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By W. H. Kerns

The Simon & Coles manganese deposit in Sherman Valley, Bedford County, Pa., was investigated by the Bureau of Mines during the fall of 1942. Two churn-drill holes; 65 and 75 feet deep were bored, and 8 channel samples were taken. Manganese occurs at this property in the form of psilomelane and manganiferous iron as replacement of the red sandy shale of the Much Chunk-formation. Two cars of manganese ore had been shipped by the owners in 1940, of which one averaged 10.9 percent manganese and the other 21.3 percent manganese. One car of hand-sorted manganese ore that averaged-45 percent manganese was shipped in 1942.

Jan 1, 1948

By R. S. Dean

"Interest in the nitrogen content of steel has increased sharply in the last few years. Investigations have indicated that its presence in steel has an important bearing on high temperature brittleness3, magnetic properties4, room temperature hardening5, and shock resistance. The steel producer may therefore look forward with certaintly to the necessity of controlling this element in a considerable proportion of his product. The literature, however, reveals a great many contradictory statements concerning the percentage of nitrogen which must be present to produce given effects on the properties of iron and steel. Most of these arise from a misunderstanding of the nature of the iron-nitrogen diagram near the iron end and a lack of recognition of the effect of state of aggregation on physical properties although both have been fairly well worked out.My thanks are due to Mr. J. L. Gregg, Prof. R. H. Dowdell, Mr, R. F. Mehl and Mr. H. C. Vacher for suggestions in connection with the preparation of this paper, and to Mr. C. H. Hefty and Mr. G. T. Motok for furnishing a valuable bibliography and translations of articles by Must and Duhr.The iron-nitrogen diagram in the solid state, so far as it concerns the nitrogen content of commercial iron and steel, consists simply in a solubility curve increasing with temperature. The important thing about this solubility curve is that without cold wore the iron nitride when precipitated does not go into solution on heating for long periods below 300°C. This slowness of solution is probably due to the fact that iron nitride when present as a separate phase has at these temperatures an equilibrium pressure of several thousand atmospheres7 and that therefore each particle of iron nitride surrounds itself with a layer of nitrogen. The precipitation of such an unstable crystal presents points of interest thermodynamically but we can not go into these here. It is quite well established that it precipitate. It can not diffuse then unless this layer is broken through or the temperature and pressure are increased to a point where the nitrogen is absorbed at an appreciable rate in the surrounding iron. This rate will depend on the degree of unsaturation of the iron and the excess pressure of the nitrogen above equilibrium pressure. The degree of unsaturation is determined by the temperature alone so that the temperature at which the rate of solution of the nitride becomes appreciable will depend on the pressure of nitrogen developed. This, in turn, will depend on the balance between rate of decomposition of the nitride and the rate o: flow of the iron. In annealed iron, this temperature of appreciable solution rate is between 300 and 350°C.8 By cold work, however, the elastic limit of the iron is increased, and conditions for the nitride to go into solution are reached at a much lower temperature, giving rise to the so-called blue brittleness. This brittleness and hardening is due to iron nitride going into solid solution and is not precipitation hardening."

Mar 1, 1931

By Mark I. Copeland

The Bureau of Mines investigated the effect of up to 1 wt-pct of copper and silicon on the heat treatment response and hardness, tensile, and impact properties of hot-rolled medium-carbon steels. The steels were prepared by induction melting and fabricated into plates by forging and rolling. The tensile strength of 0.2-wt-pct carbon steels containing 0.3 wt-pct silicon was affected significantly by copper in both the hot-rolled and heat-treated (600° C) conditions, whereas the tensile strength of the 0.3-wt-pct carbon steels was less affected. A 600° C treatment was considered optimum as a post-rolling treatment to strengthen the steels by copper precipitation. Strengthening of 0.2-wt-pct carbon steels by silicon was reduced by increasing copper contents.. Optimum impact strengths occurred at about 0.3 wt-pct silicon in 0.2-wt-pct carbon steels containing 0.6 and 0.8 wt-pct copper. The impact strengths were lowest for 0.2-wt-pct carbon steels containing over 0.8 wt-pct copper and greater than 0.3 wt-pct silicon, especially in the heat-treated condition. Copper and silicon solutes and copper precipitates strengthened the steels. This effect was augmented slightly by strengthening through grain refinement by these solutes.

Jan 1, 1973

By Kathleen M. Kowalski, Audrey Podlesny

The Maslach Burnout Inventory (MBI) was administered and scored for 154 Mine Safety and Health Administration (MSHA), U.S. Department of Labor, employees who serve as accident investigators for serious accidents and fatalities as part of their job duties. The subjects responded anonymously during a workshop on stress. The subjects consisted of randomly selected individuals, representative of locations across the country and representative of all mining commodities: coal, metal, nonmetal, stone, and sand and gravel. The Maslach Burnout Inventory assesses three aspects of experienced burnout: emotional exhaustion, depersonalization, and reduced personal accomplishments. The average results of the scores for each of the three subscales fell in the moderate range for the study group of MSHA accident investigators. The scores within the moderate range show that the subject population was at the lower end of the range for emotional exhaustion and depersonalization, tending toward a lower burnout risk, while the group evidenced a lower sense of personal accomplishment in their jobs, indicating a higher risk for burnout. It is concluded that overall this group is at moderate risk for burnout, and the authors recommend follow-up with this population.

By R. C. Buehl

Pilot-plant tests have been in progress at the Bureau of Mines, Pittsburgh, Pa., on the recovery of manganese from open-hearth slag.3/4/5/ In the process, 1 the slag is first reduced in a blast furnace to make a high-phosphorus spiegeleisen containing 12 to 22 percent manganese. A slag containing 55 to 60 percent manganese is made from this spiegel by oxidation in a basic-lined converter. The metal from this blowing operation contains about 3 percent phosphorus, 1 percent manganese, and less than 1 percent carbon. Economic efficiency in the manganese-recovery process requires that this metal be converted into steel. Because of its high phosphorus content the metal is suitable for blowing in a basic-lined converter. In most of the tests described in this report, metal of this composition was used as the starting material in a 1-ton, side-blown, basic-lined converter. Although basic-lined converters are not used for steel production in the United states, in Europe a considerable portion of the steel is made in them. Open hearths largely have replaced converters for steelmaking in the United States; mainly because open-hearth steels have better physical properties than converter steels because of lower nitrogen and phosphorus contents. However, by improving converter design and operating technique during the past 15 years, metallurgists have found that low-nitrogen steels with physical properties equal to open-hearth steels can be produced in converters.6/ Tests at Jones & Laughlin steel Corp. with side-blown, acid-lined converters of 3 and 22 tons capacity showed that steel with a low nitrogen content comparable to that of open hearths operating on scrap charges could be made by surface blowing.7/

Jan 1, 1955

By Lloyd A. Morley, Robert Stefanko

1. Anonymous (Berggewerkshaftliche Versuchsstrecke), "75 Jahre Berggewerkshaftliche Versuchsstrecke, 1894-1969," 1969. 2. Anonymous, British Symposium on Flameproofing and Intrinsic Safety, IEEE Conf. Report Series No. 3, 1962. 3. Anonymous (Ministry of Fuel and Power), "A Review of Electrical Research and Testing with Regard to Flame-Proof Enclosure and Intrinsic Safety of Electrical Apparatus and Circuits," 1943. 4. Australian Standard Specification, ASC-98, "Electrical Equipment for Explosive Atmospheres," 1970. 5. Belgium Standard Specification, Norme NBM 286, "concernant la protection par enveloppe antideflagrante," 1965. 6. Bossert, J.A., "Approval for Electrical Equipment for Hazard Locations," paper PCI 66-33, IEEE 16th Annual Petrol. and Chem. Ind. Conf., L. A., California, Sept. 15-17, 1969. 7. Bossert, J.A., "Intrinsic Safety in Canada," Electrical Safety Practices, ISA Monogram, vn. 112, 1969. ,8. British Standards, BS229, "Flameproof Enclosure of Electrical Apparatus," 1957. 9. British Standards, BS4683 Part 1, "Classification of Maximum Surface Temperatures," 1971. 10. British Standards, BS4683 Part 2, "The Construction and Testing of Flameproof Enclosures of Electrical Apparatus," 1971. 11. Brown, G.R., and Silver, S., "An Explosion Hazard Due to Inflam¬mation of Aluminum Particles in Flat Flanges of Flameproof Enclosures," CEAL No. 197, Canadian Explosive Atmospheres Labor¬atory, 1969. 12. Campbell, J.D., and Chudleigh, J.P., "Problems Encountered in Designing Electrical Systems for Hazardous Areas," paper PCI-69¬31, IEEE 16th Annual Petrol. and Chem. Ind. Conf., L. A., California, Sept. 15-17, 1969. 13. Canadian Standards Association, C22.2 No. 30, "Explosion-Proof Enclosures for Use in Class I Hazardous Locations." 14. Dainty, E.D., and Brown, G.R., "Explosion Gas Temperatures at the Entrance to Flanges of Enclosures Containing 8.5% Methane-Air Mixtures," CEAL No. 196, 1969.

Jan 1, 1974

By Jr. Karr

The Bureau of Mines studied the influence of carbonization method, temperature, and carrier gas on the composition of eight different low-temperature tars produced from a Colorado subbituminous coal. A fluidized bed was compared with an entrained bed, temperature was varied from 500° C to 650° C, and external heating using recycle gas as the carrier gas was compared with internal heating using oxygen-containing gas. The entrained bed yielded significantly more m-cresol and m-ethylphenol, indicating that thermodynamic equilibrium was more nearly approached in the system. Increasing the temperature greatly increased the yield of benzenes and naphthalenes, while paraffins, olefins, and total tar acids were reduced. Using oxygen in the carrier gas decreased the yield of low-boiling phenols and increased that of paraffins and olefins at 650° C.

Jan 1, 1966

By Kathleen M. Kowalski, Audrey Podlesny

The Maslach Burnout Inventory (MBI) was administered and scored for 154 Mine Safety and Health Administration (MSHA) employees kom the US Department of Labor. These employees serve as accident investigators for serious accidents and fatalities as part of their job duties. During a workshop on stress designed for them, subjects volunteered anonymous written anecdotes, confirming and illustrating the findings. The subjects represented locations across the USA and all mining commodities: coal, metal, non-metal, stone, and sand and gravel. The Maslach Burnout Inventory assesses three aspects of experienced burnout: emotional exhaustion, depersonalisation, and reduced personal accomplishments. The average results of the scores for each of the three subscales for the study group of MSHA accident investigators fell in the moderate range. These scores show that the subject population was at some risk for emotional exhaustion and depersonalisation, tending toward burnout. The group evidenced a lower sense of personal accomplishment in their jobs, indicating a higher risk for burnout. From this outcome accident investigators may be at moderate (note: this does not mean average) risk for burnout. The authors recommend follow-up with this population - specifically in training to work with grieving families; and greater organisational support for the accident investigators in this area would be appropriate. Keywords: Burnout; accident investigators; occupational safety and health; job stress.

By Walter R. Storms

"INTRODUCTION The New Mexico potash exploration described herein was begun in February 1944 with the object of determining the amount of potash ore in the United States Potash Reserve in Eddy County by exploring the deposit from the surface with vertical drill holes. The work was completed in October of the same year after 16 holes had been drilled on the Reserve and in the immediate vicinity.The Potash Reserve is in secs. 26; 27, 34, and 35, T. 20 S., R. 29 E., Eddy County, N. Mex., about 14 miles northeast of Carlsbad, as shown on figures 1 and 1A, Drilling was done in secs. 26 and 35 of the Reserve, in section 14 to the north, end sections 2 and 56 to the east. All work was done on Governnent-owned, unleased land.The Reserve may be reached from Carlsbad by traveling to the north-east by automobile for about 14 miles on the paved U. S. highway 62. This highway passes through the southern part of the Reserve. Other parts may be reached by a State highway that passes along the eastern side of the area, then by poor dirt roads to various drilling sites. A branch of the Santa Fe Railroad also passes across the southern part of the Reserve enroute from Carlsbad to the plant and mine of the Potash Co. of America, a few miles northeast of the project and 22 miles from Carlsbad."

Aug 1, 1947

By J. W. Paul

This circular is one of a series of reports on coal mining methods and cost s which are being prepared by the U. S. Bureau of Mines for the purpose of making available to those interested in the industry a knowledge of the mining methods employed in mines where mechanical and hand loading is practiced and the cost data on the several operations pertaining to the removal of coal from the working faces and its transportation to the tipple for loading into railroad cars. The methods employed are influenced by the natural local conditions with respect to the thickness and character of the coal beds and the overlying strata, the means employed for roof support and its control, and the disadvantages incident to the development of mines in thin coal beds.

Jan 1, 1929

By F. E. Griffith

[Unquestionably mine fires new constitute one of the chief causes of sabotaging the effort to produce maximum quantities of mineral products essential to the prosecution of the war. This applies more particularly to coal than to noncoal mines, and presumably the main reason for this is the fact that coal production in maximum quantity is still very much a "must", while the demand for much of the product of noncoal mines has eased materially in recent months.]

Jan 1, 1944

By R. W. Freedman

The gas chromatographic method, devised by the Bureau of Mines for analyzing routine mine air samples, was compared with the infrared method used for confirmatory determination of methane in mine air. While maintaining the specificity of the infrared method for methane determination, the gas chromatographic method is more precise, much more rapidly performed, and more convenient.

Jan 1, 1968

By P. B. Lorenz

Wettability measurements and laboratory waterflood tests were compared under a wide variety of conditions. Experiments were conducted with synthetic and natural crude oils, treated and untreated outcrop and oilfield sandstone cores, and synthetic brines with and without caustic, detergent, or phosphate additives. Measurements were made on equilibrated and unequilibrated systems at 77° and 150° F. Wettability was evaluated by the Bureau of Mines method from capillary pressure curves determined with a centrifuge. The waterflood data were fitted by empirical curves; the parameters of the curves characterize primary and subordinate production and also give the ultimate oil recovery. Results showed that wettability measurements at 77° F were useful predictors of recovery efficiency in waterflood tests run at both temperatures. Oil recovery in the early stages of waterflooding increased with increasing water wettability; however, the ultimate recovery was highest at a slightly oil-wet condition. The oil displaced at highest speed in the centrifuge was correlated with ultimate recovery in waterflood tests. Chemical additives to the brine sometimes lowered wettability and also sometimes improved waterflood recovery, but wettability and recovery were not correlated with additives present. The effect of additives on recovery in waterflooding was best seen in water-oil ratio curves.

Jan 1, 1974

Demonstrate the technical feasibility of using nontraditional, low-rank, coal-based fuels and new coal-based technologies for mineral and metallurgical applications. Approach A cooperative research effort was initiated between the Bureau of Mines, U.S. Department of Energy and the minerals industry to extend the application of the fixed-bed gasification process to low-rank Western coals. The research effort enabled cooperators to gain operating experience in the use of hot, raw producer gas for iron ore pellet induration and other high-temperature mineral processes. Researchers were able to gather data regarding the fundamental engineering aspects of the fixed-bed process and gas cleanup for a wide range of solid fuel properties. Applying Fixed-Bed Gasification As a prerequisite to gathering the data needed for the study, the Bureau of Mines designed and installed, at one of its laboratories, a 6.5-ft-diam. single stage, fixed-bed, air-blown atmospheric pressure gasifier. The gasifier was coupled with a hot, raw gas combustion system and iron ore pellet in. duration kiln. The gasifier is rated at 1.5 ton/h capacity of bituminous coal.

Jan 1, 1987

By Robert E. Wood

The temperature dependency of the low-density viscosity coefficients, ?°T, of helium and of nitrogen, 100° to 1,000° K, is correlated with empirical equations, and the temperature and composition dependencies of the low-density viscosity coefficients, ?°T, of helium-nitrogen mixtures are correlated with the Chapman-Enskog expressions by using the Lennard-Jones (6:12) potential function. The residual viscosity, ?T,P - ?°T (the difference between the viscosity of a compressed gas and the dilute gas at a given temperature), was found to be a function of the thermal pressure coefficient, (?P/?T)V, and two parameters, a and 1, which are characteristic of gas composition. The equation ?T, P = ?°T + a [(?P/?T)V]ß represented 1,340 higher pressure experimental viscosity values with a mean absolute deviation of 0.86 percent, and this equation was used to compute viscosities of the gaseous helium-nitrogen system for a range of temperatures and pressures including those encountered in Bureau of Mines helium purification processes and in a crude-helium conservation gas reservoir. Tabular viscosities for helium, nitrogen, and 13 helium-nitrogen mixtures are presented for 110 temperatures, 133° to 740' K, and 49 pressures in the range 1 to 240 atmospheres. The accuracy of the tabulated viscosities varies because correlation parameters were obtained from experimental data of unequal reliability. It is estimated that uncertainties in the computed viscosity values are ±5 percent for the region 325° to 740° K, ±2 percent for the region 183° to 325° K, and ±5 percent for temperatures below 183° K. The latter uncertainty may rise to y10 percent as critical conditions are approached.

Jan 1, 1970

By R. J. Pokora

This Bureau of Mines report is an applications manual that can be used by the nonmetallic mining industry for guidance in installing noise control materials into crushing and screening plants. These noise control modifications were installed and successfully tested at three operating quarries. This report identifies the major noise sources that can be encountered in crushing and screening plants, and discusses the applicable noise control materials and techniques that a plant operator can utilize on a retrofit basis to reduce equipment noise.

Jan 1, 1984

By J. C. Fowler

[This i.untra t hds bmii III c'IIILt fur till- past 1':?:u yrlr;, Till-- wurir pnrfor rw:it '. ,JS hlui.rn dawn Ilttf lit Iu i eel i ih?IS( S. 1 hesrt aIII, Phase I Candor tlri I a lest It) donurnSlrale SeiSrrlir nurihudS to hu USi!d lot ttlr? rti?tei thin and Iu" ainnl ul trapped rrlinc:rs hitting (-)it the roof with a harnrner, Phase I' Design and cunStrur.t a permanent Seismic monitor System to rrlunrtur roof (ails arm r:xploslun', III ,r 'Vol king mine. Phase III - Ire dII an an i i irr for sVstl rtl Ii i`'Smltur air quality in till, niitii iiH II ? ir,iti tin; niln !III ;I I ,, i; Phase I V - Conduct 11(21 d tests of the seismic IT IUnit UT ieq system fur a period nl two 11IUIIIIIS. Phase, V - Condirct three test periods of the seismic system over a period of six mimilis. Detailed reports covering the wurk. done in Phases I, 11, and IV have been i : . r tr I - i t report will, therefore, cuni.entrate on the work perfurmed in Phases III anti V.]

Jan 1, 1975

By E. C. Hoeman, W. C. Stoecker, R. C. Redfield

"INTRODUCTION Industrial sands, characterized by specific physical and chemical proportion, are,essential new materials for the manufacture of glass, sodium siliante and other products. Sands of suitable characteristics are used extensively for molds and cores in the casting of metals as a granular medium in municipal water filters, as abrasives, as traction sand to prevent the slipping of driving wheels of self-propelled vehicles on trucks and in various ceramic and other structural forms. In addition to the use of common silicon sands in concrete, cement, and mortar, special sands find use in sand-lime brick oxychloride cement, and flooring, for coating prepared roofing, and for placing ware in saggers although sand for sandpaper has been mostly displaced by other harder mineral or synthetic grains, other abrasive uses are numerous and include sandblasting stone sawing, glass burnishing and finishing."

Oct 1, 1945

By Miro Mihelich

The mines and prospects in the vicinity of Landlocked Bay, 25 miles southwest of Valdez, Alaska (fig. 1), were examined, mapped, and sampled in July and August 1955 as part of a comprehensive investigation by the Bureau of Mines of ore deposits adjacent to Prince William Sound. The purpose of the investigation is to establish and record the location, nature, extent, and metallurgical characteristics of copper and associated metallization in the Prince William Sound district and to indicate, if possible, those areas in which additional exploration and development may be justified. Of particular interest are the possibly numerous deposits of massive iron sulfides that were neglected during early mining operations. These deposits may constitute important reserves of sulfur and iron. At Landlocked Bay deposits of copper-bearing iron sulfide minerals have been mined or partly explored through mine workings, which are in a zone about 1 mile wide along the western side of a large overthrust fault known as the Landlock Overthrust. Eight of the principal mines along this zone were examined end sampled. Although only three of the mines have a recorded production of shipping-grade copper ore, all have deposits of copper-bearing iron sulfide minerals that are similar in occurrence. The deposits occur as lenticular masses and disseminations of chalcopyrite, pyrite, and pyrrhotite which replace crushed rock or fill cavities along shear zones in greenstones and in sedimentary rocks that are exposed between sea level and an altitude of 2,500 feet. These lenticular masses of sulfide minerals range in size from small pods to ore bodies that have been stoped to maximum widths of 9 feet, strike lengths up to 70 feet, and dip lengths as much as 350 feet. Where accessible for sampling,, the copper content of the deposits ranged from a few hundredths of a percent to over S percent; zinc, gold, and silver are present in negligible amounts. Flotation tests of a sample composited to represent typical mine-run ore indicate that 81 percent of the copper is recoverable in a product assaying 28 percent copper at a concentration ratio of 17.5 : 1. INTRODUCTION Statistical records indicate that approximately 110,000 tons of metallic copper (about 16 percent of total Alaskan production) was produced from mines adjacent to Prince William Sound during the 40-year period ended in 1938. Although the principal production was from a large-scale mining and milling operation on Latouche Island (Kennecott Copper Corp., Beatson mine), a substantial amount of the total copper was derived from direct-shipping ores selectively mined or hand-sorted from numerous other deposits in the district. No production has been made since 1938; many of the claims have long been abandoned, and mine workings are either caved or deteriorating rapidly.

Jan 1, 1957

By R. L. Andrews

The Bureau of Mines investigated means of electrodepositing iridium to form thick coatings suitable for the protection of such metals as tungsten and molybdenum, which oxidize rapidly at high temperatures. Using a fused sodium cyanide bath, thick, adherent, and coherent deposits of iridium up to 15 mils thick were plated on tungsten and molybdenum substrates at 600° C and current densities of 10 to 100 ma/cm2. Limited oxidation testing of molybdenum encapsulated with pure iridium indicates that the coating may offer protection to approximately l,000° C in flowing air, but that at higher temperatures, the volatility of its oxide limits use of pure iridium. Alloy coatings of iridium with platinum, palladium, and rhodium up to 4 mils thick were formed from a fused sodium cyanide electrolyte; because their oxides are less volatile, these alloys may protect substrates at higher temperatures. Deposits made from aqueous electrolytes either had very low rates of deposition or were highly stressed and cracked when heavy deposits were made.

Jan 1, 1967