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By J. Kempken

Driven by customers, especially from the automotive sector, the supply of 100% prime quality has become essential. Furthermore the implication of quality costs and the yield of first class products define the steel companies' profitability and overall success significantly. The SMS group together with its subsidiary MET/Con has developed a comprehensive solution to assess the product quality over the production and processing chain. Process and production parameters originating from various data sources of the process automation are examined on their impact of quality related characteristics.Expert know how and comprehensive operational experience is translated into a quality guideline and a regulation framework as the sensitive core of the PQA solution.Once implemented, the system identifies immediately steel grade specific, deviations from ideal standard and proposes corrective actions including a final evaluation for each product at each processing step.The X-Pact® PQA (Product Quality Assessment) system is a substantial tool for root cause quality analysis and provides the required support to the production team. It will become an integral part of the corporate quality management system.

Aug 17, 2017

By Susanne Hahn

The Siemens VAI software model DynaPhase calculates thermodynamic properties depending on the chemical analysis of steel. It can be used online together with Siemens VAI’s secondary cooling model SIMETAL Dynacs 3D which is a unique feature. Offline it can be used to investigate the thermodynamic properties of steel grades and therefore supports the development of new grades. The core of DynaPhase is a substitutional solution model for the Gibbs free energy to calculate multi-component phase diagrams. The parameters of this model are determined by employing the CALPHAD approach. This model is combined with a microsegregation model to account for the interdendritic solidification process. New DSC (differential scanning calometry) measurements of the department of metallurgy of the Mining University of Leoben have been used to improve the DynaPhase database for high Al or Si concentrations. By comparing this experimental data to calculations it has been found that some of the widely used commercial software tools do not describe the ternary system FeAlC for high aluminum concentration correctly. In this paper we will show how thermal properties of high Al grades change with the optimized database and what impact this has on the secondary cooling of continuous casting, e.g. how the solidus point shifts on the strand. Moreover we will show that the online use of DynaPhase has many advantages for the production. Since DynaPhase uses the actual chemical analysis of the steel grade and not just concentration ranges or averaged concentrations it is possible to optimize the cooling strategy during casting for the actual chemical analysis of the actual heat.

Jul 30, 2018

By Tiago de Abreu Siqueira

CO2 geological storage is one of the current technologies developed worldwide to reduce industrial emissions of carbon dioxide to the atmosphere. Two main mineral types of deep geological reservoir could be contemplated for CO2 storage: sandstone reservoirs and carbonaceous reservoirs. Geochemical reactivity of a dolomite-calcite mineral compound and magnesite pure mineral was studied with a set of nine experiments per crushed mineral phase with two saline solution and with mQ water and three temperatures: 50°C, 90°C and 150°C. Experiments were performed in batch reactors with 250 bar of CO2 partial pressure during 24h to assess the effect of temperature and salinity in constant CO2 pressure. Solid characterization was performed by XRD and solution analysis by ICP-OES. Acidification of solutions due to CO2 dissolution in water is the main source of reactivity in the system. Proton concentration increases and causes partial dissolution of initial dolomite, calcite and magnesite and release of Ca2+ and Mg2+ cations in solution. Bicarbonate anion (HCO3) concentration also increases due to CO2 dissolution in water and carbonate minerals dissolution. Temperatures of 90°C and 150ºC increase the kinetic of reaction and the dissolution of minerals and cations release in solution. New carbonate crystalline phase precipitates as a Ca, Mg solid solution between dolomite and calcite pure poles.

Aug 8, 2018

By Daniel Augusto Godinho de Carvalho

Since the beginning of BOF process, slag formation has been subjected to extensive development. During the initial stages of the blow, fast slag formation is primordial for the process performance. This is mainly to allow oxidizing reactions, and also to protect the refractory. A modeling of BOF process for the purpose of process optimization requires precise knowledge concerning the dissolution of CaO and MgO based materials. Using this knowledge, the optimal process conditions can be ensured by a controlling of the slag formation during the converter steelmaking process. Taking into account an application of large amount of different raw materials, as well as location-specific process conditions, the characterization of the dissolution behavior of different additives is an important key to improve the technological process. Thereby, in the frames of this project, an appropriate model for slag formation is established and compared to operational results for a 330t BOF, operating at ThyssenKrupp CSA, Santa Cruz, Brazil.

Aug 16, 2017

By Felipe Farage David

A laminação de tiras a quente de bobinas de aço apresenta alta relevância devido a possibilidade de obtenção de diversos produtos para diferentes aplicações, tais como: construção civil, industria automotiva e implementos agrícolas. O controle das variáveis de processo, tais como temperatura de reaquecimento de placa, velocidade de resfriamento e temperatura de bobinamento, é determinante para obtenção da microestrutura e, por conseguinte, das propriedades mecânicas do material. O propósito desse trabalho é estudar o comportamento da microestrutura e das propriedades mecânicas com a variação da composição química (adição de microligas de nióbio e titânio), mantendo uma rota de laminação termomecânica similar na laminação de bobinas a quente. Os aços aplicados neste estudo foram o aço microligado ao nióbio e titânio equivalente ao ASTM A1018 HSLAS 50 Classe 1 e o aço carbono comum equivalente ao ASTM A1018 SS36 Tipo 2. Apesar do aço carbono comum apresentar carbono equivalente superior ao aço microligado, foi verificado maior limite de escoamento (se) no aço microligado ao nióbio e titânio. Dessa forma, aplicando tratamento termomecânico adequado no aço microligado é possível conseguir propriedades mecânicas melhoradas principalmente devido ao refino de grão e ao endurecimento da ferrita.

Aug 16, 2017

By Gabriel Oliveira Glória

Como uma boa alternativa a outros materiais, o número de materiais ecológicos está aumentando. As fibras naturais estão substituindo fibras sintéticas, por exemplo, a fibra de vidro. Além dos aspectos ambiental, as fibras naturais são mais baratas do que os sintéticos. A caracterização do FTIR é um indicativo sobre a possibilidade de integração de fibras com as matrizes de polímeros e compósitos ambientais. Portanto, o presente estudo analisou a fibra de PALF por meio de espectroscopia FTIR. O espectro mostrou principais bandas de absorção típicas de interacções moleculares específicas de fibras PALF. A análise FTIR do permitiu a identificação de grupos funcionais moleculares de fibras PALF e as suas características de vibração.

Aug 17, 2017

By Vera Lúcia Othéro de Brito

Literature has shown that spinel Co-Mn ferrite have potential application in magneto-mechanical sensors, due to its relatively high magnetoelastic sensitivity. In this work, Co-Mn ferrite was processed by means of the ceramic method, using Fe2O3, MnO and Co3O4 as raw materials. Samples were liquid-phase sintered, using Bi2O3 additive as liquid-phase former. X-ray fluorescence analysis was carried out in the raw materials in order to evaluate their impurity content. Atomic absorption spectrometry analysis was used for quantifying the Co/Mn/Fe proportion in the ferrite. The microstructure of the sintered sample was analyzed by means of Scanning Electron Microscopy. The magnetization and magnetostrictive behavior of the ferrite were evaluated, obtaining curves for magnetic hysteresis, magnetostriction and magnetoelastic sensitivity. The impurity inclusions and the Bi-rich particles formed from the liquid phase were characterized. The sintered ferrite had a total magnetostriction of -126ppm, which is lower than the values reported in literature for a Co-Mn ferrite of similar composition. It was verified that sintering was carried out within a critical temperature range, in which the decomposition of Mn ferrites may occur when sintering in air. This decomposition affects the magnetic properties of the material, and it may be avoided by using controlled sintering atmospheres.

Aug 8, 2018

By Samuel Filgueiras Rodrigues

An austenitic stainless steel ISO 5832-9 was deformed in a torsion test machine over the temperature range of 1,000°C – 1,200°C and strain rates of 0.05, 0.1, 1.0 and 5.0s-1. The Steel plastic behavior was studied by analyzing the flow curves shapes and using the constitutive equations under the conditions of thermomechanical treatment. The curves initially presented an increase in stress characterized by hardening work, followed by a drop in stress to an intermediate level that reached or not, for certain conditions, the steady state softening. The plastic flow curves of ISO 5832-9 steel displayed in three different ways: (i) Curves with continuous softening presenting plastic instability for low temperatures and high strain rates; (ii) curves type flat, here after the peak there is little variation of stress with strain presenting softening mechanism by higher contribution of dynamic recovery at low temperatures and low and intermediate strain rates; (iii) curves with softening after the critical deformation favored by high temperatures and low strain rates. These behaviors indicate the influence of the stacking fault energy (SFE) and precipitated particles on the softening kinetics of this steel.

Aug 8, 2018

By Luan Bezerra Silva

O presente trabalho pretende estudar o comportamento mecânico do cobre eletrolítico C11000 e da liga de cobre cromo C18200. Esses dois materiais são objetos de estudos da equipe técnica que está desenvolvendo a câmara de combustão do motor foguete propelente líquido L75. Atualmente, não há disponível na literatura informações sobre o comportamento mecânico desses materiais em altas temperaturas. A fim de suprir essa necessidade, foram realizados ensaios de tração a quente, no intervalo de temperatura de 27 a 500°C. Adicionalmente, foram realizados ensaios de dureza Vickers e metalografia para avaliar a capacidade do material em resistir mecanicamente em altas temperaturas. Os resultados obtidos demostraram que o cobre eletrolítico sofre amolecimento a partir de 400ºC e que o cobre cromo, apesar de apresentar elevada resistência mecânica quando comparado com o cobre eletrolítico C11000, é um material frágil.

Aug 16, 2017

By Anna Carolina Cerqueira Neves

Fibras naturais estão cada vez mais sendo empregadas como fase de reforço em materiais compósitos com matriz polimérica, pois estas apresentam vantagens ecológicas e econômicas quando comparadas as fibras sintéticas. São fontes renováveis de matéria prima, são biodegradáveis e utilizam menos energia para sua produção. Foram avaliadas propriedades de tração de compósitos de matiz polimérica epóxi reforçada com altos volumes correspondendo a 40% e 50% de volume de fibras de juta contínuas e alinhadas. Os testes foram realizados na maquina universal Instron. A resistência à tração apresentou um aumento crescente com a adição da fase de fibras de juta na matriz.

Aug 16, 2017

By Gajraj Rathore

With the advent of modern HRM ( Hot rolling mills) with capacities beyond 5 Million tons with corresponding enriched CRM (Cold Rolling Mill) capacities, the throughput per hour exceeds invariably beyond 50 coils per hour making it possible to manage, track, handle, transport, store and dispatch inevitably with an automation system supplemented by corresponding software and hardware. This is true with respect to the production of Cold rolled Annealed, Galvanized, Continuously Annealed, Galvalume, CRGO, CRNGO and Colour coated coils which need total care in handling, tracking and dispatch. Understanding the above needs precisely JSW, Vijayanagar, India, has rightly gone in for a total automatic Yard management system and ASRS wherein the coils are handled as much as possible automatically in cradles without any damage insuring the receipt of coils to the customer as was produced. This CRM 2 has been commissioned and is operating with maximum automation with least manpower and max productivity with assured quality and safety. Pesmel OY Finland had the opportunity to Design, Supply and Commission this system which is first in the country and this technical paper analyses the above project as a case study enlisting the sound technical aspects as well as emphasis on the techno economics with assured ROI (Return on investment) and enhanced efficiency.

Aug 16, 2017

By Raúl Daniel López

Ternium-Siderar steelmaking has been focused in permanent improvements and process optimization. At present the Slab Continuous Caster N°1 has been totally transformed after 20 years of uninterrupted work. The authors of this paper summarize and comment on aspects which were the main changes and place emphasis largely on those technological developments in which they have been active during that period. Productivity and quality have been our goals during the last 20 years; it has led us to improve process and to achieve better control tools. In the development of this presentation, the authors will put special emphasis on the explanation of those works that were made following their own experiences through the technical personnel who belong to the staff of the company.

Jul 30, 2018

By Andrea Codutti, Gianni Tiussi, Andrea Tonnicchi, Morris Codarin

Essar Algoma Steel, Canada, awarded Danieli Transimissions a strategic order for the upgrade of the main drive spindles belonging to the most loaded stands of the Hot Strip Mill, F1-F2, F5 and F6. Featuring special heavy duty design and advanced torque monitoring system, these spindles replace existing competitors’ grease lubricated design with the efficient continuous oil lubricated solution to withstand the tough working conditions, increase life expectations and provide room for a product mix extension. The first couple of spindles have been installed in September 2017 by the expert Service team and are showing already good and reliable performance. Progressively all the others are being installed.

Oct 1, 2019

By Afonso Cardoso da Silva, Romeu Thomaz Viana Jr, Emanuelle Garcia Reis, José Herbert Dolabela da Silveira

The Gerdau Ouro Branco Mill, three years after the implementation of its new plate mill, has started to develop high complexity products. The plate mill’s learning curve has been increasingly challenging since products are being developed to their highest grades. This work aims to present the first results of the development of steels of the strength class of 510 MPa produced by TMCP (Thermomechanical Controlled Processing) followed by accelerated cooling. These results show the potential and advantage of the accelerated cooling process regarding to obtain products of high mechanical strength and high toughness, associated with a low equivalent carbon.

Oct 1, 2019

By Benito Barbabela e Silva

O pelotamento é a mais complexa etapa de aglomeração de finos de minério de ferro. Sua resposta é naturalmente oscilante, sendo bastante influenciada pelas características físicas obtidas nos processos de beneficiamento mineral que a precedem e tem papel crucial para a etapa de tratamento térmico de sinterização à jusante. O presente trabalho aborda o processo de classificação de pelotas verdes, sólidos singulares de aspecto deformável e pegajoso, em peneiras de rolos por modelamento por aplicação de Método dos Elementos Discretos. Esta técnica mostra-se como uma importante ferramenta pois supera as limitações impostas na modelagem física (quantificação e identificação de fluxos por ausência de instrumentação em escala industrial, amostragem sem representatividade) ao reproduzir de forma verossímil as repostas do sistema para importantes variáveis de controle: comprimento de gap, umidade, dispersão de tamanhos e resistência das pelotas.

Oct 30, 2017

By Frank Schrama

Steelmakers worldwide agree that the most efficient and cost-effective solution in BOF steelmaking is to desulfurize the hot metal between the blast furnace and converter. Various methods are currently in use, among which the Kanbara Reactor (KR, using only lime as a reagent), Magnesium mono-injection (MMI, using only magnesium; also known as the Ukraina-Desmag process) and co-injection (using magnesium and lime/CaC2) are leading. These three hot metal desulfurization methods are compared based on metallurgy, efficiency, costs and overall performance. Both available data from literature and experience from Danieli Corus engineers is used for this study. The KR process is able to reach low sulfur concentrations (> 10 ppm) in hot metal and has lower reagent costs. However, due to higher Fe-loss and heavy wear the KR process has the highest operational costs. The Magnesium mono-injection process is very fast due to the use of the reactive magnesium as reagent. Major problems with resulfurization (sulfur levels below 50 ppm cannot be reached) and the violence of the process made that this process could never get a firm foothold in the western steel industry. The co-injection process with magnesium and lime proves to be able to combine the best of both worlds. It can reach low sulfur concentrations and desulfurize fast. Co-injection is also the most flexible and cost effective.

Aug 16, 2017

By Weimar Silva Castilho

A influência do tempo de encharque criogênico no amortecimento da liga Ni-43,9%Ti foi investigada. Por meio da técnica de excitação por impulso determinou-se essa propriedade de amostras submetidas a diferentes tempos de encharque criogênico a -196oC. Observou-se que o amortecimento sofreu aumento de até 119% para corpo de prova submetido ao encharque criogênico por 24 horas.

Aug 16, 2017

By Cameron Soltys, Hamid Ghorbani, Maher Al-Dojayli

Cooling staves in blast furnaces are used to minimize the process heat loads on steel shell and refractory system. Copper staves are exposed to significant fluctuating thermal loads which may lead to premature stave failures due to cracks, water leakage, bending, abrasion and resultant wear. In this paper, an assessment methodology is presented to evaluate the effect of thermal cycling on copper staves including bending, fatigue and thermal ratcheting. This approach incorporates temperature-dependent copper properties including creep and plasticity to more accurately capture inelastic deformations, damage and fatigue in staves under transient and cyclic thermal loading conditions. Root cause failure assessment and improvements to copper stave design can be assessed using the presented methodology.

Oct 1, 2019

By Uwe Wilhelm

Pittini Group has contracted Danieli in 2011 for the supply and replacement of the existing EAF at Ferriere Nord Plant in Osoppo. This was a very challenging project: giving the fact that the Meltshop was operating already under very high performance level, there were many elements involved for the project to improve (reduce the amount of charges, promote highest possible chemical energy utilization, allow best optimization on existing transformer power, modification on Drop Out box and Water Cooled Duct, Hydraulic System for EAF, Scrap Bucket design to fit to new EAF with existing loading and transport system, Automation System Review and Upgrade) as well as limitations of the existing installation (limited space, lifting capacity building and cranes and the required solutions for fast shell and roof exchange). All furnace parts, as well as installation engineering, were developed and discussed carefully with the Customer to either provide proven and reliable concepts, but also to define solutions for fast installation/maintenance access and quick exchange for offline turnaround. In the end, from disassembly of existing equipment up to the first heat of the new furnace, only 38 days were necessary. First heat was made on January 24th 2013, on the 6th production day 32 heats where produced at nominal design capacity and 28 days after start up 100,000 t liquid steel have already been produced.

Jul 30, 2018

By Mario González Ramírez

The safe transport of sour gas requires steels with enhanced hydrogen induced cracking (HIC) resistance. Centerline segregation bands of high hardness microconstituents and non-metallic inclusions are the heterogeneities usually linked to HIC failures in pipeline steels. Full-scale production heats of a new low Mn, Nb microalloyed steel were produced by different steel mills aiming at the application in sour gas environments. The new alloy design provides both effective strengthening and control of sulphide inclusions. Coil microstructure consisted of fine grained ferrite with a small volume fraction of uniformly dispersed eutectoid aggregates. Most importantly the microstructure was uniform in both the longitudinal and transverse directions and exhibited exceptional consistency. Samples from this steel were submitted to HIC testing according to NACE standards TM0284-2003 without any sign of cracking. The results, so far, confirm that this new alloy design provides the unique opportunity to economically produce a high strength pipe steel grade with improved sour service resistance for the linepipe industry.

Aug 8, 2018