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By Kurt Herzog

State-of-the-art automation information technology and connectivity enables the digitalization of steel production that goes far beyond conventional automation of industrial production. Initiatives have been started around the globe to foster digitalization like IIoT (Industrial Internet of Things) in the US, Industrie 4.0 in Germany or China 2025. Primetals Technologies is actively driving the digitalization shaping the future of steel production. Intelligent combination of sensor technology combined with digital models as well as quality and production planning and control systems leads to new dimensions in product quality and production cost reduction. New diagnostic ways allow intuitive fault tracing or processing to support faster maintenance. Digital assistants support both operation and maintenance using context-oriented or self-learned information.

Oct 30, 2017

By Rodrigo Fina Ferreira

This paper presents a mineral liberation study on two iron ore samples from the Quadrilátero Ferrífero, in Brazil: compact itabirite of low-grade metamorphism (CI) and friable itabirite of high-grade metamorphism (FI). The quartz liberation spectrum for both samples have been obtained through QEMSCAN analyses, carried out for several comminution degrees, to compare the liberation characteristics and to evaluate the evolution of the quartz’s liberation degree after fragmentation. The results have shown significant differences in liberation spectrum between the itabirite samples studied. The liberation process of FI was easier than of CI, due its high porosity and larger crystal size compared with CI, which has shown more complex mineral assemblages with low porosity and smaller crystals. The quartz liberation spectrum has shown that grinding at P95 of 0.210 mm for the FI sample, and of 0.045 mm for CI sample, should result in satisfactory liberation for subsequent concentration step.

Aug 1, 2018

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018

By Jônatas Venancio Barbosa, Dagoberto Brandão Santos, Túlio Magno Füzessy de Melo

In this work, the mechanical and metallurgical behavior of titanium added ultra-low carbon (ULC-Ti) steel under hot and warm working conditions was studied by means of dilatometer compression tests. Double compression schedules were performed at temperatures between 700°C and 1000°C, inter-pass times of 0.5-100 s, and deformations of 0.5 and 0.3 in the first and second stages, respectively, with strain rate of 1 s-1. The analysis of the flow curves obtained allowed the evaluation of the softening characteristics of the steel. The softening and microstructure features indicate different restoration mechanisms depending on the temperature range. Static recrystallization with rapid microstructure restoration is observed at temperatures within the austenitic and intercritical field. Strain induced boundary motion and recovery mechanisms apparently control the restoration process in the ferrite region. In general, flow stress curves showed dynamic recovery behavior. Only the deformation in the intercritical region produced a peak in the flow stress curves. Isothermal holding tests associated with single hit compression indicated the presence of dynamic strain induced transformation, accelerating the softening kinetics at the intercritical region.

Oct 1, 2019

By John Hinton

Electromagnetic based (EM) sensor technology has been shown to detect changes in the magnetic permeability of steel strip travelling down the run out table after rolling. Measuring below the Curie temperature, these changes can be interpreted in terms of the phase transformation from austenite (paramagnetic) to ferrite (ferromagnetic). These real time measurements provide a detailed insight into the changes in the structure at high temperature providing the steel producer with feedback on quality control, product consistency and product development. However unlike mill microstructure models, the sensor measurement provides a point reading at a distance through the cooling course. To map the transformation in more detail, a sensor array is required along the length of the Run Out Table i.e. to measure points on the austenite to ferrite transformation curve. This paper describes the process and metallurgical factors that should be considered in the optimum design of a sensor array, i.e. the number and location of the sensor heads. Examples of cooling strategies for different steel grades e.g. low carbon, structural and dual phase steels are used to demonstrate the importance of sensor location. In addition, the effect of variability within typical industrial parameters e.g. cooling speed, on the sensitivity of sensor output and location will be considered.

Oct 1, 2019

By Guilherme Corrêa Soares

Deeper understanding about the strain hardening behavior of steels has become necessary due to its importance in industrial processes such as mechanical cold forming, rolling and drawing. In this work, the strain hardening behavior of AISI 304, non-grain oriented electrical (NGO) and dual phase steels was investigated. Tensile tests were performed and the strain hardening behavior of each steel was studied by the Hollomon’s equation. X-ray diffraction measurements and hardness tests were also carried out in order to characterize the specimens. Different work hardening stages were observed in each steel during the deformation process. The results obtained are discussed in terms of the relationship among the instantaneous strain hardening coefficient, hardness and eventual phase transformations. The instantaneous strain hardening coefficient of dual phase and NGO increases after the yield point, rapidly reaching its maximum and then steadily decreases until tensile strength is reached. In AISI 304’s case, the strain hardening coefficient keeps raising to high values in response to a large strain and then rapidly decreases before reaching the tensile strength. In comparison to the other steels, AISI 304 shows higher instantaneous strain hardening coefficient value, which persists even in large strains. This is a consequence of its strain hardening mechanism based on stress-induced martensite transformation.

Aug 16, 2017

By Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Antônio Cezar Faria Vilela

A minor change in the chemical composition and temperature affects the slag viscosity, which has a great extent of the physical properties in regarding refining slags. Optimizing those parameters may affect the steel cleanliness. The viscosity measurement process is considered expensive, so the cost-effectiveness does not favor the measures at high-temperatures. Alternatively, it is possible to apply mathematical models or thermodynamic softwares to obtain viscosities for a given range of chemical composition and temperature of slags. The present work contemplates a validation of the experimental data, collected in the literature, with a calculated data and proposes an accurate representation of iso-viscosity curves applied for secondary steelmaking slags, covering the composition ranges: 0–100 wt.% CaO, 0–80 wt.% SiO2, 0–77 wt.% Al2O3 and 0–15 wt.% MgO (CSAM) system at 1500ºC. The viscosity representation fields include fully liquid and a partially liquid slags in the CSAM system and the viscosities were calculated using the FactSage 7.2 (for Liquid Phase) and the Roscoe-Einstein equation (for Phase mixture) for a total of 5976 slags. The preliminary results indicated that there is a great convergence between the calculated and experimental viscosities data, promoting an efficient approximation of the iso-viscosity curves for the CSAM slag system in the high-temperatures.

Nov 1, 2019

By Hiago Antunes Amador de Oliveira, William Pratt Rogers, Aaron Young

Monitoring systems are highly critical components in the safety of tailings storage facilities (TSF). Internet of things (IoT) platforms present a unique way to improve TSF monitoring systems. Since there are so many available IoT technologies, this conference paper aims to create a focused list of IoT options for improving TSF safety. To achieve this aim, a brief qualitative review of available literature and state of the art technologies is presented in Section 2. The article further assists this aim by summarizing the benefits of IoT platforms which have been found in the literature. With respect to findings, literature suggests that while sensor technologies have existed as solutions for tailings dams for many years, IoT greatly reduces the cost of deploying, monitoring, maintaining, and gaining insight from these sensors. Additionally, IoT removes the need for manual data collection from sensors, enabling the monitoring of tailings dams from miles away and the use of new sensor technologies. Therefore, as a conclusion, this article recommends that IoT capable monitoring systems be considered for use in TSF monitoring.

Oct 3, 2019

By Rafael Abreu Fraga, Carlos Noberto Paula da Silva, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Since 2016 Gerdau Ouro Branco has been producing steel plates of various qualities and grades. However, it was not until 2018 that the first plates produced by accelerated cooling process were made available for external testing, in this case for large diameter UOE pipes manufacturing. Recent line pipe and OCTG specifications are showing that the oil and gas market still consumes regular API grades, such as X60, X65 and X70, however with increasing wall thicknesses, reaching values up to 1.5 inches. These specifications also demand longitudinal and transverse tensile guarantees and drop weight tear tests in temperatures as low as -40°C. Projects with these types of mechanical properties present process requirements as challenging as those necessary for higher API grades in lower thicknesses. This paper shows the steel design concepts and rolling routes for achieving the necessary properties for X70 steel plates in 28.15 mm. The microstructural features were also investigated and associated with the production process and the tensile and toughness results. Finally, challenges such as tensile anisotropy and DWTT abnormal fracture are presented.

Oct 1, 2019

By Yong Tian, Tian Zhang, Zhao-Dong Wang

To meet the requirements of high-performance steel plates, while reducing manufacturing costs and saving energy, the advanced cooling system for plate mill (ADCOS-PM) with functions of accelerated cooling (ACC), ultra-fast cooling (UFC), and direct quenching (DQ) was researched and developed by the State Key Laboratory of Rolling and Automation (RAL). Since 2003, several sets of ADCOS-PM device were developed and implemented in industrial practice. To fully utilize the ADCOS-PM technology, the combination of various strengthening mechanisms was promoted by NG-TMCP technology and low-cost, high performance plates were produced such as pipeline steels, and high-strength construction machinery steel.

Oct 1, 2019

By Hiroshi Ichikawa

In 2013, Nippon Steel & Sumikin Engineering Co., Ltd. (hereafter referred to as NSENGI), Tenova HYL and Danieli have entered into an agreement to combine ENERGION DR technology into blast furnace technology and/or with syngas technologies. This new alliance will allow the three companies to combine research and development activities with their respective expertise in ENERGIRON DR technology, Blast Furnace technology and Syngas (by-pro gas and coal gasification) technology, with the ultimate objective to develop breakthrough iron making technologies and create such EPC projects. This paper introduces the concepts and the features of our breakthrough technologies of combining of ENERGIRON DR technology, Blast Furnace technology and Syngas technology.

Aug 16, 2017

By Luca Tommasi

Danieli complemented its wide range of production plants for the iron and steel industry with a further step upstream into iron ore pelletizing and beneficiation. Danieli has engineered and constructed a state of the art and fully automated pilot plant facility – pot grate and sinter box – at Altos Hornos de Mexico S.A. (AHMSA) Pelletizing Plant, Monclova, Mexico. Installation and commissioning were completed in October 2009. Key features of the pot grate include the avoidance of the need for operator intervention during the test, automatic system preheat, absence of dead time, heat recuperation system with an air/air heat exchanger, oxygen control in preheating and firing with zirconia oxygen analyzer, possibility to test deep beds up to 625 mm. A series of projects have been accomplished by AHMSA availing of the pot grate facility with the aim to enhance pellet plant productivity and to reduce operating costs. The results obtained by use of Danieli pot grate combined with the experience and skill of plant operators has shown significant technical and economical benefits thus fully justifying the initial investment made by AHMSA and confirming the importance of having an in-house testing facility in order to optimize industrial plant operations.

Aug 16, 2017

By Luiz Bruno de Oliveira Araujo, Luciano Morais Teixeira, Luiz Gustavo Pedrosa de Melo, Altair Lúcio de Souza

The off-line simulation of the metallurgical process in an industrial line brings several benefits such as: evaluation of the influence of the main parameters that affect the results of the process, comparison between different set ups, greater assertiveness in operational adjustments, process optimization and reduction tests for development of new products. With this objective, a software for offline simulation of the hot strip mill process of Gerdau Ouro Branco was developed based on the logic of calculations implemented in the online model. The software results in important process variables such as mill pass scale, load, torque, and power at each pass, temperature and the hot mean flow stress of the simulated material. During rolling mill process the strip presents different temperatures and time between passes for different points along the length, which directly influences the hot strength of the product and consequently in the calculated variables, thus the calculations executed by the software were divided to three points of the strip, head, body and tail bringing the individual results to each of these positions.

Oct 1, 2019

By Wolfgang Kern

More and more coke oven plants worldwide face the task to improve their emission reduction at their coke oven batteries. In the 90’s PROven® was invented and developed by DMT to regulate the inner pressure of a single coke oven chamber. Generally, most of the coke oven chambers can only close and open their connection to the collecting main but without the possibility to regulate the pressure during the carbonization time. Through the installation of PROven® the load on the coke oven door sealing system and the charging lids will be decreased and so does the emissions of crude COG as well. The current PROven® system, installed in the collecting main, does not only regulate the chamber pressure, it replaces the valve between the goose neck and the collecting main, too. This variable pressure control allows decreasing the leakages at the emissions sources to a minimum and allows operating the collecting main under optimum pressure. Subsequently, this will lead to enhanced emission reduction. PROven® proved its value with more than 2,100 units installed by licensee worldwide. Nevertheless, DMT is always focused on its client’s needs and therefore enhance PROven® to provide the Best Available Technique (BAT). Among the main features of the now available system is the plain arrangement with a higher reliability and the possibility to install the system outside of the collecting main without modifying it. Hence, upgrading coke oven plants during operation is possible without any noticeable impact on the plant operation.

Aug 1, 2018

By Alberto Tremea

The eddy current system is universally recognized as a most suitable method to point out discontinuities or modifications on the roll surface. The automation of the controls through the implementation of sophisticated equipments on the grinding machine has favoured its employment in the roll shop. A big effort is still going on to clarify the best way to promptly identify situations that could be really unsafe for the roll life. The results presented in this paper have been obtained through an intensive activity conducted in field by Innse Cilindri on work rolls of finishing stands of hot strip mills. The correct interpretation of the eddy current signals and a good calibration of the automatic system have allowed, in many cases, a substantial optimisation of regrinding practices.

Aug 16, 2017

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Rodrigo Sanchotene Silva

Currently the industries of paint have directed their efforts on cleaner production of products that provide effective performance in corrosion protection of metallic materials. This work search introduce a new alternative of organic coating, without the presence of hazardous metals and replace equipments commercials used method of anodic protection for protection of oxidized metals. From this it, was produced Smart Paint (SP), consisting of Paint Acrylic Commercial (PAC) mixed the 1 % of binder, compound by the conducting polymer, Polyaniline Emeraldine Base (PAni EB) and plasticizer 4-chloro-3-methylphenol. The SP and PAC were applied to plates of carbon steel AISI 1010, with the aid of dip coat technique and then were subjected to drying for 48 h. The SP was characterized by thermals and physicochemical analyzes in order to verify possible changes in chemical properties of the ink produced, beyond perform electrochemical tests of Open Circuit Potential and Electrochemical Impedance Spectroscopy, employing equipment Potentiostat/Galvanostat Autolab PGSTAT302 Ecochemie, and aqueous 2 mol.L-1 of H2SO4. The results obtained allow us to state that the plasticizer does not alter the electrochemical properties of PAni and application of binder PAni EB to PAC does not alter the physicochemical properties of commercial coating. The binder PAni EB adds to PAC the capacity to induce the formation or maintenance of protective oxides in oxidizable metals submitted to harsh environments, method known as anodic corrosion protection.

Aug 8, 2018

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019

By Michel Rodrigo Luiz, Glaucio Augusto Polini, Giardini F. Lazzarin

ArcelorMittal's pickling and cold rolling line has been demanded to increase production since the installation of equipments in 2015. In addition to the improvement in productivity related to these new equipment, one of them the automatic surface inspection system (SIAS), work has also been developed in other equipment seeking improvement of production indicators. The present article exposes the actions and gains that were achieved with actions on two equipments in the same section as the Side Trimmer. The first one deals with the optimization of time gains with sequencing adjustments without financial contribution, using only internal labor seeking reduction of unproductive times by adjustments of the side trimmer in the cold strip mill. The second item discussed demonstrates the actions and the gains generated due to the availability of new resources (installation of SIAS equipment), the optimization of these resources seeking a focus on the reduction of ruptures in the tandem cold mill, configuring the same in the aid of the identification of critical defects and also in the automatic speed reduction action of the tandem cold mill in defects considered serious. In both cases the intention was to improve production, seeking to improve the results of the section and the line.

Oct 1, 2019