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By Ian James McDonald

Each year, approximately 400 million tons of blast furnace slag is produced worldwide with a tapping temperature of around 1,500°C. It is normally used as a substitute for cement clinker or as an aggregate material in road construction. Currently, the slag is granulated in wet-granulation plants using large volumes of water and to date, it has not been possible to utilise the remnant heat energy of the molten slag, which amounts to approximately 1.8 GJ of energy per ton. However, in an R&D project currently underway led by Primetals Technolgies and industrial partners, a new dry atomising technology is being investigated to use air to cool molten slag and recover the lost heat energy. The resultant pelletised slag fulfils the same criteria as wet-granulated slag for use in the cement industry. Phase 1 of the project has now been completed where a technical plant was set up at the University of Leoben in 2012. A series of dry-slag granulation campaigns were carried out using remelted blast furnace slag. The elevated offgas temperatures and the quality of the slag product as verified by the FEhS Building Material Institute have shown the process suitability as an industrial application and the decision was taken to escalate the project from large laboratory scale to a full size pilot plant. The phase 2 development of this plant is now underway and is scheduled for installation at the site of an industrial partner in early 2016 where full slag flow will be fed directly to the plant from Blast Furnace ‘slag runners. This paper will show the development path taken to date and the planned route to our goal in 2016 of being the first to industrialise the ‘game changing’ process of dry Slag Granulation with Heat Recovery from the slag.

Aug 16, 2017

By Samuel Filgueiras Rodrigues, Clodualdo Aranas Jr., Gedeon Silva Reis, Eden Santos Silva, Fulvio Siciliano

When austenite is deformed above the Ae3 temperature, partial amount of it transforms dynamically into ferrite by a displacive mechanism. After unloading, it retransforms back into the stable austenite by a diffusional process. This influences the rolling load which decreases under isothermal condition or does not increase with decreasing temperature as rapidly as expected under cooling. Plate rolling simulations under isothermal and continuous cooling conditions were carried out on a 0.09 wt.% Nb X-70 steel. Pass strains of 0.2 were employed together with interpass times of 10 s, and 30 s for the cooling conditions and 0.3 with interval of 10 s at 900 °C for the isothermal experiments; strain rate of 1 s-1 was used during the simulations. The mean-flow-stress (MFS`s) behavior of both conditions indicates that dynamic transformation and dynamic recrystallization were taking place during straining. The critical strains for the initiation of dynamic transformation fell around 0.06 while the critical strain for DRX was 0.12. It has been shown that ferrite is formed due to the applied deformation of roughing passes and increases its volume fraction throughout the finishing rolling stage. Under cooling conditions, the ferrite formation is also favored as the temperature approaches the Ae3 line. Such ferrite forms when the driving force for dynamic transformation is higher than the total free energy barrier preventing its formation. This obstacle consists of the free energy difference between austenite and ferrite as well as the lattice dilatation work and shear accommodation work. The addition of Nb retards the retransformation of the ferrite into austenite. Moreover, holding times after rolling increases the amount of austenite available for microstructure control on subsequent stages. The dynamic transformation (DT) mechanism can be used to design improved rolling schedules

Oct 1, 2019

By Claudio Pereira Diogo

A lot of galvalume/aluzinc steel sheet was furnished to a metallic roof manufacturer intended for tile fabrication. But, according with the roof manufacturer, that coils develops a different superficial aspect during processing. The purpose of this work was to provide an explanation for the appearance of the observed surface on one side of the coils. In order to find out the origin of the problem, mechanical and microstructural characterization tests were done at INSPEBRAS with the support of a partner laboratory. The results are described in this paper with their analysis and conclusions.

Aug 16, 2017

By Rogério Felício dos Santos

Nitriding of metallic materials using electric discharges generated during electric discharge machining (EDM) is a recently developed technique. The aim of this paper was to correlate mechanical properties of a nitrided layer produced in AISI 4140 steel by EDM nitriding with the type and amount of nitrides. A conventional die-sinking EDM equipment and electrolytic copper electrodes were used to generate the electric discharges. The electrolyte was a solution of urea in deionized water. Knoop microhardness profiles assessed the variation of hardness along the nitrided layer, whereas the elastic modulus of this layer was measured using nanoindentation tests. Optical microscopy and X-ray diffraction (XRD) were used to characterize the nitrided surface. The results showed the formation of a nitrided layer containing iron nitrides with average thickness of around 25 µm. The amount of nitrides reduced from the surface towards the centre and these results correlated well with microhardness profiles obtained.

Jul 31, 2018

By José Adilson de Castro

In the integrated steel industries the sintering process plays an important role furnishing raw material to the blast furnace. In this work, a computational simulation of the sinter process is developed that is able to predict the most important phenomena within the sintering bed. The model is based on the multi phase concept with multiple components described by conservation equations of each component coupled with the momentum, chemical reactions and heat transfer. The model validation was carried out comparing the model predictions with averaged industrial data and local temperature measurements within the sinter strand. The model predictions presented good agreement with the averaged values measured on the industrial sinter process.

Aug 2, 2018

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018

By Anna Carolina Cerqueira Neves

Synthetic fibers have been gradually replaced by lignocellulosic fibers. Compared to the synthetic fiber, natural fiber showed economic and environmental advantages presenting interfacial characteristics with polymer matrices that favor the impact energy absorption by the composite structure. However, so far little has been reported about the hemp fiber embedded in polymer matrices, such as tensile properties. This study aims to evaluate the resistance in tensile tests of epoxies composites reinforced with different percentages of hemp fiber. Tensile tests were submitted with percentage of 0%, 10%, 20% and 30% incorporated hemp fiber in epoxy matrix. The tensile strength and deformation substantially increased the relative amount of hemp fibers incorporated into the polymeric matrix.

Aug 16, 2017

By Karl Berger, Roman Schneeweis, Dietrich Mathweis

With increasing demands from customers to provide flat strip with tighter tolerances on material properties, particularly flatness of e.g. martensitic steel grades (M1500), it has become necessary to develop strategies to improve flatness without influencing the tensile properties for such hard steel grades. Usual skin pass mills are not capable to apply sufficient tension and roll force for these kinds of material to improve the flatness. Therefore, alternatives had to be searched for. This paper describes skin pass - / temper – rolling methods from the classical one to new alternatives in order to satisfy the demanding market of higher material properties and idle running mills in rolling plants.

Oct 1, 2019

By Jônatas Venancio Barbosa, Dagoberto Brandão Santos, Túlio Magno Füzessy de Melo

In this work, the mechanical and metallurgical behavior of titanium added ultra-low carbon (ULC-Ti) steel under hot and warm working conditions was studied by means of dilatometer compression tests. Double compression schedules were performed at temperatures between 700°C and 1000°C, inter-pass times of 0.5-100 s, and deformations of 0.5 and 0.3 in the first and second stages, respectively, with strain rate of 1 s-1. The analysis of the flow curves obtained allowed the evaluation of the softening characteristics of the steel. The softening and microstructure features indicate different restoration mechanisms depending on the temperature range. Static recrystallization with rapid microstructure restoration is observed at temperatures within the austenitic and intercritical field. Strain induced boundary motion and recovery mechanisms apparently control the restoration process in the ferrite region. In general, flow stress curves showed dynamic recovery behavior. Only the deformation in the intercritical region produced a peak in the flow stress curves. Isothermal holding tests associated with single hit compression indicated the presence of dynamic strain induced transformation, accelerating the softening kinetics at the intercritical region.

Oct 1, 2019

By William Sergio Flores Roman

Los aceros para armaduras de hormigón tienen que exhibir una buena relación entre resistencia y tenacidad que se ve reflejado en la performance del producto en servicio al ser aplicado a esfuerzos exigidos. Acerbrag es una empresa que produce aceros para la industria de la construcción teniendo en su gama los aceros de medio carbono para la fabricación de barras conformadas de dureza natural para armaduras en estructuras de hormigón. El objetivo de este trabajo es encontrar criterios de ventanas de trabajos operacionales y de control para la manufactura de aceros con buenas propiedades mecánicas en términos de resistencia y tenacidad. Este paper muestra los resultados de los trabajos realizados en las diferentes áreas productivas para conseguir un producto final con mayor resistencia a altas exigencias en servicio, además, reporta diferentes aspectos del proceso de manufactura del producto que van desde el ajuste de la composición química del acero, incluyendo criterios de propiedades mecánicas objetivos, criterios de calidad interna mostrando la microestructura de la barra antes y después de los cambios y finalmente la calidad dimensional y superficial de la barra nervurada, este último potenciando la falla prematura del material. Todos estos cambios, se ven reflejados finalmente en la performance de la barra, sometida a los nuevos criterios de exigencia en los ensayos mecánicos.

Oct 30, 2017

By Tiago Salzmann Vilela

No mercado de arames galvanizados destinados a indústria é exigida a uniformidade da camada de zinco sobre o arame. Neste trabalho, foram estudados os efeitos da velocidade de galvanização na uniformidade e espessura da camada de Zinco total, bem como a morfologia das fases de Zn e Ferro-Zinco sobre o substrato metálico. Verificou-se também o efeito do aquecimento após o processo de galvanização, observando o crescimento da camada intermetálica. Finalmente, serão mostradas as principais características de processo obtidas para garantir o atendimento aos ensaios de qualificação, em um estudo de caso de arames galvanizados produzidos em unidade industrial da Gerdau.

Jul 30, 2018

By Giulio Rodrigues Altoé

Environmentally correct composites, made from natural fibers, are among the most investigated and applied today. In this paper, we investigate the mechanical behavior of epoxy matrix composites reinforced with continuous fique fiber, through bending tensile tests. Specimens containing 0, 10, 20 and 30% in volume of fique fiber were aligned along the entire length of a mold to create plates of these composites, those plates were cut following the ASTM standard to obtained bending tests specimens. The test was conducted in a Instron Machine and the fractured specimens were analyzed by SEM, the results showed the increase in the materials tensile properties with the increase of fiber amount.

Aug 16, 2017

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Samuel F. Rodrigues, Clodualdo Aranas Jr., Fulvio Siciliano

The application of thermo-mechanical control processing (TMCP) in hot rolling of steels has become a common routine since the last 60 years. The understanding of the physical metallurgy behind TMCP played a major role in the early developments. Physical and numerical simulation works are performed firstly to derive the fundamental metallurgical knowledge and secondly to conceive existing TMCP practices. In this paper, a summary TMCP techniques is presented. The occurrence of dynamic transformation of ferrite in the austenite region is shown by means of synchrotron light diffraction methods. This phase transformation mechanism is taken into consideration and its effects on TMCP are proposed in an exploratory way.

Oct 1, 2019

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By Alisson Paulo de Oliveira, Altair Lucio de Souza, Jacson Morais Borges, Cleiton Arlindo Martins

A customized version of the Microsim-PM software for one Steckel rolling mill was built and adapted for specific mill parameters. The focus of this study is to use this model, which predicts the austenite grain size distribution evolution during rolling, to understand and quantify metallurgical issues happening during hot rolling. This will allow the steel mill to optimize the rolling process and chemical composition before the first industrial trial. Materials rolled for final thicknesses of 4.75, 6.30 and 12.5 mm of a carbon manganese steel and a microalloyed steel were selected to tailor the equations used by the model and to accurately reproduce the reality of the Steckel mill. This paper analyses the results from the customized model and compares them to mill data and final microstructure. Measured and predicted Mean Flow Stress (MFS) values are compared. After rolling, the material is subjected to accelerated cooling using laminar cooling. These cooling curves obtained from mill data are also considered to analyze the final microstructure characterized for all the cases using EBSD. The quantification of the microstructure allows for a better understanding of the relationship between chemical composition, process parameters and mechanical properties.

Oct 1, 2019

By Daniel Hajduk

Efficiency of back up rolls depends mostly on two parameters – length of campaign and dressing amount after the campaign. The longer the campaign (in terms of rolled tones) is, the higher the dressing amount. To solve this task properly it is necessary to know the distribution of accumulated damage in the working layer of the roll caused by previous campaigns and by loads (separating force and bending) during present campaign respecting changing conditions of material properties (hardness) through radius of the roll. To find an optimum dressing amount an algorithm has been developed and specialized computer program will be presented, that takes real measured loads during the backup roll campaign, calculates fatigue damage in the roll and suggests relevant dressing amount. This can help to prolong service life of rolls, minimize the risk of spalls and reach maximum efficiency in terms of rolled tones/km per roll.

Jul 30, 2018

By Christian Overhagen

In bar and wire rod mills, rolling procedures featuring three- and four-roll technologies are state-of-the-art to produce high-quality long products. While a rolling model for the three-roll process including an equivalent pass method was already presented by the author, pass design methods are dealt with in the current work. The geometry of the rolled product and roll grooves are described mathematically using functional contours, allowing geometric-numerical methods to be used for manipulation and deformation simulation of the rolled product. For a given pass, the output section is constructed using these methods. Roll force, torque and rolling power are calculated using the mathematical rolling model presented before. Interstand tensions are discussed as influencing parameters on the force, torque and power demands, as well as on the section shape. A mathematical model for the influence of interstand tensions on lateral spread is incorporated in the model. To complete the pass design model, elastic mill stand feedback is considered in terms of a fixed elastic modulus for each rolling stand, the elastic feedback and therefore cross-sectional variation due to elastic mill spring being calculated iteratively from the roll force by application of the Gagemeter equation. The interaction of section height and width faults due to elastic mill spring and spread variations is analyzed in detail and the consequences for the roll pass design are shown.

Oct 1, 2019

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019