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By A. W. Ashbrook

There are many methods of analysis available for compounds similar to those used in solvent extraction processes. However, the majority of these methods are not directly applicable to the determination of solvent extraction reagents, especially in raffinates. The number which are applicable is further reduced if limited to the more simple methods suitable for process control purposes. Commercial extractants are complex mixtures. The complexity is increased by the addition of diluents and modifiers in two-phase systems containing metals. Raffinates from solvent extraction processes contain the more polar components of the extractants and the products of decomposition. Only a limited amount of information is provided by total organic carbon or spectrophotometric analysis. The complexities of the systems require a combination of methods.

Jan 1, 1978

CURRENT MATTERS Page Page New York Meeting : v 27th Engineers xl Year Book, 1918 v Professional Classes War Relief. x1i Minutes of Meeting, Board of W. S. S x1i Directors vi American Engineering Standards xlii President's Report vi Hadfield Prize xlv Local Section News: Members in Military Service... xlviii Columbia xiii Personal li San Francisco xiv Positions Vacant liii New York xvi _ Engineers Available liv Southern California xxxi Forthcoming Meetings 1v United Engineering Society xxxii Library...% lvi Engineering Council xxxv Membership lix Other Societies: Institute Committees lxxviii Mining and Metallurgical Soc- Officers and Directors lxxxvi iety of America xxxix

Jan 3, 1918

Jan 1, 1945

By P. I. Lipman

Largely forgotten by today's environmentalists and mineralogists is a pioneer scientist of the nineteenth century named Ellen Swallow. Fortunately, the memory of her accomplishments has been resurrected by Robert Clarke in his biography, Ellen Swallow: The Woman Who Founded Ecology. Her direct contributions to the field of mining included authoring First Lessons in Minerals and an analysis of the rare mineral samarskite which indicated the presence of an insoluble residue; her findings led to the eventual discovery of samarium and gadolinium. While enjoying the distinction of being the first woman student at the Massachusetts Institute of Technology, she successfully isolated vanadium in an ore which other experts had examined without detecting the metal.

Jan 1, 1974

POSITIONS VACANT No. 157. Superintendent for roasting. and magnetic separating plant working on zinc concentrates. Must have mechanical experience and a working knowledge of electricity. Salary will depend on experience and results obtained. Location Canada. No. 155. Metallurgical chemist familiar with copper and steel for company just starting. Must have had technical education and practical experience with both metals. Salary moderate at beginning, but will be increased as business grows. No. 159. An experienced, up-to-date coal-mining engineer to open up and manage soft-coal mines in Spitzbergen, preferably a Scandinavian capable of handling Norwegian laborers. Employment beginning January.

Jan 12, 1916

By Emil Schroedter

The death, on May 6,1908, of Dr. Hermarnn Wedding, Privy Mining Councilor of the Kingdom of Prussia, and Professor of the Metallurgy of Iron and Steel at the Royal Mining Academy of Berlin, was a loss keenly felt by the whole metallurgical world. Not alone in his native land, but also in foreign countries, did he enjoy an esteem of which the title of honorary membership in the American Institute of Mining Engineers, the United States Association of Charcoal Iron-Workers, and the (British) Iron and Steel Institute bears eloquent testimony.

Jan 1, 1910

By N. D. Policow, J. S. Orphanos

Dewatering fine clean coal fractions, -595µm (-28 mesh), represents one of the most difficult and costly separations in typical plant circuits. Since 1969, the screen bowl centrifuge has offered an economical alternative to filtration/thermal dyer combinations. The performance of screen bowl centrifuges has been continuously modified and improved to dewater not only coarser coals, but also today's variety of ultrafine material. Test comparisons with alternative methods show the screen bowl centrifuge to be most cost effective and efficient when all factors are considered.

Jan 1, 1984

By C. W. Spencer, K. A. Semlak, F. N. Rhines

IN an effort to obtain a better understanding of sintering in the presence of a liquid phase, it was decided to study the rate of capillary rise of a relatively low melting liquid metal in a higher melting metal powder compact. By assuming that the metal powder compact consists of a great number of parallel capillary tubes and that the flow of liquid

Jan 1, 1958

By Sherwin F. Kelly

Airborne techniques enter hard rock exploration field. . . the gap between pure geophysics and engineering seen as closing rapidly.

Jan 2, 1951

For the year ending February, 1926 PRESIDENT J V W REYNDERS, District 0 NEW YORK, N Y PAST PRESIDENTS E P MATHEWSON, District 0 NEW YORK, N Y WILLIAM KELLY, District 5 IRON MOUNTAIN, MICH FIRST VICE-PRESIDENT E DEGOLYER, NEW YORK, N Y TREASURER , CHARLES F RAND, NEW YORK, N Y SECRETARY FREDERICK F SHARPLESS, NEW YORK, N Y

Jan 1, 1923

By C. A. Mezger

These districts are limited approximately on the north by the railroad from Salisbury to Ashville, and comprises the counties of Alexander, Catawba, Burke, Rutherford, McDowell, Cleveland, Lincoln, Polk and Henderson in North Carolina, and Greenville, Spartanburg, Union and York in South Carolina. The occurrence of monazite at Amelia Court House, in Virginia, belongs evidently to the same geological system, as its distance from the Alleghenies corresponds with that of the above-mentioned districts, and all the stratification runs parallel with those mountains.

Jan 1, 1896

Jan 1, 1937

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Jan 1, 1938

Coal was produced in this state, by white men, at an earlier date than in any state west of the Mississippi River, and for many years its production was larger than that of any state in that area. The coal immediately adjacent to St. Louis was mined commercially earlier than elsewhere because of a ready market which could be reached by teams. Generally the coal seams are more or less "spotty" in character, and in many places openings made in thick coal could only be mined for a few years. All of the data available from state survey reports, county histories and a few other sources are shown in Table 66.

Jan 1, 1942

By R. E. Lund, D. E. Warnes

SELECTIVE sulfation of individual constituents in ores or metalliferous products has received increased attention in recent years. The fluid-bed reactor with its advantages of close control of both temperature and atmosphere promises to have ap-

Jan 1, 1958

Jan 1, 1930

Elected Died 1884 *ADDY, MATTHEW 1896 1894 *ALLFN R B 1896 1874 *AMIOT, H 1892 1886 *AMSLER, CARL 1894 1895 *ÅNGSTROM, CARL 1901 1895 *ARMSTRONG, JOHN F 1898 1882 *ARNOLDS, HUGO 1886 1875 *ASHBURNER, CHARLES A 1889 1872 *ASIIBURNER, WILLIAM 1887 1883 *ATKINS, C M , JR 1885 1897 *AYERS, WILLIAM 1898 1885 *BABCOCK, GEO H 1893 1884 *BAILEY, EDWARD 1889 1880 *BAILEY, JACKSON 1887 1900 *BALLOU, FRANKLIN 1903 1886 *BARNES, F W 1892

Jan 1, 1910

By Paul Klopstock

(Butte Meeting, August, 1913.) THE Kennedy mining district is situated about 55 miles in a southerly direction from Winnemucca, and about the same distance south-east from Battle Mountain : two towns situated oil t the main line of the Southern Pacific railroad. History. Prospectors were first attracted to the district by the reported discovery of gold by Chinamen in Cinnabar creek in the early 90's. The prospectors came from the rich placer workings in and about American canyon ; but the new diggings were not found sufficiently rich to justify their being, worked as placer properties, and the prospectors started work in a number of places, looking for the veins which had fed the canyon. In 1893, Charles E. Kennedy, a prospector who had been attracted by the reported discoveries in the vicinity, left Hawthorne and came to the present site of the town of Kennedy. Within a short time he discovered the vein known as the Imperial, and proceeded, with the aid of some friends, to develop it. The vein was readily traced for a distance of about a mile, and about $10,000 worth of high-grade ore was shipped to the Utah smelters. At about the same time the Lawler Brothers, who had been prospecting in the district for some time, located the ?Gold Note group," which showed some extremely rich ore. Within a very short time they extracted from 'the Gold Note vein 150 tons of ore, which was shipped to the Utah smelters, and netted about $105 per ton above all expenses. Their good fortune attracted attention to the camp, and within .a short time a town was laid out, with a population of about 500 people. It was named in honor of Kennedy, who had made the first discovery of pay ore in the district.

Jan 6, 1913

By David C. Grant, Erich W. Tiepel

In situ mining is a process for recovering uranium from relatively small or low grade ore bodies. The process involves passing a lixiviant and oxidant, typically NH4HC03 and H202, through a uraniumcontaining ore body. As the solution progresses through the ore body, the uranium is oxidized from the plus four to the soluble plus six state. The bicarbonate complexed uranium laden solution is removed from the ore body and the uranium recovered in an above-ground processing plant. During the leach process lixiviant cations may be sorbed on the ore host, if the host contains exchangeable clay minerals. This report examines the implications of this clay interaction on ground-water quality, the various available in situ mining restoration methods, laboratory procedures for simulation and development of those methods, and the results of using the restoration methods in the field. Various restoration methods, including ground-water sweeping, clean water recycle, and chemical restoration are presented and discussed. The use of ore characterization, agitation leach tests, and column tests to study cation sorption and desorption, and thus, to identify and evaluate restoration methods is discussed. Ore characteristics identify the clay type and clay content, which allows the estimation of the magnitude of the cation sorption by that ore. The chemical effects of clay exchange and of chemical restoration can be examined using agitation leach experiments and packed ore column tests which also provide information on the physical effects. The agitation leach test is a relatively rapid means of determining the sorption and desorption characteristics of an ore. Unlike agitation leach tests, column tests can be used to assess the influence of solutions on permeability, on precipitation problems, and on other chemical changes. The effectiveness of using restoration methods, which were developed and tested in the laboratory, are examined by presenting field restoration data from several mining sites.

Jan 1, 1979

By W. J. Feuerstein

STRUCTURAL imperfections in crystals, in recent years, have received the attention of metallurgists concerned with single-crystal properties. Certain etching solutions cause local variations in the rate of etching at dislocations.' Dislocations are expected to be preferred segregation sites for impurities' and Dash" has shown that precipitation of copper occurs preferentially at edge-type dislocations in silicon. Diffusion rates along dislocations are probably higher than rates through more perfect crystalline regions.' These and other phenomena which may be influenced by dislocations may be studied by revealing dislocations as etch pits. This study was undertaken to develop an etch solution for silicon crystals to reveal low-angle grain boundaries associated with dislocation arrays and also etch pits with good contour definition. Additional etches have been reported by Dash," Vogel and Lovell.T rystals were sectioned on crystal lographic planes at various angles from the growth direction for microscopic examination of the etch pits. Experimental Crystals of 75-100 g mass and 3 cm diam were oriented and cut on crystallographic planes. Crystals were grown by Czochralski technique from a quartz crucible. Lapped wafers were chemically polished in a modified CP-4 etch for 1 min (bromine was deleted from the etch solution). The polished wafer was then etched* at room temperature for 5 min. The use of larger amounts of H2O and/or CH2COOH slows the reaction. The Cu(NO3),.3H2O was added to increase the reaction rate and give more definition to the etch pits developed. Some pertinent features concerning the attack of this etch on silicon can be summarized as follows:

Jan 1, 1959