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By J. G. Kirby

According to the Bureau of Mines annual survey, there were 319 petroleum refineries in the United States as of January 1, 1957 capable of processing 9,123,674 [ ]-barrels of crude oil daily. This was the first time in eleven years that the total number of refineries increased. The crude throughput capacity of the refineries increased 491,284 barrels daily (6 percent) above the January 1, 1956 capacity. The East Coast and Texas Gulf Coast refining districts accounted for 60 percent of the additional capacity installed. Three new refineries were put into operation on the East Coast during the year with a total daily crude throughput capacity of 154,434 barrels while the other refineries in the district report a net loss in capacity, installing equipment capable of processing 140,000 barrels, but dismantling equipment with a capacity of 150,100 barrels. In the Texas Gulf Coast district, one new refinery with a daily crude oil capacity of 5,000 barrels was placed in operation in 1956 and 143,700 barrels of crude capacity was added to existing refineries. The capacity of the average refinery to process crude oil increased from 27,145 barrels daily to 28,601 barrels in 1956.

Jan 1, 1957

By R. E. Stiles

The modified perchloric--EDTA method devised by the Bureau of Mines for the determination of copper in high-grade samples gives results that are more precise and more accurate than those from the classical sulfuric-iodometric method. Although the perchloric--EDTA method is more costly than the conventional method, the savings in time alone largely offsets this difference. Specifically, the modifications wade in the more conventional procedure comprise (1) use of perchloric acid instead of sulfuric acid for dissolution of copper minerals, (2) precipitation of copper as copper sulfide from dilute perchloric acid solution, (3) wet oxidation and dissolution of the precipitated copper sulfide, (4) use of larger amounts of indicator than those employed in the Schwarzenbach method of titrating low-tenor copper solutions with disodium ethylenedinitri10-tetraacetate and murexide indicator, and (5) use of refrigeration to partially stabilize aqueous solutions of the indicator.

Jan 1, 1966

By Thomas R. Bur

The patterns of variation of the 21 anisotropic elastic constants with direction arc presented for all of the symmetry systems that are normally expected to occur in rocks and in the constituent minerals. The exception, which is not discussed, is the triclinic system for which no elastic constants are available. Variations are shown for rotations about the principal axes by means of polar graphs. These include graphs for all of the n-fold symmetry axes possible for elastic symmetry and thus make it possible to visualize variational patterns for rotations about any n-fold axis. Variations throughout space are shown by means of equal area projections for the only constants (those relating axial stress to axial strain) that are uniquely defined by a single closed surface. For those unfamiliar with the compliance (Sij) and stiffness (cij) coefficients, the variations that can be shown by Young's modulus (E), Poisson's ratio (v), and shear modulus (G) are also given.

Jan 1, 2012

By R. L. Crosby

From studies of wrought magnesium alloys containing rare-earth elements, data are presented on the mechanical properties of the alloys at room temperature and at temperatures of 100°, 200°, and 300° C. Results of studies of the solid-solubility of cerium and zirconium in magnesium as determined by electrical resistance measurements are also discussed and are compared with those of other investigators. The strength of magnesium-cerium alloys did not increase with the addition of vanadium and titanium dioxide. The addition of zirconium increased the tensile strength of the alloys as much as 10,000 p.s.i. at room temperature, but this increase diminished above 100° C.

Jan 1, 1962

By C. P. Hood

"The amount of ash in anthracite coal interests every buyer, and occasionally produces caustic comment, but there is a lack of authentic figures that will take the subject out of the realm of opinion and agitated fancy and. give a true picture of the quality of coal actually delivered. What per cent ash is to be expected when the coal is good, and when have we a right to make serious complaint?During the past summer the Bureau of Mines took 127 samples of 1000 pounds each, representing nearly 30,000 tons of anthracite is dealers' yards in seventeen cities in the State of Massachusetts. There were three objects in view, to discover the average and the variation in amount of ash in anthracite in some easily described area; to demonstrate standard sampling methods, and to learn something about the feasibility of itinerant coal sampling. Massachusetts was selected because its principal cities could be visited in a single season. There also appeared need for demonstration of standard sampling of coal, since a coal quality law had been passed in the State, to be administered by those unfamiliar with coal sampling."

Feb 1, 1924

By Robert E. Barieau

This report gives the principles of the method used by the Helium Research Center of the Bureau of Mines when solving nonlinear-regression problems and contains the mathematical equations necessary to accomplish the following objectives: the evaluation of the parameters in such a way that the sum of the weighted squares of the residuals of an experimental observable is a true minimum, regardless of the functional relationship between the variables and these parameters; and the evaluation of all variances and covariances of the parameters by means of the usual approximation of the law for the propagation of errors.

Jan 1, 1967

By Charles K. Rose

The Cebolla Creek titaniferous iron deposits near Powderhorn in southern Gunnison County, Colo., were examined by the Federal Bureau of Mines as part of an overall program to investigate the Nation's titanium and iron resources. The deposits occur around the periphery of the Iron Hill stock, which underlies an area of about 12 square miles. Concentrations of magnetite, ilmenite, and perovskite arc localized along fractures in the pyroxenite stock. Mineralogical studies of composite surface samples collected in 1956 showed that most of the iron is present in ilmenite-bearing magnetite. Perovskite is the chief titanium mineral in the magnetite-rich and augite-rich types, and sphene is the principal titanium mineral in the placer material. The mica-rich rock contains approximately equal amounts of perovskite, ilmenite, and sphene.

Jan 1, 1960

By G. W. Elger

The Bureau of Mines conducted laboratory and larger scale studies on samples of domestic perovskite and ilmenite ore concentrates to devise a procedure for recovering TiC from these ores. From the concentrates, mixtures of titanium and calcium carbides were produced. The carbides were then ground and reacted with water. This reaction decomposed the CaC2 to acetylene and hydrated lime and simultaneously liberated the TiC. Using a combination of elutriation and gravity-separation techniques to separate the hydrated lime, approximately 93 pct of the titanium was subsequently recovered as purified carbide containing 54 to 70 pct titanium with CaO content as low as 0,6 pct. This combination of techniques can be used to separate more than 90 pct of the CaO from the TiC. Therefore, this carbiding procedure is a viable method for treating titaniferous materials, including perovskite, that contain more than 20 pct CaO. Tests made in a static-bed reactor showed that for the reaction of TiC with elemental chlorine to produce titanium tetrachloride (TiCI4), a temperature of at least 940° F is desirable to achieve a suitable extraction of titanium in a laboratory chlorination reactor. In fluidized-bed tests at 840° F, 98 pct of the titanium contained in TiC was extracted.

Jan 1, 1980

By M. J. Sapko

The U.S. Bureau of Mines has developed a portable meter for measuring the component concentrations in binary dust mixtures whose constituents have different optical reflectivities. The meter has been successfully tested with coal dust-rock dust mixtures taken from coal mines in Europe and the United States and fluorinated-carbon mixtures that change from carbon black to pure white during fluorination. Additional study has also substantiated the theoretical expressions used in the design of the meter.

Jan 1, 2010

By Lucien Eaton

This paper describing the mining practices at Mine No. 1, Menominee Range, Mich., is one of a. series being prepared by the Bureau of Mines on mining practices, methods, and costs in the various mining districts of the United States. It is felt that the publication of this information will be of interest and value to the mining industry at large and especially to operators whose mining conditions are similar to those described. ACKNOWLEDGMENTS The author is indebted to the superintendent, engineer, and mining captain of Mine No. 1 for much of the information presented.

Jan 1, 1929

By W. M. Deaton

The Keyes Helium Plant of the Federal Bureau of Mines was constructed under an expedited schedule, to supply the urgent and growing demand for helium in atomic energy, missiles, aerology, space exploration, shielded-arc welding, and low-temperature research. Construction began in December 1958 and ended in August 1959. The plant, near Keyes, Okla., processes 2 percent helium-bearing natural gas from the Keyes gasfield. In 1960 the plant produced and shipped 263 million cubic feet of helium (equivalent to an annual rate of 290 million cubic feet). Production cost was $9.11 a thousand cubic feet of helium. A low-temperature process involving two steps is used; the first separates a crude-helium product from the natural gas at about -250° F. and 225 pounds per square inch gage (p.s.i.g.); and the second purifies the crude helium to a high-purity product (Grade-A helium, 99.995 percent helium) at about -320° F. and 2,750 p.s.i.g.

Jan 1, 1961

By F. Fraas, H. H. Storch

"In the second paper 4 of this series, data were presented concerning the decomposi¬tion of polyhalite by saturated salt solutions. It was found that uncalcined polyhalite upon leaching with boiling saturated sodium chloride solutions yielded a brine in which the (K2 Mg) /304 ratio was considerably higher than that obtained from the calcined material, and for this reason appeared more suitable for the production of potassium chloride. It was found, in fact, that the leach liquors from uncalcined polyhalite deposited a mixture of KC1 and NaC1 upon evaporation and subsequent cooling, whereas those from calcined polyhalite yielded mixtures which contained not only potassium and sodium chlorides but also large quantities of glaserite, K3Na (S04)2. Hence it was decided to study the evaporation of the uncalcined poly—halite leach liquor and postpone experiments on the calcined polyhalite liquors until such time as a process for further removal of sulphate was developed.A considerable body of equilibrium data is available in the literature on thesystem K+ Mg++ — Na+ Cl—S04 =,— H20 for temperatures up to 83º C. Owing, however, tothe lack of data other than that corresponding to the invariant points and the complete absence of data for temperatures of 100 to 115°C., and owing to the fact that supersaturation phenomena render unsafe the prediction of the behavior of such a system upon evaporation, it was considered essential to obtain the necessary data by actual evaporation and analysis of the brines thus obtained."

Feb 1, 1931

By Herbert H. Einstein

Rock mass deformability is commonly predicted using correlations with RQD or other indices of rock mass quality, or by extrapolation from large in-situ tests. Based on the probabilistic description of rock masses empirically developed in Part I a new approach was attempted in modeling for predictions of deformability. This approach decomposes the rock mass into spatially variable joints described by probability distributions, and intact rock blocks. Stiffnesses and elastic parameters are associated with the joints and intact blocks respectively, and deformations built up by adding the contributions of each. This model allows relaxation of many of the simplistic geometric assumptions which constrain parallel attempts to model deformation in rock masses. The model has been applied to four standard cases in order to test its results against previously existing models, and to check whether it replicates empirical correlations. When joints are taken as parallel, common empirical correlations are closely approximated by the model output. However, the closeness to empirical correlation breaks down when variability of the jointing geometry is increased.

Jan 1, 1979

By H. P. Hermance

The Ore Hill zinc-lead mine in Grafton County, N. H., was investigated by the Bureau of Mines from March to July 1943 and from August to October 1944. Fourteen holes with an aggregate bore of 4,899 feet were diamond-drilled, the old workings were unwatered and sampled to an inclined depth of 250 feet, and the tailings dumps were surveyed and sampled. The deposit at the Ore Hill mine comprises a bedding-plane vein of massive sphalerite and galena with subordinate chalcopyrite and pyrite in a series of interbedded metasedimentary and metavolcanic schists about one-quarter mile east of their contact with the intrusive Baker Pond gneiss. The property was first opened about 1850 and was active at times to 1914. Production records are not available, but the output is believed to have been considerable. In 1944, leasers recovered a marketable mica product from mica schist from the dumps and certain outcrops. This report describes the work performed in the Bureau's investigation and presents the data obtained.

Jan 1, 1948

By Robert T. Langland

The Bureau of Mines, at its Denver, Colo., research center, has developed a computer program to solve nonlinear regression problems. The program is written in a general form so that, regardless of the functional relationship assumed, the unknown parameters may be evaluated by the Newton-Raphson method of iteration. Variances and covariances of the parameters are derived, based on the propagation of errors. A creep function is established from shale test data as an example of program utility. Program accuracy is compared to the accuracies of other programs in present day use.

Jan 1, 1974

By J. E. Doo1ey

To process and use the heavy ends of petroleum effectively, the development of suitable separation and characterization procedures not currently available was required. A systematic procedure was developed by the Bureau of Mines using such techniques as isothermal and molecular distillation, chemical treatment, silica-alumina gel chromatography, gel permeation chromatography, and spectrometry. Using these techniques, the Bureau achieved a detailed separation and characterization of a 370° to 535° C distillate from Gach Saran, Iran, crude oil. Such a systematic procedure and the semiquantitative data resulting therefrom should be of value in selecting feedstocks and in optimizing petroleum processing operations.

Jan 1, 1973

By Robert H. Bedford

As a result of the Bureau's general survey of quicksilver deposits in California, the Guadalupe mine area was among those chosen for exploration. Exploration, such as that at the Guadalupe, was aimed primarily at maintaining or increasing production of quicksilver during the critical wartime period. The project as originally planned contemplated sampling the dumps and prospecting some promising surface exposures by bulldozer trenches. Salvage was the objective in the first case and new ore in the second. Later, a program. of diamond drilling was added, designed to add both to ore reserves and to geological information. This report summarizes the history, notes the location and physical features, mentions property and ownership, and presents a brief description of the mine. The geology is outlined, and the work done by the Bureau of Mines is explained and supplemented with accompanying maps. The work involved repairing 1-1/4 miles of roads; bulldozing 13 trenches by removing 2,345 cubic yards of dumps to provide for sampling; digging and sampling 9,284 linear feet of hand trenches, digging and sampling numerous test pits; and drilling 7 diamond-drill holes, totaling 1,000 feet. A total of 419 samples, including 10 percent check samples, were taken. Exploration work in California at the time of this project was under the direction of Spangler Ricker, supervising engineer of the California field office, the late Robert Bedford was in charge of the fieldwork on this project.

Jan 1, 1950

Experience, it is said, is the best teacher. Some experiences, however, should be shared so that no one else will ever have to live through them again. The fire at the Sunshine Mine is one such experience. ?Hard-rock mines don?t burn.? The Sunshine Mine near Kellogg, ID, was the nation?s premier silver producer for many years. In 1972, the mine was nearly 6,000 feet deep, contained hundreds of miles of worked-out areas, and employed nearly 500 people. Because of its depth and the type of host rock for the silver (unburnable quartzite), the general thinking of the day was that fires in mines such as the Sunshine were impossible, because ?hard-rock mines don?t burn.? What wasn?t really considered was that timber supports, foam insulation, and mining equipment do burn and that the carbon monoxide gas produced by burning is far more deadly than fire itself. Thus, no one was prepared when, on May 2, 1972, a fire of un-known origin broke out below the 3100 level of the mine. Before long, 173 miners on the day shift were trapped by thick, black smoke. By the time the fire was out, 91 miners had died, and the Sunshine Mine Fire became known as one of the worst mine disasters of the 20th century. It became the catalyst for passage of the Metal/Nonmetal Health and Safety Act of 1977, which applied the same federal safety standards to hard-rock mines as those regulating coal. Mandated safety training, mine inspections, and equipment standards were brought into force.

Aug 1, 2002

By Lloyd A. Morley

This report abstracts project work performed under USBM Grant GO155003 during the period 4 November 1975 to 3 November 1976. The research was funded, as a continuance of previous support from USBM Grants GO133077 and G0155003, to gain further knowledge in mine electrical system safety. Five reports have been separately produced, all under the grant title, "Coal Mine Electrical System Evaluation," and are as follows: 1. Volume I - Continuous Monitoring, 2. Volume II - Transient Analysis, 3. Volume III - Shielded Cables, 4. Volume IV - Computer Modeling, and 5. Volume V - Battery and Battery-charging Safety. Abstracts of these comprise the balance of this document with one exception. The task ?d-c offsett currents," does not fall under the scope of the other report volumes and, further, the material to be presented does not justify a separate report. Hence, this subject concludes the Executive Summary.

Jan 1, 1977

By Jon I. Voltz

The U.S. Bureau of Mines has conducted fundamental coal fragmentation studies to evaluate the effects of impact energy and direction of bedding planes on dust generation, size distribution, and impact-output energy relationships. Product size distributions were obtained for the fragmented samples by screening to minus 150 mesh. The minus lS0-mesh fines were analyzed with a light scattering photometer with a measurement range of 176 to 1.9 /.tm. Increased input energy produced a significant increase in the weight of plus 3/8-in material for impact perpendicular to the bedding planes. No significant trend was observed for parallel impact. Impact direction had little influence on dust size distribution, and input versus output energy relationships. As expected, total airborne dust measured at time of impact and percent particulates below 11 /.tm in size generally increased with increased input energy for both directions of impact. Energy used for sample fragmentation increased with increased energy input.

Jan 1, 1989