Search Documents

By L. E. Gutiérrez

A new filtration model based on porous media transport theory is presented. It predicts capacity and final moisture content in the filtered cake as a function of design and operational variables at the plant. FilterSim® is the computer code where this new model is programmed. Application of FilterSim® to ten-month operation of an industrial copper concentrate filtration plant is shown on a daily basis and using a single set of internal parameters for the whole period. Average error is less than 5%, both in capacity and moisture estimation. FilterSim® abilities to optimize industrial filtration plants as well as to estimate future budgets are illustrated with several real examples.

Jan 1, 2007

By B. Skrotzki, E. Augenstein, C. Rockenhäuser

"The aluminium alloy 2618A is an Al-Cu-Mg alloy with additions of Fe and Ni, which is designed for long-term operation at elevated temperature in transportation and aerospace industries. The alloy degrades due to coarsening and dissolution of GPB zones and coarsening of S-Phase precipitates (Al2CuMg). This work investigates the overageing process at the application relevant temperatures of 190 °C for durations ranging up to 25,000 h. The nm-sized precipitates were selectively imaged along the <001>a direction of the Al matrix using dark-field transmission electron microscopy. The resulting images were then evaluated and allow the statistically relevant determination of radii distributions and the average radius of the precipitates dependent on temperature and heat treatment duration. Ostwald ripening of the S-phase does not describe the ageing process adequately. Instead, the evolution of GPB zones during the initial ageing regime needs to be considered in addition to the coarsening process of the S-phase. DSC measurements were performed to determine the presence of GPB zones in different ageing states. This will allow a quantitative description of the ageing process and a comparison to samples aged under external load.INTRODUCTION Alloy 2618A is an Al-Cu-Mg alloy, which is part of the 2XXX series of aluminium alloys. It is used in aerospace and transportation industry due to its desirable material properties for long term operation at elevated temperatures (Polmear, 2006). Fe and Ni are added to form intermetallic compounds, which retain microstructural stability at elevated temperatures (Bergsma, Li, & Kassner, 1996; Elgallad, Shen, Zhang, & Chen, 2014; Oguocha, Yannacopoulos, & Jin, 1996; Wang & Yi, 2006). The size and distribution of the nm-sized S-phase formed from the supersaturated solid solution (SSSS) during heat treatments mainly controls the strength (Khan, Starink, & Yan, 2008; Liu, Zhang, Ding, Sun, & Chen, 2003; Parel, Wang, & Starink, 2010; Shih, Ho, & Huang, 1996; Wang, Starink, & Gao, 2006). The S-phase has the composition Al2CuMg and is orthorhombic under equilibrium conditions (Heying, Hoffmann, & Pottgen, 2005; Perlitz & Westgren, 1943). Early experiments proposed the following decomposition of the S-phase sequence during heat treatments (Hardy & Heal, 1954; Silcock, 1961):"

Jan 1, 2018

By V. Bruned, K. Mohamed, A. Michaut

Orano Mining Somaïr uranium treatment plant (Niger) uses a pugging-curing process to leach uranium. Sulfuric acid, nitrates and water are added to the finely grinded ore in a rotary drum to leach uranium bearing minerals and solubilize uranyl sulfate ions. Reagents, sulfuric acid and nitrates, are the main OpEx of this process step. The economical optimization of their addition requires a thorough knowledge of the ore behavior in solution with these reagents. Orano Mining technical direction and Somaïr laboratories developed a model to predict the curing process uranium recovery surface with a limited number of parameters. Experimental laboratory work to fit the model needs to be done for each type of ore which can require a lot of metallurgical tests and would be time consuming. In order to optimize the required number of tests, an innovative experience plan was designed in parallel to the development of this model reducing the required number of tests to only eight. Once the parameters of the models are correctly fit, the comparison between the estimated values and the actual values for the uranium recovery is excellent (less than 0.5% error in average). Associated with an updated cost model of the curing process, this new recovery model helps the plant operator find the best set of reagents to maximize curing process profitability in the Somaïr plant day after day.

Jan 1, 2020

By W. Mirihange

Considerable mechanical property decline is always observed at the Heat Affected Zone (HAZ) of AA 5083, This occurred as a result of the thermal effect on the hardened material, It is highly beneficial to have a prospective metallurgical procedure to overcome this decline of properties. Therefore, experiments were set to evaluate the effectiveness of a quick post weld heat treatment process with the AA 5083, Optimum results were obtained at 473K and with approximately 600 seconds time, The interplay between the time, temperature and mechanical properties are possible to explain by the Lifshitz-Slyozov-Wagner (LSW) theory and by considering the composition of the material.

Jan 1, 2005

By John A. Allan

The subject chosen for this paper is not a new one, but the subject matter is so extensive that something new can always be said .about it. We are just beginning to realize how little is actually known about the character of Alberta coal, except for a few general facts. The object of this paper is not to explain that our previous information, in whole or in part, on the coal resources of Alberta, has been incorrect, but rather to present some new facts obtained as a result of recent study in the field and in the laboratory. As field investigation continues the problem of determining the character of a coal seam for any great distance laterally becomes more and more complex. Our present knowledge of Alberta coal deposits should not be discussed before due reference is made to those great pioneers who blazed the trails for later geologists, by recording their observations on the general geology of Alberta. Geologists, to-day, particularly those of us who are striving, year after year, to unravel the mysteries of stratigraphy, palaeontology, and structure, in so far as these are related to the coal resources of Alberta, fully realize our indebtedness to those three trail-makers, Dawson, McConnell, and Tyrrell. Had these geologists not recorded their observations correctly, nor interpreted the broad geological facts contained in Nature&apos;s book, with still uncut pages, how much slower would have been the progress of our coal knowledge in the succeeding years. It is true that many of the interpretations given to observations by these pioneers have had to be changed as a result of closer studies, but we must also expect that the geological interpretation from present day observations will be changed by future workers, as Nature&apos;s book is read and re-read.

Jan 1, 1925

By J. Malone, D. Loth, J. Palmer

WMC Resources&apos; Kalgoorlie Nickel Smelter was commissioned in 1972 at a design capacity of 30,000 tpa of contained Nickel in matte. A series of upgrades and progressive improvements have resulted in a design capacity increase to 110,000 tpa of contained Nickel in matte. The smelter sources nickel-in-concentrate from three Mine / Concentrators and supplies nickel-in-matte to WMC&apos;s Nickel Refinery and export customers. The Flash Furnace was last rebuilt in 1999, and is over halfway through the 10-year campaign target. The many modifications over the previous campaigns, including the Integrated Flash Furnace, are reviewed. Recent operation of the smelter and the development of the process during the current campaign are detailed herein. An overview of key interfaces with the Nickel Business Unit Concentrators and Refinery operations is provided.

Jan 1, 2005

By S. Torizuka, I. Mizushima. Kawasakitohri, A. Ohmori, K. Nagai

Strain (work)-hardening in tensile tests were examined for low carbon steels with various ferrite grain sizes ranged from 0.4µm to 16µm. The steels had microstructures composed of ferrite grains and dispersed cementite particles. They were fabricated through warm caliber rolling with an accumulative area reduction of 93%. Strain-hardening rate at a given strain increased with an increase in volume fraction of cementite particles. The balance of yield strength and uniform elongation for ultrafine-grained structures could be improved by the dispersion of cementite particles. Effects of the cementite dispersion and the ferrite grain size on the strain-hardening rate can be roughly explained by the work-hardening model with GN-dislocation density. Strain-hardening design using dispersed cementites was proved to be effective in controlling ductility of the ultrafine-grained steels.

Jan 1, 2004

By S. C. Livanou, S. P. Tampouris, E. N. Zevgolis

In ferronickel (Fe-Ni) production from oxidized nickeliferous ores, mechanical losses of ferronickel in the slag are reduced by magnetic separation. Slag from the electric furnaces (E/Fs) contains 0.16% Ni. Its magnetic separation gave a pre-concentrate with 0.76% Ni, weighing approximately 6.5% of the feed. Nickel recovery was 29.7%. This pre-concentrate was then treated in a second (concentration) plant. Concentration treatment involves screening, crushing and magnetic separation. A pre-concentrate with 0.76% Ni gave a magnetic concentrate with 2.58% Ni and a non¬magnetic part with 0.35% Ni. Smelting of the non-magnetic part without the addition of a reduction agent in a laboratory electric arc furnace, gave a ferronickel alloy with approximately 20% Ni and a slag with 0.16% Ni.

Jan 1, 2005

By L. Freitag

"The Dollard oil field in southwestern Saskatchewan is a stratigraphic trap of irregular shaped perimeter. The reservoir is a low-angle monoclinal structure with a dip of approximately 100 feet in 5 miles from west to east across the long axis of the reservoir. Production of. 23° API gravity crude is obtained from a Jurassic sand referred to as the J-2-A, at an approximate depth of 4,500 feet. Reservoir studies and fluid analyses revealed that the crude is highly undersaturated, having a solution GOR of approximately 130 cubic feet of gas per barrel, that the reservoir has no definable water table, and that it appears to be of a closed-boundary type. Oil production was marked by a rapid pressure decline and it was soon evident that the greatest ultimate recovery would be best obtained if the natural driving energy of the reservoir were augmented by some artificial energy source. In support of a pressure maintenance programme, studies were conducted on flood-pot recoveries of large-diameter cores, and a potentiometric model study of the field was made. These studies indicated that a successful water flood would be obtained. The Dollard field was unitized in 1955 and pressure maintenance started in March 1956."

Jan 1, 1959

By J. Sadaki, G. Dodbiba, S. Murakami, T. Fujita, S. Matsuo, H. Ono, K. Okaya

Printed circuit boards (PCBs) from discarded personal computer (PC) and household appliances were crushed by mechanical crushing or water explosion to remove mounted parts. More parts were stripped from PCB for PC composed of epoxy resin than from PCB for household appliance composed of phenol resin. In an attempt to raise the copper grade of PCB by removing other components, a carbonization treatment was investigated. The crushed PCB without surface-mounted parts was carbonized under a nitrogen atmosphere at 1073K. After screening, the char was classified by size into oversized pieces, undersized pieces and powder. The copper foil and glass fiber pieces were liberated and collected in undersized fraction. The copper foil was liberated easily from glass fiber by stamping treatment. On the other hand, tantalum capacitors were collected from mounted parts. The tantalum-sintered bodies were separated from molded resins by heat treatment at 723 to 773K in air atmosphere and screening of 0.5mm. Silica was removed and 70% of tantalum grade was obtained after more than 823K heating and separation.

Jan 1, 2011

By Jose Alberto Gonzalez, Said Sharif Mahboob, Jeffrey L. Shepherd

"During the industrial electrowinning of zinc, uneven growth can cause short-circuits and make the deposits more sensitive to the presence of impurities that can significantly impact current efficiency. To produce levelled zinc deposits, additives such as glue, licorice and sodium silicate are often added to the electrolyte. Even in the presence of additives, uneven zinc growth still takes place because of the combination of hydrodynamic and electrolysis conditions in the cell house. Recent advancements in imaging spectroscopy and scaling analysis have opened an avenue to further study the effects of additives on zinc growth morphology. In this study, Atomic Force Microscopy (AFM) and scaling analysis have been used to monitor zinc growth characteristics including roughness, periodicity, aspect ratios and growth mechanisms as a function of electrolyte composition as well as deposition time. Zinc was electrodeposited from an industrial electrolyte containing a host of additives onto an aluminum cathode with a platinum wire serving as the anode. AFM images of the samples were collected to obtain 3D topographical information on which scaling analysis was performed to extract details on root-mean-squared (rms) roughness, periodicity (grain size), aspect ratio of surface features and growth mechanism. This analysis provided information on the mechanism by which the previously mentioned variables can impact short term growth and also provided a prediction of expected growth at long deposition times.INTRODUCTIONElectrowinning is one of the final stages in the industrial production of zinc metal. It is during this process where dissolved zinc ions undergo electro-reduction from an acidic electrolyte onto an aluminum cathode and are later recovered by stripping the zinc metal from the substrate. However, due to the nature of zinc growth as well as the various operating conditions, zinc deposition may occur unevenly, sometimes causing short-circuits that can cause electrode damage and reduced zinc production."

Jan 1, 2016

By Tamas Kekesi, Gergo Rimaszeki, Tibor Kulcsar

The efficient purification of soldering waste material can be achieved in a single operational step by the electrolytic refining in pure hydrochloric acid - tin-chloride media. The complex formation of the ionic species may offer a beneficial level of natural inhibition. Using the PCR (periodic current reversal) technology, is efficient in affecting the morphology of the cathodic deposit. In order to optimize the process, the investigation of the solution stability and the electrode reactions is essential. The natural tendency of the Sn(II) oxidation and precipitation can be overcome by properly controlling the concentration of the main components and the ratio of Sn(IV)/Sn(II) in the electrolyte solution. Polarization curves were obtained for different concentrations tin and hydrochloric acid. Conclusions referring to the electrode reaction were derived from the overvoltage - current plots. The morphology of the deposit can be correlated with the exchange current density, also determined from the polarization curves. The cathodic current efficiency and the morphology of deposited metal are affected by the distribution of tin species and the principal electrolysis parameters.

Jan 1, 2011

By A. Kraly, M. Complojer, P. Paschen, K. Gamweger, H. Antrekowitsch

Increasing quality of aluminium alloys and continuous optimization of the production process leads to an improvement of the gas purging systems. The application of porous plugs for the treatment of liquid aluminum is nowadays not widely used in the aluminium industry especially in Europe. The Department of Nonferrous Metallurgy and the Christian Doppler Laboratory of Secondary Metallurgy of Nonferrous Metals intensified the research and development of refining and alloying processes by gas treatment during the last years. CFD-modeling supports these experiments, which should lead to lower hydrogen content, lower suspended particles and a better distribution of alloying elements in the melt. Different parameters such as temperature, bubble size, gas amount and which kind of gas is used influence the quality of the products.

Jan 1, 2006

By Muhammad Tawalbeh

The calculated temperature history of a single particle of MgCl2 hydrates when it came in contact with fused salt electrolyte at 650 °C was determined using the measured heat transfer coefficient for the molten salt bath at 650 °C. The calculations revealed that the entire interior of the particle reached the temperature required for the formation of MgOHCI from hydrated MgCl2 in less than 2 seconds. This was much less than the time required for dissolution of the prills as observed in experiments. It is very likely that the formation of MgOHCI during prill dehydration and dissolution is a result of hydrolysis in the interior of the prills.

Jan 1, 2004

By J. Shibata, N. Murayama, H. Yamamoto

As one of effective usages of wastes discharged in the non-ferrous metal industry, the syntheses of AlPO4-5 and hydrotalcite were carried out using aluminium dross as a raw material. AlPO4-5 is an aluminium phosphate condensate with properties of zeolitic materials and large pore size. Hydrotalcite is an inorganic anion exchanger and has a layered structure of complex hydroxide. They were synthesized in an autoclave at high temperature and pressure. Various physical properties such as crystal structure, surface texture, and specific surface area were measured. AlPO4-5 can be synthesized from aluminium dross under hydrothermal conditions at 180°C-200°C, and 3h. At the same time, AlPO4-34 and non-porous AlPO4 were also formed as by-products. The crystals of AlPO4-5 have a hexagonal structure. Lt is desirable to heat the reaction product at around 550 °C to remove tri-ethyl amine. The specific surface areas of the reaction product before and after heat treatment at 550°C were 17.9m2/g and 358m2/g, respectively. Hydrotalcite can be obtained by a co-precipitation method from the aluminium dross and waste MgCl2 solution discharged in the aluminium regeneration process. Small amounts of SiO2, Al2O3, and Fe2O3 remain in the reaction product as an impurity component. The interlayer distance of the obtained reaction product is about 0.3 nm. Hydrotalcite changes to Mg-Al oxide during calcination at 500 °C for 3h, and then hydrotalcite is formed again by a rehydration operation. The physical properties of the reaction products obtained from the wastes were very similar to those from fresh reagents.

Jan 1, 2004

By Michel Gauthier, Pierre Marcoux, Gaétan Morin

"The recent opening of Muscocho&apos;s gold mine at Montauban, as weil as the discovery of several new copper-gold showings of a similar nature near the confluence of the Saguenay and St , Lawrence has revealed the existence of a new metallogenic gold province which is located within supercrustal units of Helikian age within the Grenville Province. Three metalliferous belts have been identified, each one of which is related to a series of SW-NE trending faults. The first is located in southeastern Ontario and southwestern Quebec. The second extends from the Balmat-Pierrepont mining district of New York State up to the Lac St. Jean region of Quebec, and includes the Montauban camp. The third follows the St. Lawrence river in Charlevoix County and along the north shore of the Gulf of St. Lawrence.The gold mineralization which is present in the central portion of the Grenville Province is of two types: either stratiform or vein. Deposits of the first type, of which the Muscocho is the type locality, are economically the more interesting of the two. Not only is this mineralization stratiform, but also shows a distinct affinity to AI-rich, Mg-rich or calc-silicate-rich bands. As is the case with the Bousquet and Hemlo regions of the Superior Province, they are associated with layers which are rich in sillimanite and occasionally staurolite. A second parallel between the Bousquet and Montauban deposits might be the presence of manganesian gamets, which have been recognized at the two localities. Some of the mineralization in the central Grenville Province is located within thin bands of iron formation which are rich in arsenic.The stratiform gold deposits of the central Grenville Province are of exhalative origin and are located within a volcano-sedimentary terrane. It is probable that a part of the gold present in these Helikian deposits have been derived by remobilization of Archean mineralization. The vein showings form as a consequence of the remobilization of the Helikian strata during the Grenville metamorphism,"

Jan 1, 1985

By S. H. Schulz

100 YEARS AGO, on the first of August, 1877, the mining engineer Friedrich Koepe was granted the patent rights for a hoist driving ropes on the principle of friction. It was named after him: the Koepe hoist. On the occasion of this centenary, the main features of the Kcepe principle are described.

Jan 1, 1977

By K. Sun, S. A. Argyropoulos

The assimilation and the exothermic behavior of Zn-Zr metallic powder compacts into molten aluminum was studied by measuring simultaneously the temperatures inside at the centerline of the compact, at its surface, and inside the molten aluminum bath, as well as the net downward force acting on the compact. In addition, the exothermic behavior of these compacts was also investigated in an argon protected atmosphere. The temperature rise inside the compact increases significantly with the mass ratio of zirconium in the compact and to a lesser degree with the aluminum bath temperature. Experimental results on the recovery of these compacts in molten aluminum will also be presented.

Jan 1, 2008

By N. T. Avard

THE Joggins coal field, Cumberland county, Nova Scotia, is on the easterly side of Chignecto bay, at the head of the bay of Fundy. In area, so far as proven, the field extends easterly from the town of Joggins about fifteen miles to Chignecto. The distance across the outcrops of the several seams exposed is approximately one mile. HISTORY Early records of coal mining in this locality are somewhat obscure, but it is known that prior to 1750 the French settlers were mining coal for their own use from the seams which outcrop in the floor of the bay adjacent to the shore, where, at low tide, the reefs are bared for a mile or more. Coal was also mined from the seams outcropping in the cliffs. It is known, too, that at Joggins coal has been mined commercially for over one hundred years. At first, all shipments were made by water, but in 1882 a railway connecting with the Intercolonial railway at Maccan was built to serve this field. GEOLOGY Due to the abundance of fossils in the strata forming the Joggins cliffs, this area was for many years a mecca for geological students from all over this continent. A &apos;sunken fcrest&apos; in the shoreline was of particular interest but, due to constant erosion by the sea, this has apparently been all washed away. On the Joggins shore, the cliffs stand sixty to one hundred feet high, and six workable coal seams, with numerous smaller ones, are there exposed. Others outcrop in the reefs extending from the shore toward the bed of the bay. In working underground, fossilized trees are often found immediately overlying a coal seam, and standing at right angles to the pitch of the seam. This is said to be an unusual condition. In most cases, the bark of the tree is a fine-quality coal, with high carbon content, whereas the pulp has turned to &apos;stone&apos;. There is a definite tendency for the coal to run out, or turn to shale. One seam, workable two miles from the shore, has almost completely disappeared in the outcrop at the shoreline. ? It was thought that a large area could be mined under the bay from an opening near the shore, but the first submarine level had to be abandoned at a distance of 4,000 feet, where the coal became very dirty and shaly, and the mine able area to the westward became more restricted as the mine was developed to the deep. This tendency is common to all seams.

Jan 1, 1944

By J. J. McDougall

Until quite recently, the coal in the Cape Breton field was won from comparatively thick seams with light cover, and from submarine areas, and the system of mining naturally followed was pillar-and-stall. This sytem permitted of cheap extraction, and enabled production from localities where other methods could not be employed to good advantage. Thus the pillar-and-stall system, applied to conditions as stated, justified its adoption. Our working seams today, however, are practically all under heavy cover, or are moving in that direction, and with this gradual increase in cover came the increased cost of roadway maintenance. At Princess colliery, the system of pillar-and-stall was followed until roof and bottom conditions became such that further operations were unprofitable, and the longwall method was then adopted as an economic necessity. This fact should be borne in mind when operating costs of both systems are being compared. The longwall method is not held as a cure for all difficulties of heavy cover, but through it these difficulties can be overcome with less expense than by pillar-and-stall. The longwall system of mining, strictly speaking, is one by which a seam of coal is totally extracted in one operation. There are, however, many modifications of longwall, and in some cases it is difficult to determine whether certain practices should be classed as longwall or pillar-and-stall, or a combination of both.

Jan 1, 1928