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By Fred N. Kissell

A parachute-type stopping intended for changing the course of mine ventilation air during mine emergencies has been designed and tested. Some production uses are also visualized for metal mines. Preliminary tests in the laboratory and underground indicate that the parachute stopping is a workable concept, but further developmental research is required.

Jan 1, 1975

By F. B. Tough

"INTRODUCTION Organizations formed for the purpose of conducting conservation work in oil fields, in order to conserve and prolong the supply of crude petroleum are rare and novel. Such an organization is the Rocky Mountain Petroleum Association, Denver, Colo, As our production of petroleum can no longer keep with the consumption, the plan of organization, character of work, and results obtained by this association are well worth considering. It is hoped that the results achieved in the Wyoming fields will serve to stimulate similar organizations among operators in the state or other oil fields of the United States, The Rocky Mountain Petroleum Association, Danvers Colo., was formed in May, 1919. It comprises the Midwest Refining Co,. The Ohio Oil Co., and the Continental Oil Co. These three companies entered into a cooperative agree¬ment with the Federal Bureau of Mines whereby $30,000 would be spent under the direction of the bureau, which agreed to furnish competent men, and to furnish the work and expenditure of funds. Although the financial burden for the first year's work, now drawing o a close, was carried by only three companies, they stipulated their desire that the benefit of the work should accrue to the industry, and that the personnel employed should be as zealous to assist one operator as another, without regard to whether ha was contributing to the support of the work or not."

Apr 1, 1920

By Donald R. Corson

The Bureau of Mines is conducting research on the effects of various established and potential soil-stabilization additives to hydraulic backfill. This initial phase is an evaluation of the effect of inclusion of varying amounts of Portland cement and combinations of cement and a dispersant on the bearing strength of backfill. Results of unconfined compression tests are given for over 200 sample cylinders incorporating a fill material with cement or cement and dispersant. Inclusion of a minor amount of dispersant (0.2 percent by weight) is found to yield a significant increase in strength for 20-to-1 and leaner sand-cement mixes. An apparent optimum concentration of dispersant exists beyond which no further increase in strength is achieved. A dispersant-cement ratio of l.8- to-1 yielded a strength increase of 515 percent over the strength of untreated 40-to-l sand-cement mixes.

Jan 1, 1966

By H. W. Kilau

Thermodynamic calculations indicate that an electrochemical cell might serve as an analytical device for determining the composition of high-purity metals. An equation, readily derived, for the cell voltage, E, is as follows: [E I RT In F NFe unknown sample T of L NFe standard] The cell, however, must come to equilibrium, must be reversible, and must have no thermal effects or complicating side reactions whose magnitude is indeterminable. This Bureau of Mines investigation explores the feasibility of an electrochemical technique for the analysis of high-purity iron. Experiments were conducted using room-temperature aqueous cells and high-temperature molten salt cells. The room-temperature cells proved to be irreversible. The high-temperature cells utilizing FeCl2 and a eutectic mixture of KC1-LiCl were reversible, but did not attain a constant voltage necessary for analytical considerations.

Jan 1, 1963

By E. C. Tarpley

The Federal Bureau of Mines has studied solvent extraction as a means of concentrating the mineral components in coal. Solubilities of a number of American coals were determined using abietic acid as a solvent. The effect of rank on solubility was investigated, and maximum solubility was found with coals of intermediate rank. Vitrinite is the most soluble petrographic component; fusinite, micrinitc, and exinite are nearly insoluble. Spore exines also have a low solubility. Abietic acid is a hydrogen donor and reduces pyrite to ferrous sulfide. Mild hydrogenation of high-molecular-weight fragments of the coal structure to those of lower molecular-weight probably contributes to the solvent action. Even where solubility of the coal substance exceeds 90 percent, contamination of the mineral matter with coal makes identification of the mineral components difficult. Further separation might be possible by the application of float and sink techniques to the residue. INTRODUCTION Work n the solvent extraction of coal is conducted to recover commercially useful products and to characterize coal;. and obtain information on their structure. Some coals, particularly those of low rank, contain waxes, resins, and humic acids which can be removed by solvent extraction and find varied industrial uses. In World War II, solvent extraction of coal was conducted on a commercial scale in Germany to obtain a low-ash feed material for hydrogenation and to produce electrodes carbon for the aluminum industry.4 5/

Jan 1, 1960

By Motohisa Kanda

The time and amplitude statistics necessary to adequately describe electromagnetic (EM) noise in mines are illustrated through computer software techniques. They are 1) Allan Variance Analyses (AVA), 2) Interpulse Spacing Distributions (ISD), 3) Pulse Duration Distributions (PDD), 4) Average Crossing Rates (ACR) , and 5) Amplitude Probability Distributions (APD) . These statistics are illustrated using data taken from a rather large store of raw analog data recorded in operational mines. The curves generated for the illustrations characterize the noise environment in the mines from which the corresponding data were taken, and should aid in the design of reliable communication systems for such mines.

By M. A. Mahtab

This report describes the procedures used by the Bureau of Mines for obtaining attitudes of joints surveyed with a borescope in inclined boreholes. An algorithm for computing the dips and azimuths of the observed joints is presented. The algorithm is used to solve an example problem. A computer program based on the algorithm is listed. It is hoped that the procedures described here will be useful in treating large quantities of data obtained from comprehensive borehole surveys.

Jan 1, 1973

By Thomas R. Bur

The order of identification and in same cases the magnitude of the elastic constants of an anisotropic material depends on the orientation of the cartesian coordinate axes with respect to a set of reference coordinate axes within the material; thus confusion will result unless standard orientations are used. In this paper the relationship between the cause (the internal fabric) and the effect (the elastic properties in this case) is discussed for single crystals and for polycrystalline and amorphous materials. While reference axes based on the cause are used in the IRE (Institute of Radio Engineers) standard for piezoelectric crystals) it is shown that a reference coordinate system that would be suitable and practical for all anisotropic polycrystalline and amorphous materials must be based directly on a three-dimensional expression of the effect. The conventions offered are similar to the IRE standards for piezoelectric crystals) but use the elastic coordinates of the wave surface which can be quite readily established experimentally as the reference coordinates.

Jan 1, 1969

The twelve latexes listed in Table XI penetrated A horizon soil as shown by elution through a laboratory soil column and gave good sealing efficiency. See details in Table XII. High elution through laboratory soil columns of 4 to 6 inches depth is desirable because it predicts penetration of latex to a greater depth in the field. No definite correlation was evident between penetrating ability and particle size, surface tension, or pH. Most of the materials, however, were characterized by low surface tensions in the 36 to 53 dynes/cm range while particle sizes were usually in the intermediate range of about 1500 to 2500 Å. Naugatex J-3471 (a highly crosslinked styrene-butadiene copolymer) was the most promising of this group for stability, penetrating ability; and sealant efficiency. It also showed utility with [B] profile soil. Many of the other latexes tested in this investigation showed good sealing efficiency but were judged unsatisfactory because they gave low penetration or formed surface films with & horizon top soil. In general, latexes containing cationic surfactants were not satisfactory because they formed a heavy surface film. This is due to neutralization of the positive latex charge by the negatively charged soil particles.

Jan 1, 1972

By J. M. Riley

A fluorometric method using morin in an alkaline-buffered chelating solution has been developed by the Bureau of Mines for determining beryllium in ores and mill products. Apparatus for measuring fluorescence intensities of the beryllium-morin reaction is described. Preparation of the sample for analysis consists essentially of digestion with sulfuric, nitric, and hydrofluoric acids, fusion of the residue with sodium carbonate and sodium borate, Solution of the melt with sulfuric acid, and proper dilution. Chemical separation of other ions is usually unnecessary. The method rave reliable beryllium determinations on samples in the 0.01- to 0.37-percent BeO range. The method is particularly applicable to low-grade beryllium ores; however, semiquantitative beryllium determinations have been made on beryl containing 12.0 percent BeO.

Jan 1, 1956

By Harry W. Campbell

A mineral survey by Bureau of Mines personnel identified no mineral resources or mineral occurrences with development potential at prospects in the Mecca Hills Wilderness Study Area (WSA). Bentonite occurrences are in Skeleton Canyon and Surprise Canyon. Sand and gravel occurrences are numerous in and near the WSA. Much of the Mecca Hills WSA was leased for oil and gas exploration in 1983. No current mining claims or other leases were found in the study area. The Skeleton Canyon Clay Mine yielded clay to seal irrigation canals, Clay to seal ponds was also mined from the Red Top Clay Mine west of the USA. A sand and gravel pit south of the study area (near Box Canyon Wash) supplied material for local construction projects. A commercial sand and gravel pit was operating in 1983 near the mouth of Thermal Canyon 4 miles west of the WSA.

Jan 1, 1984

By Brian G. White, Theodore J. Williams, Jeffrey K. Whyatt

Detailed mapping and examination of the site of a large rock burst at the Lucky Friday Mine, Mullan, ID, demonstrated conclusively that damage was caused by a splitting and buckling failure mechanism initiated by separation of rock into layers along steeply dipping metamorphic shear foliation subparallel to the affected crosscut. The thin tablular layers then buckled into the crosscut from both sides. Rigorous control of the burst by these layers suggests practical measures for avoiding bursts in crosscuts in the future by repositioning and reorienting openings so that splitting and buckling are reduced or precluded.

By Claude W. Sill

In the course of a series of investigations on vanadium deposits of the western United States, the Bureau of Mines collected many hundreds of samples for chemical analysis. As uranium is often associated with these vanadium minerals, they were also analyzed for uranium, which was pound to be absent in a large percentage of the samples. Since the usual methods for determining uranium are laborious and time-consuming it is very desirable to have some simple qualitative test that can be applied prior to a quantitative analysis to determine whether uranium is present or absent and thus save the time and expense of applying the quantitative analysis to the large proportion of samples containing no uranium. To be acceptable, the test should be specific for cranium, sensitive enough to detect small amounts of uranium, and. simple enough to make it worthwhile to apply. The available methods for detecting uranium lacked one or more of the desired characteristics. Eventually, however, a method was worked out that satisfied all the requirements. This method is probably more specific and sensitive than the usual qualitative methods for uranium, and its simplicity and speed of application make it ideal for testing samples prior to quantitative analysis.

Jan 1, 1945

Investigate the use and placement of lightweight concrete to improve ground control technology in deep mines where deformation occurs under heavy ground conditions and where there is danger of rock bursts. Approach Investigations of lightweight concrete properties and placement methods were conducted in the laboratory and in the field. Three test sections were completed: a monolithic, portal-type structure with integral walls and arch constructed aboveground; an underground test section constructed in a mine drift using plywood forms; and a test section constructed in a mine drift using an air-supported formwork. In the two underground test sections, the light-weight concrete was placed using a piston pump with concrete discharge line. A cooperating mine also used lightweight concrete, in the density range of 25 lb/ft3, to replace timber blocking in a raise preparation structure (the enlarged area across a vein where chutes and manway access arc placed). Other experiments included the use of precast lightweight concrete blocks in situations where ground support was needed, such as fur mine, ventilation doors, stoppings, and barricades.

Jan 1, 1990

By A. Wahab Khair, S. Jung

"This paper deals with the fracturing process of laterally confined blocks of coal subjected to impact indentation. During the test, blocks of coal with approximate dimensions of 10 in. x 10 in. x 6 in. were laterally confined to predetermined equivalent in-situ stresses and then subjected to an impact indentation by dropping coal cutting bits (various shapes) attached to a known weight from a known height. During the test a number of parameters, namely surface strains (using strain gages), penetration depth (using L.V.D.T.) and acoustic emission characteristics were measured. After the test, the fractured surfaces were photographed with the aid of a camera attached to a microscope. The fracture, its intensity and extended zone within the coal blocks were mapped using sonic techniques. By correlating measured parameters, fractured zones under a given set of test parameters were identified and characterized.INTRODUCTION To improve the understanding of basic failure mechanisms in coal cutting, a better knowledge of fracture and crack regions caused by the indentation in coal is needed. This study reports the detailed experimental procedure used in fracture analysis of indentation experiments on coal specimens using the Acoustic Emission (A.E. hereafter) and sonic techniques. The relationship between microcracking and the inelastic deformation of rock was confirmed by a series of experiments in which the A. E. generated by the cracking in the rock specimen were recorded and the number of events were compared to the strain measurement. (Scholz, 1967).According to fracture mechanism theory, crack initiation in brittle materials such as rocks begins from ""flaws"" either pre-existing or induced by the indentation process itself. Rocks are pervaded by natural cracks and pores, from which numerous possibilities for crack initiation arise (Lindquist, Lai and Alm, 1984)."

Jan 1, 1989

By J. W. JOYCE

The Geophysical section of the United States Bureau of Mines has received many inquiries regarding the application of geophysical methods to the location of small, buried metallic objects. The object of this paper is fourfold: (1) To sketch as briefly and non- technically as possible the principles underlying the operation of several elec- trical geophysical methods of prospecting applicable to the finding of small, buried metallic objects; (2) to point out the possibilities and limitations of these methods; (3) to present, whenever possible, data showing actual results obtained from their use; and (4) to enumerate and describe methods that lack scientific background or foundation.

Oct 1, 1935

By A. W. Khair, L. D. Gehl

"This paper describes the mechanism of coal and rock cutting from quasi-static indentation through dynamic indentation to rotary cutting. The results indicate that during quas~static indentation, a crushed zone, and subsurface fractures develop. The crushed zone is a potential source of dust generation. Dynamic indentation produces a crushed zone due to the frictional resistance offered by the coal or rock during penetration of the bit. Confining pressure changes the mode of failure from tension to mixed tension and shear. The wider bit causes larger crushed zone and more dust generation. The rotary cutting is a combination of quasi-static and dynamic indentation which results in chip formation. 1. INTRODUCTIONThe trend from conventional mining to continuous machine-cutting of coal, using more productive machinery is inexorable. Intolerable levels of dust generated at the face is an indication of inefficient coal or rock cutting by these machines. The Federal Government of the United States paid about 11.7 billion dollars workman compensation to more than 470,000 miners with Coal Workers Pneumoconiosis (Newmeyer, 1981). Bieniawski and Zipf (1985) reported that annual benefit payments were about 2 billion dollars. The need for research m improving coal cutting 1s therefore paramount. The enactment of Health and Safety Act in 1969 in the United States triggered the initial investigation into coal cutting mechanism and cutting tool design. The European countries were also engaged in the same area of research, however, their emphasis was in the use of wedge shaped bits. In 1981, the United States Bureau of Mines commissioned the South West Research Institute to investigate the effect of operating parameters mainly on airborne respirable dust in order to provide a healthier and safer atmosphere for coal mine workers.A research program by the Department of Mining Engineering, West Virginia University, USA was initiated to study the fragmentation mechanism during coal/ rock cutting. The research program was divided into three areas of research, namely quasi-static indentation, dynamic indentation and rotary cutting."

Dec 1, 1995

By John Ward Smith

The Bureau of Mines derived equations expressing the theoretical relationship between density of oil-shale rock and its organic content. Effects on theoretical shale density produced by variations in mineral composition and organic matter properties were evaluated. The theoretical relationship was extended to relate oil-shale density to oil yield in both oil weight and volume units by considering the fraction of organic matter converted to oil and the specific gravity of the oil produced. Corollary equations relating organic content by volume to organic content by weight and to oil yield were developed. The general relationships apply to an oil-shale deposit uniform in character. Application of the theoretical relationships to Green River Formation oil shales was demonstrated.

Jan 1, 1969

By John Nagy, Henry G. Dorsett, Murray Jacobson

Laboratory studies show that ignition of a dispersed combustible dust in an open vessel may be prevented by adequate inerting . Factors affecting the inerting requirements are -- dust concentration , spark energy , ignition temperature , composition of the substances used for inerting , fineness of dust and type of combustible . The oxygen concentration of the atmosphere and in some instances the proportion of admixed inert powder and moisture required to prevent ignition are given for 367 dust samples . Variations in inerting requirements with strength of igniting source are discussed .

Jan 1, 1964

By L. J. E. Hofer

The Bureau of Mines determined rates of adsorption and desorption of methane as a function of particle size and temperature, using coals from the Pocahontas No.3 seam (lvb) from the Bishop mine of western Virginia, and the Pittsburgh seam (hvab) from the Pursglove No. 15 mine of northern West Virginia. For a given coal sample and temperature, the rate curves for adsorption and desorption are essentially the same when expressed on a fractional approach to equilibrium basis. The rates of adsorption and desorption increased eightfold as the particle size was decreased from 6-8 to 270-325 mesh per inch. The adsorption process appears to be diffusion controlled. Rate of sorption processes increased with increasing temperature; however, the amount adsorbed at equilibrium decreased.

Jan 1, 1966