Search Documents

By Fabiano Almir Barbosa, Eduardo Alves Machado, Felipe Ferreira Cajano, Bruno Rodrigues Henriques

Spring steels are usually classified as medium to high carbon low alloy steels with very high yield strength, enabling the part to return to its original shape regardless of significant bending or twisting. Despite the fact that plain carbon steels are suitable for small springs, larger and high performance springs usually requires alloy steels such as Cr-V or Si-Mn in order to achieve an even microstructure throughout the cross section. Clutch diaphragm spring is a high performance part that requires very good cleanliness and microstructure homogeneity, thus requiring an alloy steel. In this paper was studied, in an industrial scale, the process parameters and critical characteristics for the development of a Cr and V alloyed high carbon sheet steel for the production of clutch diaphragm spring. The steel was characterized throughout the entire process (casting, hot rolling, cold rolling + batch annealing and heat treated) using tensile test, hardness test, optical microscopy (OM) and scanning electron microscopy (SEM) to assess the mechanical and metallurgical properties of the studied steel. The results have shown the material’s microstructure evolution after each main stage of the process, from a ferrite-bainite/perlite based microstructure as hot band to fully spheroidized as cold-rolled/annealed and then fully martensitic as ready-to-use part.

Oct 1, 2019

By Michaela Böberl

State of the art sinter coolers are working based on the cross flow cooling principle. Thus, only a part of the thermal energy can be used for heat recovery application. The other part of the cooling air is brought unused to the environment. Furthermore, environmental regulation regarding dust emission and intelligent usage of exergy are getting stronger. Therefore, Primetals Technologies developed sinter coolers based on the counter flow principle. The cooling air passes the sinter bed in counter-flow direction enabling a direct heat transfer from the hot sinter to the air. The exhaust gas temperature can be maximized by using the total heat of the hot sinter. Due to the possible usage of the total exhaust gas amount, diffusive dust emission is reduced to zero. Two types of counter flow coolers are in the portfolio of Primetals Technologies. One type is based on a stationary shaft, in which the hot sinter is charged. The flow of the hot sinter is in vertical direction from top to bottom, in counter direction than the cooling air. The second type is a circular hopper cooler. The hot sinter is charged on top of a moving bed. At the bottom of the bed the sinter is discharged. The cooling air flows also from the bottom to the top, following the counter flow principle. Depending on the requirements, one of the two counter flow cooler types can be chosen for optimized and efficient cooling of hot sinter..

Oct 30, 2017

By José Fagundes Junior, Cleudson dos Santos Rego, Bruno Bastos da Silva Murad, Vitor Borlot Borba

Since the startup in 2002, the Hot Strip Mill at ArcelorMittal Tubarão has increased gradually the coil output as the customers demand new and more resistant dimensionally challenging (thinner and/or wider) steel grades. As a critical feature for customer applications, improvements have been carried out aiming a higher thickness performance and reduction of internal losses while still meeting the more restrict tolerances booked by the customers. This paper presents the recent thickness performance evolution since 2017 and the main actions deployed to improve it.

Oct 1, 2019

By Carlos Martins de Oliveira

The trucking industry is constantly seeking improvement and cost reduction of their vehicles, studying new lighter and robust materials to meet the needs of its customers. The objective of this work is to study the application of DCPD Telene, PU. R. RIM and PP-TD 20 materials in aesthetic components of trucks: bumper, calender, upper and lower bracket and side air deflector. A multifunctional work team was created to work in such parts of IVECO trucks. The work began with an analysis of possible improvements to the current parts and followed the subsequent phases: definition of new materials, virtual modeling, new tools, and durability test in vehicles. It could then be verified that the proposed DCPD Telene, PUR. RIM and PP-TD 20 materials showed greater strength, better painting surface, and reduced weight and cost in parts.

Aug 8, 2018

By Darina Manova

Plasma assisted surface modification methods have been used to nitride stainless steels in order to enhance hardness and therefore the lifetime of industrial components. Nevertheless, the corrosion resistance is not always preserved since it is very sensitive to the process parameters, either in implantation or in thermochemical diffusion techniques. AISI 316L stainless steel was plasma nitrided using three different techniques: Low Energy Ion Implantation (LEII), Plasma Immersion Implantation (PI3) and conventional DC pulsed plasma nitriding (DCPN). For each method several parameters were tested and some of them were selected to achieve the so called S phase of about 3 µm thickness and no nitrides precipitation. The nitrided layer was characterized with OM and SEM. Hardness was assessed on the surface with Vickers indenter and 25 g load. XRD was performed to characterize the S phase and to detect other phases if present and electrochemical corrosion tests were carried out in 3.5% NaCl solution. Although the S phase thickness in the three groups of samples was comparable, hardness was not and neither was the corrosion resistance. The PI3 samples were the hardest with the best performance in corrosion experiments, resulting in a higher breakdown potential and lower currents.

Aug 8, 2018

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By Jorge Madias

Neste trabalho se leva a cabo uma revisão da literatura sobre defeitos em beam blanks. O foco é no mecanismo de formação e as soluções propostas para diminuir sua ocorrência. Os defeitos superficiais incluidos são as trincas longitudinais e transversais, bleeding, pinholes e escória. Os defeitos internos levados em conta são os blowholes, as trincas centrais e as trincas nas pontas das abas. A revisão incluie as técnicas utilizadas para pesquisar os defeitos: caracterização metalográfica, CFD, modelagem termodinâmica e termomecânica, etc. As medidas adotadas estãorelacionadas a mudanças no sistema de lingotamento (por exemplo o design da vâlvula submersa), design do molde, mudanças e regulação do resfriamento secundário, suporte dos veios.

Oct 30, 2017

By Eric Yoshimitsu Sako

One of the main difficulties in the operation of trough and runners at Arcelor Mittal Tubarão (AMT) Blast-furnace no.02 is the reduced amount of time available for repair procedures. The consequence is that the castable installation must often be performed during hot conditions and the installed castable could easily detach from the base material during the early stage of operation, exposing the previously oxidized base material to molten iron and corrosive slag attack. When events like this happen, emergency repairs must be executed, resulting in increased refractory unit consumption and an unplanned shutdown of unit operation. Considering these targets, Nippon Crucible Co. and Saint-Gobain HPR Brazil have developed a high-performance Al2O3-SiC-C composition based on an entirely novel anti-oxidation technology. Oxidizing reactions could be attenuated by adding an oxidant inhibitor and a water reducing agent. As a result, the open porosity was significantly reduced, resulting in an improvement of campaign life in terms of pig iron throughput when compared with the regular castable. An analysis of this life improvement showed successful results for the material after 250 days of campaign. The main reason for such successful results was that the deterioration caused by the oxidation was significantly less and that this change made on the high cohesive structure of the base material was maintained for a long time. The attained results allowed Arcelor Mittal Tubarão to achieve longer trough campaigns, and avoid any unplanned stoppages with zero breakdown risks.

Oct 30, 2017

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Alain Denis, Marcelo Curtes Martins, Jeferson Rocio de Oliveira

In this work we present a study of optimization of a new inhibitor for turbulence pickling line. The efficiency of inhibition was measured and the weight of loss was evaluated in four different materials to optimize the dosage of the inhibitor. In seven months we had 8.7% of reduction in pickling losses.

Oct 1, 2019

By Elizaveta Cheremisina

In steelmaking process lime serves as flux. Rapid lime assimilation and slag formation of the desired composition have a significant effect on the refining reactions. It is important to know the rate limiting step of lime dissolution to control and improve the converter process. Kinetics of pure CaO and industrial lime dissolution in model slag has been studied in the range of temperatures 1300 –1600°C. Lime samples were prepared in cylinder form and immersed in the melt for predetermined time. Considering the total mass balance of CaO in the slag and linear dimensions of lime samples, mass transfer coefficients were derived. Diffusion coefficients were calculated under conditions of non-stationary diffusion. The derived activation energy of less than 200 kJ/mol indicates that diffusion is the limiting step in the process of lime-dissolution in slag.

Oct 30, 2017

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Sara Hornby

After almost half a century of experience in using DRI/HBI in electric arc furnaces (EAFs), and taking into account the decrease of natural gas cost in the USA, it is interesting to revisit some trends and controversial issues around this alternative iron source. This paper reviews aspects like the evolution of iron ore quality and its influence on EAF operation; DRI stockpiling and transport, regarding the risk for selfcombustion; optimum charge design; cold DRI/HBI charging (fifth hole, bucket, transporter); hot charging (ways and results); carbon content, metallization and silica in DRI/HBI, and its influence on EAF operation and performance; oxygen / carbon balance; chemical energy and DRI/HBI charge.

Aug 16, 2017

By Leszek Maldzinski

The present concept assumes carrying out the process of controlled nitriding with NH3 alone. This is a simpler process than that using two-component mixes of ammonia diluted with N2 or NH3diss. The regulation of the chemical composition of the atmosphere in the retort, and therefore the regulation of the nitriding potential KN, is obtained through the variation of the inflow rate of NH3 into the retort. What is a completely new things in a relevant process, the inflow of NH3 into the furnace is at times reduced to zero, which widens the range of the gas composition in the retort (and by the same token, of KN). The amount of NH3 introduced into the furnace is regulated (controlled) with the aid of a gas analyzer (for example an infrared analyzer). The gas analyzer opens and closes periodically the NH3 inlet valve with a frequency maintaining a desired gas composition (a desired KN) in the retort. The concept was based on experimental and theoretical investigations in term of thermodynamic and kinetic of gas nitriding. Investigations were carried out in a laboratory furnace with a quartz tube and also in an industrial furnace with a steel retort and a circulating fan. Nitriding was performed using NH3, NH3+H2, NH3+NH3diss. mixtures. In an industrial furnace the supply of NH3 into the retort was periodically closed, though with an operating circulation fan. The studies demonstrated that the growth rate of nitrided layer depends only on the composition of the atmosphere, (or KN), in the retort. It depends neither on a type of atmosphere introduced into furnace (NH3, NH3+NH3diss. or NH3+H2) nor a type of furnace (laboratory with a quartz tube or industrial with steel retort and fan). The results proved also that entirely closing of NH3 supply to the retort does not affect the growth rate of nitrided layer. A detailed analyses of the results was performed in a paper.

Aug 16, 2017

By Osvaldo Guilherme Comineli

While the hot cracking of Cu-containing steels is a serious and widely known problem for the industry, the literature reports that copper only slightly impairs the hot-ductility measured in laboratory. A distinction is drawn between hot ductility and hot shortness and the respective cracking operating mechanism involved at the respective range of temperature. The representability of the laboratory assessment of hot cracking of Cu-containing steels by hot tensile tests compared with actual results in industrial practice is discussed. The effectiveness of the variable affecting in each cracking mechanism and respective temperature range, focused in improving the hot cracking assessment of Cu-steels and the relative importance of oxidation will also be discussed. It is concluded that the hot tensile test in argon might be a good simulation if properly interpreted and that the role of oxidation is secondary in causing hot shortness. A schematic diagram for the hot tensile test is proposed.

Oct 30, 2017

By Mariana Macedo de Oliveira Lima, Pedro Emílio Gazola, Andrei Locatelli

Boron steel is used in the industry due to its great wear and impact resistance. During the hot rolling production of 15B29 steel flat bars it is a recurrent problem that the bars will present warping while on the cooling bed. Control this phenomenon is an opportunity to have better productivity, preventing metallic losses. Through the observation of the macro and microstructure samples produced with different reheating temperatures and cooling rates, it was found the presence of residual stresses and cracks on warped bars macrostructure. The residual stresses appearance suggest that the material cooling is too fast. Billets temperature on the reheating furnace of 1230°C reduced to 1100°C and the production pace slowed down. Bars temperature when arriving the cooling bed was reduced from higher than 670°C to 625°C. The results obtained made it possible to produce the material with better quality, reducing the warping effect at the cooling bed. The major influence on the materials warping was identified as the cooling rate at the cooling bed and the reheating furnace temperature was adjusted to provide a homogeneous temperature along the bars.

Oct 1, 2019

By Samuel F. Rodrigues, Clodualdo Aranas Jr., Fulvio Siciliano

The application of thermo-mechanical control processing (TMCP) in hot rolling of steels has become a common routine since the last 60 years. The understanding of the physical metallurgy behind TMCP played a major role in the early developments. Physical and numerical simulation works are performed firstly to derive the fundamental metallurgical knowledge and secondly to conceive existing TMCP practices. In this paper, a summary TMCP techniques is presented. The occurrence of dynamic transformation of ferrite in the austenite region is shown by means of synchrotron light diffraction methods. This phase transformation mechanism is taken into consideration and its effects on TMCP are proposed in an exploratory way.

Oct 1, 2019

By Guilherme Guidugli

The hot blast stoves are a regenerative heat exchange system, accounting for 10 to 20% of the total energy requirement in an integrated steel plant, responsible for the supply of about one-third of the blast furnace heat input and responsible for a constant flow of hot air to the blast furnace, according to the required production. Because of their important role in the hot metal production, a stable operation and an appropriate combustion control is necessary. This paper aims to present the results of an investigation and modifications performed as an operating multi-furnace plant, as well as the parameters considered to ensure thermal equilibrium, improving in the stoves heating cycle.

Aug 16, 2017

By Gabriel Oliveira Glória

Due to growing concern about the ambient impacts, lignocellulosic fibers are been investigated to replace the synthetic ones in polymer composites The giant bamboo fiber, a relatively unknown lignocellulosic fiber with potential for composite reinforcement, still needs to characterize for possible engineer applications. However the giant bamboo fiber has low adhesion with the polymeric matrix. In order to understand the interaction that occurs between the bamboo fiber and the polymer matrix is necessary to evaluate its physical and chemical characteristics. Therefore, the present work analyzed the giant bamboo fiber by means of Fourier Transform Infrared (FTIR) spectroscopy. The spectrum revealed main absorption bands typical of giant bamboo fiber specific molecular interactions.

Aug 16, 2017