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By Jan Lückhoff

The introduction of the EAF Quantum furnace by Primetals Technologies represents an important milestone in the field of electric steelmaking during the last 15 years. In this process the latent and chemical heat of the off-gas generated during a melting process in an EAF is used to pre-heat scrap in an integrated shaft prior the melting of the scrap in the vessel. Combining proven own technologies, Primetals EAF Quantum enables nearly continuous process, cutting down idle times and enhancing availability for production. The essential benefits will be shown in this Paper.

Aug 16, 2017

By Jesús A. Carlos Cornelio

Since their discovery in 1991 Carbon nanotubes (CNTs) have attracted much interest due to their remarkable mechanical, thermal, electrical, chemical and optical properties. In connection with their mechanical properties, CNTs have been studied in various forms for tribological applications including their use as lubricant additives for oil and water. In this paper the tribological properties of CNTs (SWCNTs and MWCNTs) when used as lubricant additives are studied under rolling-sliding conditions in a twin-disc testing machine. The tests were performed using 5% of creepage and pressures of 0.8 GPa and 1.1 GPa. Used functionalized nanotubes were modified with carboxylic acid ultrasonically dispersed at different concentrations (0.01, 0.05%). The results indicated that the presence of carbon nanotubes leads to a decrease in both friction coefficient and wear rate for both systems studied (oil and water).

Jul 31, 2018

By Daniel Stickel

Current political, economic and ecological guidelines demand the increase of power densities of nearly all machinery parts today. In order to further lower the wear rate towards the ultra-mild sliding wear regime an integral approach is needed, which has to regard contact conditions, surface topography, surface chemistry, as well as sub-surface properties. Still there are no simple parameters to classify the performance of tribosystem. In this study the area and volume affected by tribocontacts are calculated by means of a three dimensional elastic-ideal plastic contact model. The surfaces are generated by means of conventional machining procedures and characterized by scanning white light interferometry. The further input data as to normal and friction forces are derived by ultra-mild sliding wear tests under boundary lubrication conditions of carburized steel against carburized steel and 52100 steel against case-hardened spheroidal cast iron. This contribution will depict the distinct influence of the topography on friction and ultra-mild sliding wear of common Fe-base materials and point on the marked importance of highly localized effects, which govern the acting mechanisms.

Jul 31, 2018

By Hongshuang Di, Tianyu Zhang, Huiqiang Huang

A CMnSiAl transformation induced plasticity (TRIP) steel was used to study the effect of retained austenite on room-temperature mechanical properties. The steel plates with retained austenite were obtained by hot rolling, cold rolling and subsequent continuous annealing. The starting and finishing temperature of hot rolling are between Ac1 and Ac3. Reduction ratio of cold rolling is 75%. The continuous annealing is carried out at different intercritical temperatures. The relationship between work hardening exponent and retained austenite was discussed. The results show that, the Ac1 and Ac3 were much high because of the alloy elements, and the temperature range between them was wide. Due to the high hot rolling temperature, the grains was hereditarily refined as a result of dynamic recrystallization. Annealing at intercritical temperature of 930 ºC, retained austenite with relatively high stability reached a maximum volume fraction of 25%, a maximum total elongation of 30.2% and a best ultimate tensile strength × total elongation of 20.1 GPa·%. Instantaneous work hardening exponent reflects strengthening mechanisms at different strain stages. The TRIP effect of retained austenite is the main mechanism during deformation. With retained austenite of sufficient amount and high stability, continuous work hardening was observed in the tensile specimen of 930 ºC.

Oct 1, 2019

By Aitor Elorriaga Fernandez de Arroyabe

The purpose of Sinter plants is to heat iron ore fines along with fluxes and coke fines or coal, to produce a semi-molten mass that solidifies into porous pieces of sinter with the needed size and strength. Fluxes used in the sintering process need to have an appropriate size distribution and TI to avoid generation of fines, which could reduce the productivity of the Sinter. Besides, a homogeneous chemical composition and high absorption characteristics are necessary to control the basicity and to combine the flux with P, S, Si, etc, respectively. PASEK Dunite is an ultramaphic rock exploited in the north of Spain with a basic chemical classification, being olivine and serpentine its principal minerals. It is a very homogeneous and hard stone and its main characteristics are: high hot and cold resistance to mechanical stresses, softening and melting points of a flux not of a refractory material. In addition, due to its mechanical and chemical properties, less fines are generated in the sintering process and during the handling and transportation to the blast furnace, improving the productivity of these processes. In this way, the use of PASEK Dunite allows increasing the homogeneity structure of sinter, reducing the percentage of return fines and improving the Sinter productivity.

Oct 30, 2017

By Yong Tian, Tian Zhang, Zhao-Dong Wang

To meet the requirements of high-performance steel plates, while reducing manufacturing costs and saving energy, the advanced cooling system for plate mill (ADCOS-PM) with functions of accelerated cooling (ACC), ultra-fast cooling (UFC), and direct quenching (DQ) was researched and developed by the State Key Laboratory of Rolling and Automation (RAL). Since 2003, several sets of ADCOS-PM device were developed and implemented in industrial practice. To fully utilize the ADCOS-PM technology, the combination of various strengthening mechanisms was promoted by NG-TMCP technology and low-cost, high performance plates were produced such as pipeline steels, and high-strength construction machinery steel.

Oct 1, 2019

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By Gustavo Borges Tiboni

The erosive wear caused by the impact of solid particles against a surface is a tribological phenomenon present in many segments of the industry, such as transportation, aerospace, mining, power generation, among others. The most usual method to set the wear rate is by measuring the mass loss of the material. In order to apply one technique with potential to determine the rate of erosion wear, this study developed a dedicated equipment and conducted preliminary erosion tests monitored by non-destructive testing known as acoustic emission technique (AE). This can be defined as a technique able to detect mechanical waves generated by the release of elastic energy accumulated in the material. Erosion tests were performed in order to evaluate the ability of equipment to collect data from AE and to correlate these data with the wear of the samples. Samples of low carbon steel eroded by the impact of angular aluminum oxide particles suspended in air at three different velocities: 45, 57 and 67 m/s. The impact angle between the particles and the sample was set at 30 degrees and the test temperature at approximately 20°C. The wear rate has changed with the velocity in accordance with the kinetic energy of the particles and the AE parameter RMS showed sensitivity to the variation of particle impact velocity and to the wear of the sample eroded. The rate of AE signals collected over time correlated with the flow of particles striking the sample, and with the parameters of energy, rise time and duration of the signal.

Jul 31, 2018

By Dalila Chaves Sicupira

A pitting corrosion study of welded joints of lean duplex stainless steel (LDSS) UNS S32304 has been performed. LDSS S32304 thick plates were welded by different processes commonly employed in equipment and piping construction: SMAW (Shielded metal arc welding), GMAW (Gas metal arc welding) and FCAW (Flux cored arc welding). The electrochemical behavior of different weldment zones (fusion zone (FZ), base metal (BM) and heat affected zone (HAZ)) was characterized both independently using an electrochemical microcell and together through whole sample analysis. The electrochemical method applied was performed in acidified glycerin, a process fluid of the biodiesel industry. The results were correlated to the microstructural features of the materials. Based on the results, is possible to conclude that the breakdown potential (Eb) of the fusion zone (FZ) was higher than the Eb obtained for the heat affected zone (HAZ). In general, top samples show higher breakdown potential than root samples and also the samples welded using filler metal 2209 has a better anodic behavior than the filler metal 2307. According to the results, GMAW welding process with 2209 as filler metal was revealed as the optimum chosen for application of 2304 duplex stainless steels in this case.

Jan 16, 2018

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019

By Jônatas Venancio Barbosa, Dagoberto Brandão Santos, Túlio Magno Füzessy de Melo

In this work, the mechanical and metallurgical behavior of titanium added ultra-low carbon (ULC-Ti) steel under hot and warm working conditions was studied by means of dilatometer compression tests. Double compression schedules were performed at temperatures between 700°C and 1000°C, inter-pass times of 0.5-100 s, and deformations of 0.5 and 0.3 in the first and second stages, respectively, with strain rate of 1 s-1. The analysis of the flow curves obtained allowed the evaluation of the softening characteristics of the steel. The softening and microstructure features indicate different restoration mechanisms depending on the temperature range. Static recrystallization with rapid microstructure restoration is observed at temperatures within the austenitic and intercritical field. Strain induced boundary motion and recovery mechanisms apparently control the restoration process in the ferrite region. In general, flow stress curves showed dynamic recovery behavior. Only the deformation in the intercritical region produced a peak in the flow stress curves. Isothermal holding tests associated with single hit compression indicated the presence of dynamic strain induced transformation, accelerating the softening kinetics at the intercritical region.

Oct 1, 2019

By L. Martins Demuner, D. Burzic, V. Cunha Aranda, F. L. Lourenço, G. Romeu Trindade dos Santos, F. Ramstorfer

For many years, Dynamic Soft Reduction has been regarded as a proper method in improving internal quality of slabs. Even though processes models improved significantly over the past years, the efficiency of Soft Reduction was always limited by the discretization error, which inherently exists if segment rollers cannot be positioned individually. The recently developed SRD segment type allows for an individual roller positioning within the mushy zone by avoiding any discretization deviation from the optimal gap. This paper provides a detailed technological overview of the SRD segments as well as operational results at their very first implementation at Ternium Brazil.

Oct 1, 2019

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Daniel Hajduk

Efficiency of back up rolls depends mostly on two parameters – length of campaign and dressing amount after the campaign. The longer the campaign (in terms of rolled tones) is, the higher the dressing amount. To solve this task properly it is necessary to know the distribution of accumulated damage in the working layer of the roll caused by previous campaigns and by loads (separating force and bending) during present campaign respecting changing conditions of material properties (hardness) through radius of the roll. To find an optimum dressing amount an algorithm has been developed and specialized computer program will be presented, that takes real measured loads during the backup roll campaign, calculates fatigue damage in the roll and suggests relevant dressing amount. This can help to prolong service life of rolls, minimize the risk of spalls and reach maximum efficiency in terms of rolled tones/km per roll.

Jul 30, 2018

By Darina Manova

Plasma assisted surface modification methods have been used to nitride stainless steels in order to enhance hardness and therefore the lifetime of industrial components. Nevertheless, the corrosion resistance is not always preserved since it is very sensitive to the process parameters, either in implantation or in thermochemical diffusion techniques. AISI 316L stainless steel was plasma nitrided using three different techniques: Low Energy Ion Implantation (LEII), Plasma Immersion Implantation (PI3) and conventional DC pulsed plasma nitriding (DCPN). For each method several parameters were tested and some of them were selected to achieve the so called S phase of about 3 µm thickness and no nitrides precipitation. The nitrided layer was characterized with OM and SEM. Hardness was assessed on the surface with Vickers indenter and 25 g load. XRD was performed to characterize the S phase and to detect other phases if present and electrochemical corrosion tests were carried out in 3.5% NaCl solution. Although the S phase thickness in the three groups of samples was comparable, hardness was not and neither was the corrosion resistance. The PI3 samples were the hardest with the best performance in corrosion experiments, resulting in a higher breakdown potential and lower currents.

Aug 8, 2018

By Davide Onesti

Electrode regulation is the technology at the heart of the AC and DC Electric Arc Furnace. As such, in the last decade it underwent continuous improvement to maximize the EAF performances, in terms of process efficiency, machine utilization and operator safety. Given this background, Danieli Automation’s efforts in the field of electrode regulation have been focused on fast response to scrap cave-in, compensation of supply variations, automatic resonance detection, transformer protection, dynamic regulation of the electrical and chemical set-points, coordination and control of slagging and foaming agents, arc irradiance supervision. An extensive analysis of operator utilization and feedback was also carried out to develop an innovative system HMI. In this field, the choice of the variables shown to the user is the key aspect to allow a prompt process evaluation by the operator, who can refer to a condensed set of useful data. This paper will describe the innovative features and embedded models of the electrode regulation module (Q-REG+) and the supervision HMI, together with the effects of their application on EAF process efficiency and system usability.

Oct 30, 2017

By Cristina Escudero Martinez

The purpose of the Basic Oxygen Steelmaking (BOS) is to refine the hot metal produced in the blast furnace into raw liquid steel, which may be subsequently refined in the secondary steelmaking shop. Appropriated fluxes for the BOF could require low melting point to reduce the energy consumption, to reduce the energy to fluidity the slag at lower temperature and to melt at lower temperature than steel. It is necessary a good Tumble test result and the fluxes do not generate fines which could obstruct the blowing plugs, so we would have a homogeneous flux. A homogeneous chemistry that allows to control the basicity (Si and MgO levels) and a high absorption characteristics to combine the flux with P, S, Si, etc. are necessary. PASEK Dunite is an ultramaphic rock exploited in the north of Spain with a basic chemical classification being olivine and serpentine its principal minerals. It is formed by orthopyroxene, clinopyroxene and olivine in variable proportion. Dunite is a very homogeneous and hard stone. The main characteristics are: High hot and cold resistance to mechanical stress (shatter / crushing / abrasion), softening and melting points of a flux, not a refractory material, large porosity which is increased more than 20% when dunite is heated at BOF process temperature, and high absorption level, and stable components with low melting points. PASEK Dunite is a good flux in BOF process and its use is recommended if the BOF process produces pig iron with low Si content, generates high levels of slag and it is necessary maintaining the basicity index and the MgO amount and with high value of hot metal ratio (high amount of phosphorus to remove).

Aug 16, 2017

By Evan Thomas

It has been shown before that liquids can slip at a solid boundary, which prompted the idea that parallel-surface bearings can be obtained by the use of alternating slip and non-slip regions in the direction of fluid flow. The amount of slip at the wall depends upon the surface tension at the liquid - solid interface, which in turn depends on the chemical composition of the surface and its roughness. In the present study a heterogeneous surface was created by coating half of a circular glass disc with a coating repellent to glycerol. A rotating glass disc was placed at a known distance above the coated stationary surface and the gap was filled with glycerol. With the top surface moving in the direction of slip to non-slip region, a pressure build up can be theoretically predicted. The pressure gradient in the two regions is constant, similar to that in a Rayleigh step bearing, with the maximum pressure at the boundary. In order to accurately measure the force generated by the pressure increase, a load cell was attached to the heterogeneous disc. Experiments were conducted by varying both sliding speed and distance, and the resultant load carrying capacity was measured and compared with theoretical calculations. This allowed the slip coefficient of the coated surface to be evaluated.

Jul 31, 2018

By Jean-François Stumper, Mario Moser, Mark Kruessmann, Volker Langer, Daniel Bastos Martins Cruz, Claude Meisch

The latest generation of probes and casthouse machines provide a wealth of data that has not been available a few years ago. The evaluation of this data gives direct feedback to improve the blast furnace efficiency, the equipment maintenance and design and it allows the early detection of critical or deviating process situations. A stable operation with lower operation and maintenance costs are the final customer benefits.

Oct 1, 2019

By Marcelo Rebellato, Beatriz Pereda, Beatriz Lopez, Pello Uranga

The classical application of Nb microalloying in the development of thermomechanical processes for flat products has been related to its suitability to enhance strain-induced precipitation and get a pancaked austenite prior to transformation. As new steel grades or new lay-outs are being developed, more complex metallurgical conditions need to be evaluated. In this context, Nb microalloying, alone or combined with other microadditions, needs to intervene in a more controlled way in additional steps of the thermomechanical process, besides its conventional strain-induced precipitation role. For example, the hardenability enhancement associated with Nb to properly achieve lower temperature transformation products, demands a proper balance of the Nb amount precipitated during rolling and the one remaining in solid solution. Similar effects are also sought when the final available Nb is used to increase strength through precipitation hardening. This manuscript evaluates how changes in the rolling strategies affect the interaction between Nb(C,N) precipitation and austenite recrystallization at different steps of the rolling process. As the possible interactions between parameters intervening simultaneously are quite complex, the application of microstructural models helps to properly define the best austenite conditioning combined with the convenient amount of Nb in solution, as a function of the final property requirements. Along the manuscript, several strategies will be discussed for the case of hot rolling of flat products comparing both normal and coarse initial austenite grain sizes.

Oct 1, 2019