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By Edilson Alves Maranhão, Willi Anton Buehler, Andrea Pezza

O processo de vácuo é a solução típica aplicada quando é hora de atualizar o nível de qualidade do aço de uma aciaria existente. A instalação do novo RH de 150t na planta integrada no México e do novo Tanque de Desgaseificação à Vácuo (VD) de 135t no Canadá para a produção de tubos de alta qualidade na América do Norte, é um exemplo típico disso. A nova instalação inclui o mais recente conceito de design para este tipo de equipamento: operações totalmente automatizadas e menor impacto ambiental são os principais aspectos do projeto. A solução de bomba mecânica a seco continua sendo a melhor abordagem de investimento e custo operacional para a tecnologia de vácuo. Os principais aspectos do design da planta são descritos neste documento. O desgaseificador a vácuo RH é responsável pela melhoria das performances metalúrgicas, especialmente em termos de nitrogênio, remoção de hidrogênio e nível de pureza do aço. O processo a jusante e os resultados estão estritamente ligados aos desempenhos do desgaseificador a vácuo. O monitoramento de processos através da linha completa é uma prática padrão para obter uma melhoria efetiva da qualidade do produto. Os desempenhos metalúrgicos do desgaseificador a vácuo RH são analisados e comentados neste trabalho.

Oct 1, 2019

By Edilson Alves Maranhão, Willi Anton Buehler, Andrea Pezza

O processo de vácuo é a solução típica aplicada quando é hora de atualizar o nível de qualidade do aço de uma aciaria existente. A instalação do novo Tanque de Desgaseificação à Vácuo (VD) de 135t no Canadá e do novo RH de 150t na planta integrada no México para a produção de tubos de alta qualidade na América do Norte é um exemplo típico disso. A nova instalação inclui o mais recente conceito de design para este tipo de equipamento: operações totalmente automatizadas e menor impacto ambiental são os principais aspectos do projeto. A solução de bomba mecânica a seco continua sendo a melhor abordagem de investimento e custo operacional para a tecnologia de vácuo. Os principais aspectos do design da planta são descritos neste documento. O desgaseificador a vácuo VD é responsável pela melhoria das performances metalúrgicas, especialmente em termos de nitrogênio, remoção de hidrogênio e nível de pureza do aço. O processo a jusante e os resultados estão estritamente ligados aos desempenhos do desgaseificador a vácuo. O monitoramento de processos através da linha completa é uma prática padrão para obter uma melhoria efetiva da qualidade do produto. Os desempenhos metalúrgicos do desgaseificador a vácuo VD são analisados e comentados neste trabalho.

Oct 1, 2019

By Martim Hideki Nakayama Kurauchi

One of the main issues regarding the use of charcoal in metallurgical processes is its mechanical strength, which is much lower than coke. There is no defined standard to determine charcoal compression strength, and the methods described in the literature consist in using a prepared specimen and applying compressing load in the same direction of the charcoal fibres. As charcoal is highly anisotropic, it is proposed a procedure that does not use a specimen and with load applied on a specific direction. Instead, it intends to simulate industrial conditions by randomly dumping charcoal inside a tube, without preferential directional arrangement. This is an attempt to determine charcoal mechanical strength and predict the behaviour of bulk charcoal under a static load, as in a blast furnace. Experiments with controlled loads have been carried out on randomly distributed bulk charcoal with controlled initial size and their effect on the size distribution has been analysed. After compression, charcoal is screened and each size is weighed, determining the particle size distribution of the experiment. This method can therefore be used to evaluate charcoal mechanical strength.

Aug 1, 2018

By Jean Viana Bahia, Antônio Adel dos Santos, Vicente Tadeu Lopes Buono

During cold rolling of Cr-Mo alloyed DP steel, considerable oscillation of thickness may occur. The literature points out that such occurrence is due to non-uniform cooling of the coil after the hot rolling process. Since the austenite transformation in this steel continues after coiling, the microstructure and, consequently, mechanical properties are very susceptible to natural variations in cooling rates associated with distinct positions of the coil. The influence of coil cooling conditions on thickness oscillation during cold rolling was evaluated in this work by using both industrial experiments and dilatometer tests. It was verified that an industrial coil presented large variation of mechanical properties associated with its heterogeneous microstructure. Consequently, thickness oscillation occurred during cold rolling. Dilatometer tests simulating hot run-out table and coil cooling showed that the austenite transformation is very slow under small cooling rates that occur after coiling. Thus, the slow transformation rate makes the coil very susceptible to environmental conditions around it during its natural cooling and is responsible for variation in mechanical properties of the coil. To ensure the formation of a more homogeneous microstructure in the whole coil, it is necessary either to make use of technologies that improves the cooling uniformity or to adjust the steel alloy design. The latter alternative has been done with relative success by using conceptions with lower amounts of Cr and Mo.

Oct 1, 2019

By Marjorie Benegra

This study aims to compare the wear resistance assessed in rubber wheel abrasion test of nickel aluminide coatings deposited by for Plasma Transferred Arc (PTA) and High Velocity Oxigen Fuel (HVOF) manufacturing, using the same raw material. A nickel aluminide powder was atomized and deposited on 316L steel plate substrate. After deposition, some specimens were submitted to a heat treating (1200 °C for 24 h followed by 760°C for 24 h). The coatings deposited using PTA developed different microstructures due to the incorporation of substrate elements, its performance was better than the HVOF coatings, although their Vickers hardness was similar. After heat treating, a significant variation in hardness and wear resistance was observed. For PTA specimens, there were decrease in hardness of 35%, while for HVOF ones this drop was approximately 20%. Nonetheless, the effect of thermal exposure in wear resistance was quite different: an increase of 21% was observed for HVOF coatings, while a reduction of 20% occurred in PTA ones. Microstructures modifications in PTA coatings were significant for their wear resistance. On the other hand, the reduction of porosity and sintering were responsible for a better performance of heat-treated HVOF coatings.

Jul 31, 2018

By Alessandro Marques

Based on a short overview regarding steel defects in the final product, several refractory approaches to maintain or increase steel cleanliness are reviewed in this publication. By applying a ladle to mold approach, one potential to maintain cleanliness is to reduce the probability of air ingress by selection of a suitable slide gate system. Following this path, also the influence of a special configured impact pot is presented to maintain steel quality. Finally, higher productivity as well as cleanliness can be provided by selection of PROIL as a revolutionary product at the casting machine.

Oct 30, 2017

By Roberto Balarini Junior

Tribological behavior of Si3N4 balls sliding against Al2O3 discs in water was investigated by studying the influence of parameters such as initial surface roughness and circular axial run-out of the discs. The objective was to relate these parameters with the occurrence of the phenomenon known as ultra-low friction coefficient (ULFC), which is characterized by µ < 0.01, including the correlation with running-in duration. As a general trend, greater initial surface roughness and circular axial run-out resulted in greater running-in duration. In addition, it was verified that a mixed lubrication regime (hydrodynamic and boundary) is required to guarantee the occurrence of ULFC by comparing the calculated minimum film thickness with the composite roughness of the worn surfaces. Also, ICQ-OES analysis of the water after the tests indicated that a silicon concentration greater than 1.3 mg/l should be fundamental for the occurrence of µ < 0.01.

Jul 31, 2018

By Steven George Jansto

The hot ductility behavior of different microalloyed steel chemical compositions was examined simulating the thermal and strain conditions through the straightening or unbending section of the continuous casting machine. All samples were obtained from industrial slab casters ranging from 200 to 300 mm in slab thickness from steel mills throughout the world including China, Brazil, North America and Europe. The slabs were crack-free and hot rolled into prime quality products. No laboratory heats were tested. Although these microalloyed steels exhibit inherently lower hot ductility behavior, as measured by percent reduction in area at elevated temperature, these steels still exhibit sufficient ductility to satisfactorily meet the unbending stress and strain gradients existing in the straightening section of most casters. The majority of the published hot ductility data, as measured by % reduction in area (%RA), were based on laboratory heats and hence, are inaccurate in accessing the propensity for slab cracking on an industrial caster. This situation then results in invalid conclusions for different chemistries. This research has determined the minimum required %RA for crack-free casting is significantly lower than results based upon previously published laboratory generated data. For example, the literature quotes 40% RA minimum for Nb-bearing steels when in fact as low as 10% minimum RA is more than sufficient to assure crack-free casting based upon the extensive testing and analysis performed in this study. Instead of %RA, the measurement of strain energy has been introduced to evaluate hot ductility behavior. It is concluded that strain energy is a better measure of hot ductility behaviour than %RA. There is considerable value in the evaluation of the hot stress and strain curves, process metallurgy parameters and their relationship to slab quality instead of just basing hot ductility decisions on simple %RA measurements.

Aug 16, 2017

By Wolfgang Oberaigner

Primetals Technologies has always been a driver of innovation in steelmaking, especially by providing sophisticated process expert models for continuous casting machines. This capability is demonstrated by recent advancements in automation solutions that include: DynaPhase, Dynacs 3D, and DynaGap. This state-of-the-art suite of dynamic secondary cooling and soft-reduction packages take into account thermodynamic effects such as shrinkage and phase transitions, and thereby significantly contribute to direct quality improvements during the solidification phase in the continuous casting process. Speed Expert calculates an optimum casting speed for every casting situation, and additionally recommends a strand speed so that the point of final solidification is positioned at the end of a segment for optimum soft reduction. In the case of steel grade changes, the Intermix Expert precisely calculates the chemical properties of the mixed steel, thereby minimizing losses due to deviations from required specifications. The Nozzle Expert is a new model that detects clogged nozzles and broken hoses in secondary cooling systems. The first installations were highly successful and customers are pleased with impressive reductions in maintenance costs and improved steel quality. This paper describes these innovative process automation solutions and gives an overview about the successful results achieved within the first installations.

Aug 16, 2017

By Davidson Marcos de Oliveira, Antonio Adel dos Santos, Vicente Tadeu Buono

The benefits of using the controlled rolling process followed by accelerated cooling (TMCP), currently used in the main rolling mills in the world are already well known and metallurgically based. The need to obtain mechanical properties with a high degree of homogeneity means that in some situations the ends of the rolled material are discarded, negatively affecting the metallic yield of the process. Therefore, this work focused on the determination of the mechanical properties variation at the ends of thick plates processed by TMCP of steels for application in oil and gas pipelines, in order to map the extent of these differences and to correlate them with the microstructure obtained, the profiles of temperature and cooling rates in these regions. To perform the work, two slabs of the studied material were rolled, and the temperature profile was recorded along the plate in the controlled rolling and accelerated cooling processes. The ends of the material were sampled in sections at every 100 mm and subjected to tensile test, hardness and the Charpy V-notch impact test, as well as dilatometry and microstructure evaluations. For the used process conditions, the results indicated the formation of a banded microstructure, basically consisting of polygonal ferrite and bainite, occasionally containing small fractions of perlite. The mechanical properties in the top and the base were higher than the values found in the plate middle, justified by the microstructure found. The work allowed understanding the relationship between the mechanical properties, microstructures and process conditions at the ends, helping the team to improve the process in order to result in a high degree of homogeneity of the product and, thus, lead to optimization of the metallic yield.

Oct 1, 2019

By Dagoberto Brandão Santos, Kairo de Barros Guimarães, Túlio Magno Füzessy de Melo

The effect of the cooling conditions on the microstructure and hardness of a Dual Phase hot-rolled steel 800 MPa strength was investigated. Simulations of the cooling conditions using a dilatometer were carried out from samples of a hot rolled coil with variations of the intermediary temperature from 620 to 740°C, isothermal holding time between 1 and 10 s and coiling temperature between 50 and 400°C. In addition, two CCT (Continuous Cooling Transformation) diagrams were developed to evaluate the effect of the isothermal holding time on the phase transformations of the remaining austenite. It was observed that the intermediary temperature has a strong influence on the kinetics of the phase transformation, as well as the isothermal holding time influences the amount of ferrite formed and, consequently, the final microstructure and hardness of the material. The coiling temperature did not cause significant changes in the amount and morphology of the ferrite, but a gradual replacement of martensite with bainite was observed, which, in addition to the self-tempering effect, contributed to the hardness reduction.

Oct 1, 2019

By Mario González Ramírez

The safe transport of sour gas requires steels with enhanced hydrogen induced cracking (HIC) resistance. Centerline segregation bands of high hardness microconstituents and non-metallic inclusions are the heterogeneities usually linked to HIC failures in pipeline steels. Full-scale production heats of a new low Mn, Nb microalloyed steel were produced by different steel mills aiming at the application in sour gas environments. The new alloy design provides both effective strengthening and control of sulphide inclusions. Coil microstructure consisted of fine grained ferrite with a small volume fraction of uniformly dispersed eutectoid aggregates. Most importantly the microstructure was uniform in both the longitudinal and transverse directions and exhibited exceptional consistency. Samples from this steel were submitted to HIC testing according to NACE standards TM0284-2003 without any sign of cracking. The results, so far, confirm that this new alloy design provides the unique opportunity to economically produce a high strength pipe steel grade with improved sour service resistance for the linepipe industry.

Aug 8, 2018

By João Luiz do Vale

In standard wear tests, such as pin on disk (ASTM-G99) or block on ring (ASTM-G77), the apparatus simulates conditions that are often different from a machine element real application. Therefore, for an accurate investigation of a tribological application, it is essential to test the real condition in which there are similarities as: geometry, contact details, force application mode, materials, among others. It emphasizes that for studies involving polymeric materials it becomes extremely relevant. Thus, the Laboratory of Surfaces and Contact (LASC) at UTFPR developed an apparatus for sliding bearing on shaft test. In that equipment, loads are applied by a dead-weight system and the frictional force is measured on a load cell. The apparatus operating ranges for load added to the dead weight system and rotation shaft are from 0.2 to 5.0 kgf and from 260 to 3500 rpm, respectively. This paper presents a detailed evaluation of such apparatus, which includes free-body diagrams analysis and a deduction to obtain an equation for the kinetic friction coefficient. Also, the standard measurement uncertainties of a caliper, an electronic scale, and a cell load were determined. It was verified that the kinetic friction coefficient equation is dependent on the apparatus geometry, the applied load, and the frictional force value. Additionally, through the statistical significance analysis it was concluded that some terms in the equation were not significant. Finally, through the application of the error propagation theory in the kinetic friction coefficient equation, the standard measurement uncertainty of the apparatus which showed a value nearby 0.002 along the operating range of the apparatus was obtained.

Jul 31, 2018

By J. Bas A. F. Smeulders

Traditional laboratory lubrication tests, including those for cold rolling lubricants often involve measurement of neat oils. To achieve increased levels of test severity, such tests are often carried out at high temperatures and prolonged durations. However, we found that the levels of lubricant degradation and wear in these tests can be much higher than in the field. Moreover, steel rolling is not done with neat oils, but with emulsions, where the presence of water influences film formation, surface chemistry and oil composition in the roll bite. To better approach the situation in the field, and thus to be able to develop rolling oils with improved lubrication performance, several lubrication tests were developed for emulsions: direct measurement of film formation and measurement of Stribeck curves, in which the emulsions can be assessed in terms of their boundary lubrication and elastohydrodynamic behaviour. The key innovation is that also another test method was developed, which focuses on boundary lubrication and wear, and the role of extreme pressure and anti-wear additives. Realistic levels of test severity are achieved in the tribometer by mimicking frictional power intensities and flash temperatures for typical cold rolling or tinplate mills. Test conditions can be adapted according to the mill stand or pass number and other cold rolling process parameters. The emulsions are kept at normal operational temperature. Clear differences could be observed between emulsions of various concentration and composition. The viability of the method is illustrated by a number of field cases, in which a good correlation is demonstrated between the laboratory tests and the performance in a pilot or production mill.

Jul 30, 2018

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Markus Reifferscheid

Industry 4.0, Digitalization, Internet of Things (IoT) and Cloud Computing are predominant topics in the world economy at the moment. At the ABM week 2017 Dr. Markus Reifferscheid, Head of Research &amp; Development of SMS-group, will talk about the proceeding digitalization in the steel industry with selected examples of SMS-group. He will present advanced concepts and solutions which are currently being developed.

Oct 30, 2017

By Antônio Adel dos Santos

O controle da temperatura é fundamental no processo de laminação a quente dos aços, motivando a dedicação de esforços em estudos sobre a transferência de calor e na aplicação de melhorias operacionais. Neste sentido, o objetivo deste trabalho é apresentar o desenvolvimento, os resultados e as aplicações de modelos de cálculo da evolução de temperatura do aço durante a laminação a quente, desde o reaquecimento da placa até o produto laminado e resfriado na forma de chapas. São mostradas formulações matemáticas, métodos numéricos de solução usados, validação dos cálculos e a contribuição dos modelos para o entendimento e melhoria de processo. Todo esse desenvolvimento foi baseado em trabalhos realizados na Usiminas, nos últimos anos, cuja fundamentação teórica, buscada na literatura, foi adaptada e validada de acordo com as especificidades de cada linha. Além disso, os modelos foram implantados como simuladores offline, tornando prática sua aplicação pelos analistas de processo. São mostrados exemplos de cálculo do aquecimento de placas, da evolução térmica das placas nos fornos até a entrada dos laminadores, e da evolução do esboço durante a laminação de chapas grossas.

Jul 30, 2018

By Adriano de Assunção Rodrigues, Gustavo Henrique Pinto de Oliveira, Wemerson Junio Gandra

O processo de obtenção de coque em uma coqueria convencional Non-Recovery consiste no aquecimento de uma mistura de carvões, provocando sua desvolatilização, gerando o coque que é principal combustível utilizado em altos-fornos. O aquecimento da mistura de carvões se dá de forma indireta. As paredes dos fornos recebem calor da câmara de combustão alimentada por uma mistura de gases de alto-forno, coqueria e aciaria ou, exclusivamente pelo gás de coqueria. O gás de coqueria COG (coke oven gas) é composto basicamente de hidrocarbonetos e recebe tratamento para retirada de impurezas, alcatrão, sulfato de amônia e óleos leves. Os elementos residuais no gás, mesmo após o processo de tratamento são extremamente prejudiciais às tubulações de distribuição, formando compostos corrosivos, podendo ocasionar o colapso de tubulações, gerando acidentes, gastos com reparos e perda de produção. Neste contexto, o presente trabalho tem por objetivo apresentar os fatores que levaram a necessidade de substituição das tubulações principais de distribuição de gás no subsolo da Coqueria 3 da Usiminas Ipatinga, conferindo segurança ao processo e estabilidade operacional.

Oct 1, 2019

By Carlos Vinícius Domingos de Carvalho

As perdas geradas nos processos de uma Aciaria contribuem de forma significativa para a perda metálica do processo. Eventualmente, mesmo com uma operação correta, do ponto de vista de características do produto, pode ocorrer comprometimento do ponto de vista econômico, e uma forma de redução direta dos custos e aumento de performance é a redução das perdas geradas no processo. Desta forma, tornou-se importante realizar um estudo para reduzir as perdas metálicas na Aciaria. Foi utilizado a metodologia Seis Sigma, sendo estratificadas as perdas por processo na Aciaria, onde as maiores perdas na rota dos processos de Lingotamentos Contínuos foram: perda no Distribuidor (24,7%), corte de sequência (17,5 %), retorno de corrida por baixa temperatura do aço na panela (16,3 %); perda por obstrução da válvula da panela (8,8 %). A perda metálica foi reduzida em 50,8%. Além da redução expressiva das perdas, houve uma grande contribuição em relação à compreensão dos modos de falhas para apropriação correta das perdas, tornando as informações mais seguras e facilitando o tratamento de possíveis falhas no processo.

Oct 30, 2017

By Thiago Pires Nagasima

O refino de grão da estrutura bruta de solidificação da liga Cu-30%Zn (latão 70/30) a partir de adições de P e Zr ao banho líquido foi investigado utilizando-se microscopia óptica, microscopia eletrônica e microanálises. Foram conduzidas medidas de tamanho médio de grão pelos métodos planimétrico e do intercepto linear e foram realizadas microanálises por espectroscopia de dispersão de energia (EDS) e de comprimento de onda (WDS). Nas amostras obtidas observa-se que, quando são adicionados P e Zr, sempre ocorre a diminuição do tamanho médio de grão em relação àquele das amostras onde apenas P é adicionado. O menor tamanho médio (? 200 ?m) ocorre para um teor de 0,16% de Zr. O refino de grão coincide com a formação de precipitados geralmente facetados, contendo Zr e P em uma proporção equivalente à da fase ZrP. Sugere-se que as adições causaram a formação de partículas sólidas de ZrP, sobre as quais ocorreu a nucleação heterogênea de grãos da fase Cu-?, resultando no refino de grão.

Oct 30, 2017