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By Eugene Baker, Joseph Cervik, Albert Sainato

In Europe, water infusion is used widely to reduce generation of respirable dust during mining. Its use in the United States is limited to a few plow operations in the Pocahontas No. 3 Coalbed. This Bureau of Mines report describes the technology for infusing water in to a longwall panel and reports the results of a recent demonstration in the Lower Sunnyside Coalbed that achieved dust reductions averaging 58 pct. Because water infusion increases moisture content of the coalbed, face air velocities in excess of 500 ft/min (2.5 m/s) are possible, further diluting dust levels before dust entrainment occurs. An economic analysis shows a 23-pct reduction in operating costs when coal production is increased by changing from unidirectional mining to bidirectional mining with water infusion.

Jan 1, 1983

By C. C. Shale

A semicommercia1, high-temperature electrostatic precipitator and adjunct equipment are described, and operating characteristics at 1,470° F and 80 psig are presented for both positive and negative polarity. Removal efficiency for negative corona waS about 91 to 96 percent while that for positive corona was only about 75 to 77 percent. Results are compared with those from bench-scale investigations, and equipment limitations are discussed. Theoretical aspects of the precipitation process are related to the operating characteristics.

Jan 1, 1969

By Parviz F. Rad

The Bureau of Mines conducted rock-cutting experiments under constant normal force and constant penetration in an effort to correlate laboratory data with those obtained in the field. Both independent and interacting groove spacing regions were studied, and optimum and critical cutter spacings were determined. For the laboratory work, the effects of specific energy, muck weight, groove depth, cutting coefficient, and size distribution of the muck for both independent and interacting grooves were studied. For field operations, forward thrust, torque, advance rate, and muck size distribution were the parameters studied. Satisfactory correlation is obtained between laboratory cutting results and field performance data.

Jan 1, 1974

By E. J. Kloos

Bureau of Mines-approved self-contained breathing apparatus of the compressed air demand type were evaluated for performance at low temperature. Apparatus durations, breathing resistances, and airflow rates were measured on machine tests at room temperature and -25° F. Man tests under actual wearing conditions verified the machine test results. Many serious functional changes in apparatus performance occurred at low temperature. Pressure regulators malfunctioned when diaphragms lost flexibility. Under certain conditions frozen condensed moisture sealed exhalation valves and fogged eyepieces. High-pressure leaks, not encountered at ordinary temperature, developed at low temperature. Tests results are discussed generally and specifically for each apparatus. Recommendations are given to obtain optimum performance from demand type breathing apparatus at low temperatures.

Jan 1, 1968

By L. A. Haas

The degree of reduction of various silica-graphite mixtures was studied in a batch reactor to determine optimum physical conditions for maximizing the carbothermic reduction of silica. The extent of interaction was determined for reactant mixtures in loose powder and briquet forms at pressures less than 0.01 torr and temperatures up to 1,445° C. Molar ratios were varied from 0.05 to 6.5 with maximum reaction at a ratio of about 1.5. The solid-solid reaction did not appear to involve gaseous intermediates. The extent of reaction better correlated with the number of interparticle contacts than with the true surface area of the reactants. Carbonized dextrose was a better reductant than graphite.

Jan 1, 1968

By Kathleen Madland Kowalski

In recent years the issue of human stress response in emergency workers has begun to receive attention. This paper presents a rationale for considering human stress as a significant factor in the management of emergencies It discusses the concept of stress, Critical Incident Stress in emergency responders, and intro¬duces the Critical Incident Stress Debriefing (CISD) process. It is suggested that in a disaster, the CISD process can improve the effectiveness of response teams on site, their turnaround time on site, and post disaster time off the job. This paper, prepared by a US Bureau of Mines research psychologist, offers some ideas to the mining industry in general, mine rescue trainers and more universally, to those responsible for developing emergency management plans.

Aug 1, 1998

By J. L. Konchesky

The Bureau of Mines investigated the main reactions of coal gasification by steam. Coal (minus 70 mesh)-water slurry was fed into a laboratory-scale tube-coil gasifier to show the effects of residence time (0.6 to 1.1 sec), steam-coal ratio (2 to 11 lb/lb), and temperature (1,600° to 1,900° F), at about 1-1/2 atm. Devolatilization was very rapid: about 70 pet of the coal's volatile matter evolved within 0.6 sec at about 1,600° F; temperature increase released more volatile matter until about 95 pct was driven off at 1,900° F. Devolatilization was not increased by raising steam concentrations and was only slightly increased by extending residence time. Below 1,600° F, there was no evidence of the steam-carbon reaction, but at 1,900° F more than 80 pct of the coal's fixed carbon was converted to gas; the conversion was increased Significantly by increased residence time and steam concentration. The water-gas shift reaction occurred simultaneously with devolatilization, and the steam-carbon reaction, approaching equilibrium with increased residence time and temperature and decreased steam concentration.

Jan 1, 1969

By J. G. Walters

In a survey of the coking properties of United States coals, the Bureau of Mines has accumulated data on more than 500 coals and blends tested by the Bureau of Mines-American Gas Association (BM-AGA) method.4/ The importance of these tests depends upon the fact that a greater number of different coals has been tested in this apparatus than in any other of similar scale, thus permitting comparison of the carbonizing properties of many coals. Evaluation of BM-AGA results with respect to industrial data supplied by member firms of the American Gas Association was one of the first objectives in developing this test apparatus and procedure. Early data showed that, de-pendent upon BM-AGA carbonizing temperature, BM-AGA and commercial results agree closely.5/ Because of limited data, statistical relationships were not established at that time.

Jan 1, 1959

By H. C. Miller

[California's sensational rise to supremacy as an oil-producing State in 1923 was accompanied by a loss of 62 lives. These 62 deaths were from oil-producing accidents alone and do not include fatalities at the refineries, on tankers, or on any work not directly connected with the drilling for and the production of oil. The number of facilities for 1923 was 82 per cent greater than in 1922, the next most fatal year, with a record of 34 lives lost. The data submitted in Table 1 show that for the calendar years 1917 to 1923 inclusive, an average of 4.74 million barrels of oil were produced per Vitality in the California oil fields. On this basis, the record for 1923, hough a trifle below the average, shove up slightly better than that for 1922.]

Jan 1, 1924

By Parviz F. Rad

The Bureau of Mines conducted groove cutting experiments in marble, lime-stone, granite, and quartzite with a 7-inch disk cutter under a normal thrust of 7,000 lb. The values of muck weight per unit length, specific energy, cutting coefficient, and groove depth for each of these rocks were determined for groove spacings ranging from 0.1 to 4 inches, and from these results the values of optimum and critical spacing were computed" The results indicate that compressive strength may be used to predict some of the cutting characteristics of the independent grooves. Considering all the cutting characteristics, particularly those for the interacting grooves, Shore hardness, coefficient of rock strength, and torsional velocity correlate with cutting characteristics better than do other physical properties. Some of the field applications of the principles established in this report are identified.

Jan 1, 1974

By Thomas E. Marshall, Timothy Batchler, Anthony T. Iannacchione

As the amount of new fractured surfaces or "damaged rock layers" within roof rock increases, the stability of the rock mass decreases. While direct measurements of this phenomenon are not easily made, there is good circumstantial evidence to support this hypothesis. For example, it is common to observe increased cracks or fractures in the immediate mine roof rock before a roof fall. Likewise, roof drill holes placed in areas that later fail often reveal increased numbers and/or separations of fractures within the rock column through time. And finally, the frequency of microseismic activity, representative of rock fracturing, increases before a roof fall. For this study, more than 700 microseismic emissions were collected from two underground limestone mine roof fall areas in southwestern Pennsylvania. Microseismic events were located and magnitudes determined using the moment magnitude technique. Moment magnitude is based on the event seismic moment, which is a measure of the seismic deformation. The amount of new fracture surface length was calculated based on the stored strain energy within the rock prior to fracture. In the two case studies presented, a significant amount of microseismic activity was observed as much as two days before the first signs of failure in the roof fall areas. Additionally, results from this analysis reveal much about the behavior of strata prone to failure and allows for the construction of hazard maps based on microseismic emissions. The potential use of this technique as a means of anticipating roof falls is analyzed and discussed.

By David S. Yantek, Paul Jurovcik, Eric R. Bauer

Workers in coal preparation plants, where vibrating screens are significant noise sources, are often exposed to sound levels exceeding 90 dB(A). The National Institute for Occupational Safety and Health, a major coal company, and a vibrating screen manufacturer conducted a cooperative study of vibrating screen noise. Rubber isolators reduced sound levels by 1 dB. Urethane screen panels did not reduce sound levels in this case. Drive noise was determined to be the dominant noise source on the screen. Damped side plates reduced vibration levels on the screen sides by 1 to 7 dB(A). Detailed results of the study are presented.

By Philip A. Holland

The Bureau of Mines has developed a method for determining helium in water for use in sampling and analyzing surface and subsurface waters for geochemical survey work. The accuracy of the analytical method is within ±10 percent for samples containing above 20 x 10-8 cm3 He (STP)/cm3 H20. The minimum detectable helium-in-water concentration is calculated to be 2 x 10-8 cm3 He (STP)/cm3 water. Water samples are collected in 500-cm3 stainless steel cylinders. The dissolved gases are extracted into a cylinder of equal volume containing a known quantity of neon. The resulting gas mixture is subsequently analyzed for helium and neon-21 by mass spectrometry. The volume of helium in the sample is calculated from the mass spectrometric determination of the helium-to-neon-21 ratio, the known quantity of neon used, and the extraction efficiency of helium.

Jan 1, 1981

By Seth C. Schaefer

The Bureau of Mines investigated thermodynamic properties of Mn304 (manganomanganic oxide) and Mn203 (manganese sesquioxide). The standard Gibbs energies of formation (?Gf°) of Mn304 and Mn203 from their lower oxides were determined with high-temperature galvanic cells using stabilized Zr02 (zirconia) as the electrolyte. Potential measurements were obtained for the cell Pt, MnO, Mn304//Zr0 2//02(g, 0.0112 atm), Pt, with the overall cell reaction 6Mn0(c) + 02(g, 0.0112 atm) = 2Mn304(c), where- 02 refers to indicated partial pressure of oxygen at the reference electrode. Similar measurements were obtained for the cell Pt, Mn304, Mn203//ZrO2//02(g, 0.0115 atm), Pt, with the overall cell reaction 4Mn304(c) + 02(g, 0.0115 atm) = 6Mn203(c). Equilibrium oxygen pressures for the Mn0-Mn304-02 and Mn304-Mn203-02 systems were measured and may be expressed for the respective systems as [23,400 109 P02 T + 11.91 (764.9 - 1,208.6 K) and log p02 = - 11,957 + 9.66 T (968.6 - 1,208.2 K),] where pressure (p02) is in atmospheres and temperature (T) is in kelvins. Standard thermodynamic properties of Mn304 and Mn203 were derived from these measurements and auxiliary thermodynamic data from the literature.

Jan 1, 1982

Impermeable geologic faults in the coal seam can cause intermittent production problems or can cause unexpected amounts of water or gas to issue from degasification boreholes. These faults also can impact methane emissions into the mine workings, especially if they hinder proper and effective degasification of the coal bed. They may also act as barriers for methane flow in the coal seam. Although this might seem beneficial for advancing mine workings, faulting may also cause gas pressure buildups and result in compartmentalization of the gassy regions from which large quantities of water and methane may rush into mine workings. This study uses reservoir simulations to illustrate the effects of impermeable faults, with and without throws, on the production performance of vertical and horizontal degasification boreholes. These boreholes were drilled from the surface to intercept the coal layer and fault and were assumed to produce methane two years prior to mining of the coal seam. Longwall advances and face position related emissions and reservoir properties were characterized using sector definitions along the path of the panel grids. This work numerically evaluates water and gas productions of each borehole and presents the effects and the impacts of impermeable faults on methane emissions due to an advancing coal face. The results can be used to understand the effects of impermeable faults on borehole productions and face emissions due to these coal seam anomalies.

Jan 1, 2008

By M. J. Kovalik

The effects of the process variables on the production of chemical coke on a chain grate stoker, a type of traveling grate, were studied. Six bituminous coals, ranging in volatile matter from 16.7 to 43.8 percent, were successfully carbonized, yielding chemical coke with acceptable physical properties. The coke yields were dependent on the volatile-matter content of the coal. The air fuel ratio had the most marked effect on the yield and characteristics of the resultant coke, and the general furnace performance. Results can only be predicted; the actual yield and quality of coke obtained from any given coal can only be determined by actual tests using the optimum processing variables to obtain a coke with minimum volatile-matter content and to retain as much of the fixed carbon in the original coal as possible.

Jan 1, 1967

By W. E. Robinson

Oil-shale samples selected from a core of the Green River Basin (Wyoming) were studied to ascertain differences in the composition and/or chemical structure of the organic material in the samples relative to stratigraphic position within the Green River Formation. This involved a systematic study of the soluble organic material and the insoluble kerogen present in the samples. Emphasis was placed upon the distribution of the alkanes (normal and isoprenoid compounds) in the soluble extract and upon the aromaticity of the kerogen. In general, it was concluded that significant differences exist in the chemical structure of the oil-shale organic material from various strata within the Green River Formation of Wyoming. Most of the compositional and structural changes were not related to burial depth but were related to source material variations, environmental differences, or other factors.

Maintain good blowing face ventilation while taking deeper cuts with a radio-remote, scrubber-equipped miner. Approach A six week in-mine study of face ventilation effectiveness was made by comparing the existing MSHA-approved blowing curtain setback distance of 25 ft with brattice set back distances of up to 50 ft. Effectiveness was determined by measuring methane levels at the face and in the immediate return. How It Works Blowing ventilation systems are commonly used in mines because the high velocity air stream created by these systems rapidly mixes with and dissipates methane generated during the cutting of coal. A drawback to blowing ventilation is that the work area is placed in return air and this may create dust compliance problems for the shuttle car and mining machine operator. To clean dust from the return a number of mining machine manufacturers supply dust scrubbers built into the machine. Dust-laden air is drawn into ducting at the front of the mining machine's boom and is ducted to a scrubbing unit located on the machine's main frame. The clean air from the scrubber is discharged as a high velocity jet toward the return, generally from the left fender of the mining machine. When taking cuts deeper than 20 to 25 ft with a scrubber-equipped machine, the machine's discharge is in by the mouth of the blowing curtain, creating a concern by mine workers that a loss of air to the face could result. However, Bureau of Mines research found that the push or throw of air toward the return by the scrubber discharge jet allows good face ventilation to be maintained with extended curtain setbacks.

Jan 1, 1984

By C. M. Frost

Crude shale oil produced during in situ retorting by the Bureau of Mines at Rock Springs, Wyo., was refined by three schemes. In the first, the crude oil was fractionated to raw naphtha and 400° F+ residuum. The residuum was hydrogenated over cobalt molybdate catalyst at 815° F and 1,100 psig. The blended raw and 160°-400° F hydrogenated naphthas were hydrodenitrified and then catalytically reformed. The 400° F+ hydrogenated oil was catalytically cracked. In the second scheme, the crude was hydrogenated over nickel-tungsten catalyst at 800° F and 1,500 psig. The hydrogenated fractions were processed by methods used in the first scheme. The third scheme resembled the second but, prior to hydrogenation, the crude was "hydrostabilized" over cobalt molybdate at 500° F and 500 psig. Yields of reformate and cat-cracked gasoline as volume-percents of the crude, and research-method octane numbers (with 3 ml TEL) for the three methods were as follows: First method, 32 pet reformate, 90 octane; 19.5 pct cracked gasoline, 99.2 octane. Second method, 29 pet reformate, 81.1 octane; 21.3 pct cracked gasoline, 99.6 octane. Third method, 28.2 pet reformate, 86 octane; 28.7 pct cracked gasoline, 95.9 octane.

Jan 1, 1974

By K. P. V. Lei

The Bureau of Mines as part of its research effort to minimize the generation of hydrometallurgical waste, investigated a sodium sulfide leaching-electrolysis procedure for treating hydrometallurgical residues for elemental sulfur and base-metals recovery. Research was conducted on a leaching residue from a lead concentrate. The following procedure was developed. 1. The elemental sulfur was dissolved as polysulfide with an Na2S solution. 2. The resultant metal sulfide bearing residue was oxidatively acid leached in a cationic membrane electrolysis cell; the metals were solu¬bilized at the anode, and a base was generated at the cathode. 3. The elemental sulfur was recovered from the polysulfide solution by neutralizing with the acid in the anolyte. Byproducts of the neutralization were H2S and a sodium salt solution. 4. Sodium sulfide was regenerated by reacting the H2S byproduct with the base in the catholyte. 5. Lead as PbCL2 was recovered from the anode residue by brine leaching, and the other metals were recovered from the sodium salt solution as metal sulfides. 6. The barren filtrate from the metal sulfide precipitation constituted the recycled electrolyte. Ninety-eight percent of the elemental sulfur, 98 pct of the lead, and up to 80 pct of other accessory metals were recovered from a residue obtained from the FeCl3-NaCl leaching of a lead concentrate.

Jan 1, 1982