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By Hiroshi Ichikawa

In 2013, Nippon Steel & Sumikin Engineering Co., Ltd. (hereafter referred to as NSENGI), Tenova HYL and Danieli have entered into an agreement to combine ENERGION DR technology into blast furnace technology and/or with syngas technologies. This new alliance will allow the three companies to combine research and development activities with their respective expertise in ENERGIRON DR technology, Blast Furnace technology and Syngas (by-pro gas and coal gasification) technology, with the ultimate objective to develop breakthrough iron making technologies and create such EPC projects. This paper introduces the concepts and the features of our breakthrough technologies of combining of ENERGIRON DR technology, Blast Furnace technology and Syngas technology.

Aug 16, 2017

By Osvaldo Guilherme Comineli

An extensive investigation into the role of low copper contents on the hot ductility of C-Mn-Al steels has been carried out in order to better understanding the problem of “hot shortness”. Previous work has suggested that this problem results from the build up of Cu that occurs at the surface of the steel as a consequence of the preferential oxidation of iron. This causes the formation of a Cu-rich film of low melting point. A nickel addition has been reported as a solution to the problem, since it increases the solubility of copper in the austenite. After hot tensile testing to failure, samples of Cu-containing steels have been examined using optical, scanning and transmission electron microscopes. Recently published results indicate that copper, in addition to precipitating out as CuS, also segregates to MnS inclusions forming a shell around them. This does not seem to impair the hot ductility under an inert atmosphere, but may have serious consequences under an oxidising environment and lead to “hot shortness”. The influence of nickel in improving the hot ductility seems to be due to it forming a higher melting point alloy with the segregated copper. Data from this incomplete work also suggests that Ni reduces the precipitation of CuS particles. Current investigation carried out using confocal microscopy still to be completed will improve the understanding of the role of copper and nickel on the problem of “hot shortness”.

Aug 8, 2018

By Adriano Gonçalves dos Reis

In the development of the structural materials for the advanced applications, as in the aerospace industry, there is a constant strive to increase both strength and toughness. Maraging steels are iron-nickel alloys designed to combine both properties that are achieved through the age-hardening of low carbon martensite. This alloy have a metastable martensitic structure that can revert to austenite when heated in temperatures close to the aging temperature, and this effect can be enhanced with the temperature increasing and time of treatment. Therefore, the study of creep behavior in elevated temperatures has technological importance to the development of this material. In this work the creep behavior of a maraging 300 steel solution annealed is evaluated by carrying out creep tests at 650ºC and in a stress of 200, 300 and 500 MPa. Creep parameters, such as steady state creep rate (?????), final creep time (tf), and stress exponent from secondary creep (n) are determined, considering that they are important to evaluate the creep resistance of the material.

Aug 7, 2018

By Renata Cristina Teixeira

The lubricant oil is a complex mixture of different basestocks and additives. Engine oils evolved from the use of pure mineral basestocks back in the early years of automotive industry to the advent of synthetic, fully formulated, low ash lubricants. This evolution was driven by a number of factors, such as new engine designs, extended durability needs, increased fuel economy needs, environmental concerns, feedstock prices and availability and legal issues. This paper uses technology prospecting on literature and patents databases to allow an investigation on the historical evolution of engine oils. Main basestocks (mineral, hydrotreated, polyalphaolefins, esters) and additives (antioxidants, antiwear, friction modifiers, detergents and dispersants) are characterized according to their research effort. Technology prospecting data is crosschecked against the evolution of engine oil classes, allowing an analysis of how the main drivers push the development of lubricant oil quality. A research effort was identified in late 1990’s until mid-2000’s and related to the adoption of chemical limits for lubricants. Different patterns for the articles and patents publication account for the high value technological knowledge has in this industry. Technology prospecting is seen as a useful methodology for the understanding and forecast of lubricant technology movements.

Jul 31, 2018

By Dalila Chaves Sicupira

A pitting corrosion study of welded joints of lean duplex stainless steel (LDSS) UNS S32304 has been performed. LDSS S32304 thick plates were welded by different processes commonly employed in equipment and piping construction: SMAW (Shielded metal arc welding), GMAW (Gas metal arc welding) and FCAW (Flux cored arc welding). The electrochemical behavior of different weldment zones (fusion zone (FZ), base metal (BM) and heat affected zone (HAZ)) was characterized both independently using an electrochemical microcell and together through whole sample analysis. The electrochemical method applied was performed in acidified glycerin, a process fluid of the biodiesel industry. The results were correlated to the microstructural features of the materials. Based on the results, is possible to conclude that the breakdown potential (Eb) of the fusion zone (FZ) was higher than the Eb obtained for the heat affected zone (HAZ). In general, top samples show higher breakdown potential than root samples and also the samples welded using filler metal 2209 has a better anodic behavior than the filler metal 2307. According to the results, GMAW welding process with 2209 as filler metal was revealed as the optimum chosen for application of 2304 duplex stainless steels in this case.

Jan 16, 2018

By Esteban Ruisanchez Rodriguez

In this paper we will discuss the process of the grain size customization of the EBT filler sand in relationship to the technical characteristics of the furnace and its tap hole. By customizing the grain size distribution, the glassy area formed on the top of the tap hole varies and supports differently the metallurgical pressure of the molten steel providing increased free opening speeds. Taylor made sand improves therefore the free opening rate, reduces the tap to tap time and increases the lifespan of the tap

Aug 16, 2017

By Mariana Macedo de Oliveira Lima, Pedro Emílio Gazola, Andrei Locatelli

Boron steel is used in the industry due to its great wear and impact resistance. During the hot rolling production of 15B29 steel flat bars it is a recurrent problem that the bars will present warping while on the cooling bed. Control this phenomenon is an opportunity to have better productivity, preventing metallic losses. Through the observation of the macro and microstructure samples produced with different reheating temperatures and cooling rates, it was found the presence of residual stresses and cracks on warped bars macrostructure. The residual stresses appearance suggest that the material cooling is too fast. Billets temperature on the reheating furnace of 1230°C reduced to 1100°C and the production pace slowed down. Bars temperature when arriving the cooling bed was reduced from higher than 670°C to 625°C. The results obtained made it possible to produce the material with better quality, reducing the warping effect at the cooling bed. The major influence on the materials warping was identified as the cooling rate at the cooling bed and the reheating furnace temperature was adjusted to provide a homogeneous temperature along the bars.

Oct 1, 2019

By Jefferson Lisboa Lelis, Marcos Roberto Soares da Silva, Maiara Rodrigues Gouveia

Nowadays, due the development of new hot rolled strips at USIMINAS, established the necessity of realizing studies to define new parameters for the welding machine of new pickling line, in order to improve mechanical and metallurgical properties of these materials. The aim of this study was to evaluate the weldability of high strength low-alloy steel with low boron content with tensile strength above 600MPa.The influence of energy input and preheating temperature on the mechanical properties of hot rolled strips were analyzed at three distinct thickness (2, 4 and 6 mm). To perform these evaluations were used tensile test, micro-hardness, metallography (micro and macro examination) and scanning electron microscopy analysis. In resume, a good welding performance was achieved, increasing preheating temperature and the welding energy higher than 60%.

Oct 13, 2019

By William Sergio Flores Roman

Los aceros para armaduras de hormigón tienen que exhibir una buena relación entre resistencia y tenacidad que se ve reflejado en la performance del producto en servicio al ser aplicado a esfuerzos exigidos. Acerbrag es una empresa que produce aceros para la industria de la construcción teniendo en su gama los aceros de medio carbono para la fabricación de barras conformadas de dureza natural para armaduras en estructuras de hormigón. El objetivo de este trabajo es encontrar criterios de ventanas de trabajos operacionales y de control para la manufactura de aceros con buenas propiedades mecánicas en términos de resistencia y tenacidad. Este paper muestra los resultados de los trabajos realizados en las diferentes áreas productivas para conseguir un producto final con mayor resistencia a altas exigencias en servicio, además, reporta diferentes aspectos del proceso de manufactura del producto que van desde el ajuste de la composición química del acero, incluyendo criterios de propiedades mecánicas objetivos, criterios de calidad interna mostrando la microestructura de la barra antes y después de los cambios y finalmente la calidad dimensional y superficial de la barra nervurada, este último potenciando la falla prematura del material. Todos estos cambios, se ven reflejados finalmente en la performance de la barra, sometida a los nuevos criterios de exigencia en los ensayos mecánicos.

Oct 30, 2017

By Franz Reufer

At Rogesa in Dillingen, Germany, a joint venture company of AG der Dillinger Hüttenwerke and Saarstahl AG and at Salzgitter Flachstahl GmbH in Salzgitter the sinterplants are equipped with the Paul Wurth EFA™ process for the final sinterplant off-gas cleaning. In Dillingen two and in Salzgitter one EFA™ plant are in operation at the respective sinterplants to comply with the very stringent environmental rules prevailing in Germany according to the German Clean Air Act called “TA Luft”. The main target is to eliminate or reduce emissions like dust, sulfur components, dioxins/furans and others in the sinter process off-gas. Since 2006 and 2011 the two EFA™ plant are in operation at Rogesa while the EFA™ plant in Salzgitter was also commissioned in 2011. These installations significantly contribute to the improvement of the emission situation of the Dillingen and Salzgitter Works. The EFA™ technology is the state-of-the-art process for such kind of application in terms of additive and energy consumption, reliability and availability. The report gives an overview of the EFA™ process and the performance results of the Dillingen and Salzgitter plant.

Aug 1, 2018

By Ruediger Holz, Tommaso Settimo, Luciano Vignolo

Optimized CAPEX, OPEX, new products, yield and product quality in new process equipment as well as by upgrading of existing facilities are the key factors for success and profitable operation. For this, innovation in processes and design is crucial. Danieli can support their clients by offering innovative and well-thought-out process equipment and upgrade solutions. In 2018, Danieli has put into operation a complete cold processing complex in Turkey, which includes a new continuous pickling tandem mill featuring latest generation of market oriented technologies. In this line, dedicated to run a broad range of size and grades (IF to AHSS as DP1000), the highly efficient Turboflow® pickling process was selected. This technology already proved its efficiency and ability in former applications handling ultra-thin gauges at speeds even exceeding 400 m/min in the pickling tanks. The 5-stand 6-high OSRT tandem mill features important developments, like actuators to improve significantly strip flatness and a special air knife arrangement on the tandem mill exit side to generate perfect strip surface cleanliness. In galvanizing lines, the zinc pot is the most effective area to reduce costs in operation and consumables and increase the product quality. Danieli has spent significant efforts in developing most advanced technology for the wiping process. A fully integrated system solution has been designed to perform a wiping process with high quality, economy, accuracy and productivity. Center part is the newly developed X-Jet / Compact X-Jet air knife, added by new generation electromagnetic stabilizer as well as robotic systems to reduce human intervention and health risks in this area. This technological package is ideal also for upgrade of existing lines, typically generating a return of investment less than 1 year. On top, Danieli has developed advanced automation systems including L2 and L1 controls to achieve outstanding product performances.

Oct 1, 2019

By Daniel Augusto Godinho de Carvalho

At thyssenkruppCSA, a positive heat balance at BOF process is faced, mainly because of low utilization of scrap and plant design. A singular logistic concept for hot metal transport between blast furnace and steel plant was established to optimize transportation and energy balance. Up to 80 kg of iron ore pellets/t steel is necessary for 340t BOF heat balance. In order to accomplish this challenge a stable blowing process, intensive operational development have been successfully executed: slopping rate reduction of 80% achieved without changing the blowing time. This paper describes steps and results of this development.

Oct 30, 2017

By Wolfgang Kern

More and more coke oven plants worldwide face the task to improve their emission reduction at their coke oven batteries. In the 90’s PROven® was invented and developed by DMT to regulate the inner pressure of a single coke oven chamber. Generally, most of the coke oven chambers can only close and open their connection to the collecting main but without the possibility to regulate the pressure during the carbonization time. Through the installation of PROven® the load on the coke oven door sealing system and the charging lids will be decreased and so does the emissions of crude COG as well. The current PROven® system, installed in the collecting main, does not only regulate the chamber pressure, it replaces the valve between the goose neck and the collecting main, too. This variable pressure control allows decreasing the leakages at the emissions sources to a minimum and allows operating the collecting main under optimum pressure. Subsequently, this will lead to enhanced emission reduction. PROven® proved its value with more than 2,100 units installed by licensee worldwide. Nevertheless, DMT is always focused on its client’s needs and therefore enhance PROven® to provide the Best Available Technique (BAT). Among the main features of the now available system is the plain arrangement with a higher reliability and the possibility to install the system outside of the collecting main without modifying it. Hence, upgrading coke oven plants during operation is possible without any noticeable impact on the plant operation.

Aug 1, 2018

By Douglas Glenn Stalheim

Production of structural steel with a minimum yield strength of 700 Mpa produced as hot rolled coil has become increasingly popular due to cost considerations when compared to quench and temper equivalent product. This grade when produced as hot rolled coil requires the use of microalloy precipitation strengthening mechanisms. This is typically a combination of niobium and titanium microalloys. While the metallurgical concept of structural steel precipitation strengthening mechanisms has been well researched and published, actual implementation into the production process can be very challenging. In addition to achieving a minimum yield strength of 700 Mpa, in many applications additional mechanical property attributes of formability as measured by hole expansion testing along with low temperature toughness properties are now required. Achieving a balance of all the mechanical properties in a stable and repeatable performance in production using microalloy precipitation strengthening mechanisms further increases the challenges. This paper will discuss the metallurgical/process strategies required to successfully produce 700 Mpa minimum yield strength hot rolled structural steel coil. In addition, the role and goals of both niobium and titanium in this product design will be presented.

Oct 30, 2017

By Ivan César Lopes Diniz, César Romero Afonso Goulart Júnior

Mandrels are tools applied to manufacturing seamless tubes. In VSB plants (Vallourec Soluções Tubulares do Brasil), it is used in two mills. Mandrel and PQF Mills. This is an expensive tool due its alloy (hot work tool steel – AISI H13) and lengh (between 12 meters and 22,5 meters). An opportunity to apply mandrels from PQF in Mandrel Mill has been identified. However, mechanical properties of PQF mandrels must be improved. This work presents the heat treatment process of Quenching and Tempering developed internally at VSB to improve PQF mandrel properties aiming to achieve Mandrel Mill requirements. Hardness and metallography tests were performed before and after some steps of the heat treatment to characterize and validate the process.

Oct 5, 2019

By Alexander Fleischanderl

Steel market has become somehow unpredictable and requires quick adjustment in production conditions to survive in the harsh market environment. Steel production is not anymore driven by output records, but by efficient cost reduction measures to remain competitive under strongly varying production conditions. Energy efficient production and flexible raw material scenarios have become decisive factors to succeed and survive in our industry. Such scenarios have to be carefully investigated to be well prepared to adopt production steps continuously. The paper analyses various process opportunities to optimize energy and raw material consumption in the production route. Off-gas treatment systems have still a huge untapped potential to recover energy from the hot waste gases. This is valid for the EAF mini mills as well as for the integrated route. Various examples for waste heat recovery systems including resulting benefits are discussed for the EAF, agglomeration, blast furnace, direct reduction and BOF. New innovative bag-filter systems feature extremely low emission levels at lowest pressure loss and sound emission conditions. Also improved control and automation solutions support the operators to minimize the operation and maintenance costs of their off-gas system. Steelmaking by-products shall not be considered as residues, but as a valuable and cheap raw material source. The paper presents some show cases how to valorize slags as well as utilizing coke and iron oxide fines to increase productivity and minimize raw material cost. A new process for highly flexible converter steelmaking allowing for extraordinary high HBI and scrap rates above 50% and improved yield is discussed and evaluated

Oct 30, 2017

By Eric Yoshimitsu Sako

One of the main difficulties in the operation of trough and runners at Arcelor Mittal Tubarão (AMT) Blast-furnace no.02 is the reduced amount of time available for repair procedures. The consequence is that the castable installation must often be performed during hot conditions and the installed castable could easily detach from the base material during the early stage of operation, exposing the previously oxidized base material to molten iron and corrosive slag attack. When events like this happen, emergency repairs must be executed, resulting in increased refractory unit consumption and an unplanned shutdown of unit operation. Considering these targets, Nippon Crucible Co. and Saint-Gobain HPR Brazil have developed a high-performance Al2O3-SiC-C composition based on an entirely novel anti-oxidation technology. Oxidizing reactions could be attenuated by adding an oxidant inhibitor and a water reducing agent. As a result, the open porosity was significantly reduced, resulting in an improvement of campaign life in terms of pig iron throughput when compared with the regular castable. An analysis of this life improvement showed successful results for the material after 250 days of campaign. The main reason for such successful results was that the deterioration caused by the oxidation was significantly less and that this change made on the high cohesive structure of the base material was maintained for a long time. The attained results allowed Arcelor Mittal Tubarão to achieve longer trough campaigns, and avoid any unplanned stoppages with zero breakdown risks.

Oct 30, 2017

By Jan Lückhoff

The introduction of the EAF Quantum furnace by Primetals Technologies represents an important milestone in the field of electric steelmaking during the last 15 years. In this process the latent and chemical heat of the off-gas generated during a melting process in an EAF is used to pre-heat scrap in an integrated shaft prior the melting of the scrap in the vessel. Combining proven own technologies, Primetals EAF Quantum enables nearly continuous process, cutting down idle times and enhancing availability for production. The essential benefits will be shown in this Paper.

Aug 16, 2017

By Andreas Cestonaro

Roll grade evolution in plate mill applications is traditionally following the development in hot strip mills. New grades normally find their way into service only after being successfully implemented in hot strip production. The majority of the plate mills worldwide are using work roll grades that have been invented before the 1980’s. But today the demands in the mills are pushed by sophisticated product mixes and longer rolling campaigns. The result of this development is a higher wear rate on the work rolls and as a consequence roll hardness is increased and advanced roll materials are used. The backup rolls are also affected by this. The wear rate is higher and the mechanical impact in terms of contact pressure and work hardening is increasing. This paper outlines the results of the roll grade development at Gontermann-Peipers and introduces new materials for work and backup rolls for plate mills.

Jul 30, 2018

By Michel Rodrigo Luiz, Glaudistoni da Silva Félix, Osmar Duarte Junior

This article deals with a project to reduce the preparation time and threading the coils in the input section of a pickling line coupled to the cold strip mill (PLTCM) at ArcelorMittal Vega. The project developed serves for the detection and elimination of bottlenecks in the input section. The project was conceived by the philosophy of the Theory of Constraints (TOC) and Lean Six Sigma (6 sigma), here seen as sequencing serial / parallel in the preparation and threading the coils. In this context, a proposal to modify the automatic sequencing and reduction of interruptions due to failure of the automation / equipment confirmed its effectiveness reducing the total time preparation time and threading the coils in the entry section by 15%. This project was developed without investment costs, bringing gains on the order of US$613,769.00.

Oct 1, 2019