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By Leonardo Araújo Peruch, José Fagundes, Henrique Carneiro Pinto, Marco Túlio Costa, Nayara Coutinho, José Fabiano Martins Assunção

The objective of this project was to increase the hot charge by reducing reheating energy consumption and raising the productivity of ArceloMittal Tubarão's hot strip mill by changing the HSM’s schedule process with optimization of the relocation process of slabs after HSM’s chance with focus on slab temperature in reheating time. The project began with the revision of metallurgical rules for the relocation of materials, definition of criteria temperature setting (hot / cold), definition of restrictions of the process and review of modus operandi scheduling process. With the implementation of the process / system it is expected to achieve a 10% increase in the hot charge index in slabs reheating furnaces and increase productivity of the ArcelorMittal Tubarão hot strip mill

Oct 3, 2019

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By Osvaldo Guilherme Comineli

An extensive investigation into the role of low copper contents on the hot ductility of C-Mn-Al steels has been carried out in order to better understanding the problem of “hot shortness”. Previous work has suggested that this problem results from the build up of Cu that occurs at the surface of the steel as a consequence of the preferential oxidation of iron. This causes the formation of a Cu-rich film of low melting point. A nickel addition has been reported as a solution to the problem, since it increases the solubility of copper in the austenite. After hot tensile testing to failure, samples of Cu-containing steels have been examined using optical, scanning and transmission electron microscopes. Recently published results indicate that copper, in addition to precipitating out as CuS, also segregates to MnS inclusions forming a shell around them. This does not seem to impair the hot ductility under an inert atmosphere, but may have serious consequences under an oxidising environment and lead to “hot shortness”. The influence of nickel in improving the hot ductility seems to be due to it forming a higher melting point alloy with the segregated copper. Data from this incomplete work also suggests that Ni reduces the precipitation of CuS particles. Current investigation carried out using confocal microscopy still to be completed will improve the understanding of the role of copper and nickel on the problem of “hot shortness”.

Aug 8, 2018

By Gustavo Borges Tiboni

The erosive wear caused by the impact of solid particles against a surface is a tribological phenomenon present in many segments of the industry, such as transportation, aerospace, mining, power generation, among others. The most usual method to set the wear rate is by measuring the mass loss of the material. In order to apply one technique with potential to determine the rate of erosion wear, this study developed a dedicated equipment and conducted preliminary erosion tests monitored by non-destructive testing known as acoustic emission technique (AE). This can be defined as a technique able to detect mechanical waves generated by the release of elastic energy accumulated in the material. Erosion tests were performed in order to evaluate the ability of equipment to collect data from AE and to correlate these data with the wear of the samples. Samples of low carbon steel eroded by the impact of angular aluminum oxide particles suspended in air at three different velocities: 45, 57 and 67 m/s. The impact angle between the particles and the sample was set at 30 degrees and the test temperature at approximately 20°C. The wear rate has changed with the velocity in accordance with the kinetic energy of the particles and the AE parameter RMS showed sensitivity to the variation of particle impact velocity and to the wear of the sample eroded. The rate of AE signals collected over time correlated with the flow of particles striking the sample, and with the parameters of energy, rise time and duration of the signal.

Jul 31, 2018

By Douglas Glenn Stalheim

Production of structural steel with a minimum yield strength of 700 Mpa produced as hot rolled coil has become increasingly popular due to cost considerations when compared to quench and temper equivalent product. This grade when produced as hot rolled coil requires the use of microalloy precipitation strengthening mechanisms. This is typically a combination of niobium and titanium microalloys. While the metallurgical concept of structural steel precipitation strengthening mechanisms has been well researched and published, actual implementation into the production process can be very challenging. In addition to achieving a minimum yield strength of 700 Mpa, in many applications additional mechanical property attributes of formability as measured by hole expansion testing along with low temperature toughness properties are now required. Achieving a balance of all the mechanical properties in a stable and repeatable performance in production using microalloy precipitation strengthening mechanisms further increases the challenges. This paper will discuss the metallurgical/process strategies required to successfully produce 700 Mpa minimum yield strength hot rolled structural steel coil. In addition, the role and goals of both niobium and titanium in this product design will be presented.

Oct 30, 2017

By Guilherme Corrêa Soares

Deeper understanding about the strain hardening behavior of steels has become necessary due to its importance in industrial processes such as mechanical cold forming, rolling and drawing. In this work, the strain hardening behavior of AISI 304, non-grain oriented electrical (NGO) and dual phase steels was investigated. Tensile tests were performed and the strain hardening behavior of each steel was studied by the Hollomon’s equation. X-ray diffraction measurements and hardness tests were also carried out in order to characterize the specimens. Different work hardening stages were observed in each steel during the deformation process. The results obtained are discussed in terms of the relationship among the instantaneous strain hardening coefficient, hardness and eventual phase transformations. The instantaneous strain hardening coefficient of dual phase and NGO increases after the yield point, rapidly reaching its maximum and then steadily decreases until tensile strength is reached. In AISI 304’s case, the strain hardening coefficient keeps raising to high values in response to a large strain and then rapidly decreases before reaching the tensile strength. In comparison to the other steels, AISI 304 shows higher instantaneous strain hardening coefficient value, which persists even in large strains. This is a consequence of its strain hardening mechanism based on stress-induced martensite transformation.

Aug 16, 2017

By Xihuai Gong, Hongshuang Di, Jianping Li, Ning Yan

In this work, we investigated the effect of the rolling process (warm-rolled or cold-rolled) on microstructure evolution and mechanical properties of 9Mn steel. After intercritical annealing at 670°C for 10min, both cold-rolled and warm-rolled microstructures are composed of ultra-fined austenite and intercritical ferrite. The austenite in warm-rolled sample includes two types of morphology, namely equiaxed and lamellar, which exhibits a wide distribution of grain-size. The incomplete recrystallization or recovery behavior of ferrite in warm-rolled and annealed sample results in higher yield strength and shorter yield point elongation. Moreover, the warm-rolled and annealed sample extends the TRIP-related work hardening over a broad strain range, resulting in a better combination of ultimate tensile strength and total elongation.

Oct 1, 2019

By Dalila Chaves Sicupira

A pitting corrosion study of welded joints of lean duplex stainless steel (LDSS) UNS S32304 has been performed. LDSS S32304 thick plates were welded by different processes commonly employed in equipment and piping construction: SMAW (Shielded metal arc welding), GMAW (Gas metal arc welding) and FCAW (Flux cored arc welding). The electrochemical behavior of different weldment zones (fusion zone (FZ), base metal (BM) and heat affected zone (HAZ)) was characterized both independently using an electrochemical microcell and together through whole sample analysis. The electrochemical method applied was performed in acidified glycerin, a process fluid of the biodiesel industry. The results were correlated to the microstructural features of the materials. Based on the results, is possible to conclude that the breakdown potential (Eb) of the fusion zone (FZ) was higher than the Eb obtained for the heat affected zone (HAZ). In general, top samples show higher breakdown potential than root samples and also the samples welded using filler metal 2209 has a better anodic behavior than the filler metal 2307. According to the results, GMAW welding process with 2209 as filler metal was revealed as the optimum chosen for application of 2304 duplex stainless steels in this case.

Jan 16, 2018

By Wenting Zhu, Liqing Chen, Junjun Cui, Zhenye Chen

In this presentation, a low carbon high strength steel microalloyed with Nb and Ti was processed by thermo-mechanical controlled process (TMCP) containing two stages of controlled rolling. The austenite with various grain sizes was obtained by austenitizing this hot-rolled steel at different temperatures. And the effect of austenite grain size on bainitic transformation was investigated in a dilatometer to reveal microstructural change. The results showed that the microstructure of the hot-rolled steel was mainly composed of granular bainite, lath-like bainite, and martenite/austenite constituents (M-A constituents). With increasing the austenitizing temperature, or increasing the austenite grain size, the microstructure was changed from granular bainite to lath bainite. When the steel was reheated to a lower temperature of 860 ºC, a relatively higher start temperature (Bs) was measured for bainitic transformation. This was mainly caused by the formation of solute-depleted region in the austenite and the promotion of the granular bainitic nucleation. The highest reaction rate occurred at austenitizing temperature of 1000 ºC with fine grain size, while the coarse austenite grain can lead to a sharp increase in the amount of bainite. An analysis was made on the kinetics of bainite transformation which was controlled by the volume diffusion of C atom.

Oct 1, 2019

By Eduardo Dominguez Trindade

Lubricant oils are subjected to reciprocating movement in the piston ring/cylinder tribocouple of automotive engines. In this kind of movement, the relative speed oscillates between zero and a maximum, and therefore the lubrication regime goes from boundary to hydrodynamic. Tribotests are widely used in laboratories to hint at the friction developed in these systems. In the present work, a SRV tribometer was used to evaluate the friction behaviour of lubricant oils under reciprocating movement up to 60 Hz. A high acquisition rate allowed the analysis of data inside each reciprocating cycle. Both a pure base oil and a fully formulated lubricant were used. Changes in the contact pressure, viscosity and speed were seen to influence friction, which was correlated to the relative thickness predicted by Hamrock-Dowson equation. While some observed characteristics were typical consequences of the Stribeck curve, other effects were also observed, such as the occurrence of seizure at high reciprocating frequency. A lower boundary coefficient of friction due to additive package in the formulated oil was also observed. The results allow a better understanding of friction in reciprocating cycles and can be used to evaluate the performance of oils and surfaces in laboratory prior to engine testing.

Jul 31, 2018

By Guilherme Guidugli

The hot blast stoves are a regenerative heat exchange system, accounting for 10 to 20% of the total energy requirement in an integrated steel plant, responsible for the supply of about one-third of the blast furnace heat input and responsible for a constant flow of hot air to the blast furnace, according to the required production. Because of their important role in the hot metal production, a stable operation and an appropriate combustion control is necessary. This paper aims to present the results of an investigation and modifications performed as an operating multi-furnace plant, as well as the parameters considered to ensure thermal equilibrium, improving in the stoves heating cycle.

Aug 16, 2017

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Francisco Morganti

This report gives in the first part the metallurgical basics for the production of AHSS grades in integrated steel plants starting at the melt shop and ending at the annealing lines of the cold mill. The corresponding process and plant technologies in each production step with its specifics and rules are explained. In the second part by way of example the practical requirements for TRIP 780 steel grade are highlighted like a recipe for process control in the steel plant, hot and cold rolling mill, annealing line and finally skin pass mill. Measuring of mechanical technological properties on samples shows that the specifications according to DIN EN 10268 are fulfilled.

Oct 30, 2017

By Florian Markus Penz

The increase in Basic Oxygen Furnace (BOF) plants in steelmaking has given rise to renewed interest in a dynamic simulation of the BOF process. Material and process costs can be saved with optimized process times and targeted charging of scrap and slag formers. Beside hot metal, scrap is the main source of iron in the BOF process. Furthermore, scrap is used as a coolant during the process due to exothermal chemical reactions occurring in the BOF. In this paper, the melting and dissolution behaviour of scrap in the BOF process is discussed. A new dynamic thermodynamic and kinetic Matlab® model used to simulate scrap melting behaviour as a function of various scrap surface parameters and particle size is presented, as well as the influence of scrap properties on liquid bath temperature and final crude steel composition after a defined blowing period.

Oct 30, 2017

By Túlio Magno Fuzessy de Melo, Luciano Santos Marques, Vicente Tadeu Lopes Buono

The influence of the coiling temperature after hot strip rolling on the microstructure and on the tensile and hole expansion properties of a 800 MPa multiphase steel was investigated. For the temperatures between 150°C and 600°C the microstructure consisted of a ferritic matrix with a dispersion of fine martensite-austenite (MA) and regions of degenerated upper bainite. In all cases the ferrite presented a heterogeneous mixture of polygonal, quasi-polygonal and acicular grains. The yield and tensile strengths showed a tendency of decreasing with the increasing coiling temperature, probably because of the larger fraction of MA particles at lower temperatures and higher fraction of quasi-polygonal ferrite at higher temperatures. The elongation was not significantly affected by the variation of coiling temperature. The average hole expansion ratio showed a maximum of 80% for the material coiled at 400°C and fell below 50% only for the coiling temperature of 150°C, probably due to the larger hardness difference between the ferrite matrix and the MA particles.

Oct 1, 2019

By Helênio Resende Silva Júnior

Arcelor Mittal Asturias coking plant at Gijon works, Spain, is undergoing a complete modernization of the whole coke making complex. In this context, Gijon has to be considered a brownfield project, where Paul Wurth has been awarded with the engineering, supply of key equipment as well as erection and commissioning supervision services for the rebuild of two coke oven batteries the modernization of the adjacent by-product and relevant waste water treatment plants. Main objective of this paper is to present the technological improvements introduced by Paul Wurth in the rebuild of a modern plant focusing on fulfilling all the recent environmental regulations.

Oct 30, 2017

By Ramon Augusto Moretti, Henrique da Rocha Severino, Renato Nascimento de Castro, Fernando Cesar Sousa

Rolling stand 12 (LTx) of long steel, installed in the company A, Piracicaba - SP unit, had presented high levels of vibration, which affected its internal components, such as: shaft, gears and bearings, generating downtime. To evaluate this equipment a study was proposed by the following engineering techniques: Conventional Vibration Analysis, Operational Deflection Shape (ODS) and numerical simulation by the Finite Element Method (FEM). In the Conventional Vibration Analysis, high levels of vibration were observed during manufacturing process, especially when the material reaches the equipment. Impacts generate high values in acceleration, on average 80 m/s² peak to peak. In the moment of impact, misalignment of internal components was observed by ODS. Field results were correlated to those obtained by the Finite Element Method, which allowed to calibrate FEM model. Thus, the most effective structural modification already numerically evaluated was implemented in the system. Afterwards, new measurements by vibration and ODS techniques were performed, and attenuation of vibrational levels and operational mode, which overloaded the internal components rolling stand, were verified.

Oct 1, 2019

By Antônio Aldenor Pinheiro Neto, Matheus de Lima Vieira

In mid-2015 the steel industry faced a strong crisis due to the weak performance of the Brazilian economy and the persistent entry of Chinese steel into Brazilian territory. This situation demanded that Brazilian steelmakers seek to develop products to meet new export markets. within the volume of exports possible are the rebars, where its applications are in the construction industry. One of the largest importers is Peru which has a large percentage of this export volume. This market demands as a priority requirement the surface quality of blue condition (low oxidation index) and mechanical properties normative.in order to meet the items required by the customer at a competitive cost, a vanadium microalloyed steel was applied to the hot rolling process without heat treatment after the last rolling pass. Where the great challenge was to achieve a high level of stretching without compromising the minimum limits of tensile strength. Assuming that the steel used is the correct one interventions were made on rolling parameters such as set-point temperature, residence time of pieces in the furnace, linear mass and rolling speed. All the changes made were based on statistical tools and practical tests. Finally, with the execution of actions generated from the statistical analyzes and tests it was possible to reduce process losses by 96%.

Oct 1, 2019

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Yong Tian, Tian Zhang, Zhao-Dong Wang

To meet the requirements of high-performance steel plates, while reducing manufacturing costs and saving energy, the advanced cooling system for plate mill (ADCOS-PM) with functions of accelerated cooling (ACC), ultra-fast cooling (UFC), and direct quenching (DQ) was researched and developed by the State Key Laboratory of Rolling and Automation (RAL). Since 2003, several sets of ADCOS-PM device were developed and implemented in industrial practice. To fully utilize the ADCOS-PM technology, the combination of various strengthening mechanisms was promoted by NG-TMCP technology and low-cost, high performance plates were produced such as pipeline steels, and high-strength construction machinery steel.

Oct 1, 2019