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By Fernando Hernández Polanco

Transportation and handling metals and alloys from mills to consumption factories as well as dosing in conventional processes with ingots and scrap has always been considered a complicated activity with high operating costs. Several manufacturers of ferroalloys willing to solve these problems have chosen an alternative for their products that can be used to secure, during transport and dosage in the processes to making special steels, with more efficient consumption of ferroalloys. The trend for the production and sale of ferroalloys is to provide the product in the form of granules packed in bags or in bulk. In this paper we will show you how the granulation process was developed and rapidly adopted the ferroalloys industry as an effective solution to reduce operating costs, create cleaner and safer working environments.

Oct 30, 2017

By Armando Vazquez

When water enters the EAF, some chemically dissociates to H2 while some remains as H2O vapor. Depending on operating conditions the levels of combustible gases (CO and H2) and H2O are continually changing throughout the course of any individual heat and on a heat-toheat basis. The EFSOP® system has been implemented in more than 80 installations as a powerful tool to reduce furnace operation costs but with water detection technology the off gas technology is a valuable solution to improve safety. This paper describes the latest results when using Tenova Goodfellow’s new standalone water detection technology that for the first time provides real-time analysis of both H2O vapor and H2 from start-to-end of a heat. It involves a newly designed water cooled probe and heated line that eliminates condensation during off-gas sampling and an analyzer equipped with a proprietary system for analyzing both H2O vapor and H2.

Jul 30, 2018

By Antonio Augusto Gorni, Kenji Camey, José Herbert Dolabela da Silveira

Recently several studies have been developed on the use of microalloyed steels with low Mn content (below 1%) in the controlled rolling of heavy plates for the manufacture of pipes. However, this novel concept of alloy has peculiarities in its thermomechanical processing. Lower Mn contents should lead to the acceleration of NbCN precipitation kinetics during rolling, leading to a reduction in the soluble Nb content in austenite that delays its recrystallization by drag effect. This fact, plus the heavy and fast passes applied under virtually isothermal conditions in a heavy plate rolling mill with high power, increases the risk of partial recrystallization during the finishing stage of the controlled rolling, since strain hardening of austenite becomes significant and the interaction between precipitation and recrystallization is increasingly delayed. The objective of this study was to analyze the evolution of mean flow stress during the finishing stage of controlled rolling in these low Mn, high Nb microalloyed steels, in order to better understand the metallurgical mechanisms acting during this process and identify conditions that allow full compliance with the requirements of this product class.

Oct 1, 2019

By Rudolf Hubmer

In October 2013 JSW Steel decided to place an order to Primetals Technologies Austria (former Siemens VAI Metals Technologies) for the installation of a comprehensive Level 2 process optimization system for more than 20 existing production facilities of various suppliers. For SMS-I new L2 systems are provided for two hot metal pretreatment stations, three hot metal desulphurization stations, three ladle furnaces, two 1-strand slab casters, a ladle tracking system as well as a shop supervisory system. Additionally the existing L2 system for one 1-strand slab caster is being upgraded in the course of the project. In SMS-II new L2 systems for the 7 hot metal desulphurization stations, 4 ladle furnaces, 1 new RH vacuum degasser, ladle tracking system and a shop supervisory system are supplied. Despite of the challenging time schedule the commissioning of the single facilities started within less than 12 month after contract effectiveness. The installed Level 2 process optimization systems together with the achieved results are described in this paper.

Aug 16, 2017

By Augusto César Barrios Tamayo

The high temperature erosion of Thermal Barrier Coatings (TBCs) is one of the main factors that define the lifespan in gas turbine components as it is considered the second source of failure of hot path components in power and propulsion turbine operation. The worn Top Coat (TC) surface in components such as first stage turbine blades affects the turbine efficiency due to energy losses and the increment in heat transfer to substrate. The first part of this work consists in describing a HTE test facility developed to emulate the damage conditions found in a number of components of gas turbines; in this testing machine, the samples were exposed to combustion gases moving at velocities close to 1.5 Mach and temperatures of 1100°C. The second part consists in the characterization of liners and first stage turbine blades of a GE7FA gas turbine used for power generation. The last part deal whit correlation of the features of TC’s worn surfaces with the erosion conditions and the dominant degradation mechanisms between test samples and turbine components were compared.

Jul 31, 2018

By Débora Cardoso de Oliveira Silveira, Jean-Christophe Huber, Hamzeh Hamadeh, Kateryna Pastel, Guillaume Brosse

The dynamic behavior of oxygen gas flow, determined by the lance nozzle and blow pattern, is a key factor for determining jet efficiency in BOF Steelmaking. The present work compares the performances of Laval and parabolic nozzles with the aid of the Computational Fluid Dynamics (CFD). The Method of Characteristics (MOC) was applied to design a minimum length parabolic nozzle. The results show that the parabolic nozzle generates more uniform and stable jet, with 2% longer potential core and supersonic length and less shock waves. For the parabolic nozzle, the pressure nearby the nozzle wall is higher, which can protect this region from reverse flow of converter gases and offer longer life for the lance tip. Likewise, the flow rate variations would affect less this nozzle. In addition, the nozzle wear was investigated, and the parabolic nozzle has proven relatively less sensitivity to the presence of this deformity.

Oct 1, 2019

By Julián Andrés Ortiz González

This work presents a series of experiments of Fatigue Crack Growth (FCG), which are intended to provide evidence about the main parameter controlling this phenomenon, whereas still no agreement about this, since the Paris´ theory is based on the principle that FCG is controlled by the ?K and the Elber´s theory says that the driving force is ?Keff. For the development of the experiments, some DC(T) specimens were machined with two different thicknesses: 2 and 30 mm to perform FCG tests in plane stress and plane strain state, respectively. Besides this, all FCG tests were carried out with a constant ?K e Kmax, measuring the strain with a Strain-Gage bonded on the back face of the specimen and seven Strain-Gages located on the crack growth path. The data needed to measure the crack opening load, and the ?Keff, were collected through a program developed in Labview. Finally, the data post-processing was carried out based on the ASTM standards and several articles of recognized authors in this field, in order to compare the two positions with the experimental data, and this way conclude which is the most consistent theory with the observed behavior.

Aug 16, 2017

By Daniel Augusto Godinho de Carvalho

Since the beginning of BOF process, slag formation has been subjected to extensive development. During the initial stages of the blow, fast slag formation is primordial for the process performance. This is mainly to allow oxidizing reactions, and also to protect the refractory. A modeling of BOF process for the purpose of process optimization requires precise knowledge concerning the dissolution of CaO and MgO based materials. Using this knowledge, the optimal process conditions can be ensured by a controlling of the slag formation during the converter steelmaking process. Taking into account an application of large amount of different raw materials, as well as location-specific process conditions, the characterization of the dissolution behavior of different additives is an important key to improve the technological process. Thereby, in the frames of this project, an appropriate model for slag formation is established and compared to operational results for a 330t BOF, operating at ThyssenKrupp CSA, Santa Cruz, Brazil.

Aug 16, 2017

By Uwe König

Traditionally quality control of iron ore sinter, its raw materials and raw mixtures has relied on time-consuming wet chemistry. The mineralogical composition that defines the properties is often not monitored. XRD analysis in combination with Rietveld quantification and statistical data evaluation using Partial Least-Square Regression (PLSR) has been successfully established to determine the mineralogical composition and process parameters such as the FeO (Fe2+) content and basicity of iron sinter within an analysis time of less than 8 minutes per sample. Both methods take the full XRD pattern into account and can be simultaneously applied on the same measurement. In addition the Rietveld method was used to quantify the phase content of raw mixtures to monitor the composition of blending beds.

Aug 16, 2017

By Johanna Alegría-Ortega

Cr/CrN bilayer coating was deposited on AISI 440C by Cathodic Arc. The composition and structure of the Cr/CrN coating were investigated by scanning Electron Microscope, X-Ray Diffraction and X-ray Photoelectron Spectroscopy. The results show that crystal structure obtained was CrN phase with preferred [220] orientation. The hardness and adhesion of coating also were studied. The evaluation of erosion-corrosion (EC) on 440C bare and coated with Cr/CrN was performed by carrying out wear tests using a slurry jet with impingement angle 90° at 4 and 8 m/s. Corrosion, erosion and synergism wear rate were evaluated following the procedure described in ASTM G-119-09. This study presents that the synergism wear rate exceeds 40% of the total mass loss for coating and 60% of mass loss for the 440C, being the most aggressive wear component. The increase in impact velocity generated a rise in mass loss for both 440C bare and coated. The Cr/CrN coating offers better corrosion and erosion–corrosion resistance under all the tested conditions.

Aug 8, 2018

By Rodrigo Perito Cardoso

Low-temperature nitriding of stainless steels is applied to obtain wear resistant surfaces without losing its corrosion resistance. The treatment consists in introducing nitrogen into the steel surface avoiding chromium nitride precipitation. The corrosion resistance of martensitic stainless steels is expected to be improved if the treatment parameters are correctly selected. It can be related to ?Fe2-3N and a'N phase formation on the treated surface. In the present work the influence of the pretreatment and treatment temperature on corrosion resistance of plasma nitrided AISI 420 steel samples is studied. Annealed, as-quenched and 400ºC-tempered samples were nitrided at 300, 350, 400, 450 and 500°C, for 6 h at 600 V. The pressure was 3 Torr and the gas mixture was composed of 70%N2, 20%H2 and 10%Ar, at a gas flow rate of 3.34×106 Nm3s-1. Plasma was generated using a square-wave pulsed DC power supply and the sample temperature was controlled by the duty cycle. The modified layers were characterized by optical microscopy, X-ray diffraction and microhardness measurement. The corrosion resistance was studied by electrochemical characterization, by means of Open circuit potential and Anodic polarization curves. The maximum surface hardness was achieved at 400°C. This temperature seems to be near the limit temperature for low-temperature treatment aiming to improve or at least to keep unaltered the corrosion resistance in relation to that verified for non-treated steel samples. Results confirm that the pretreatment and treatment temperature significantly affects the corrosion resistance of the treated surface.

Aug 8, 2018

By Jorge Madias

Pin holes as a surface defect, and blow holes as an inner defect, occur in billet / bloom / beam blank casting, particularly for Si-Mn killed steel cast with metering nozzle and oil lubrication. If they are present in abundance or have a large size, they may originate defects in the rolled products. Their characteristics, factors behind their formation, as well as usual processing conditions that promote their occurrence are discussed. Finally, the evolution of these defects during reheating and rolling is analyzed, with industrial examples.

Aug 16, 2017

By Ivan César Lopes Diniz

Stretcher Reducing Mill (SRM) is a mill used in production of tubes. It is composed with a set 24 of stands responsible to define the final outside diameter (OD) of tubes. External appearance is critical in this process even though this requirement has no effect on mechanical properties. For this reason, an investigation of external longitudinal marks mechanism is in progress using 6 Sigma methodology. This paper is a part of the investigation with focus on the rolls and its mechanical properties. Destructive tests were performed in the rolls and compared with the project. After a detailed investigation, it was concluded that rolls were out of hardness specification and the project was poor of information. A new supplier was developed (internal market) based on the new project and all requirements were achieved as demonstrated in this paper. A monopolistic market for this product in VSB (Vallourec Soluções Tubulares do Brasil) was eliminated. Concerning the effect on the external longitudinal marks, the new rolls developed within hardness range minimized the mechanism of wear on rolls surface and consequently on tubes surface. A collateral effect has been faced, but still better than external longitudinal marks on tubes surface. The quenched and tempered rolls are more sensitive for process variation, mainly linked with cooling system and temperature of tubes (mechanical resistance for deformation). Nevertheless, a new material has been aimed focusing on reduction of rolls breakage with good tenacity and affordable cost.

Oct 4, 2019

By Luiz Alberto dos Santos

. In this work, samples of the alloy with composition of 50.9 % at. Ni were machined and were subjected to hot tensile test, after the machining all the samples were solubilized so that all were in the same condition during the hot tensile test. The hot tensile tests were performed between the temperatures 350-650°C and the yield stress were between 800 and 597.1 MPa and area reduction between 17 and 75% with respect to the initial area. The test at 350°C shows a fragile fracture characteristic while the hot tensile test above this temperature showed a predominantly ductile fracture. The fragile fracture is evidenced by the river marks that are characteristic of this type of fracture, because in this condition does not promote much plastic deformation. The higher temperatures present ductile fracture, because present the dimples that also characterize this type of fracture. This work shows the temperature relationship in the mechanical properties, more specifically the hot tensile test, in the NiTi alloy.

Oct 30, 2017

By Edo Engel

Whereas only a handful of decades ago, typical blast furnace working volumes were below 1000 m³, such furnaces are currently designated compact or even mini blast furnaces. For certain business cases, however, small furnace sizes remain an attractive option. Decades ago, this size blast furnace would have produced a maximum of 0.3 Mtpa with its 600 m³ working volume over a campaign of up to four years. The current state of technology and operational know–how will allow a similarly sized furnace to produce over 0.7 Mtpa while achieving the multiple decade campaigns that have become familiar to steel producers in full sized operations. This level of productivity, but especially the reliability and supply security associated with mature technology, allows for integration into minimills or taking a first step towards a full scale BF–BOF integrated mill. Steel producers considering such scenarios, which are typically attractive for emerging economies, are confronted with fundamental decisions, one of which is for the technological basis for the compact or mini blast furnace to be included in the plant. This article addresses some of these decisions from an operations–based perspective. A small number of case studies is included.

Aug 16, 2017

By Andrea Zanon

Slitting processes have been used for many years to increase the productivity of smaller diameter deformed bars, without making major investments in the rolling mill. This technology is used mainly for the production of reinforcing bars (7-20 mm diameter), but successful applications exist also for round bar production. The multi-slitting process enables to produce up to 5 bars starting from one billet, thus increasing the productivity of the smaller products. Danieli Morgårdshammar, world leader in the supply of rolling mills for long products, has been a front-runner in slitting technology since its first applications and has recently developed, first in the world, the technology to produce 5X8mm rebar. This process has been recently applied in BRSM steel, a company based in Bangladesh which is a worldwide benchmark for slitting technology performances. This paper presents the necessary modifications which need to be considered when developing a 5-strand slitting project (and multi-strand slitting projects in general), as well as the results obtained at BSRM Steel when the process was implemented in 2016, the first rolling mill in the world rolling 5X8 mm slit rebars.

Oct 30, 2017

By Dilermando Nagle Travessa

High strength-light weight materials are very attractive for the transportation sector, particularly to the aerospace industry. High strength-age hardenable aluminium alloys are widely used in airframes due to their unique combination of strength, density, toughness, corrosion resistance, cost and easy processing. However, the hardening capacity of such alloys is somehow saturated due to thermodynamic issues related to the conventional processing. The production of aluminum-matrix composites is a promising strategy to overcome this limitation, resulting in strength levels that cannot be reached by actual commercial aluminum alloys. In the present work, multiwall carbon nanotubes were used to reinforce the AA6061 aluminium alloy. 1 and 2% weight percent of MWCNT were mixed to the alloy powder by high-energy ball-milling process. The blended powder was consolidated by hot extrusion. The obtained composite bars were submitted to heat treatment for the T6 condition in order to combine both CNT dispersion and precipitation hardening effects. Optical and scanning electron microscopy, as well as hardeness testing, was used to characterize the bars. Typical wrought microstructure, free of defects, was observed on the extruded bars. Hardness of the composites was observed to increase by 20, 28 and 68% for 1% MWCNT 6 h milling, 2% MWCNT 6 h milling and 2% MWCNT 10 h milling, respectively, in the as-extruded condition. The better performance for the composites blended at higher milling time was attributed to a better nanotubes dispersion. Subsequent heat treatment to the T6 condition did not result in additional hardening.

Aug 8, 2018

By Mingyu Ma, Lingling Liu, Liqing Chen, Houlong Liu

In this article, a 444-type heat-resistant ferritic stainless steel containing 0.05wt% Ce and 2wt% (Mo+W) was used as an experimental material and a study was carried out on the effect of rolling processes on the microstructures and texture evolution as well as on the mechanical properties and formability. The rolling processes contain hot rolling at different hot rolling finish temperatures, annealing after hot rolling, cold rolling and subsequent annealing. As for the hot rolling process, two hot rolling finish temperatures, 860 C and 770 C, were adopted, and their influence on the microstructures and mechanical properties was comparatively studied. The results showed that the microstructures after hot rolling and subsequent annealing could be refined by lowering the hot rolling finish temperature. The resultant microstructures after cold rolling and annealing were hereditarily refined. Lowering the hot rolling finish temperature can weaken the -fiber texture in hot rolled or cold rolled ferritic stainless steel strip. However, the -fiber texture was homogeneously strengthened by annealing the cold rolled ferritic stainless steel strip. Enhanced mechanical property and formability in terms of strength and average plastic strain ratio could be obtained by lowering the hot rolling finish temperature of ferritic stainless steel.

Oct 1, 2019

By Charles Sóstenes Assunção

A mathematical model of heat transfer and solidification for a continuous casting of round billets was developed. The water flux density of the secondary cooling zone was experimentally measured, using an apparatus in industrial scale with two types of nozzles, flat jet and full cone jet. The profiles of water distribution were applied on the mathematical model. The results showed that the water distribution is not uniform in both longitudinal and angular directions owing to the unevenness of the spray and to the curvature effect of the round billet. This non-uniformity causes important variation of the heat transfer coefficients and superficial temperature of the billet, especially in the first cooling zones, where the temperature is higher. The mathematical model was used to simulate a change of nozzle type in the first cooling zone. The results showed that the heat flux and superficial temperature variations were reduced with a full cone jet nozzle in comparison with the flat jet nozzles.

Aug 16, 2017

By Felipe Darabas Rzatki

Polyether ether ketone (PEEK) is a high performance thermoplastic often selected for high temperature tribological applications under chemically aggressive environments. The present work evaluate the tribological behavior of a high performance PEEK composite under ambient and high temperature (30 and 80°C, respectively). The atmosphere was also varied (air or tetrafluorethane). An AMTI tribometer equipped with a hermetic chamber and a heating system was used to carry out sliding tests of PEEK cylinders on 304 stainless steel polished discs (Sq < 10 nm) with reciprocating movement and 175 N normal force. Surfaces roughness analyses were performed with a white light interferometer. As expected, there was a strong influence of temperature on the tribological behavior of the samples tested in ambient atmosphere (25% decrease in friction coefficient associated with a 100% increase in wear rate). On the other hand, samples tested in tetrafluorethane atmosphere showed no significant friction temperature dependence.

Jul 31, 2018