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By G. Merazchiev

In the selection of copper ? molybdenum concentrates with the use of reagents containing sulfide ion ? sodium sulfide, sodium hydrosulfide etc for depression of copper minerals and pyrites, big part of depressor is oxidized by oxygen, which is dissolving in pulp during aeration with air in flotation machines and it is expended unproductively. This is the main reason for the big expenditures of depressor, reaching up 15~20 kg/t collective concentrate and the high exploitation expenditures for the copper ? molybdenum selection. Effective direction for lowering expenditure of depressor and increasing of the technical ? economical effectiveness of moly production is the conducting of the selection in nitrogen medium. In the paper are shown the results, obtained by applying of this direction in selection of collective copper ? molybdenum concentrate from the porphyry copper deposit ?Ellatzite? ? Bulgaria, in which the ratio Mo:Cu is over 1:120. In laboratory conditions, through comparative experiments in medium of air and nitrogen are defined: expenditure and initial concentration of NaHS in pulp for effective depression of copper minerals and pyrites; kinetics of flotation process of molybdenite; influence of pulp density; emf (negative milivolts) of pulp and the expenditure of nitrogen on tech-nological indexes of molybdenum flotation. When working in nitrogen medium decrease of NaHS in rougher molybdenum flotation from 40% to 45% is settled. When nitrogen is also fed in cleaner stages, the total expenditure of depressor is lowered by 64%. The quality of end molybdenum con-centrate is raised with over 5%. On the ground of the results of laboratory studies and of world practice data, an industrial installation for selection of copper ? molybdenum concentrate in nitrogen medium in Wemco inert ? gas machines.

Jan 1, 2014

By H. Lieberwirth, M. Hesse

"Selective comminution (SC) is beneficial for the treatment of primary raw materials, especially if it is utilized in the pre-concentration process. Pre-concentration processes are applied in mineral processing to relieve subsequent processes and to achieve a higher efficiency. SC is also a promising method for the treatment of low-grade ores and waste dumps. With SC, various components can be separated such as valuable minerals from waste, ore from wall rock and different ore varieties within a deposit. SC is a property of a comminution system and leads either to a preferred crack propagation in one component (called preferential breakage) or to a preferred crack propagation along the grain boundaries (called interfacial breakage). SC results from different comminution behavior of various components in the feed material. For mechanical comminution, the preferential breakage seems to be the most important case of SC. Hereby SC generates only the difference in the particle size which can finally be used as a sorting parameter. A sorting process which uses SC depends on three parts: the feed material, the comminution machine and the separation machine. The feed material defines the potential for SC. Differences in properties like strength, toughness and density which are related to comminution are often used. The comminution machine has to exploit this potential. The extent of the exploitation can be influenced by the machine design, material and operational parameters. After SC, the various components are still combined in the product. So ultimately, a separation machine is needed. At preferential breakage, a simple screening machine can be used. The basics about SC will be presented at first. This contains relationships between material properties, the kind of loading in the comminution machine and the SC effect. These basics can be used for example to exploit a potential to SC for a pre-concentration step or to avoid the SC for a higher efficiency of subsequent processes. Based on recent investigations with impact load, the influence of the important parameters compressive strength, density, particle size and impact velocity to the SC will be shown, using examples of lead-zinc ore comminution and fluorspar processing."

Jan 1, 2018

By Leena Vesa, Antti Remes

Design of thickeners is based on laboratory test work, characterizing the material and determining the optimal reagents, dosages and settling regimes. Several methods for dimensioning plant scale equipment exist. Kynch and Talmage-Fitch design procedures has been applied widely for a long time. Nowadays, besides them, a dynamic laboratory test work is applied for design of high rate thickeners. In that the laboratory unit is operated with known solids load per area, feed and flocculation conditions and with raking of the underflow. All these test methods afford useful data for setting up and calibrating a dynamic simulation model of a plant scale thickener. This paper presents a flocculation kinetics based dynamic thickener simulation model and a procedure to calibrate the model parameters. With the model, the underflow stream composition can be simulated over time as a function of the thickener operating parameters, which are: the feed rate and composition, underflow pumping rate, flocculant dosage and dilution of the feed. In addition, the model incorporates calculation of the slurry bed level, the cone pressure, the yield stress and the rake torque. Such a dynamic modeling scheme enables setting up simulation aided operator trainings and developing and testing of advanced control strategies, for example. The unit model can be integrated as a part of concentrator-wide flow sheet simulation model as well. Here, calibration of the kinetic flocculation model based on a laboratory test case data and further the operation of a simulated plant scale thickener are presented.

Jan 1, 2014

By Heinrich Hutchison, Thomas von Moltke, Roelof F. Sandenbergh, Katarina P. Cerovic

Although the cyanidation process for gold leaching has been applied for more than a hundred years, some aspects of it, such as the passivation of the gold and the depassivating action of heavy metals, are still not well understood. In this work the anodic behaviour and surface composition of gold in alkaline aqueous cyanide with lead additions were investigated using polarization experiments and XPS. It was found that lead in the solution activated the gold at low concentrations, somewhat more positive than the reversible potential for gold, but that the activity again decreased at higher concentrations of lead. The potential range for the activation of the gold coincides with that where underpotential deposition of lead occurs, i.e. –200 to –600 mV(SCE), as indicated by the surface composition of the gold, shown in figure 1. Note that the concentration of lead on the surface of the gold only increased with time in the bulk plating potential range for lead, where gold is not activated by the presence of lead. It is also shown that up to 20 mg/L of lead added to the solution will activate the gold, provided that bulk plating of the lead is avoided. It is also important to avoid reducing conditions during leaching, where bulk plating of lead may occur, if the gold is to be activated by lead to achieve a high leaching rate, as the bulk plated lead screens the surface rather than activating it.

Jan 1, 2003

By Christopher Greet, Alfred Van den Bosch

"A range of media alloys with different chromium content has been developed for different milling applications. When selecting the grinding media alloy for a specific application, consideration must be given to the mineralogy of the ore as well as the water chemistry and mill operating conditions. The paper describes the influence of the microstructure of the alloy on the wear resistance and the influence of the chrome content on the pulp chemistry and downstream processing. It also provides information about the in-house tools which Magotteaux have developed to predict the media wear rate with different chromium content alloys and predict their flotation efficiencies that can be expected when the right alloy is selected for a particular application."

Jan 1, 2014

By Andrei Kolesnikov

"The results of CFD modelling of complex heat transfer and fluid flow in DC electric arc furnace are presented. The model includes energy and momentum conservation equations for gas phase (freeboard), liquid phase (molten bath) and solid phase (walls and graphite electrode). Simulation revealed the temperature distribution in all elements of the furnace. The influence of the arc and melt resistance on the temperature distribution is discussed.Computational Fluid Dynamics (CFD) becomes a powerful tool for better understanding of the heta and mass transfer processes in industrial equipment. In current work commercial CFD software STAR-CD was used to analyse complex heat transfer in DC EAF, including forced and natural convection, conduction and radiation. The finite volume solver using body-fitted grid was used. The grids are non-staggered hexahedral grids and all variables are evaluated at cell centers. Steady-state calculations were performed with PISO algorithm. For the convective terms in equations the hybrid differencing scheme was used. An upwind differencing scheme was used for other terms. Conjugative heat transfer was taken into account in heat transfer calculations on gas-liquid and gas-solid interfaces. Radiation from the arc and inner surfaces of the furnace was calculated by a “discrete beam” approach. Source term in energy conservation equation was used to represent heat release in the zone occupied by the DC electric arc. The volume of this zone was calculated from semi-empirical equations. The Joule heat and heat due to chemical reaction in the melt were calculated through the source term expression in the energy balance equations for the slag and metal in the molten bath. The gas acceleration in the electric arc zone and stirring of the slag due to gas bubbles motion were accounted for by momentum source terms in the momentum conservation equations.All simulations were carried out using axisymmetric two-dimensional grid. The grid resolution was 20 cm per cell in most part of the furnace, except the arc region, where resolution was 5 mm per cell."

Jan 1, 2003

By Anatoly N. Vinogradov, Vyacheslav A. Tsukerman

The North-West Russia for 70 years is one the main producers of Cu, Ni, Co, Al, P, REE, Zr, Ti, Ta, Nb, Fe ores and other minerals in the Europe. The largest mining companies locates in the Murmansk region, and they extracts about 100 mln. tons of ores and damps up to 250 mln. tons of waste annually. Nevertheless an environmental situation in the region is stable due to rational management and treatment of wastes on a base of the Noosphere Concept for Nature-using suggested by Vladimir Vernadsky. The Concept was performed practically in the Fersman’ scheme of “non-waste mining and metallurgical complex”, published in the monograph “Minerals of the Kola Peninsula: current status – analyses – prognoses” (1941) and served till now as a sort of “Bible” for industry managers lightening a strategy for an industrial “trophic chain”. The recent status of this scheme is shown on the picture below, and one can see that our concept is coincide with modern ideology known as the “Industrial Ecology”. Moving along this mainstream in the Kola Peninsula since 1929, when the first mining company “Apatit” was established, we provided the water close circuit in mineral dressing plants, hydrometallurgical treatment of slag and tailings, productions of building materials and adsorbents of wastes. The innovation set of technologies designed by the Kola Science Centre allow recently to involve tailing damps in re-exploitation as the technogenic deposits of valuable raw materials for fertilizers, tanning and cleaning agents, pigments, concretes and etc.

Jan 1, 2003

By Zhaohui Qiu, Yaguan Ji, Hong Zhong, Qingxia Liu, Yada Liu

"Water is a necessary process medium in mineral processing. For the operations where fresh water is not available, sea water could be used as an alternative processing medium to replace the fresh water if we would have built a solid understanding of the interfacial science and flotation chemistry of sulfide minerals in sea water. In this research, micro flotation of chalcopyrite and pyrite in deionized water and sea water were investigated. For chalcopyrite, the recovery starts to drop from pH 10 in deionized water and from pH 9 in sea water, and the flotation recovery close to 100% before it drops. We can found from the results that chalcopyrite flotation is depressed much at pH 11 in sea water when much white precipitate is found. For pyrite, the flotaion recovery changs a lot in deionized water with 1*10-5 M potasium amyl xanthate (PAX) as collector. It’s relatively high at pH 8~10 compared with that at pH<8 and pH>10. While in sea water, the trend is almost the same as that of chalcopyrite. Zeta potential measurements and chemical equilibrium calculation were used to find out that magnesium hydroxide species coats on the surfaces at high pH in sea water are the main reason for depressing the chalcopyrite and pyrite flotation. Through understanding the interfacial science and the solution chemistry of sea water and its impact on processing efficiency, this research will not only helps reduce the use of fresh water to minimize the disposal of spent water for environment protection, but also enhance the recovery of valuable minerals in froth flotation."

Jan 1, 2014

By J-P Franzidis, P. O. Gyebi

"Coal-water mixtures (CWM) of concentrated fine coal may be transported in pipelines but this is influenced by both CWM rheology and stability. Here, a low viscosity is required to reduce power requirements, as well as good stability for transport and storage. The objectives of this study are to investigate the importance of surface charge, solids concentration and dispersant addition on the rheology and stability of a fine Witbank coal-water mixture (<75 m). Zeta potential, rheology and stability were measured with a Malvern Zetasizer, a AR1500EA rheometer and a static rod penetration test, respectively. Sendep 30D, Sendep 30F and Norilose 8058, all supplied by Senmin International, were used as dispersants, at dosages of between 0.1 to 0.5% dry coal (w/w). Solids concentration was varied from 10 to 58% (w/w). The zeta potential was found to be positive at low pH and decreased sharply with increasing pH to a minimum of -50 mV at pH 10. The zeta potential decreased with increasing dispersant concentration for all dispersants. The lowest zeta potential of -63 mV was obtained for Norilose 8058 at a dosage of 0.3%. CWM rheology was Newtonian at lower solids concentrations but became non-Newtonian at solids concentrations over 40% (w/w), with an initial yield stress and pseudo plastic behavior. The yield stress decreased sharply with increasing dispersant concentration for all dispersants. The lowest yield stress was obtained for Norilose 8058. The addition of dispersants resulted in significant improvements in stability. A penetration ratio of over 70% was obtained for Norilose 8058 after 10 days. In summary, the addition of dispersants resulted in a decrease in the zeta potential which increased the electrostatic repulsive forces between particles, thus improving both CWM rheology and static stability.INTRODUCTION Coal Water Mixtures South Africa’s energy economy depends heavily on coal. It accounts for about 70% of primary energy consumption, 93% of electricity generation and 30% of liquid petroleum fuels (Eberhard, 2011). The transportation of coal to export markets and power generation stations is a problem in the South African coal industry due to ageing and inefficient rail infrastructure. This problem is intensified by the long distance of coal haulage, delays in the time required to load and unload wagons, and environmental challenges related to air pollution and water contamination. Fine coal may be transported more efficiently and economically in a pipeline as a highly concentrated coal water mixture (CWM). Typically a fine coal CWM will contain 60-75% coal, 25-40% water and nearly 1% of dispersing additives (Atesok et al., 2005; Dincer et al., 2003). However, the transport of CWMs in pipelines is strongly influenced by both CWM rheology and stability. Here, a low viscosity is required to reduce power requirements, as well as good stability for transport and storage. These quantities are affected by the coal composition/mineralogy, solids concentration, particle size and size distribution, particle shape, inter-particle forces and dispersant type and dosage (Laskowski, 2001)."

Jan 1, 2018

By Julian Dimitrov, Kremena Dedelyanova

"The paper presents research on hydrodynamic processes occurring at the elementary act of flotation. Discussed existing models to determine the effectiveness of conflict of bubbles with particles in vibration column flotation machine. The paper presents a disperser for a column flotation machine, in which the dispersion of the gas phase is carried out using vertical vibration with defined frequency and amplitude. The paper presents research of mechanism for the creation of air bubbles in vibratory column flotation machine. The factors influencing the increase in the duration of the bubble in the area of contact with the mineral particles are discussed. Research was carried out on the effect of frequency and amplitude of vibrations on speed of precipitation of mineral grains of different density. Formulas are derived for the parameter effect of vibrations, applicable to the design of flotation machine. The collision efficiency of the bubbles in vibratory column flotation machine is determined. The vibrations of the hydrated layer allow for cost-effective implementation of the elementary act of flotation by providing larger relative velocities at the contact point between the bubble and the solid phase. It is proposed to complement the model more accurate representation the mechanism of attachment of the particles to the bubble."

Jan 1, 2014

By P. A. Harvey

Previous studies have reported that inorganic electrolytes can enhance floatability of coal. The research has shown that the enhancement, if any, is highly dependent on changes in solution pH, type of electrolyte, and electrolyte concentration. The reasons for this are still not clear. In this study the floatability of coal particles in mono and divalent salt solutions was investigated. The zeta potential and hydrophobicity of the coal was measured experimentally, and a modified Hallimond tube was used to determine the floatability of coal particles by single bubbles, where the collision efficiency was equal to unity. The experimental information was used in conjunction with the Hogg-Healy-Fuerstenau equation to quantify the electrical double layer interaction. It was found that for low electrolyte concentration (less than 0.1 M) solutions the flotation recovery of coal particles was less than that for distilled water, and decreased with increase in concentration. Conversely, at electrolyte concentrations above 0.1 M, flotation recovery increased with increasing concentration (Figure 1). Both of these results are consistent with previous observations, but are inconsistent with expectations when considering the possible influence of electrical double layer interaction. Modelling of the system indicates that the electrical double layer is compressed with increasing electrolyte concentration, resulting in an increase in flotation recovery due to a diminishing of the (electrical double layer) repulsion between the bubble and the coal particles. Moreover, for electrolyte concentrations above about 0.1 M the electrical double layer is completely depressed and would have little further influence, if any, on the flotation process. Therefore, the electrical double layer interaction is not the principal determining factor for the flotation of coal in electrolyte solutions.

Jan 1, 2003

By Nicolás Caussade

"The IMPC 2014 slogan "Optimizing Water and Energy Usage for Sustainable Mining" refers to the ever decreasing availability of fresh water and energy, which has turned out to be a crucial aspect in assuring the competitiveness of the mining sector in Chile and the Andes region in general. The concern for sustainability and the supply of water and energy is nowadays part of the top priorities of mining countries and communities. This is also the case for Antofagasta Minerals. Several years ago its mining group implemented an energy policy based on intelligent, strategic and sustainable management, in order to successfully face the challenges imposed by the market. It is called an intelligent policy because it intends to provide energy through a diversified range of sources, which includes the development of in-house alternatives. It is also a policy focused on efficient energy consumption and one that is strategic. Because it is in line with the characteristics of the mining activity, it is developed for the long term. Finally, what makes the policy sustainable is that it gives priority to energy usage from renewable resources and as such, the required capacities have been developed to generate innovative solutions that respond to the restrictions that characterize the industry today."

Jan 1, 2014

By Stefan Mutz, Thomas Pretz, Jörg Julius, Frank Hilbk-Kortenbruck, Aachen, Hartmut Harbeck

"The annual global production of primary aluminium was about 22 million tons in the year 2000. This represents the second largest production rate in the world market after steel. Experts are predicting that the global demand for aluminium will rise in the near future.In contrast to other metals such as copper, the recycling of aluminium is considered relatively difficult. There are two main alloying groups, namely cast and wrought. In the case of aluminium it is important that the constituents within the scrap aluminium to be smelted are clearly identified. Within the secondary remelting process alloying does take place, but a removal of unwanted metal constituents is problematic. Therefore mixed aluminium scrap (not genuine in-house collected material) can only be used to produce cast aluminium. Thus, in other words a down-cycling of wrought (extrusions and rolled) products occurs. However, in spite of these difficulties there is an increasing trend to produce aluminium from secondary scrap (approx. 35% in Germany). Similar trends have been identified in the USA and other industrialised countries. This development is mainly caused by the high energy consumption for the production of aluminium from bauxite. Producing aluminium from scrap is saving about 95 % of the energy in comparison to the processing of primary raw materials.An improvement in sorting technology is necessary to separate wrought and cast alloys of aluminium as the absolute amount of recovery from old scrap is higher than the demand for cast.This contribution presents some alternative methods, utilizing automatic picking technologies, which will be used to separate secondary aluminium in the future. During the recent years, some major progresses have been made in automatic picking technologies for different applications in the processing of primary and secondary materials.For the sorting of aluminium scrap a special additional sensor will be necessary. The best detection will ultimately be based on online elemental analysis of single particles. First investigations in the field of laser based systems for these applications have already been performed several years ago. One of the laser based techniques is the laserinduced breakdown spectrometry (LIBS)."

Jan 1, 2003

By Sanja Miskovic, Manjunath Basavarajappa

Numerical investigation of fluid flow characteristics and mixing efficiency of different impeller designs, based on the mixing characteristics of a passive scalar/tracer, is conducted using CFD for lab scale flotation cells of diameter D and height H equal to 300 mm. Fine computational mesh containing close to 1.6 million cells is used to obtain fully resolved steady state flow field close to the impeller. Unsteady scalar mixing simulations are performed on a relative coarse grid consisting of approximately 450,000 cells. Based on detailed numerical simulations, flows are fully characterized for four impeller designs at two off-bottom clearances C of 50 and 25 mm (D/6 and D/12). Passive scalar is injected from the cell bottom and the time required to attain uniform concentration distribution inside the cell volume is taken as the mixing time by monitoring scalar concentration at four discrete locations. The effect of varying agitation speed and off-bottom clearance on mean flow characteristics is also investigated. The scalar mixing results reveal regions of low mixing efficiency and are used to understand mixing process in greater detail. Through the previous research work, it was found that the main flow pattern undergoes transition from double-loop to single-loop configuration with decrease in off-bottom clearance below a certain critical height for stirred tanks using flotation impellers in the absence of stator. The inclusion of stator is found to alter the mean flow behaviour by preventing the jet from transitioning to axial type flow for lower clearance. Power numbers for different impeller designs are calculated based on the torque generated on impeller blades, and also from the total turbulent kinetic energy dissipation in the overall fluid volume. Power number is found to exhibit a significant dependence on off-bottom clearance based on the CFD results.

Jan 1, 2014

By Andrzej Luszczkiewicz, Magdalena Duchnowska, Jan Drzymala

A selected flotation system of beneficiation of the copper ore at KGHM Polska Miedz S.A. has been analyzed in the article. It was found that a proper assessment of upgrading must be based on two elements, that is the upgrading process selectivity and working point of the considered flotation unit, both determined, preferentially by means of the Fuerstenau recovery-recovery upgrading curve. The Cu recovery - non-Cu components recovery upgrading curve was selected for calculations because its background lines (no separation and ideal separation) are insensitive to changes in the grade of feed of the processed material. This approach allows a comparison of upgrading results for feeds having different grade, being upgraded in various flotation machines and under different physicochemical conditions. It was shown in the paper that the main criterion for comparison of two working in parallel systems is selectivity of upgrading. However, when two flotation machines, despite of the same selectivity, produce concentrate and tailing of different grades, it is necessary to analyze their working points using upgrading curves. The proper position of the working point depends on the criterion imposed on the process and is a result of not only basic parameters of the upgrading process such as feed, concentrate and tailing grades but also on economic parameters such as costs associated with the production of concentrates and the time needed for their production.

Jan 1, 2014

By Edgar Schach, Tom Leistner, Markus Buchmann, Urs A. Peuker, Martin Rudolph, Marius Kern

"In this study, the flotation characteristics of a cassiterite-bearing fine-grained and complex skarn ore from a deposit in the Ore Mountains is investigated. The tests are performed using an oil-assisted column flotation approach to process very fine ore fractions and avoid losses of cassiterite into the tailings. First, process parameters are obtained for a finely ground artificial mixture of quartz, magnetite and cassiterite, simulating the real ore. Thereby, magnetite is used, as iron oxides can have a detrimental effect on the flotation due to a similar flotation behavior. In addition, they can act as a source of multivalent ions, which are known to reduce the concentration of collector molecules, active for flotation. Based on the results, selected parameters are further tested for cassiterite skarn ore from the Hämmerlein deposit including a pre-conditioning and a water exchange step to remove ionic contaminants. The process response is analyzed in detail by XRF (X-ray fluorescence) and MLA (mineral liberation analysis) to get a better understanding of the behavior of the single ore components. Sulfosuccinamate type surfactant is utilized as the collector, emulsifier and to reduce the froth destabilization through nonpolar oil. Sodium hexafluorosilicate is added as the depressant.INTRODUCTION Complex skarn ore deposits containing considerable amounts of tin, indium and other metals are located in the Ore Mountains region (Germany). In this study, a skarn ore from the Hämmerlein deposit was investigated. Due to the finely disseminated nature of this ore, past beneficiation attempts failed, and the ore was considered economically unprocessable. However, increasing resource demands brings it back into focus (Schuppan and Hiller, 2012). Cassiterite is the main tin bearing mineral in this ore. Due to its high density (~7 g/cm³), the predominant beneficiation technique is gravity separation (Angadi et al., 2015). Tin ores from disseminated deposits have to be extensively comminuted to reach a sufficient degree of liberation of the cassiterite grains. As cassiterite has a brittle nature, it is preferable enriched in small size fractions, during comminution (Angadi et al., 2015). Gravity separation methods become more and more inefficient for particles smaller 40 µm (Falcon, 1982), causing tin losses of up to 30 to 40wt.-% (Angadi et al., 2015). Thus, froth flotation of cassiterite was first utilized in Altenberg in the Ore Mountains as an additional processing step to reduce the cassiterite losses into gravity separation tailings (Bulatovic, 2010; Gruner and Bilsing, 1992). Although the reported lower size limits for an effective cassiterite floatability are often smaller compared to other minerals, the flotation performance is in general decreasing for small particle sizes < 10 µm (Trahar and Warren, 1976). Therefore, different approaches have been already investigated for the flotation of such fine cassiterite fractions to overcome the limits in particle size. Bilgen et al. investigated the shear flocculation of cassiterite with a sulfosuccinamate collector (Bilgen et al., 1994). The agglomeration flotation of cassiterite has been tested by Schubert et al. (Schubert et al., 1966), in which the selective coagulation of fine hydrophobic particles and oil droplets leads to an increase of the effective particle size. Recently, Leistner at al. investigated an oil-assisted agglomeration flotation for ultra-fine cassiterite ore fractions (Leistner et al., 2016). However, a poor response due to an increased concentration of Fe and Ca ions, unselective oil/gangue coagulation and froth instability, that is caused by oil/frother interactions, has been observed."

Jan 1, 2018

By Wieslaw Wszolek, Kazimierz Trybalski, Ryszard Tadeusiewicz

"The present work is an attempt of neural networks application to the description of complex technological processes of useful minerals enrichment. Neural networks are among the most convenient tools that have been added recently to the professional toolbox of modelling specialists, and they are particularly useful in realisation of multiple practical tasks, characterised by great complexity and relatively low amount of available a priori knowledge about the nature of the modelled processes. They are successfully applied in a wide variety of problems related to data processing and analysis, their prediction, classification or process control. The object of the study was the technological site for copper ore enrichment by floatation, being a part of technological line in the Ore Enrichment Plant ZG „Polkowice”, KGHM „Polska Miedz” S.A.The main floatation is described by parameters measured by the supervision and control system, which can be grouped with respect to the functions performed for the object:a) input function: aFG - copper contents in the feed material for the main floatation [% Cu]b) control: LFG I - level in the first section of the floatation unit [%], LFG II - level in the second section of the flotation unit [%], LFG III - level in the third section of the floatation unit [%], LFG IV - level in the fourth section of the floatation machine [%]. These quantities compose the five elements long input vector.c) output function: ? - copper contents in the waste from main flotation (final waste) [% Cu]The measurement data, containing the above-mentioned parameters, have been collected during the normal operation of the plant. The data contain momentary values of the parameters, registered every 10 minutes, covering the period of 196 hours of the plant’s operation (1176 measurements for each quantity).For construction of the model used in the study classical multi-layer perceptron-type neural network has been used, with one hidden neuron layer, trained by the error back propagation method."

Jan 1, 2003

By Henrique Kahn, Daniel Uliana, Carina Ulsen, Guilherme Nery

"Gold has been a material in high demand since the dawn of humanity. After hundreds of years of exploitation, the increasingly search for gold occurs in lower grade deposits with greater extraction difficulty. Therefore, for maximum efficiency, deep knowledge of the characteristics of these minerals and their associations is crucial, which is acquired through an accurate and rigorous routine of process mineralogy and batch extraction tests. The industrial gold process extraction occurs by gravity concentration, sulphides flotation and cyanidation. For gravity concentration, it is fundamental to establish the proportion of free or coarse gold grains and its association to heavy minerals; regarding flotation, the most relevant data are the proportion of gold associated to sulphides and their liberation by the surface area; for cyanidation, it is crucial to evaluate gold accessibility and the kinetics of leaching. Thus, the characterization of gold associations and liberation is vital to establish the plant design, to optimize operating plants and to reduce gold losses. Our aim is the characterization of gold occurrence in low-grade Brazilian deposits with complex mineralogical assemblages to support processing flowchart definition and to predict metallurgical recoveries. Gold distribution in light and heavy minerals was evaluated by heavy liquid separation and the occurrence of gold in free or locked particles was carried out on heavy products by SEM-based automated image analysis using the MLA system. All the products of heavy liquid separation were cyanidated in head samples with different milling conditions to evaluate the reaction kinetics and maximum recovery."

Jan 1, 2014

By Vincent C. Smith, Agit Singh, Daniel de V. van der Spuy, Bernard Muller

"Process control in the minerals industry is made difficult by factors such as the multivariable nature of the processes, noise, many disturbances, the changing nature of the processes, nonlinearities, process constraints, slow responses and large deadtimes. A good example of such a process is a milling circuit, where all these problems are experienced. Since model predictive control (MPC) effectively handles most of these difficulties, Mintek decided to develop, customise and test an MPC controller for milling control.Conventional MPC uses a dynamic model of the plant to calculate the future (predicted) plant outputs based on the movements of the manipulated variables in the past. The future moves of the manipulated variables can then be calculated using an optimisation algorithm that will minimise the difference between the setpoints and the predicted outputs. The least squares optimisation method is the quickest, but it does not cater for process constraints. Constraints can, however, be handled explicitly by using a quadratic programming optimisation method. This method ensures that the variables stay within the constraints at all times, but the calculation procedure is much more computationally intensive.• modifying MPC for the Minerals Processing IndustryIt was found that in order to obtain good, robust control using MPC in the minerals processing industry, the conventional MPC algorithm had to be adapted. The MPC controller was first tested on an extensive milling simulator, which was specifically developed for that purpose. Problem areas were identified and the MPC controller was specially adapted to accommodate for these difficulties. Some of the adaptations to the conventional MPC algorithm and special features added were as follows:Since milling plants contain many integrating processes (e.g. sumps), and integrating errors can cause offsets and poor control, it was essential that integrators be handled explicitly. This problem was solved by adapting the algorithm and also using an integrating error portion to compensate for integrating errors.Constraints on the inputs and outputs adversely affected the control. The controller using simple least squares optimisation was tuned with the constraints in place, while the maximum expected setpoint changes were made. This ensured that the process would be able to handle most setpoint changes up to these expected values without violating the constraints. A later improvement on this method was the incorporation of a quadratic programming algorithm to perform the optimisation. This method handles limits explicitly and was shown to perform better than the least squares methods (at the expense of a much higher computational cost)"

Jan 1, 2003

By Renato S. Costa, Afonso H. Martins, Flávia D. Mendes

"This paper presents some important aspects regarding the ion exchange treatment of an Ni and Co sulphate acidic liquor using chelating resins. Chelating resins possessing iminodiacetic or bis-picolylamine functional groups were compared in terms of nickel and cobalt recovery. The experimental resin with bispicolylamine functionalities (Dowex M4195) was evaluated with respect to Ni and Co uptake, and compared with Rohm &Haas commercial chelating iminodiacetate acid resin.The use of selective ion exchange to recover metals from sulphuric acid liquors has been studied for a long time. Companhia Vale do Rio Doce (CVRD) has been actively involved in hydrometallurgical applications of IX and has researched in selecting the optimum resin for nickel and cobalt selective removal and the design of a suitable IX circuit. When an IX operation is contemplated for a specific application, it is followed a screening process which generally involves consideration of the solution composition and pH, speciation of the metals in the liquor to be treated and other possible techniques that can be applied to achieve the desired specifications or recoveries. Once a decision has been made to use IX for a specific application, relevant testwork should be done to select the most cost-effective resin and design the IX circuit to achieve the desired criteria. The experimental part dealt with the working conditions, resin characteristics and the influence upon the resin maximum exchange capacity of the following factors: nickel concentration, temperature, pH and resin-to-solution ratio. Based on the experimental data obtained, it has been proposed a innovative technological treatment"

Jan 1, 2003