not the entire reason for this contract from the Bureau of Mines, however. The contract objective is outlined later. IIT Research Institute has done pioneering work in high pressure jet development in the United States.5-8 Similar schemes have been investigated abroad. 9-13 Hydraulic mining of coal at relatively low pressures is successfully being done in the Soviet Union, Japan, Canada, and most recently, in Germany.

Jan 1, 1973

By Almon F. Robertson

The floor of Shady Valley, Johnson County, Tenn., is underlain by the Shady dolomite formation. In places the residual clay derived from this formation contains considerable manganese oxides. Nine properties in Shady Valley and two in Doe Valley were prospected by the Bureau of Mines from January 1943 to April 1943. The results obtained indicate that the ore bodies are small and spotty and, that the ore is not well-adapted to gravity concentration. The work of the Bureau was confined to the open end of the valley. One mile northeast of the Ham Greer property, Beaverdam Creek enters a rocky gorge, and it was believed that the few prospects in this area were of secondary impor-tance and, owing to the steep slope and general roughness of the terrain, that exploration with the rite', bucket-drill would be impracticable. A total of 4,398.5 feet was drilled in 131 holes. In addition, 235 lineal feet of bulldozer trenches were cut and 4.5 feet of test pits were sunk. The following nine properties were explored in Shady Valley: Bentley, Walker, Blevins, Scott, North Ham Greer, South Ham Greer, Lipford, Blackburn, and Steagall In Doe Valley, the Gerd Shoun and Brookshire properties were explored.

Jan 1, 1949

By V. E. Homme, M. M. Wong

Tests were made in reactors ranging from 12 to 30 inches in diameter to develop methods for the preparation of sodium chloride - titanium lower chlorides ( dichloride and trichloride ) melts that contain titanium predominantly in the divalent state . Such melts are desirable as a starting material for the production of titanium metal or as an electrolyte for electrorefining of titanium . Sodium reduction of TiCl with an 18 - hour period of holding the reaction products in the molten state produced melts that contained titanium lower chlorides in TiCl₂ - to - TiCl , molar ratio of approximately 8 to 1. Sodium reduction of TiCl in a reactor with a shielded pipe weir , that required no melt -holding period , produced melts with a TiCl₂ - toTiCl , molar ratio as low as 4 to 1 . Reduction of TiCl4 with scrap titanium metal in molten sodium chloride produced relatively pure melts containing about 27 percent titanium in a Ticl₂ - to - Ticl , molar ratio of approximately 4 to 1 .

Jan 1, 1964

By M. B. Bransford

A calculation procedure was evolved by the Bureau of Mines for determining the heat-transfer characteristics of dilute gas-solid mixtures in an externally heated tube. The procedure accounts for differences in gas and particle velocities and covers a range of particle sizes. Heat transfer coefficients obtained by the calculation procedure are compared with values reported in the literature.

Jan 1, 1970

By L. Keith Hudson

The purpose of this study is to provide data that demonstrates that the Alcoa flash calciner design can be used for the decomposition of AlCl3?6H2O to A1203. Heat and material valance data for calcination provides data on the partial pressure of HCl in the off-gases. Experimentally determined data for the HCl partial pressure, over solutions expected in producing alumina from clay by the hydrochloric acid process, show that HCl can be absorbed from the off-gases into process solutions to effect crystallization of AlCl3?6H2O.

Jan 1, 1979

By Jr. Watts, B. K. Cantrell, D. H. Carlson, K. L. Rubow

"The use of diesel equipment in underground coal mines is controversial because ""whole diesel exhaust"" is regarded as ""a potential occupational carcinogen"" by the National Institute for Occupational Safety and Health (NIOSH). Threshold limit values (TLVs) are recommended for the gaseous pollutants; CO, CO2, NO, NO2, SO2, and some hydrocarbons emitted in diesel exhaust. There is, however, no TLV recommended for diesel exhaust aerosols (DEA) nor is there a standard method for sampling these aerosols.The University of Minnesota and the Bureau of Mines have collaborated to develop a personal diesel exhaust aerosol sampler (PDEAS) which utilizes size selective, inertial impaction and gravimetric analysis. During the field tests of this sampler, numerous air quality measurements were conducted in underground coal mines using diesel equipment. The objective of this report is to present these data and to assess the impact of diesel face haulage equipment on mine air quality.Air quality data were collected in four underground coal mines using continuous mining methods with diesel haulage equipment. Daily samples were collected at the section intake, haulageway, and on haulage vehicles. Both full-and partial-shift samples were collected using a variety of aerosol instruments, including the PDEAS and the micro-orifice, uniform deposit impactor (MOUDI) which sample the mine aerosol diesel exhaust fraction. Two of the mines were also monitored for the major gaseous constituents found in diesel exhaust CO, CO2, NO, NO2, and SO2. These measurements were made by either collecting bag samples for subsequent gas analysis or by Palmes dosimeters.The concentrations of CO, CO2, NO, NO2, and SO2, were well below regulated levels. The mine average DEA concentration determined by the PDEAS in the haulageway for the three mines surveyed using this instrument was 0.79 mg/m3, with a standard deviation of 0.19 mg/m3. DEA contributed 65% of the respirable aerosol, at this location. These results were the same as the mean DEA concentrations calculated from size distribution measurements obtained using the MOUDI. This was 0.78 mg/m3, with a standard deviation of 0.22 mg/m3."

Mar 1, 1992

By R. P. Bush

The U.S. Bureau of Mines performed Cu exchange capacity (CuEe) tests on Ca and Na mont-morillonites and attapulgite clays. Mathematical models were developed from the data that the CuEe's are derived from for each clay as a function of pH, Cu concentration, and the concentrations of metal ions, which compete with Cu for exchange sites. An analysis was made of the impact of competing ions on Cu losses due to ion exchange. The results show that the CuEC's of clays, and hence Cu losses, are decreased by the presence of competing ions, and that AI and Mg have the largest impact of those cat-ions normally present in Cu leaching solutions.

Jan 1, 2010

By Charles K. Rose

The Cebolla Creek titaniferous iron deposits near Powderhorn in southern Gunnison County, Colo., were examined by the Federal Bureau of Mines as part of an overall program to investigate the Nation's titanium and iron resources. The deposits occur around the periphery of the Iron Hill stock, which underlies an area of about 12 square miles. Concentrations of magnetite, ilmenite, and perovskite arc localized along fractures in the pyroxenite stock. Mineralogical studies of composite surface samples collected in 1956 showed that most of the iron is present in ilmenite-bearing magnetite. Perovskite is the chief titanium mineral in the magnetite-rich and augite-rich types, and sphene is the principal titanium mineral in the placer material. The mica-rich rock contains approximately equal amounts of perovskite, ilmenite, and sphene.

Jan 1, 1960

By Albert W. Deurbrouck

This report describes the preparation characteristics of the significant, presently producing coalbeds in Mercer County, W. Va. Approximately 650,000 tons of coal was produced in Mercer County, W. Va., in 1960, of which over 630,000 tons was cleaned in four preparation plants. In 1960 the Pocahontas Nos. 3, 6, and 11 coalbeds supplied 99.5 percent of the total coal mined in the county. Because the number of working mines In this county was small, only six samples were collected; four of which were of metallurgical quality as mined. The remaining two samples could be upgraded by washing at suitable specific gravities. Many of the samples taken were of metallurgical quality as mined; however, the float-and-sink analysis on these coals has been included to point out their amenability to the production of premium quality, special purpose coals. In general the coals were low-volatile bituminous in rank with low ash and sulfur contents.

Jan 1, 1963

By Frank E. Cash

Accident prevention is an integral part of the operating procedure of the petroleum industry, and refinery officials and employees throughout the United States are exerting concerted effort to reduce the frequency and severity of accidents and are realizing definite results. In other words, the petroleum industry is safety conscious to a much creator decree than most of the other mineral industries. On January l, 1936, there were 11 operating, refineries in Louisiana with a crude-oil capacity of 199,750 barrels per day.4/ This report deals with safety in four of these refineries representing. 72 percent of the refinery capacity of Louisiana.

Jan 1, 1940

By A. B. Hooker

Many attempts have been made to develop methane detectors that will be safer and more accurate than the flame safety lamps used to detect methane in mines. The development has taken two general forms, namely: (1) Methane detectors, in which the evidence of methane depends entirely upon changes in the appearance of the detecting element, such as a flame or filament; (2) indicating methane detectors or those equipped with scales upon which the approximate percentage is definitely indicated. As an aid in the development of suitable detectors, the United States Bureau of Mines has assembled and published in its Schedule 8B a set of minimum requirements which tests and experience have shown desirable for methane detectors. Any manufacturer may submit his detector for inspection and tests leading to approval under this schedule.

Jan 1, 1930

By William E. Bruce

The Bureau of Mines performed drill calibration tests on two industrial percussive drills of 2-5/8- and 3-1/2-inch piston diameters to determine operating characteristics for their use in conjunction with penetration rate data in developing drillability equations and furthering the knowledge of percussive drills. The use of a linear velocity transducer for measuring piston velocities and application of its instrumentation are described. Data presented include relationships between maximum piston velocity and feed air pressure other results confirm the theory or data of previous investigators, and some comparisons are made with the performance prediction formulas of other investigators.

Jan 1, 1969

By T. F. Mitchell

As a part of the program of investigation of domestic sources of manganese ore, mining engineers of the Bureau of Mines examined and obtained samples of ore from two properties in the vicinity of Bettie Mountain, Lander County, Nev. In addition, samples from three claims in the Carico Lake region, Lander County, Nev., were submitted by private interests. RS the ores were too low in grade to be acceptable for the direct production of ferromanganese, their amenability to concentration by ore dressing was investigated. The Black Bock property is 16 miles south of Valmy, Nev., and is owned by Western Alloys, Inc., Salt Lake City, Utah. The deposit is a replacement of sedimentary rock by manganese oxides. Ore occurs in two main ore bodies designated as the "upper bench" and "lower bench", which could be mined separately. Examining engineers obtained samples from each ore body, and laboratory experiments were made on each sample. The Black Eagle group of claims is in Lander County, Nov., about 43 miles southwest of Battle Mountain. Ore occurs as a replacement of manganese oxides in shale and chert. The 2-ton sample of ore used for laboratory testing was taken by a Bureau of Mines examining engineer from an adit that partly transversed a 28-foot bed of ore. The property is controlled by Western Alloys, Inc.

Jan 1, 1951

By R. V. Lundquist, A. E. Morris, E. L. Singleton

This experimental research was performed to determine rate - of - reaction constants on the MnO - C and Mn , C₂ - 3MnO systems at 1,100 ° , 1,150 ° , and 1,185 ° C. Reactions were conducted at atmospheric pressure under controlled flow of purified helium through the furnace chamber . The weight - loss method defined reduction percentages , and reaction products were identified by X- ray methods . The system Mn0 - C followed a linear reaction rate , and experimental results produced an apparent activation energy of 55.8 kcal per mole of Mn0 . The system Mn, C - 3Mn0 followed a parabolic rate of reaction law and yielded an apparent activation energy of 114.4 kcal per mole for the reaction .

Jan 1, 1964

By M. J. Kovalik, D. E. Wolfson, F. Fischler

Plastometric tests were made to determine the maximum thickness of the plastic layer for different U.S. coals . The effect of test variables on the maximum thickness of the plastic layer was studied . The values for the maximum thickness of the plastic layer were found to be related to the Gieseler maximum fluidity , plastic temperature range , free swelling index , and other plastic properties of coals . Only a general relationship was observed between the plastometric parameters obtained in these tests and the coking properties of coal .

Jan 1, 1964

By Eugene Frey

"INTRODUCTION The Good Fortune mine was sampled by an engineer of the Bureau of Mines in June 1944. Project 984 was set up under the strategic minerals program to make old workings accessible for this sampling program. Actual operations commenced June 1, 1944, and were completed June 30, 1944.The deposit was visited and discussed briefly by Sidney H. Ball 3/ of the Federal Geological Survey in the summer of 1906 and by H. M. Chance 4/ several times from 1887 to 1900.LOCATION AND ACCESSIBILITYThe Good Fortune mine is situated in the Hartville mining district in Platte County, Wyo., approximately 9 miles northwest of the town of Guernsey. The property is about 100 miles north of Cheyenne, Wyo. (fig. 1).ACKNOWLEDGMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metal¬lurgical Branch, O. C. Ralston, chief, analyzes samples and performs beneficiation tests."

Aug 1, 1947