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By Nobuhiro Shinihara, Makio Naito, Keizo Uematsu, Tadashi Horta, Hiroya Abe, Masataro Okumiya

"A significant variation of strength was noted in silicon nitride ceramics made through the powder compaction processing with minor processing changes. The relevance of the fracture strength to the microstructure was examined in these ceramics. In the examination of microstructure, the ceramics were made into thinned specimens, and their internal structures were observed with an optical microscope in the transmission mode. This technique can distinguish a difference in microstructure associated with the minor processing changes. The strength of all ceramics examined in this experiment was qualitatively correlated with the -pore size distribution in the specimens. Clearly, the elimination of these detrimental defects will enhance the reliability of ceramics.IntroductionIn ceramics made through powder processing, a variation of properties is often encountered [l ,2]. This brings a major problem on producing reliable and cost-effective ceramics. The variation is often ascribed to the changes in the characteristics of defects. However, there is no clear evidence f\)r this explanation due to the lack of an adequate tool for identifying the defects determining the properties. Details of the origin of the variation have still been poorly understood.A new technique is very promising for clarifying the origin of the variation [3,4]. This has very high potential in detecting minor differences in structure for .engineering ceramics. With this technique, ceramics are made transparent with its thinning down to about 50 µ m and their internal structures are observed with various types of optical microscopes in the transmission mode. The characteristics of the defects determined through this approach were found to be directly related to the strength of the ceramics [4-6].The objective of this study is to clarify the ongm of fracture strength of silicon nitride ceramics. This material is representative of high performance ceramics, and the origin is of great practical interest. For this study, silicon nitride ceramics with minor changes in processing condition were prepared. Specific feature focused in this study is the difference of large pore structure determined with the new technique and its relevance to the strength of the silicon nitride ceramics."

Jan 1, 2000

By S. S. Vasan, K. A. Natarajan, J. M. Modak

The biological removal of calcium from a bauxite ore in the presence of the soil bacterium Paenibacillus polymyxa is demonstrated. A column bioreactor that can be either operated in a fluidized-bed (FB) mode for coarser particles or in a total-recycle-slurry (TRS) mode for finer particles was designed, fabricated and tested for this purpose. For the efficient removal of calcium from the ore to the required levels, leach solution should not be allowed to accumulate in the reactor. Therefore, the solution needs to be drained out periodically. Cascade leaching was found to be more effi¬cient. A direct correlation between pH changes in the leach solution and calcium solubility could be made. More than 85% of the calcium could be removed through cascade leaching.

Jan 1, 2000

By Mingchun Lu, Zhijia Liu, Xueqi Zhang, Jianliang Zhang

"In order to solve the problem of shortage of scrap, especially high quality scrap, a new substitute for scrap or DRI has been developed. The decarbonization mechanism of granular pig iron has been analyzed and the technical process and decarbonized granular pig iron have been evaluated in this paper. The research result shows that this new process is superior to direct reduction process in product quality, construction investment, operation flexibility, production efficiency etc. Decarbonized granular pig iron (DGPI) not only can be used as conventional scrap but also can be charged into EAF as high purity .burden equivalent to heavy scrap:IntroductionIn the past years, with the universal application of continuos casting technique in China, the amount of scrap generated inside steelworks has been reducing continually. On the other hand, the EAF steel proportion is increasing and this gives to the obvious change in structure of steel product. At present, the requirement on both scrap quantity and scrap quality is being paid more and more attention. Because China is a country which is devoid of scrap and poor in resource (nature gas and high grade iron ore) for developing direct reduction iron (DRI) so that sponge iron can not be produced cosmically in China and has to be mainly imported. Instead of part of scrap, some cold pig iron in cold state has been charged into EAF in China. However the high carbon content in pig iron has limited its proportion in EAF metal burden. Because the price of pig iron is lower than that of imported DRI in China, the technique of granular pig iron decarboniztion is hopeful to become effective way to produce substitute for scrap or DRI."

Jan 1, 2000

By G C. Reed, J M. Murray

During more than 100 years continuous mining of the lead-zinc orebody at Broken Hill, an immense amount of geological data has been collected about shear zones related to the orebody. The challenge to current mine geologists is to synthesise and interpret these data sets in a way that is applicable to production demands. Precise knowledge of the locations of major shear zones is important not only for the determination of ground conditions but also to develop an understanding of ore remobilisation along these structures. Traditionally, geological information has been collected from drill core and back and wall mapping underground, and interpreted on sections that are approximately 20 m apart. The recent introduction of MaptekÆs Vulcan software has enabled the shear zones to be modelled in three dimensions. The new three-dimensional shear models have been combined with seismic data from the Southern Cross area. The seismic data is collected from a microseismic monitoring system installed in the Pasminco Southern Operations in August 1996 (Rauert and Tully, 1998). The addition of seismic information to the shear zone models has led to a greater degree of certainty about the shear zone locations and has provided information about shear zones in areas yet to be drilled.

Jan 1, 2000

By Erik M. Westerberg

The Soilex Pile combines a slender shaft, for quick and easy installation, with an enlarged pile toe, for high capacity. The key component is the Expander Body, which is inflated by injecting cement grout when in position. The latest development in the Soilex Pile System results in a reduction of the total cost of Soilex Piles, in many cases values that are competitive with pre­cast concrete piles and displacement piles. Soilex Piles can now be installed on top of a bearing soil layer, instead of 3 to 4 m into that soil as previously required, further minimising the ground disturbance. Soilex Piles achieve high capacity in relatively loose soils, with ultimate loads typically between 1000 and 2000 kN in a sand with CPT qc = 5 to 10 MPa or SPT N= 10 to 20. It is possible to pre-load and proof-load all piles with dynamic testing up to 2000 kN or using built-in jacks, thereby verifying the capacity. The vibratory installation method, which is extremely quick and causes very little soil disturbance and noise, is exemplified by two case histories.

Jan 1, 2000

By M. Grodner

Underground excavations exhibit different hangingwall conditions in response to varying geotechnical and mining situations. These differences need to be quantified so as to accurately determine the effectiveness of the mining and/or support strategies. A useful tool for the quantification of these differences is hangingwall profiling. Two methods of hangingwall profile measurement are described?termed irregular and periodic methods. Several data analysis techniques are reviewed for these methods and the suitable ones are discussed in detail. For irregular data the suitable techniques are the determination of the length, the average of the profile and the average absolute deviation from the mean of the profile. All of these techniques as well as determination of the moving average of the height and examination of the spectral image of the profile can be successfully applied to regular data. The effect of preconditioning on the hangingwall is discussed as an example and it is quantitatively shown that it results in improvements of conditions. The techniques described allow the engineer to quantitatively identify the appropriate support type or mining strategy and thus represent a valuable decision-making tool. It is suggested that these techniques should be employed on a routine basis by the rock engineers on the mines as part of their geotechnical classification, as well as support manufacturers to quantify the effectiveness of various support types.

Jan 1, 2000

It would be a good thing when reviewing the challenges to be faced by the Australian gold industry to set the backdrop and scene for them, by briefly examining the history of this vital and dynamic industry in the Australian context. Gold mining in Australia had its official beginnings in 1851 when John Lister and William Tom discovered gold at YorkyÆs Corner, later renamed Ophir by Edward Hargraves. From that first tentative beginning, the ensuing rush of prospectors into New South Wales and Victoria meant that the annual gold production in those early years surpassed that of the next 40 years. This early rate of production was only eclipsed when AustraliaÆs production was once again lifted by the discovery of gold on the other side of the continent, in Western Australia. (Figure 1). The years leading up to the First World War saw Australian production peaking once again at over 115 tonnes of gold, a production rate that would not be surpassed until 1988. This renaissance in production at the beginning of the 1980s was achieved by the application of technology. The advent of bigger trucks and shovels meant that earth-moving costs dropped dramatically. This, coupled with the highly effective and efficient carbon-in-pulp processing route, stimulated the Australian gold mining industry into a state of frenetic activity. These two innovations were the principal factors that enabled the economic exploitation of the lower grade haloes left by the æold-timersÆ around the deposits exploited at the beginning of the last century-no high finding costs here. AustraliaÆs production through the 1980s and the early part of the 1990s was largely supported by the exploitation of these haloes. As these were depleted, the aggressive exploration effort stimulated by the strong cashflows of these early oxide deposits resulted in new æblindÆ discoveries which are now emerging as the backbone of the Australian industry (Figure 2). Gold production is a major contributor to the Australian economy. In 1998/99 the Australian gold industry accounted for approximately 16 per cent of the value of all mineral exports, which in turn accounted for over 35 per cent of AustraliaÆs total exports. As such, the Australian gold industry, by itself, accounts for just under six per cent of AustraliaÆs total exports (Figure 3). Consequently, the industry is responsible for over one per cent of AustraliaÆs gross domestic product. These statistics are all the more compelling when we consider that, at the beginning of the 1980s, goldÆs contribution to exports and GDP was insignificant (Figure 4). Within the Australian resources industry, gold mines and associated infrastructure account for ten per cent of all capital expenditure (Figure 5). From an employment point of view, in 1997/1998 the industry directly employed (excluding contractors) about 7700 people, approximately 15 per cent of all those employed in the minerals industry. Just under nine per cent of the workforce in the minerals industry are female, whereas in the gold industry over 16 per cent are female.

Jan 1, 2000

By Thomas M. Barczak

The decade of the 90's brought an unprecedented increase in the development of innovative technologies to provide more effective and easier to install roof support in underground mines. To facilitate the application of these technologies to improve mine safety. National Institute for Occupational Safety and Health (NIOSH) developed the Support Technology Optimization Program (STOP). STOP is a windows based software program that provides mine operators with a simple and practical tool to make engineering decisions regarding the selection and placement strategy of these various standing roof support technologies. This program includes a complete data base of the support characteristics and loading profiles obtained through safety performance testing of these supports at the NIOSH Safety Structures Testing Laboratory. Support design criteria in the form of the required support load density at a specified convergence can he established from four options: ( 1 ) a data base of measured ground reaction data from various mines or ground behavior information inputted by the user. (2) determination of loading requirements based on a detached roof block or rock failure height. or (3) criteria based on the current roof support system, and (4) arbitrary criteria set the by user. Using these design criteria, the program will determine the installation requirements for a particular support technology that will provide the necessary support load density and convergence control. Optimization routines are also available to determine the most efficient support design for a user specified support installation- In addition to these performance measures. STOP can be used to compare material handling requirements and installation costs. Comparisons among the various support technologies are easily made including graphical analysis of relevant support parameters. This paper describes the STOP and its application to optimize standing secondary roof support systems.

Jan 1, 2000

By S. A. Beeson, C. Poole

"This paper reports on the development of selective flocculation processes for the direct recovery of KCl values from low-grade Canadian sylvinite and carnallite potash ores.Two reagent suites, consisting of either a non-selective cationic or selective non-ionic flocculant, together with the same selective anionic dispersant, were evaluated. Initial data from component mineral behaviour investigations, reagent adsorption studies and selective flocculation tests on a synthetic potash ore were used in the successful development of processes capable of recovering KCl values without the necessity for desliming to remove water-insolubles.Enhanced multi-stage treatment (involving redispersion and reflocculation) and subsequent floc recovery techniques (including sedimentation, hydrocyclones and froth flotation) were examined, and in all cases the influence of process parameters such as reagent dosages, conditioning times, solids concentration, particle size and other physical design criteria were investigated.The data reported clearly demonstrate the scale-up potential of these processes and possible applications in potash operations."

Jan 1, 2000

By K. Severin, B. Flanigan, P. Marion

“Plutonic-related” gold deposits in Interior and SW Alaska (Tintina Gold Belt) vary significantly in size, grade, vein/deposit morphology, depth of emplacement, distance from causative pluton and metal association. Metal associations such as Au-Bi and Au-As-(Sb-Hg) are a good empirical indicator of depth of emplacement and distance from causative pluton and have been used successfully in exploration. Results from a variety of analytical techniques also suggest a phenomenological cause for these metal associations, e.g. gold and bismuth have linked metallogenesis at high temperatures and thus are best correlated at deposits that are deep and/or close to causative intrusions.

Jan 1, 2000

By L. G. Austin

Equations are derived to allow for different mean velocities of axial flow for different sizes of particles in fully mixed ball mills. The equations are modified to allow for the exit classification that occurs in grate-discharge autogenous and semiautogenous tumbling mills. An approximate treatment is given that applies for other forms of residence time distribution, provided that the mill contents are close to fully mixed.

Jan 1, 2000

By John C. Stankus

The success of cable bolts for mine ground control have been well documented in papers presented at this conference too numerous to reference. Cable bolts have proven effective over the years mainly utilized in the form of supplemental support. Some limited work has been conducted on the use of cable bolts as primary support This work has been mainly confined to the West and the bolts utilized were of a non- tensioned type MSHA requirements for primary support have been that the bolt system he tensioned or if non-tensioned, then fully encapsulated with resin. Many operators are now interested in using cable bolts as primary support Further, despite the enormous success of cable bolts, there have been questions raised about the longevity and corrosion characteristics of the cable itself particularly for long tern applications. To improve the corrosion characteristics of cable bolts, galvanized cable has been used for some applications However. although improving the corrosion resistance of cable, galvanized cable for mine ground control does not provide complete protection under certain types of situations and mine environments. Realizing a need for a cable bolt that can be used for primary support and provides consistent installed tension, complete corrosion protection, and a fast installation, Keystone Mining Services. LLC (KMS), an affiliate of Jennmar Corporation, has developed the INSTáL CableOx system. This paper will detail the development and specifics of this system including two underground case studies

Jan 1, 2000

By Hitoshi Iijima, Fumitaka Tsukihashi

"Fine powder of tantalum is used as materials of electric condenser. It is important to control the distribution of particle diameter of tantalum fine powders for the commercial use. In this study, fine powders of tantalum were produced by reducing tantalum chloride vapor with hydrogen gas at 1673 and 1773K. The tantalum chloride vapor was reduced with hydrogen and the produced fine particles of tantalum were collected to observe the distribution of particle diameter. The effects of reaction temperature, partial pressure of hydrogen gas and vaporization temperature of tantalum chloride on the distribution of particle diameter and reaction efficiency of reduction were determined. The mechanism of reduction reaction of tantalum was discussed.IntroductionThe ultra fine powder shows various different physical properties from that of bulk materials. Therefore, the application of ultra fine powder to various fields such as magnetic material, electric material, catalyst, etc is anticipated. The control of shape of powder, size distribution, property of agglomeration, purity is required for the practical use of ultra fine powder. Although the ultra fine powders of ceramics are produced by various methods, the ultra fine powder of metals are produced by the evaporation in gas atmosphere, plasma evaporation process, chemical vapor deposition process, and reduction and precipitation in liquid phase depending on the metal and productivity. The chemical vapor deposition process has features that pure metal powder can be obtained and the control of the distribution of powder size is easy. [1,2,3,4,5]"

Jan 1, 2000

By Paul F. Ph. D. Ziemkiewicz, Courtney D. Black

According to the American Coal Ash Association, 105 million tons of coal combustion products (CCP) were produced by the power generating utilities in 1997. Of that total, 1.68 million tons were used in mining applications (ACAA, 1997). Results have ranged from the environmentally beneficial to neutral and, in some cases, detrimental. Twenty years ago coal ashes: bottom and fly ashes constituted nearly all CCPs. With the shift to new emission control technologies at power plants, however, large volumes of new products are being generated. Many do not lend themselves to traditional ash applications such as cement formulation. Many CCP disposal sites are not documented with reliable pre and post application monitoring. In this report we discuss types of CCP, their relevant characteristics and the mining environment. We have attempted to identify a range of documented applications and to draw conclusions about their environmental effects including benefits and adverse impacts.

Jan 1, 2000

By Raj P. Singh

Applications of cementation in the recovery of metal ions from process solutions have been known for a long time. Cementation reactions involve electrochemical precipitation of a noble metal from solutions of its salts on a more electropositive metal which, in tum, progressively dissolves. For example, addition of zinc metal powder in a solution containing zinc and cobalt ions would allow for the precipitation (separation) of cobalt according to the following chemical reaction. This paper pertains to the recovery of cobalt from cobalt process solutions via a cementation reaction on aluminum shavings (metal scraps from cans etc). Specifically, we report on the characterization of cobalt process solutions, a by-product obtained from cobalt chemicals, and the kinetics of cobalt, nickel and manganese cementation from process solutions on aluminum shavings.

Jan 1, 2000

By Dale Ramsey

Emulsion explosives have become the product of choice for many blasting applications and are not limited to just extreme wet hole conditions or special application environments as in the past. Today’s novel emulsion technology has evolved over many decades, allowing a great diversity of formulations, Emulsion explosives can be effectively designed to produce very high energies, cap sensitive high explosive cartridges to bulk blasting agents, with varying viscosities, stable VOD’s, excellent water resistance, long shelf life and sleep time. They are also conducive to the mixture of emulsion, An/F0 blends in varying proportions and are amenable to any type of sensitizer. The key to a stable, reliable and consistent emulsion formulation is the careful mixing of the internal phase, which consists of a solution of oxidizer salts suspended as microscopically fine droplets, with the surrounding continuous fuel phase. There are few blasting applications today where some form of an emulsion explosive cannot fit the application. In massive, hard rock, dense, tightly jointed and fine grained rock types, the emulsion explosives are the best choices in creating new fracture networks for good fragmentation with a few alternatives. In such environments, emulsions with expanded drill patterns often result in better economics than the use of straight AnLFo. This paper will cover emulsion formulations, sensitizing options, product testing, material handling, and blast optimization, Emulsion explosives characteristics have also proven to reduce adverse environmental effects such as noxious fumes, ground vibration, and airblast while still remaining cost effective.

Jan 1, 2000

By Kirk Yeager

All explosive formulations display some sensitivity to heat. A common technique utilized to measure an explosive’s response to thermal stimulation is differential scanning calorimetry (DSC). As DSC analysis is run on quantities of material easily handled in a laboratory setting, and is relatively inexpensive, it tends to be one of the more predominant tools utilized to determine potential thermal hazards of energetic materials. The analysis of energetic materials via DSC provides unique challenges, as both large energy outputs and significant production of gaseous products result from their decompositions. In addition, the unique thermal decomposition characteristics of ammonium nitrate (AN) based materials have also created difficulties in DSC analyses. A wide variety of techniques have been developed to study the decomposition of explosives. Traditionally, sealed glass capillaries were utilized to house samples. Recently, the introduction of specialty cells designed to withstand high pressures has enabled new sampling techniques to be developed. Analyses of explosives with both traditional and “high-pressure” cells will be compared and contrasted. Lessons learned about the application of both techniques towards analyzing thermal hazards such as incompatibilities will be presented. Inconsistencies in the results displayed during analyses of AN-based explosives will be highlighted. Recommendations on the best approach for analyzing the more problematic AN formulations will be given.

Jan 1, 2000

By Guido Deissnann, Jennifer L. Kirkaldy, Stephan Kistinger, Carol M. Pettit

Contaminated mine drainage presents a potential hazard for aquatic ecosystems and groundwater resources. Reliable predictions of long-term developments in seepage quality are necessary to select reasonable decommissioning options and remediation measures for waste-rock heaps during mine closure and/or mining site rehabilitation to minimize future risks and environmental hazards. Extensive geochemical modeling work was used to assess the consequences of various remediation options for waste rock heaps at a former uranium mine in Eastern Germany. The predicted contaminant discharges are used for an assessment of long- term benefits of decommissioning alternatives to derive conclusions for sustainable remediation measures using risk-based cost/benefit analyses.

Jan 1, 2000

PURPOSE: Evaluate practical technological advances in level-dependent hearing protectors and inexpensive personal acoustic monitors. RESEARCH SUMMARY: The results of previous NIOSH research show that miners develop hearing loss much more quickly than nonoccupationally noise-exposed individuals and that miners experience a greater severity of hearing loss than would be expected for nonoccupational noise-exposed persons of the same age and gender. Using hearing thresholds at 4,000 Hz as an indicator, coal miners experience hearing loss 2.5 to 3 times greater than would be expected for persons not exposed to occupational noise. At age 50, 90% of coal miners and 49% of metal/nonmetal miners were found to have a hearing impairment. In comparison, only 9% of a nonoccupationally exposed control group had a hearing impairment at age 50.

Jan 1, 2000

By J. van Deventer

Testwork was done with two different adsorbents, Dowex-Minix gold-selective resin and activated carbon, to detemine their relative performances with regard to gold recovery from clarified low-grade solution employing a fixed-bed operation. The mill discharge from the milling-in-cyanide operation at a Witwatersrand gold mine was used as feed to the adsorption columns. A small amount of gold was leached during the milling process, so that this solution simulates, to a certain extent, a low-grade solution representative of a heap-leach operation. A speciation of the feed solution was done to establish which metal complexes were present in the milling-in-cyanide solution. This information was necessary to interpret metal loadings on the resin, as base metal cyanide species and their respective charges have an effect on the final gold loading capacity of the resin. Equilibrium isotherms were established for both adsorbents to estimate the rate of adsorbent flow anticipated for this specific feed solution. Breakthrough profiles were obtained at two different superficial linear velocities for each adsorbent. Mass transfer zone heights determined from the test work and the elution/regeneration time requirements were used to size a 150 m3/h full-scale plant for both adsorbents. A counter current configuration of adsorption columns, using three columns, should be suitable to recover gold effectively and to produce an effluent with a gold concentration below 0.01 mg/l. Based on the results obtained from the breakthrough tests, a preliminary techno-economic comparison was done between the resin-in-solution and carbon-in-solution options for the recovery of gold from low-grade solutions. This study indicated that the capital expenditure for a carbon-in-solution plant would be about 33 percent higher than that of a resin-in-solution plant. The operating expenditure for a resin-in-solution plant is expected to be only 60per cent of that for a carbon-in-solution plant. Keywords: resin-in-solution, carbon-in-solution, heap leach.

Jan 1, 2000