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By Maurice Deul

This bulletin summarizes the work conducted under the Bureau of Mines methane control research program during the years 1964 to 1979. This research effort was directed toward improving existing methods and developing alternative methods of reducing the explosion hazard during mining. The research was performed in three general areas: (1) basic factors that control the emission of methane into coal mines, (2) methane control during mining, and (3) methane drainage in advance of mining. Topics discussed in this bulletin include the magnitude of the methane problem; the equipment and instruments developed; the geological, chemical and physical parameters that control the movement of methane in coalbeds; the direct method of determining gas content; the estimates of gas content from adsorption data; and methane drainage, through shafts, through horizontal boreholes, through vertical boreholes, or through slant holes. Improvements in ventilation, control of methane in gob areas, and water infusion are also discussed, as is the potential use of coalbed methane as a supplement to natural gas supplies. This bulletin provides a comprehensive source of information on the accomplishments of the Bureau's methane control research program, on the technology developed, and on the direction of further research.

Jan 1, 1986

By R. J. Fantel

The Bureau of Mines investigated the resource availability of titanium minerals from 63 mines and deposits in 12 market economy countries. These mines and deposits contain, at the demonstrated resource level, an estimated 438 million metric tons (mt) of titanium dioxide (TiO2) in the minerals rutile, ilmenite, leucoxene, and anatase. An additional 314 million mt of TiOz is available from inferred resources. If all titanium minerals and other recovered heavy minerals are sold at total costs at least equal to the January 1984 market prices, approximately 200 million mt of contained TiO2 could be recovered in total. In terms of mineral concentrates, this equals approximately 11 million mt of rutile concentrate, 187 million mt of ilmenite concentrate, 3 million mt of leucoxene concentrate, 13 million mt of synthetic rutile concentrate (in addition to the ilmenite), and 89 million mt of titanium slag. The study indicates that world resources of low-cost rutile are declining. In order to maintain future supply for high-grade titanium resources, alternate sources will need to be developed, which may include higher cost rutile mines, Brazilian anatase deposits, increased production from slag operations, or more synthetic rutile capacity from ilmenite resources, which are abundant.

Jan 1, 1986

By Louis Schaffer

The purposes of the research were to assess the applicability of new accident investigation methods to mining accidents, and to adapt those found to be applicable in the development of a new methodology for use in mining. The development included field testing, evaluation and modification of the new methodology. The report is in two volumes. This, volume one, discusses primarily the Phase I work: background research, design of a methodology for field evaluation, and preliminary field tests in Utah mines. Phase I was completed in June, 1980. Also discussed are some activities to prepare for a field evaluation during the period May 1980 -October 1981. Volume 2 discusses the subsequent field tests, modifications of the initial methodology and the results of use of the methodology in two mining companies for a period of approximately eighteen months, and in other companies for selected loss incidents during that period.

Jan 1, 1986

By J. K. Whyatt

This report describes a microcomputer-based instrumentation system for structural monitoring of the circular, concrete-lined Silver Shaft in northern Idaho, The 1-ft-thick concrete lining and surrounding rock mass were instrumented with a total of 12 multiple-point borehole extensometers, 16 pressure cells, 22 concrete embedment strain gauges, and 12 thermistors. The instruments were distributed among four test sites and installed immediately above the shaft bottom during sinking at the 2,414, 4,063, 5,191, and 5,955 levels. Limited access to the instruments prompted the development of a microcomputer-based remote data acquisition system that could be operated from the surface. The system scanned the instruments on a programmed schedule, printed out reduced data, and stored the data for plotting and recall. Data acquisition from off-site and uploading of data to mainframe computers were accomplished by the addition of modems to the basic system. The system is suitable for use in monitoring the structural behavior of any deep mine opening, especially in harsh operating environments and where access is limited.

Jan 1, 1986

By K. C. Dean

The Bureau of Mines, following passage of the Solid Waste Disposal Act of 1965, was authorized to conduct research on methods for utilizing, stabilizing, or reclaiming mineral wastes. This report summarizes laboratory research conducted by the Bureau and cooperative field studies made with the mineral industry to reduce the environmental impacts of air and water pollution deriving from mineral wastes. Utilization research showed that both dry-press and steam-cured building bricks and ceramic tile could be made from copper mill tailings and other discarded mineral wastes. Sponge iron was produced from steel mill and amination industry wastes, and valuable mineral products were extracted from such diverse sources as flue dusts and uranium tailings. Mineral wastes were combined with agricultural and/or sewage wastes to make artificial soils that have the potential of resolving several disposal problems by production of a useful commodity. Physical, chemical, and vegetative stabilization methods were evaluated, singly and in combination, for reclamation potential on copper, uranium, lead-zinc, and asbestos tailings. Suitable methods were developed in the laboratory for overcoming major adverse conditions of these wastes such as salinity, heavy metal toxicity, acidity, basicity, lack of nutrients and organics, and unstable surfaces. Field testing of these methods was performed on a variety of mineral wastes. Costs for the various stabilization and utilization-procedures developed were also determined.

Jan 1, 1986

By Robert G. Bottge

The Bureau of Mines investigated the availability of the land in south-central Alaska for exploration and mineral development of locatable minerals under State or Federal laws. The land ownership for an area of nearly 72.5 million acres in south-central Alaska was divided into 3 availability categories and 15 subcategories. In July 1985, 31.0 million acres of the study area were available for mineral exploration and development, 6.2 million acres were available with restrictions, and 35.3 million acres were unavailable. About 23.6 million acres in the study area are underlain by mineral terranes. About 9.9 million of the 23.6 million acres are available for mineral entry, 2.4 million acres are available with restrictions, and 11.3 million acres are unavailable. While much of the land currently classified as unavailable will be reclassified once it is conveyed to the State or to Native corporations, about 22% of the unavailable lands underlain by mineral terranes are now Federal parks, preserves, wildlife refuges, wild and scenic rivers, and military lands, all of which are considered permanently unavailable for mineral exploration and development.

Jan 1, 1986

By G. S. Beaumont

This report presents a programme of work to demonstrate the use of a surface-based centralised computer control system for the remote monitoring and control of underground conveyors in a US coal mine. The system selected for demonstration was the 'Dynalink' Micro MINOS system which is manufactured by Hawker Siddeley Dynamics Engineering Limited. The site selected was Barnes S Tucker Lancashire No. 20 Mine located near Carrolltown, Cambria County, Pennsylvania. The system concept, operating and application software was designed and developed by the. British National Coal Board. The report describes the selection of the site, specification of the system requirements, commissioning, operation and evaluation of the system under typical US mine operating conditions. Experience with the system, based primarily on the system reliability and performance of conveyor control, was favourable. Mine management personnel felt that the system had successfully achieved its objectives and were keen to expand monitoring and control to other activities.

Jan 1, 1986

By M. R. Paterson

Operational and economic factors tend to favor the application of continuous processes in preference to batch processes in the majority of mineral processing applications. In this paper, the requirement for a Continuous Elution Process is established and the development of a large-scale pilot plant is described. It is based on a Continuous Elution apparatus which has a number of special features. These are the subject of various patent applications. The apparatus is suitable for adaptation to the AARL, Zadra and other methods of elution. The performance of the Atmospheric Continuous Elution System (ACE) is concluded to have significant advantages over the batch process.

Jan 1, 1986

By Robert L. Frantz

The U.S. Bureau of Mines (USBM) established on August 15, 1983, a Generic Mineral f Technology Center (GTC) for Respirable Dust within the Mining and Mineral Resources Research Institutes (MRIs) at The Pennsylvania State University (PSU) and West Virginia University (WW) in association with participating MRIs at Massachusetts Institute of Technology (MIT) and the University of Minnesota (UMN). The primary goal of the Center is to reduce the incidence and severity of respirable dust disease through researching and advancing the fundamental under- standing of all aspects of respirable dust associated with mining and milling and the interaction of dust and lungs. Other Center activities include the training of engineers and scientists, graduate students and undergraduate students through their respective institutions, and the technology transfer to the industry. The Center also serves as the reference center for publications in the respirable dust area.

Jan 1, 1986

1. Book reviews Dislocations and properties of real materials, edited by M.H. Loretto. London, The Institute of Metals, 1985. 392 pp. Reviewer: F.R.N. Nabarro Au &Ag heap and dump leaching practice, edited by J.B. Hiskey. AIME, 1984. 162 pp. $20 (member), $15 (student member), $30 (non-member) plus $3.50 for postage and handling. (Order from SME Books, Caller no. D, Littleton, CO 80127, U.S.A.). Reviewer: R.A. Snodgrass The cost and availability of Colombian coal, by Eric D. Jamieson, with the assistance of Kathleen Jamieson. London, lEA Coal Research (14/15 Lower Grosvenor Place, London SWl W OEX). £50 (in member countries), £100 (in non-member countries). Reviewer: W.C. Mather Extraction Metallurgy '85. London, The Institution of Mining and Metallurgy, 1985. £42. Reviewer: R.A. Snodgrass 2. Recent publications Mining annual review 1985. London, Mining Journal, Jun. 1985. 600 pp. £26.50 (surface), £39.50 (air). High heat production (HHP) granites, hydrothermal circulation and ore genesis. London, The Institution of Mining and Metallurgy, 1985. 593 pp. £27 (members), £30 (non-members). Potential mineral resources of Egypt. 144 pp. US$10. Available from Bendix Field Engineering Corporation-MPGAP, Box 1237, Grand Junction, CO 81502, U.S.A. 3. Mintek reports Report M212 South African costs of equipment for the metallurgical industry (1984). Report M213 The response of as-rolled 3CR12 steel to heat treatment. Report M214 A computer programme for use in the development of multi-element X-ray-fluorescence methods of analysis. Report M221 Commodity profiles for selected metals. Report MIO7D Upgrading of alaskite rock to feldspathic sand. (First issued Jun. 1983; reissued Nov. 1985). IMM awards Given below are details of the trust funds to which applications are invited for grants, etc., payable in 1986. Application forms, which must be returned to the Secretary before 17th March, 1986, are available on request. Applicants should note that, in general, preference will be given to members of the Institution.

Jan 1, 1986

By C. B. Barlow, T. A. Mekelburg

Due to a tight ash constraint on the clean coal product and difficult middlings washability characteristics, a considerable amount of coal was being lost in the jig middlings at the Monterey No. 2 Mine. An investigation was conducted into circuitry to recover this lost coal with minimal effect on the total clean coal ash. A reverse two-stage hydrocyclone system cleaning at low specific gravities was selected. This system is currently recovering approximately 5.8 kg/s (23 stph) of 11.5% to 12.5% ash coal. The specific gravity of separation for the system is about 1.5 and the probable error is 0.13.

Jan 1, 1986

1. Reviews Steel and its heat treatment, by K-E Thelning. 2nd Edition. London, Buterworths, 1984.678 pp. R201,60 (incl. OS1). Reviewer: J.P. Hofman The Southern Queensland Conference 1985. Parkvile (Australia), The Australasian Institute of Mining and Metallurgy, 1986. A$ 15.00. Reviewer: R.B. McGilivray Rock mechanics, by A.R. Jumikis. 2nd edition. Clausthal-Zelerfeld (West Germany), Trans Tech Publications, 1983. US$ 58. Reviewer: R.W.O. Kersten The XVIth International Coloquium on Refractories. Freiburg, West Germany, 1985. DM 80. Reviewer: H.J. S. Kriek Diamond driling handbook, byW.F. Heinz. Johannesburg, South African Driling Association, 1985. 517 pp. R30. Reviewer: S.A.G. Martins Processing and utilization of high sulfur coals, edited by Y.A. Atia. Amsterdam, Elsevier, 1985.788 pp. Oft. 385. Reviewer: L.M. Falcon Weighingand proportioning of bulk solids, by Hendrik Colijn. 2nd edition. Rockport (U.S.A.), Trans Tech Publications, 1983. 398 pp. $60.00. Reviewer: G. Cunningham Investment appraisal and economic evaluation of mining enterprise, by S. von Wahl. Clausthal-Zelerfield (West Germany), Trans Tech Publications, 1986. US$ 40. Flotation of sulphide minerals, edited by K.S. Eric Forssberg. NewYork, Elsevier Science Publishers, 1985. 480 pp. US$1O1.75. Reviewer: T.R. Twidle 5th Meeting of the European Clay Groups (5th Euroc/ay Meeting), Prague, edited by J. Konta. Praha (Prague), Univerzita Karlova, 1985. Reviewer: D. Bibmann 2. Recent publications CSIRO. Research review1982-84: CS/Ra Division of Mineral Engineering. Melbourne, Commonwealth Scientific and Industrial Research Organization, 1985. 77 pp. The world copper market: structure and econometric model, by Gerhard Wagenhals. Berlin, Springer- Verlag, 1984. 202 pp. DM 37,00.Materials data of high-strength aluminium aloysfor durability evaluation of structures, edited by L. Schwarmann. Disseldorf (West Germany), Aluminium- Verlag GmbH, 1985. BRITISH GEOLOGICAL SURVEY. UnitedKingdom mineral statistics 1985, compiled by H.c. Squirel, A. Jones, N.E. Sharp, M. Lowe, and D. Slater. Keyworth (U.K.), the Survey, 1986. 175 pp.3. Mintek reports Report Ml66D The effect of calcining on the recovery of gold in a sand residue. (1st issued Sep. 1984.) Report M168D The treatment of Uitkomst concentrate. (1st issued Oct. 1984; reissued Mar. 1986.) Report M175D Supergene alteration at the Pering zinc-lead deposit: The nature and extent of the oxidation zone. (1st issued Oct. 1984.) Report M176D Bench-scale tests on the extraction of cobalt and nickel from COMAT leach liquors. (1st issued Nov. 1984; reissued Mar. 1986.)Report M241 PLA TO at Mintek. Report M243 The performance and wear characteristics of grinding media as affected by metallurgical and dimensional factors. Project development The Second Project Development Symposium on Planning, Construction and Commissioning will be held in Sydney, Australia, from 7th to 10th October, 1986. Hosted by the Sydney Branch of The Australasian Institute

Jan 1, 1986

By G. W. Elger, H. E. Bell, J. E. Tress, J. B. Wright

This paper describes laboratory techniques and subsequent results of US Bureau of Mines (USBM) research to produce chlorination-grade feed- stock from an abundant, low-grade, domestic, rock ilmenite ore. The research is part of the Bureau effort to devise technology that may help decrease US dependence on imported raw materials. A rock ilmenite containing about 46 wt % TiO2 was smelted in an electric arc furnace with coke, wood-chips, and Na2CO3 to separate most of the iron as pig iron and to form a low-iron, titanium-enriched slug. The slug was ground, pelletized, oxidized, and then sulfated with mixtures of SO2 and air in a continuous 4.5- to 9.1-kg/h (10- to 20-lb per hour) apparatus at 1023° to 122J0 K (1380° to 1740° F). The sulfated slug, containing 60% to 65% TiOb, was reground and leached in water at ambient temperature to decrease the combined levels of the troublesome calcium, magnesium, and manganese impurities from 7.0 to 1.7 wt 70. The final product was upgraded to about 8.4 wt % TiO2. This material is potentially suitable for chlorination in a fluidized bed reactor. The most favorable results were achieved with leached slug sulfated at a feed rate of 4.5 kg/h (10 lb per hour) and at temperatures of 1073° to 1123° K (1470° to 1560' F).

Jan 1, 1986

By G. A. Savanick

Borehole (slurry) mining, where a tool incorporating a water-jet cutter and a downhole slurry pump mines phosphate through a borehole, was field tested in northeastern Florida as part of a US Bureau of Mines program to increase the domestic availability of critical minerals. About 1.5 kt (1700 st) of phosphate ore were mined at 23.6 t/h (26 stph) from a depth of 76 m (250 ft). The borehole was filled with water during mining for roof support and to assist slurry pumping. Underwater cutting was enhanced with an air-shrouded water jet. Mined cavities were backfilled to prevent subsidence after abandonment. Roof subsidence during mining was avoided only when the cavity was filled with water. Environmental monitoring before, during, and after mining included hydrological studies and measurements of water quality. Significant water quality changes occurred only in the zone being mined and were confined to the immediate area of the borehole.

Jan 1, 1986

By D. Hodouin, T. Gelpe

A digital simulator of classification and grinding circuits is used to evaluate the performance of various flowsheets. For a given flows he et configuration, unit process dimensions, and operating conditions, the simulator calculates the steady-state values of the process variables and determines the conditions that meet the required operation criteria for tonnage and product quality. Calculation examples are proposed for the design of wet and dry grinding circuits. The performance of different configurations of cement clinker and sulfide ore grinding flowsheets is evaluated and discussed.

Jan 1, 1986

By A. Wahab Khair, Negendra P. Reddy

INTRODUCTION The continuous mining machines which were introduced in the 1950's now account for more than half the production of coal from underground mines. Unfortunately, these continuous miners which were designed for increased productivity have also increased the concentration of respirable dust in mines. Inhalation of this respirable dust by miners causes the Coal Worker's Pneumoconiosis (CWP). Concern for CWP increased in the United States following a 1963-65 survey that showed definite x-ray evidence of CWP in 9.8 percent of working miners and in 18.2 percent of nonworking miners in the Appalachian bituminous coal region (Breslin and Niewiadomski, 1982). One of the major objectives of the Federal Coal Mine Health and Safety Act of 1969 was the prevention of CUP. This law initially limited the daily average exposure of coal miners to 3 mg/m3 of respirable dust. However, following the results of a probabilistic model developed by Jacobsen, et. al. in 1971, the limit was reduced to a mass concentration of 2 mg/m3 unless quartz content exceeds 5 percent, a rare occurrence in mines. Based on x-ray categorization prior to death it is believed that the mass concentration in the respirable fraction is a parameter of primary interest for hygenic evaluation of dust exposure. Elorgan, Burgess and Jacobson (1973) suggested that the quantity of inhaled dust, although influential is not the only aspect of exposure which is significant in producing CWP. Miners working in higher rank coal (anthracite) mines are more susceptible to CWP (Morgan, Burgess and Jacobson, 1973). This also confirms the findings of the British (Bennett, Dick and Kaplan, 1979 and Hurley, et. al., 1979) and Germany (Reisner and Rubock, 1977). Based on the cy to toxicological evidence Reisner and Rubock (1979) suggested that when coal properties are similar, increasing quartz and mineral content increases toxicity. David, Ottery and Le ?oux (1975) examined that as the severity of the CWP increased the retention of the coal dust content in the pulmonary region remained the same, while that of quartz content increased significantly . Leiteritz, Baur and Bruckman (1971) studied the various components of coal dust and showed that coal particles comprised a smaller fraction of the mass of fine dust than did particles , of quartz and minerals. It is ironic that quartz and mineral matter both comprise smaller fractions of the higher rank coal dust (Dodgson, et. al., 1971 and Dwiggins, 1981). Results of a recent research revealed that quartz or any other mineral examined had no strong or consistent effect on the incidence or progress of CWP (Attfield,

Jan 1, 1986

This report presents the results of a study for the Bureau of Mines to compare loan terms for non-fuel mineral projects in developing countries, from various International Financial Institutions (IFIs), and from private sector commercial sources. The study compares IFI and commercial loan terms for seven mineral projects in developing countries. The International Financial Institutions represented are: ? International Bank for Reconstruction and Development (World Bank) ? International Finance Corporation (IFC) ? Inter-American Development Bank (IDB) ? Asian Development Bank (ADB) ? International Monetary Fund (IMF) In addition, the costs of financing for these mineral projects were compared with the costs of long-term debt to the five largest U.S. mineral producers.

Jan 1, 1986

By B. R. Eichbaum, J. E. Murphy, J. A. Eisele

The US Bureau of Mines demonstrated ferric chloride leaching of galena concentrate on a continuous bench scale basis. Leaching was performed at 95°C (200°F) and with a contact time of 15 minutes. The ferric chloride leaching solution was continuously fed to a leaching tank at a constant rate for periods up to 45 hours. In each test, a constant redox potential was maintained in the slurry exiting the leaching tank by controlling the concentrate feed rate. In the 45 hour test, lead extraction exceeded 99.5%, and the lead chloride produced was 99.97% pure.

Jan 1, 1986

1. Book review The geology of some northern Nigerian anorogenic ring complexes, by J.N. Bennet, D.C. Turner, E.C. Ike, and P. Bowden. The British Geological Survey: Overseas Geology and Mineral Resources, no. 61. London, HMSO, 1984. 66 pp. Reviewer: R.H. Ingram 2. Mintek reports Report M226 The separation of tungsten and molybdenum by the formation of sulphide complexes and extraction into a weak-base resin. Report M228 The solvent extraction of zinc, iron, and indium from chloride solutions by neutral organophosphorus compounds. Report M230 Shear flocculation of fines for improved flotation. Report M239 A mineralogical study of residue from the column leaching of a low-grade nickel-copper sulphide ore.3. Recent publication Driger Review, special edition, act. 1985. 48 pp. (Copies obtainable from Roly Nyman, HAMPO PMIE Division, P.O. Box 170, Joham1esburg 2000.) Black Mountain's achievement The 13 689 t consignment of metal concentrate that was loaded aboard the bulk carrier 'George' and shipped out of Saldanha Bay early in December brought the number of tons exported from Black Mountain via the Sishen-Saldanha railway and harbour system to one million.

Jan 1, 1986

By R. L. Grayson, S. S. Peng

Sampling of respirable dust and analyses of samples have been partially completed for a longwall panel. Physical and compositional properties which have been characterized include: 1. Respirable mass concentration, 2. Mineral composition, 3. Particle size distribution by mineral, 4. Particle shape distribution by mineral, 5. Particle angularity distribution by mineral, and 6. Respirable size distribution. Analytical techniques used in the characterization of samples are described, and results are reported with emphasis placed on relationships between the various characteristics and worker locations. Details of existing mining conditions, equipment arrangements, dust control methods and operating system parameters are presented.

Jan 1, 1986