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By C. L. Brown

Among the more recent developments for breaking coal in mines is the Airdox system, in which high-pressure compressed air is conducted to the points of application by means of heavy-duty steel and copper tubing. Stray electric currents can be detected on y of the compressed-air lines, and evidence of such currents is rev led, by arcs and sparks when contact is made between the tubing and mine track or other equipment forming a current path with the track. Explosive gas is liberated in many coal mines; therefore, from the standpoint of safety, it is desirable to eliminate all possible sources of gas ignition, including stray electric currents. The purpose of this report is to reveal the source, magnitude, and possible methods of controlling stray currents in compressed-air lines that are used in connection with Airdox systems. Stray electric currents have been studied in most coal-mining localities in the United. States where Airdox equipment is used. The information given in this report is based on the find of these studies.

Jan 1, 1949

By Brian G. White

Two examples of en echelon mining-induced fractures seen in hard-rock mines provided a basis for inferring that fracture zones and bedding plane separations immediately surrounding mine openings are promoted by oblique shear into the openings. It is hypothesized that initial fractures or separations form at the corners of openings as a result of high stress and physical constraint on the rock's ability to deform elastically toward the opening. These conditions result in a locally preferred direction of shearing. The shearing, in turn, generates tensile stress that initiates a progression of systematically offset fractures approximately parallel to the direction of greatest compressive stress. The fractures or bedding separations create tabular rock layers that amplify shearing displacement through bending and dilation. Such shearing effectively reduces and redistributes the compressive stress, but significant dilation is an inevitable consequence. The combination of dilation and shearing and the progressive development of fracture zones have important implications with respect to ground support. The concept of mining-induced fractures forming as a result of shear is illustrated by two examples from coal mines. First, fractures seen at longwall faces probably result from shear associated with subsidence. The fracture zone that develops approximates or possibly defines the draw angle of subsidence. As the face advances, fractures extend downward along the lower edge of the fracture zone, while upper extensions of the fractures are pressed closed. Fracture zones in entry roofs provide a second practical example. Here, mining-induced fractures typically follow bedding planes. The shear zone model suggests that the first bedding separations develop near the edges of the roof and successive separations progress upward and toward the center. However, if the direction of greatest stress is inclined with respect to the roof, a fracture or bedding separation zone may propagate from one side only and also extend higher. Because coal ahead of the face provides some support against lateral shear deformation, bedding separation is inhibited near the face. Rock bolts installed close to the face ultimately become more strained and bent than bolts installed a few meters from the face, and bolts installed through the more remote part of a separation zone may ultimately experience the greatest tensile and bending strains. This model is supported by field data documenting progressive bolt failures that rapidly propagated downward across the roof during face advance.

By B. R. Eichbaum

To develop technology to assure an ample supply of zinc and to reduce environmental pollution, the U.S. Bureau of Mines investigated alternatives to the roast-leach process for treating complex sulfide concentrates. Previous studies proved that low-grade zinc sulfide (ZnS) concentrates could be leached using chlorine-oxygen to produce zinc chloride (ZnCI2). The process involves high energy requirements for evaporating the pregnant solution to produce anhydrous ZnCl2 needed for electrolytic cell feed. An efficient hydrometallurgical process would facilitate treatment of lower grade ores than can be used in conventional processing and would render roasting unnecessary. An alternative method was devised for recovering ZnCl2 from solution. Zinc diammine chloride [Zn(NH3)2CI2] was precipitated from solution by adding ammonium chloride (NH4CI) and sparging with ammonia (NH3) to a pH of 6 to 7.5. The spent solution was treated with calcium hydroxide [Ca(OH)21 at 60° to 80° C for 1 to 4 h to remove remaining zinc and NH3. The Zn(NH3)2CI2 was heated to 300° to 400° C to remove NH3 and produce anhydrous ZnCI2. A possible flowsheet was devised and is included.

Jan 1, 1991

By R. M. Ray

The Bureau of Mines evaluated five commercial badge-type carbon monoxide dosimeters. Color changes in the badge reagent indicated the presence of carbon, monoxide. Possible effects of ambient conditions on dosimeter response to CO during or after coal mine fires or explosions were studied. Temperature and humidity changes did not change dosimeter sensitivity to CO. Contaminant gases such as CO2, N02, S02, and H2S had effects that varied with brands of dosimeters ranging from no effect to increased sensitivity to CO. Dosimeters tested after 6 months of storage showed an increase in failure rate as high as 25 percent. Tests were conducted to determine the effects on dosimeter time-for-color change caused by observer's sight (colorblind); lighting, and coal dust on dosimeters. No significant effects were observed. Observer variance was the most pronounced factor observed in all tests.

Jan 1, 1975

By L. Kaufman

A range of processing conditions and compositions have been evaluated in order to optimize the properties of TiB2-(Ni,Cu) composites for application as a non-sparking tool material for use in coal mining operations. Fifty billets containing from 70 to 9S weight percent titanium diboride were hot pressed at 3000 psi between 2400°F and 2650°F. Samples which were cut from these billets were used to measure hardness, bend strength and impact strength so that composition/processing optimization could be effected. Eight compositions selected on this basis were evaluated by incendivity tests in order to choose the best composition. The best results were obtained for an 85 w/o TiB2-12 w/o Cu-3 w/o Ni composite hot pressed at 2650°F and 3000 psi. This material appears to be the best choice for fabrication of coal cutter bits to be evaluated in field tests.

Jan 1, 1973

By C. M. K. Boldt

The Bureau of Mines surveyed waste disposal sites at 18 metal and non-metal mines and conducted laboratory and full-scale field tests to de-termine the effects of tailings deposition techniques on physical properties of tailings pond beaches. Survey data included measurements of beach slopes, descriptions of deposition techniques, and measurements of beach physical properties taken at various distances from the point of discharge. Laboratory tests involved depositing two types of tailings, each with different grain-size distributions, into a settling trough and determining the resultant physical properties of settled materials along the length of the beach. Side confinement and the closeness of the water pool to the point of deposition caused the laboratory results to be inconclusive. Full-scale field deposition tests conducted at the tailings pond of a cooperating mine showed that there were similarities in relationships between exit velocities of tailings slurry and physical properties of the settled tailings on the beach.

Jan 1, 1988

By Andrew B. Cecala

This U.S. Bureau of Mines report provides a detailed description of the Bureau-designed modified shearer clearer system. Engineering drawings are provided for all major components of this system. The modified shearer clearer system is a revised version of the original system and is intended to improve the ventilation around both cutting drums. The original shearer clearer technique was solely a dust control technique that has been effective in lowering shearer operators' dust exposures. The technique uses a series of water sprays that not only knock down a portion of the dust cloud but also act as small fans that move a substantial amount of air and keep the dust cloud from dispersing over the shearer body. The modified version is composed of two additional spray blocks for improved air movement around both cutting drums, thus lowering methane levels and the likelihood of an ignition. A laboratory study performed with the modified version in a full-scale longwall gallery resulted in a 73-pet reduction in methane concentrations at the shearer machine for both cut directions. The air-moving capabilities of the system provide more turbulence at the cutting drums and reduce methane levels.

Jan 1, 1994

By H. M. Cooper

The determination of moisture in coal is an empirical test, because the time, temperature, and equipment are specified. The essential features of the equipment and details of the procedure are given in A.S.T.M. Designation: D271-44.:2. According to the specifications, the following features should be incorporated in the equipment used: 1. Oven must have uniform temperature in all parts. 2. Oven must be constructed with minimum of air space. 3. Oven must have means of changing the air two to four times per minute. 4. Air must be dried over sulfuric acid (sp. f-7. 1.84). The analytical procedures governing most of the nation's coal purchases are those given in A.S.T.M. Standards referred to above. These standards are general arid of such scope as to cover all ranks and types of coal. In cases where only the moisture is required, a faster method than the standard procedure is desired.

Jan 1, 1948

By Manuel Gomez

Dehydrogenation factors, proximate analysis, and ultimate analysis were examined as predictors of the low-temperature -carbonization properties of coals varying in rank from lignite through anthracite. All factors studied contributed to reduction in variance of the sample populations investigated. Response surface regression models based on variables from proximate and ultimate analyses of coal were constructed for eight low-temperature carbonization assay product and gas component Fields. These models were tested with independent samples that included drill cores, sized fractions, petrographic fractions, and run-of-mine coal. The models developed were used to predict low-temperature carbonization yields or coals from major fields of Wyoming. This information was cast in the form of contour plots describing the potential low-temperature carbonization product yields of Wyoming coals and the properties of the resultant char or coke. The variables used as input v the models may be measured and collected during exploration; thus, the carbonization properties of a seam can be determined in advance of mining. The information presented in this report is useful in that it broadens the deciionmaking base for management when either mine locations or coal conversicl plant sites, or both, are being considered.

Jan 1, 1971

By B. W. Madsen

A nearly dormant copper sulfide pilot-scale experimental leach containing 8.7 tons of are was injected with oxygen to determine its effect on the copper-leaching rate. Prior treatment of the uncrushed 0.25-percent-copper, mine-run stripping material consisted of 461 days of acid ferric sulfate leaching, which extracted 47 percent of the total copper. The permeability of the bed had decreased, and the percolation rate had decreased from an initial 20 gallons to 0.8 gallon per square foot per day. Copper extraction had nearly stopped. After injecting oxygen into the ore column and leaching for 30 days, the percolation rate was increased to 6 gallons per square foot per day. In an additional 298 days of leaching, an additional 40.7 percent of the copper was extracted. The improved leaching after the use of oxygen is attributed to stimulated bacterial action, better oxidation, and increased permeability.

Jan 1, 1975

By John A. Breslin

This publication provides an historical overview of research undertaken by the U.S. federal government over the last 100 years to improve the health and safety of our nation?s miners. Federal research efforts began with the establishment of the U.S. Bureau of Mines (USBM, or the Bureau) in 1910. They have continued over the past century, even after the Bureau?s closure in 1996. It is hoped that this publication will give the reader an appreciation for the work of mining health and safety researchers over the past century, and of the miners served by this research. Although not a comprehensive history, this report highlights the key organizational changes made within the Bureau and the federal government that affected mining safety and health research. Some mention is also made of Bureau research not directly related to mining health and safety. Note that the work classified as safety and health research has varied over the last century. For example, before 1970 the Bureau separated mining research and safety and health research. At that time, mining research included ground control and methane drainage because they had direct implications for mine safety. Explosives research was also reported separately from health and safety, even though permissible explosives research was obviously related to safety. Therefore, where budget figures from the Bureau are mentioned in this report, it is often not possible to separate safety and health research from other types of research. This history is generally chronological, with a few exceptions. Because of their prominence and direct links to Bureau research, most of the Public Health Service mining studies completed before 1970, when NIOSH was established, will be discussed in a single section, even though the work spanned many decades. Likewise, for convenience, the brief histories of the Bureau?s mining research centers are located in one section.

Feb 1, 2010

By Jack R. Woodyard

Scientists at the U.S. Bureau of Mines are studying iron aluminides as possible substitutes for stainless steels to reduce the Nation's dependence on imported strategic and critical materials. In a Bureau investigation on the mechanical properties of Fe-28Al, it was found that the material's machining properties were significantly improved at slow tool and feed speeds. Machining techniques normally used for brittle materials failed or were costly. Further experiments using a 5-in (12.7-cm) mill cutter with carbide inserts, operating dry at minimum machining speeds, produced visually smooth sample surfaces with no tool damage. As a result of these experiments and a review of published data on hydrogen embrittlement of iron aluminide under tension, non-water-based (e.g., sulfur-based) lubricants were chosen for production machining. Four-flute, 3/4-in (19-mm) carbide end mills were used at slow speed under lubrication. This latter procedure reduced tool wear and breakage by a factor of 2. Machined surfaces and specimen cross sections were analyzed by scanning electron microscopy to detect microcracking. Tensile tests gave the expected yield and ultimate strengths, indicating that no degradation by low-speed machining occurred. This study extends this work to show that the alloy can be machined at higher speeds using high-speed steel end mills, and that water-soluble cutting oil is a suitable lubricant and coolant.

Jan 1, 2010

By J. Dean Warner

In 1984, as part of a project to evaluate Alaskan occurrences of certain critical and strategic minerals, the Bureau of Mines investigated a columbium-bearing regolith on upper Idaho Gulch, near Tofty, AK. The regolith is derived from weathering of a dolomitic marble and consists mostly of iron oxide minerals with accessory apatite, zircon, xenotime, rutile, monazite, and the columbium minerals aeschynite, columbite, and ilmenorutile. Two regolith lenses contain 340,000 lb of columbium resources at an average grade of 0.07 pct. Calculated composite concentrates from two regolith samples (approximately 200 lb each) contained 53 and 57 pct of the columbium at grades of 0.97 and 0.86 pct, respectively. In each case the grade could be improved to 1.1 pct Cb with a sacrifice of 9-pct recovery. The regolith's mineralogy, trace-element geochemistry, and similarity to descriptions of other columbium-enriched regoliths suggest that the underlying marble may be a carbonatite. The lack of associated alkalic igneous rocks and the stratiform nature of the regolith, however, may be interpreted as evidence for sedimentary origin of the marble. The marble and regolith are a lode source for some of the minerals in the Idaho Gulch placer deposit.

Jan 1, 1986

By W. F. Marshall

This Bureau of Mines report discusses tests conducted with four different catalytic reactor designs to determine the influences of exhaust treatment systems on emissions from diesel engines. Although there was significant differences in oxidation efficiencies at light to intermediate engine loads, all four catalysts were very effective in reducing emissions at heavy loads. Compositional determinations included carbon monoxide, carbon dioxide, unburned hydrocarbons, oxides of nitrogen, aldehydes, sulfur dioxide, sulfates, and particulate loading. Particulate size, exhaust odor intensity, and the character of the unburned hydrocarbon component were also determined.

Jan 1, 1978

By J. D. Ramsdell

The study described in this report was undertaken to obtain information on the character and effect of antimony additions to titanium. The availability of high-purity, low-hardness titanium metal, resulting from fused-salt electrorefining techniques, permitted a reassessment and evaluation of the physical behavior of titanium-antimony alloys. Alloys, based on several grades of titanium containing up to 10 percent antimony, were arc-melted and processed to sheet by hot and cold rolling. Properties and characteristics were evaluated by hardness tests, hot and cold rollability, annealing treatments, metallographic examination, and tensile tests.

Jan 1, 1960

By S. W. Parr, T. E. Layng

There is presented below the results of experiments made on six samples of Utah coals furnished through the U. S. Bureau of Mines , under an agreement dated June 16th , 1920. The details of all values for all runs are tabulated and presented herewith . Clear The samples, consisting of approximately 150 pounds each, were received at the University of Illinois , on June 15 , 1920 , and are listed as follows : Creek , Wattis , Castle Gate , King , Standard , and Aberdeen . The proximate and ultimate, analyses of the various ccals from that region , representing all the types included in these samples , have already been made by the Bureau of Mines , and are available . * Similar determinations were also made on the particular samples forwarded for purposes of these experiments . The results obtained on the coal as received did . not very in any material feature from the values reported by the Bureau, they are shown in Table 1. It is of importance to note only that the oxygen content is uniformly high , namely approximately 9.5 to 11.5 per cent of the as- received coal , while the oxygen - hydrogen ratio is also high, being on the average approximately 2 ( oxygen) to 1 ( hydrogen) .

Sep 1, 1921

By H. H. Schrenk, L. B. Berger, Robert L. Beatty

"INTRODUCTION Toxic oxides of nitrogen 5/ are formed or liberated in many industrial process and may constitute a definite hazard to the health of persons exposed to the atmospheres thus produced. Oxides of nitrogen occur in the gases involved in the use of explosives, in the gasoline products of welding operations in the exhaust of internal-combustion engines, in the vicinity of electrical discharges, in the combustion of nitrated materials, and in chemical process involving nitration or the use of nitric acid, Itis evident that oxides of nitrogen may constitute an occupational hazard in many industries, and therefore it is important that those concerned with the control of such hazards be equipped with a technique suitable for the determinations of oxides of nitrogen in the concentrations of,hygienic significance."

Feb 1, 1943

By H. V. Makar

The Bureau of Mines successfully demonstrated, on a pilot plant scale, a sodium sulfate (Na2S04) refining process for removal of copper from molten ferrous scrap. Previous tests established technical feasibility on a bench scale for achieving low copper concentrations and determining the principal factors controlling process efficiency. The pilot plant study involved a 1-ton arc furnace for melting ferrous scrap and a 1-1/2-ton treatment ladle. Results of these tests showed that copper removals obtained in laboratory tests (approximately 40 relative percent copper removal with 10 weight-percent surface addition of sodium sulfate) could be achieved on the pilot plant scale when excess carbon was added with the sodium sulfate compacts. Data were obtained on temperature losses and carbon consumption related to Na2SO4 treatment.

Jan 1, 1974

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

1, Introduction This report is submitted in fulfillment of the requirements of USBM Contract No. J0255017, "Development of Emergency Escape Systems Guidelines for Underground Metal and Nonmetal Mines" Under this contract the history of past mine fires was studied. Representative metal and nonmetal mines were surveyed and escapeways, refuge chambers, life support, and emergency hoist requirements were studied to determine the problems in complying with the proposed regulatory standards and their enforcement by MESA Mine Inspectors. In addition, a computer program was written to evaluate mine evacuation performance. The completed program is included in the appendix. 1. 1 Historical Review of Metal and Nonmetal Mine Fires Early records of mine fires are poorly documented because there was no statutory provision for reporting fires to the Bureau of Mines. The survey of representative mines during the course of this contract indicated that many small fires still go unreported even though they are now required to report all fires A recent report survey approximately 80 disasters in metal and nonmetal mines, (6 ) Table I is a summary of some of these fires. Historically most metal and nonmetal mine fires have been caused by electrical problems. Spontaneous combustion and the use of welding equipment are the other major causes of mine fires(14) Although not documented, many mine personnel agree that 30 percent to 40 percent of underground metal and nonmetal mine fires have their origin from cigarettes and other smoking related materials. The number of fires related to spontaneous combustion is decreasing and equipment fires are on the increase. The reduction of spontaneous combustion fires can be attributed to the use of sandfill in more mines and the increase in equipment fires to the increased use of LHD equipment.

Jan 1, 1976

By B. W. Gandrud

At the Southern Experiment Station of the Federal Bureau of Mines, reports are prepared from time to time on results of washability studies of commercially important coal beds in the Southern Appalachian region. The investigations that provide the material for these reports are made by the Bureau of Mines, United States Department of the Interior, in cooperation with the University of Alabama and the mine operators. This report records the results obtained on a sample of run-of-mine coal taken in June 1953 from the Pratt bed at the Davidson Coal Co. mine about 1 mile west of Graysville, Ala. One of the main objectives of a washability study is to obtain technically and commercially important data in connection with the best methods for preparing and utilizing the Nation's limited reserves of good coking coal. Such information is important from the standpoint of conservation in that it facilitates selection of preparation methods that will yield an acceptable grade of coking coal with a mini-mum of losses of coal in the rejects. The Pratt bed is one of the main sources of coking coal in the Jefferson County part of the Warrior field. This is the first time, however, that data from a complete washability study of coal have been obtained from this bed in Jefferson County. In the Graysville area, Pratt-bed coal has good coking characteristics and is used for blending with other coals in making metallurgical coal. The extent of its use in such blends is severely limited in this area, however, by the fact that it has a high sulfur content, which has not been reducible to any great extent by washery treatment.

Jan 1, 1955