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By M. B. Shongwe, G. Freemantle, M. Botha, S. Brill, J. D. Steenkamp

During steelmaking, one important factor for production efficiency is the free opening of the ladle nozzle during continuous casting. Free opening occurs when the well filler sand and the steel flow freely when the slide gate is opened. Well filler sands are used for the slide gate of a ladle to separate the slide gate refractory and the molten steel. The well filler sand is partially sintered by the heat of the molten metal, which can result in the ladle nozzle failing to open if the sand is not sintered to an appropriate extent. It is therefore of great importance that the sintering behaviour of well filler sand is understood. We studied the effect of the well filler sand chemistry on its sintering properties. Samples of well filler sand with various chemical compositions were sintered in a high-temperature chamber furnace. Quantitative X-ray diffraction (XRD), inductively coupled plasma optical emission spectrometry (ICPOES), and wavelength dispersive spectrometry (WDS) by electron microprobe analysis (EMPA) were used to analyse the various well filler sand mixes. Points of analysis were indicated on backscattered electron (BSE) micrographs. Quantitative element mapping was undertaken by energy dispersive spectrometry (EDS). Thermodynamic calculations in FactSage predicted the percentage liquid phase present for the various well filler sand compositions at equilibrium conditions. The results of this work show that the degree of sintering of chromite-silica well filler sand depends strongly on the silica content. The amount of liquid phase formed increases with increasing silica content.

Feb 2, 2022

By J. Hadjigeorgiou, T. R. Stacey

This paper introduces the Quantified Value-created Process (QVP), a decision-making process for use in mine design and operation. The implementation of the QVP is founded on a ten-step rock engineering design process and a ten-step strategic planning process. The potential of this approach is demonstrated by examples of value created as a result of good research, design, and planning. The QVP is divided into two parts, namely, a ‘planning the process’ section and an ‘implementing the process’ section, and can be considered to be an extension of the risk approach. All costs, direct and indirect, associated with a significant mining decision (design, operational, investment) must be quantified in advance of committing to that decision, to determine the value that will be created in the short, medium, and long terms. Ethical values, associated with health, safety, the environment, public perception, and social aspects, may be difficult to quantify in economic terms, but must nevertheless also be considered. In contrast with a traditional risk approach, the QVP will identify the upside, and allow executives to make more informed strategic decisions. In this context it is essential to actively engage upper management in the decision process.

Feb 2, 2022

By Ting-Wei Wang, Yung-Wen Chen

Artificial ground freezing is commonly used globally during excavation of shield tunnels and for groundwater control. It is a special construction method for temporary ground improvement that involves introducing coolant into underground pipes to freeze water in the soil. The frozen soil is cemented together as a result to form a frozen wall, which provides high strength and low permeability. Once the thickness of the ice wall reaches design requirements, underground excavation can be conducted with the coolant removed afterward to return the soil to its original state. This technique is cost-effective in scenarios where complete groundwater cut-off and excavation support are required; where work is deep underground and faces difficult ground conditions and where access restrictions limit the use of other displacement-type ground improvement techniques. Due to the demand for shield tunnel construction for utilities in Taiwan, ground freezing has become an important soil stabilization method there. In this article, we will share two brine freezing case studies and an in situ liquid nitrogen experiment that was conducted to develop this technique.

Feb 1, 2022

By Anne Lemnitzer

When a major storm system stalled over Western Europe last summer, it pro- duced the deadliest flood on European territory in the last two decades. Beyond record-setting rainfall over countries such as Luxembourg, Switzerland, France and the Netherlands from the storm's "Bernd" low pressure system, more than 230 people were killed in Germany and Belgium. The storm system also caused over an estimated $20 billion (€17.7 billion) of damage. A team from the Geotechnical Extreme Events Reconnaissance (GEER) Association, supported by the National Science Foundation, was mobilized to investigate the potential impacts of the widespread flooding in Germany, Belgium and the Netherlands. Members of the DFI Europe regional chapter closely collaborated with the U.S.-based GEER team and many other engineers and scientists in Europe to collect perishable data and study flooding effects and the event's resulting impacts on geostructures, such as bridges, retaining walls, dikes and embankments. This article features some of the vast information collected by the team, which has recently been published in a comprehensive reconnaissance report and made available for free at geerassociation.org. All data will also be accessible at the NEHRI DesignSafe Cl data repository.

Feb 1, 2022

By Richard Guenther

As available space in urban centers becomes more scarce, builders and developers are increasingly turning to vacant, existing structures to meet cities' growing needs. The developers of City Ridge Roadside Development and North America Sekisui House (NASH) - - found a suitable site for their "urban village" at the former Fannie Mae headquarters complex on Wisconsin Ave. NW in Washington, D.C., which had been vacated in early 2018. The urban village will consist of eight new structures centered around the building that currently sits on the site. All told, the project will include 687 residential units, a 150-room hotel, over 150,000 sq ft (13,935 sq m) of retail space, and 62,000 sq ft (5,760 sq m) of office space. A below-grade parking structure will extend across most of the footprint. The Fannie Mae building, which was designed in the Colonial Revival style to mimic the Governor's Palace in Williamsburg, Virginia, was named a historical landmark following a request from the development team. The central portion of its existing masonry structure was built in 1956 on pile caps with small-diameter cast-in-place piles. Two wings, which were added in 1962, were built on belled caissons. There are three levels above grade and one below.

Feb 1, 2022

By Andy Boeckmann

In early 2021, DFI formed a Foundation Reuse Task Force due to concurrent and coincidental discussions of this topic during meetings of the Subsurface Char- acterization for Deep Foundations and Testing and Evaluation committees. Interested members from both commit- tees, as well as of the Sustainability Com- mittee, joined forces to form the task force. The task force mission is to promote foundation reuse by leveraging experi- ence among DFI members and collabo- rating across pertinent committees. General goals of the task force are to identify, assess and reduce risks associated with reuse; to educate owners and decision-makers about reuse; and to improve the investigation, design, construction and testing practices associated with reuse. One of the first orders of business for the task force was to organize a roundtable discussion of foundation reuse for DFI's 46th Annual Conference on Deep Foundations in Las Vegas. Last fall's discussion was framed as a continuation of the successful "Horses for Courses" session of SuperPile '21, which also focused on foundation reuse. However, whereas the SuperPile session focused on technical content, the annual conference panel on October 13, 2021, was envisioned as a less technical conversation that emphasized audience participation while addressing approaches to decisions about foundation reuse issues. The roundtable consisted of five panelists: • • • Bryan Hartnagel, Ph.D., state bridge engineer, Missouri DOT (MODOT) Tom Bradley, project director, Stanhope, London Hilary Shields, senior geotechnical engineer, Arup, London Jim Mackey, vice president/chief marketing officer, McGee Group, London Susan White, attorney, Benesch, Cleveland The roundtable was moderated by Andy Boeckmann, Ph.D., P.E., a senior engineer who works in Dan Brown and Associates' Missouri and Illinois offices, and is an article co-author.

Feb 1, 2022

By ANGELA NAIR AVELAR, Reiner Neumann, PAULO R. G. BRANDÃO

The understanding of the influence of the different types of apatite on the performance of mineral processing of igneous phosphate ores is still a challenge due to the difficulty to explain why some types of apatite floats in the froth flotation cell and others do not under the same conditions. Three types of apatite were identified by means of cathodoluminescence (CL) images in flotation concentrate and tailing samples from the Catalão mine: predominantly blue apatite, followed by green apatite and less frequently yellow apatite. The chemical composition of these types of apatite was determined by electron microprobe analysis (EPMA) and LA-ICP-MS. Blue and green apatite respond well to the process, thus remaining in the concentrate, while yellow apatite remained in the tailings. Yellow apatite is the one bearing the lowest P2O5 content and the largest anionic and cationic sites substitution, followed by green apatite, whereas blue apatite is the most homogeneous, with highest P and Ca grades and lowest substitution level. A negative correlation of the amount of phosphorus with fluorine was observed. Furthermore, impregnation of iron oxide-hydroxides in the yellow apatite was also observed. Therefore, the low flotation behaviour is due to low crystallinity coupled with impregnation onto its surface.

Jan 31, 2022

By GRANT COLLIGAN, BROCK O’KELLEY, Corby Anderson

With the world’s ever-expanding push to expand technological capabilities, the need for specialized materials including rare earth elements has exploded. One source found in the USA is bastnaesite, a rare earth bearing fluorocarbonate mineral, currently mined at the Mountain Pass Mine in California. To increase production, it is essential to optimize existing processes and create new ones to better utilize current resources. Therefore, a US Department of Energy Critical Materials Institute sponsored research program was carried out at the Kroll Institute for Extractive Metallurgy to expand the fundamental understanding of the industrial bastnaesite concentrate leaching system. With the help of prior knowledge, thermodynamic calculations and design of experimentation based lab testing, a novel single-stage hydrochloric leach system was created to optimize the rare earth extraction from bastnaesite. Historically, the existing industrial process has utilized a two-stage leach system involving a high-temperature hydrochloric acid leach with liquid solid separations followed by a caustic crack stage of the leach residues. A series of single-stage leach experiments were run by reacting locked cycle flotation concentrates with hydrochloric acid to test common leaching parameters. The results of these patent pending single-stage tests have shown rare earth recoveries significantly higher than reported recoveries of historic two-stage caustic crack processes, all while decreasing the equipment required and the type and amount of reagents needed.

Jan 31, 2022

By Ji Fang, Chong Fan, Fengrui Wang, Dongxin Bai

Unmanned mining technology in underground mines offers high efficiency, safety, and low cost. However, ground operators face challenges in accurately perceiving the underground environment through videos. This paper presents an augmented reality (AR) platform developed to enhance the unmanned mining process. The platform uses cameras and 5G technology to transmit high-fidelity video streams to the ground, where key targets are identified and virtual models are registered in the video to enhance the real scene. Tests in the Xinli stope of the Sanshandao gold mine showed the platform’s effectiveness in improving ground operators’ perception and production efficiency.

Jan 30, 2022

By Saurabh Kundu, Shakuntala Tudu, Indrajit Paul, Chandra Sekhar, Manikanta Nallamilli, Shaik Mahaboob Basha, Neha Gupta, Srinivas Dwarapudi, Dhiraj Madhukar Kadhe

Iron ore pelletizing using compressive and shear action on wet mixture feed has been studied. The physical properties, namely, moisture content, drop strength, green compressive strength (GCS), dry compressive strength (DCS), porosity, and cold crushing strength (CCS), have been studied. Pelletizing tests were carried out on four different types of ore, namely, hematite ore, magnetite ore, goethite ore, and sinter return fines. The inference of shear forces on silica distribution index in dry pellet has been studied using optical and scanning electron microscopy. Significant improvement in physical strength was observed due to compressive and shear forces on the pellet mixture feed. However, decrease in moisture content and ball porosity has been observed. Silica distribution index improved by 1.72 times for hematite ore, 1.47 times for magnetite ore, and 1.68 times for goethite ore. It has been found that bubble cavity has been reduced which is good indicator in terms of physical properties.

Jan 29, 2022

By Serdar Aktaş, Özgün Küçükoğlu, Burcu Nilgün Çetiner, Mehmet Hakan Morcalı

This study compares the cementation performance of metallic iron, metallic aluminum, and metallic tin in terms of the reaction conditions and parameters in synthetic antimony chloride solutions. The effects on the antimony recovery (%) caused by the cementators’ types, stirring speed, reaction time, and temperatures were explored thoroughly. The cementation kinetics of antimony were also explored for each cementator. The activation energies were determined to be 10.99, 9.09, and 13.58 kJ mol– 1 for Al, Fe, and Sn, respectively. The results reveal that the reaction is diffusion controlled, and comparable results were obtained for each cementator. At 25 °C, 40 mg of iron powder was found to reduce all antimony ions (i.e., approx. 99% recovery), but even when 100 mg of Al and Sn cementators were used, the antimony recovery did not reach 100%. This result shows that iron is the best candidate to cement antimony out of the solution.

Jan 28, 2022

By Yucheng Li, De Huang, Yonghong Liu

Mine frictional resistance is one of the essential parameters of mine ventilation systems, and it is of considerable significance for the prevention and control of mine risks and accident hazards. Frictional resistance requires a lot of resources and time and has errors. To reduce the errors of frictional resistance, a regression model of frictional resistance is proposed based on the correlation analysis of the affecting factors. Through the comparative test analysis of seven regression methods, it is found that the classification and regression tree method for solving the proposed regression model has better performance than other methods. The least square error criterion is used to calculate and rank the importance of the factors affecting frictional resistance. The results show that the cross-sectional area of the tunnel, the support method, and the presence or absence of devices or pedestrian ladders have the most considerable influence on the prediction accuracy of frictional resistance. The support methods and cross-sectional areas are essential input variables. Through the combination test analysis of the influencing factors, the results show that the regression model does not have predictive ability when the number of input variables is less than 3 and the best predictive performance cannot be obtained using all the influencing factors. The best prediction model of resistance is to combine the shape of the tunnel, the support method, the presence or absence of devices or pedestrian ladders, and the cross-sectional area. The method proposed in this paper does not require a lot of resources and time investment, and the frictional resistance error is small. At the same time, it solves the problem of resistance prediction with incomplete data of influencing factors and provides a compelling new method for obtaining frictional resistance parameters.

Jan 28, 2022

By Mostafa Benzaazoua, Mariam El Adnani, My Ahmed Boumehdi, Rachid Hakkou, Salah Ouhamdouch, Abdelmalek Goumih

This study focuses on the environmental characterization and assessment of long-term neutral mine drainage (CND) potential from waste rock piles at the abandoned Erdouz mine in Morocco. The study involved metallographic analysis, static tests, and column tests. Results indicate that the waste rock is not an acid mine drainage generator but produces CND, mainly with sulfates exceeding Moroccan standards. The waste rock is relatively stable and could be reused after pretreatment.

Jan 25, 2022

By Martín Antonio Encinas‐Romero, Patricia Guerrero‐Germán, Jesús Leobardo Valenzuela‐García, José R. Parga‐Torres, María A. Bracamontes‐Landavazo, Agustín Gómez‐Alvarez

A study was carried out to process a sulfide mineral concentrate from Norwest of Mexico containing 97 g/t Au, 0.15% Cu, and 15% Fe. An oxidative acid pretreatment was investigated using ferric sulfate as oxidant, followed by leaching of gold with sodium cyanide. Scanning electron microscopy, SEM-EDS, and X-ray diffraction, XRD, the analysis confirms the presence of quartz and pyrite species. First, a leaching was carried out without pretreatment, at ambient conditions, T = 25 °C and P = 1 atm, obtaining only a 45.2% gold extraction. Once the presence of Fe and Cu sulfides had been confirmed, the Eh-pH diagrams were constructed for the Fe-S-H2O and Cu-S-H2O systems, where it is appreciated that pyrite and chalcocite can dissolve with high oxidation potentials and forming sulfur, oxidizing to sulfate at highly acidic conditions. The oxidized concentrate was neutralized and adjusted to pH > 10.5; it was leached at ambient conditions, at different particle sizes, 44, 37, and 26.5μm, achieving an Au extraction of 75% using a concentration of 0.5% NaCN, 26.5μm particle size, 20% solids, and P = 1atm. Then the oxidized material was subjected to different temperatures, 25, 50, and 70 °C, under the same conditions and obtaining Au extractions up to 92% at 70°C. Additionally, the leaching process was compared using an autoclave reactor at moderate pressures, obtaining an increase in the extraction of Au up to 98% in 2 h, at T = 70 °C and P = 0.62 MPa.

Jan 23, 2022

By Yi Yang, CHENGLONG XU, HAORAN LI, YALI FENG, JINRONG JU

This study presents a method for recovering valuable metals and synthesizing anhydrite from steel slag using sulfuric acid leaching and solvent extraction. The process achieved high leaching efficiencies for V, Ti, Fe, and Mg, and produced anhydrite with 93.09% purity. The leachate was further processed to separate and recover V, Ti, Fe, and Mg using selective stripping and precipitation methods, offering a sustainable approach to steel slag utilization.

Jan 22, 2022

By A. M. El Shafey, Ahmed W. Hussein, Ibrahim M. Gaafar, Mona M. Fawzy, Mohamed Diab, Mohamed S. Abu El Ghar

The Quaternary stream sediments of the Diit area, southern Red Sea coast, Egypt, were mineralogically studied for their content of economic heavy minerals. The study area covered approximately 450 km2 and included three main parts: Wadi and Delta Diit, as well as Diit lens. The mineralogical investigation revealed that these sediments contain considerable amounts of placer ilmenite, magnetite, zircon, sphene, apatite, garnet, and rutile. Also present, in minor or trace amounts, are uranothorite, monazite, xenotime, fergusonite, khatyrkite, and gold. The magnetic fractionation tests, supplemented with the XRD and SEM mineral analyses, indicated the presence of Fe-oxide minerals as wuestite, hematite, and maghemite accompanied with magnetite as products for hand magnet separation. Ilmenite separation was carried out using a high intensity magnetic separator at a current of 1 A, while the paramagnetic minerals (e.g., garnet, pyroxene, amphibole, epidote, monazite, xenotime, and fergusonite) were separated as magnetic fraction at a current of 3 A. The non-magnetic minerals (e.g., zircon, apatite and rutile, uranophane, uranothorite, gold, and khatyrkite) were obtained at 3 A current. On a mineralogical and geochemical basis, the present work suggests that Diit stream sediments should be considered as a potential source for Ti, Fe, Zr, Zn, and Cu after the physical upgrading processes for concentrating the minerals carrying the aforementioned economic elements.

Jan 21, 2022

By İsmail İnce

The purpose of this study is to investigate the index-mechanical properties of igneous rocks by using the electrical resistivity method. Electrical resistivity, index (P-wave velocity, dry density, and porosity), and uniaxial compressive strength values of 48 different igneous rock samples were measured in the laboratory. Simple regression analysis was performed between index-mechanical properties and electrical resistivity values. Strong exponential and logarithmic correlations were found between electrical resistivity and the index-mechanical properties of the igneous rock samples.

Jan 21, 2022

By Yanan Zhang, Hongwei Deng, Feng Gao, Bo Ke

Recently, liquid carbon dioxide (L-CO2) blasting technology has attracted attention due to its good fracturing effect and safety performance, especially in coal seam permeability improvement. This paper analyzes the blasting effect of L-CO2 based on experiments and studies the fracturing mechanism from the perspective of stress wave action via theoretical analysis and peridynamic simulations. The results indicate that L-CO2 blasting achieves a good fracturing effect without forming a crush zone, and the loading rate and strength of the stress wave are key factors.

Jan 19, 2022

By Cheng Li, Yanlei Wang, Lingrui Kong, Jianxin Tang, Fang Yuan

Coal mined-out areas have a significant impact on mining safety and affect the pressure distributions of neighboring coal faces. The PFC3D software is used to study the goaf mechanical characteristics, and the core loading test verifies the rationality of the numerical simulation method. The results from the numerical modeling showed that the void ratio, particle size ratio, and particle size distribution of the rock particle sample (RPS) had a significantly remarkable influence on the compression deformation characteristics of the rock block. The parallel-bond tensile strength and parallel-bond cohesion had a notable impact on the compression deformation traits of the rock block only when the axial stress level was lower than 12 MPa. By contrast, when the axial stress exceeded 5 MPa, the effective modulus significantly influenced the compression deformation features. However, the stiffness ratio, loading rate, and parallel-bond friction angle had almost no effect on the compression deformation characteristics. Furthermore, when the stress level was less than 10 MPa, the stress–strain curves from the rock core samples’ numerical simulation and loading tests were approximately linear. In addition, the Pearson correlation coefficients of the stress–strain curves suggest that the goaf zone’s core numerical simulation results had a robust correlation with the loading test results. The findings of this study can serve as a reference for the field application of PFC3D software and safety assessments in goaves.

Jan 18, 2022

By Mehdi Noori, Atefeh Azizitorghabeh, Fereshteh Rashchi, Ataollah Babakhani, Sarah Mahmoudi

The focus of this research was to evaluate the synergistic effect of bis(2,4,4-trimethylpentyl) phosphinic acid (CYANEX 272) and di-(2-ethylhexyl) phosphoric acid (D2EHPA), diluted in kerosene, on the extraction and separation of Co(II) and Li(I) from synthetic sulfate solution. The results indicated that using a mixture of CYANEX 272 and D2EHPA was efficient in extracting and separating Co(II) from Li(I). The optimum ratio of CYANEX 272/D2EHPA was found to be 5:1, in which the highest separation factor was obtained (5973.23), and ΔpH0.5 was 4.10. Adding tributyl phosphate (TBP) as a modifier and increasing the temperature improved the metals’ separation rate and extraction efficiency. Thermodynamic studies were also carried out, and ΔH, ΔS, and ΔG values were computed, revealing the endothermic nature of Co(II) and Li(I) extraction by CYANEX 272/D2EHPA mixture. The conducted experiments for the McCabe–Thiele diagram showed the possibility of using two stages to extract over 99% of Co(II) and Li(I). Slope analysis and Fourier transform infrared spectroscopy (FT-IR) were employed to comprehend the Co(II) and Li(I) extraction mechanism using a mixture of CYANEX 272 and D2EHPA.

Jan 17, 2022