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By E. V. Koporulina, E. L. Chanturiya, M. V. Ryazantseva, E. S. Zhuravleva

"The morphology of the surface of sphalerite, galena and chalcopyrite and the adsorption of butyl xanthate under conditions of preliminary treatment of minerals by the products of water electrolysis were studied using atomic force microscopy (AFM) and Diffuse Reflection Infrared Fourier Transform Infrared Spectroscopy (FTIR). It was determined that practically all types of treatment by electrochemically modified water (a product of non-diaphragmatic treatment, anolyte and catholyte) lead to an increase of surface roughness of the studied minerals due to formation of small rounded shape particles. In contrast to that, after treatment of chalcopyrite by anolyte, its surface becomes smoother. Various effects of treatment by the water electrolysis products on the adsorption of chemical and physical forms of butyl xanthate on the studied sulfides were established. As a result, the efficiency of the complex of AFM and FTIR methods, as one of the ex-situ approaches for monitoring the surface state of sulfide minerals and direct investigation of BKx adsorption products was demonstrated.INTRODUCTION In mineral processing, copper-zinc sulfide ores are one of the most complex products in view of their mineral composition, fine dissemination, complex inter-growth and the proximity of the technological characteristics of copper, zinc and iron sulfides. For the most complete disintegration, fine grinding of ores to a size of 0.074-0.044 mm is necessary. Consequently, the main method for processing of such ores is flotation, which bases on the difference in physical and chemical properties of the mineral surfaces, in particular, degree of wettability. The separation of copper and zinc minerals and their separation from ferrous and other sulfides, sulfosalts and rock mineral is a very difficult task (Chanturiya, 2000). For the successful separation of copper and zinc minerals in the appropriate selective concentrates, it is necessary to find conditions for the most complete liberation of ore and rock-forming minerals and for increase the contrast in physical and chemical properties of their surfaces. Despite significant progress in the processing of copper-zinc sulfide ores, the problem of the selectivity of the separation of the main ore minerals has not yet been fully solved and requires innovative approaches (Chanturiya, 2015). To date, various methods of preliminary energy processing of complex ores are used: magnetic pulse treatment, impact by high-voltage nanosecond pulses, electrochemical effects (including products of water electrolysis (Chanturiya et al., 2014; Bunin et al., 2015; Chanturiya et al., 2014a; Chanturiya et al., 2016), processing with flotation reagents, etc. Electrochemical treatment of water in various modes allows to obtain products of electrolysis with different oxidation-reduction properties: acid anolyte with a high oxidation potential and dissolved oxygen content, an alkaline catholyte with high reducing properties and a product of non-diaphragmatic treatment with enhanced reduction properties."

Jan 1, 2018

By V. Z. Sun

One of the major concerns of ground control in a coal mine is safety against failure of one of three components (i.e. roof, pillar, or floor) of the mine entry. In order to better design and evaluate stability of the mine entry with a certain confidence, a reliability approach is introduced rather than using the conventional safety factor (SF) method only. Advantages of using the reliability approach is that it not only takes variability of both rock/coal properties and stress distribution into consideration, but also assesses the stability of each component and mine entry as a whole system. Therefore, it is anticipated that, by using this approach, the current ground control technology in coal mine will convey a better sense of confidence. The results of a case example show a significant influence on the current design concept and stability evaluation of mine entry.

Jan 1, 1997

By K. Schimann, H. D. Knipping, J. P. Fouques

"The Cigar Lake uranium deposit, in the Athabasca area of north Saskatchewan, was discovered in May 1981 by Cogema (Canada) Ltd., as operator of the Waterbury Lake Joint Venture.The deposit, which is devoid of direct surface expression, is located at the unconformity between the Lower Proterozoic (Aphebian) Wollaston Group meta-sediments and the Middle Proterozoic (Helikian) Athabasca sandstone, at a depth of 410 m to 450 m below surface.At the end of 1984, the deposit had been defined by 105 mineralized holes over a length of 1800 m and a width of between 25m and 105m. It has the shape of flat-lying /em 5 m to 30m thick and shows a remarkable longitudinal and lateral continuity from the information obtained to date. A well defined bulge of the unconformity underlies the mineralized zone over its entire length.The deposit appears to be controlled by an east-west trending structure within which a particular rock facies (""augen gneiss'') has developed in the graphitic metapelites of the Wollaston Group. It is surrounded by a strong alteration halo affecting both sandstone and basement, characterized by extensive development of Mg-AI rich clay minerals (illite-chlorite). The mineralization is hosted principally by the Athabasca sandstone, and consists mainly of uraninite and sulfa-arsenides of nickel and cobalt. Numerous geochemical and geophysical surveys have been carried out in the Cigar Lake area, and although no specific geochemical or geophysical anomaly can be directly associated with the mineralized body, there may be locally a good coincidence.However, a combination of several methods proved extremely useful in interpreting the regional geology and defining the drilling targets within the favourable areas.Although the Cigar Lake deposit shows many similarities with several classical deposits of the Athabasca region, it is characterized by the intensity of its alteration processes and the presence of massive, extremely high grade mineralization.At the end of 1984, the global geological reserves estimated by geostatistics on the main mineralized ""pod"" of the deposit amounted to 110,000 metric tonnes of uranium at an average grade of 12.2% U, with a precision of 25% at the 95% confidence level."

Jan 1, 1986

By M. J. S. Innes

Abstract This paper is an account of an investigation made by the Dominion Observatory with a gravity meter and magnetometer over sulphide concentrations at East Sullivan, Val d'Or, Que., in June, 1947. The topographic relief over the area does not exceed 20 feet. The overburden varies from 0 co 50 feet. The west orebody had been outlined by extensive drilling. The average density contrast between the sulphide body and surrounding rocks is 0.5. Two hundred and sixty gravity and one hundred and ninety magnetic stations were observed. The results are shown on contour sketches. A derailed account is given of the methods employed to reduce the gravity observations. The survey shows that both gravimetric and magnetic methods are useful in delineating sulphide deposits under the conditions in which they occur at East Sullivan. The results indicate that the buried contact of the syenite intrusive southeast of the orebody could be traced with the gravimeter and chat the magnetometer was of little value for that purpose. Gravity anomalies due to the varying depths of overburden are negligible as compared to the magnitude of the total anomalies. Introduction The project was first suggested at a meeting of the Associate Committee on Geophysics of the National Research Council in September, 1946. At that time it was pointed out that the accuracy and speed of operation of the new gravity meters made them of special importance for geophysical prospecting and it was highly desirable to have an objective test of the performance of an instrument of this kind in delineating an orebody of known dimensions and density characteristics. Several years ago, a private company did some work with a gravimeter over the Amulet deposits, near Noranda. Unfortunately, the topography there is rather rugged, with hills and ravines exceeding 100 feet, so that the topographical effects rendered it impracticable to distinguish between anomalies due to the sulphides and those due to surface irregularities. An orebody of a typical nature, where the disturbing topographical corrections were not excessive, was therefore sought.

Jan 1, 1949

By Joseph Sofra

It has become increasingly evident that sustainable metals production in the 21st century requires producers to balance the needs of cost effective, high value production with that of responsible plant operation. This is becoming more difficult as lower grade and more complex feed materials, including recycled scrap and residues, are being processed to reduce production costs and decrease exposure to primary metal market fluctuations. One particular facet of the metals industry facing these challenges in the 21st century are copper producers, The recent steady decline in the copper price has seen the industry cut expenditure, tighten control on income streams and focus on high returns on capital investment. For these reasons copper producers are looking towards flexible technologies that can deliver high value products, with minimal environmental impact at low capital and low sustainable operating costs. Ausmelt's Top Submerged Lancing (TSL) technology for copper production is a low cost, proven technology for the processing of both primary and secondary copper materials. Both the smelting and converting operations introduce significant advantages in environmental performance, improved process efficiencies and high rates of metal recovery, Ausmelt has made significant gains in the past 4 years in establishing a strong market position for its copper technology, New installations in China, South Africa and India as well as existing operations in Zimbabwe and China have demonstrated its effectiveness. This paper reviews the application of Ausmelt Technology for both smelting and converting of primary and secondary sources, It discusses Ausmelt's design and implementation philosophy, and how this philosophy meshes with the needs of the end user.

Jan 1, 2003

By B. Tolwinski

Long-Term Open Pit Scheduler or L-TOPS is a new software package for evaluating, planning, and design of open pit mines. L-TOPS transforms geological, economic, and technical information about a mineral deposit into a detailed mining schedule that maximizes economic efficiency without neglecting the practical requirements of mining operations. L-TOPS has been customized for integration with Placer Dome Inc.'s existing in-house resource/reserve optimization software to function as a primary tool for property acquisition studies and for the designing of mines for feasibility studies. This pa-per presents an overview of L-TOPS and reports on its application to Placer Pacific's (Placer Dome's Australian affiliate) Mt. Rawdon project.

Jan 1, 1996

By M. Hozayen, Q. Ni, E. S. Radwan, P. Nawrocki, A. Jebbouri

"A major geomechanical study was conducted for one of the UAE onshore oil fields with the purpose of studying reservoir rock properties and stress distribution, based on which a 3D coupled reservoir geomechanical model was built. This model was later used for wellbore stability analysis and for analyzing the effect of fractures on future reservoir production performance, including fracture deformation and permeability evolution occurring due to reservoir depletion and resulting changes in local stress field. The subject of this study was a complex fractured Upper Cretaceous carbonate reservoir characterized by high degree of heterogeneity, both vertically and laterally. Wellbore instability related drilling problems were encountered while drilling the wells in this field. The problems were mainly in drilling the horizontal wells, including breakouts and mud losses. Experimental results of laboratory tests used in this study are summarized in Part I of this paper whereas wellbore stability analysis and formulation of a3D geomechanical model that was built for that purpose is summarized herein.A 3D geomechanical reservoir model was developed, which included natural fractures. The mechanical properties of the reservoir rock, such as Young’s modulus, Poisson’s ratio, UCS, friction angle and tensile strength were populated based on the correlations established in Part I of this paper and the developed model was then used to simulate the 3D mechanical-property distribution and the evolution of the in situ stresses in the field due to depletion from 1983 to present-day. Based on the full field model, mud weight cubes were developed to predict the safe mud weight windows in different drilling directions. In addition, well stability prediction for two planned wells was performed using a 3D near-borehole model. Firstly, the computed stress state and mechanical properties simulated in the full field model were extracted along the well trajectory of an existing horizontal well which was drilled recently and then, a3D near-borehole model was constructed along the well trajectory. The wellbore stability analysis along the well trajectory, including stress state, strain distribution and displacements, was performed to identify the instability events along the well trajectory. It has been seen that the presence of natural fractures is closely related to the recorded borehole instability incidents. The computed plastic strains which indicate the wellbore failure were consistent with the recorded wellbore instability events in the FMI image logs, what provide further verification of the developed model. Then, this 3D near-borehole model was applied to two planned horizontal wells and the wellbore stability analysis for the two wells was carried out.The results showed that drilling vertically in the reservoir is safer than drilling horizontally. However, the drilling mud weight window in the vertical direction is narrow, being as narrow as 18.7 pcf or 0.299 sg locally. Drilling horizontally is less stable towards the maximum far field stress direction than towards the minimum far field stress direction. The mud weight cubes were used to identify the optimal well placement and well trajectory. For planned well trajectories, this technology can also be used to determine the optimal mud weight."

Jan 1, 2015

By Pawan Bharadwaj, Wim Mulder, Thomas Tscharner, Guy Drijkoningen, Rob Jenneskens

"The Earth’s properties, composition and structure ahead of a tunnel boring machine (TBM) should be mapped for hazard assessment during excavation. We study the use of seismic-exploration techniques for this purpose. We focus on a seismic system for soft soils, where shear waves are better and easier to interpret than compressional waves, as has been shown over the last decade. The system is intended to be deployed on the machine’s cutter head, with a few seismic sources and sufficiently many seismic sensors to tackle spatial variability and noise characteristics. An important property of the newly developed system is its ability to process data with very little human interaction. Images need to be available in near real time, without human interactions slowing down the imaging process. This can be achieved by employing Full Waveform Inversion, which minimizes the difference between modeled and observed data. Because this method may suffer from local minima in the cost function if the data lack low-frequency information, we employ a dedicated seismic source that can generate sufficiently low frequencies for the relevant length scales. With data acquired in a number of field settings that mimic realistic TBM configurations, we show that the designed seismic system can successfully look ahead of the TBM and offers a valuable capability to support decision-making during tunnel excavation. INTRODUCTION While excavating a tunnel with a Tunnel Boring Machine (TBM), the geology and the ground conditions along the planned tunnel trajectory need to be investigated in order to safely and efficiently carry out the underground operations. This entails detecting the occurrence of boulders, foundations, pipes and faults, necessary to prevent hazards and time-consuming delays in the tunnel boring operations. In order to facilitate ground prediction ahead of a TBM, techniques as used in seismic exploration can be deployed. Two components common to seismic-exploration techniques are data acquisition and processing, the latter including inversion. We will discuss each of these for the application to tunnel excavation with TBM, in particular for soft soils."

Jan 1, 2016

By O. D. Maurice

"This paper will essentially update the information that is already known and published on the limestones of the Province of Quebec. The excellent report by M. F. Goudge (1935)m is difficult to improve upon and the areas of limestone quarrying are generally the same as they were at the time of Goudge's report. Our knowledge of the limestones of Quebec has been improved considerably in recent years by the publications of T. H. Clark, 2 who, since 1938, has been mapping and reporting on these lime-stones and has discussed their stratigraphy, their structural features, their history and their economic value. One economic aspect is the presence of natural gas in these formations and the possible occurrence of oil. A total of 150 test holes had been drilled to a depth of more than 500 feet by the end of 1967 and, in addition, at least 256 more shallow holes had been put down in the St. Lawrence Lowlands. The information from these test holes has greatly improved our knowledge of the thickness and extent. of the various formations of Paleozoic limestone and shale in Quebec.This paper will then review briefly the limestone occurrences in Quebec, using the old as well as the more recent reports as principal references"

Jan 1, 1970

By A Hosseinzadeh Barforoosh, A Abedi, M Taji

The effect of blast loads on beams is one of the main issues in the analysis of steel structure. In this study, experimental tests on steel beam under blast loading, and also numerical simulation by the Autodyn software to analyse these structures, is discussed. Experiments on steel beam size of 12 by Emulite4 explosive with 30 mm diameter and cortex is done. The patterns of cutting and bending generated in the two tests (empirical and simulation) show a good match.CITATION:Taji, M, Hosseinzadeh Barforoosh, A and Abedi, A, 2015. Comparison of experiment and simulation of blast loading on the steel beam, in Proceedings 11th International Symposium on Rock Fragmentation by Blasting, pp 161–168 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 24, 2015

By S Van Duin, I Porter

This paper discusses how advanced manufacturing technology (AMT), which is fundamentally reliant on and developed via multi-disciplinary skills, has benefitted non-mining industries, and what lessons can be derived from this experience to benefit the mining industry, particularly underground coal mining. Examples of AMT use in æconventionalÆ industry, some drawn from the more than 25 years experience in many different industries of the Automation and Robotics team at the University of Wollongong, are described to show typical benefits, risks and opportunities expected in using AMT. Applying AMT to mining brings many unique challenges and this paper expands on these and then provides practical examples of how a multi-disciplinary team can develop new processes and systems leading to productivity, safety and other benefits for underground coal mining.

Sep 26, 2011

By M. Botz

Alacer Gold Corporation is constructing the Çöpler Gold Mine in eastern Turkey. Mining commenced in the fourth quarter of 2009 and gold production started in the fourth quarter of 2010. The mine is a 15,500 t/day oxide heap leach with three-stage crushing, agglomeration, carbon adsorption and electrowinning for final metal recovery. Leach solution copper levels are expected to be relatively low during the first two years of production, but will increase in later years due to higher copper content in the mined and processed ore. Over the mine life, approximately 40 Mt of ore will be placed on the leach pad, which will contain about 35,000 t of copper. Metallurgical testing indicates copper extraction will vary by ore type and, if controls are not implemented, may lead to copper levels exceeding 1,000 mg/L in pregnant solution. High copper levels in leach solution have the deleterious effect of increasing cyanide consumption and potentially overwhelming the ability of the carbon circuit to effectively adsorb the principal economic metals, which in this case are gold and silver. Using data obtained from laboratory leach column testwork, the heap leach facility was modeled using METSIM process simulation software to estimate the build-up of copper in leach solution over the life of the mine. Laboratory testwork was also performed to evaluate process conditions for treating a portion of pregnant leach solution via sulfide addition to precipitate saleable copper as copper sulfide (Cu2S).

Jan 1, 2011

By Luisa Pérez, Carlos Perea

En el caso de la minería de zinc es común emplear el método de explotación por subniveles, el cual exige rellenar los caserones vacíos, por ejemplo, con una mezcla del relave producto de la planta concentradora de mineral con un 3.5% de cemento, lo que actúa como pilar de sostenimiento de la mina (0.8 MPa). Debido a que al momento de avanzar en los tajos aledaños se producía una dilución con el mineral a explotar y, también, a que era necesario automatizar las operaciones; se decidió evaluar el relleno detrítico cementado, mediante análisis de resistencia, estudios de factibilidad, rendimiento en costos, aumento de productividad y seguridad en la operación. Como resultado, se obtuvieron valores máximos de resistencia de los pilares de 1.6 MPa, lo que evitó la dilución y mejoró el porcentaje de recuperación de mineral.

Jun 30, 2020

By P. Somasundaran

Treatment of mineral surfaces with appropriate surfactants plays an important role in mineral processing operations such as flotation, flocculation and dewatering. Recently biosurfactants, in particular, have received a considerable amount of attention because of their unique surface active properties and biodegradability. In this work we examined the performance of biosurfactants, sugar based alkyl glycosides and sophorolipid esters as reagents to control the hydrophobicity of minerals with selectivity of adsorption on mineral surfaces for flotation applications. It was discovered that n-dodecyl-ß-D-maltoside adsorbs on alumina, titania and hematite but, interestingly, not on silica. The hydrophobicity obtained is governed both by the surface coverage as well as the nanostructure of the adsorbed layer in terms of orientation of the adsorbed species. Surprisingly, even though the above surfactants are non-ionic, their adsorption was pH-dependent. We have correlated this pH dependence to the type of species on the mineral surface. Also it is shown that mixing of these surfactants with traditional ones can help reduce the carbon footprint due to synergy between the reagents and help selectivity due to antagonism. The experimental results were analyzed to get information on optimal pH and dosage conditions, for mineral surface modification. The study provides guidance for mineral treatments using biosurfactants and the potential use of these next generation reagents in mineral processing.

Jan 1, 2014

By R. Lestari

Newmont Batu Hijau operates with an accelerated mining rate to optimize life of mine (LOM) project economics. This results in a portion of ore mined being stockpiled for reclaim and processing throughout, and at the end of mine life. LOM economics can be further enhanced by preserving stockpiled ore value by mitigating oxidation effects. A detailed stockpile ore oxidation study was conducted to: ?? Develop a practical understanding of how oxidation affects ore value; ?? Determine how oxidation rate can be controlled, and; ?? Determine how oxidation effects can be mitigated to preserve ore value. The result of the study is a stockpile management strategy that significantly reduces oxidation related losses and, implementation of that strategy within practical constraints. Implementation includes installation of Controlled Potential Sulfidisation (CPS) flotation to facilitate oxidised sulfide copper recovery and, recovery of dissolved copper from stockpile drainage solution into saleable product. This paper describes the study results including managing and predicting stockpile oxidation with time, monitoring performance of implemented CPS flotation and recovery of dissolved copper from stockpile drainage. These are essential elements of successful long term mine operation in Batu Hijau.

Jan 1, 2014

An iridium oxide coated titanium electrode was tested as anode in copper electrowinning. Initial results confmed that the DSA-type anode was significantly more active for oxygen evolution than traditional lead anodes. However, during longer runs, the anode potential was observed to increase linearly at a rate of 220 mV/year. Scanning elecuon microscopy (SEM) and energy dispersive spectroscopy (EDS) showed that the anode passivation could be attributed to elecuochemical dissolution of the coating. The effect on the anode potential of organic additives (glue and thiourea) and lead in solution was also examined. A preliminary economic evaluation of the anodes is given.

Jan 1, 1992

By MacDonald AJ, Raffield MP

The South Deep massive orebody consists of 20 to 30 in of payable conglomerates ranging in dip from 11¦ to 20¦ and at depths of between 2400 in and 34(10 in. The mine design process selected a mining method with a proven record of application that could be adapted to overcome the inherent difficulties associated with the depth, thickness and structural influences of the South Deep orebody. A modified cut and fill mining method provides a concentrated and highly flexible method of extraction. An integrated destressing cut will enable the modification of the stress environment such that it is suitable for massive mining operations. The choice of backfill type and stoping width in the destressing cut ultimately determines the characteristics of the stress modification and, as such, is critical to the success of the cut and fill operation. This paper discusses the decision process undertaken to determine the optimum backfill type and stoping width combination in terms of, conditions in the destressing cut faces and in the massive mining environment. Numerical modelling has been extensively used to analyse arious scenarios to aid in the decision process.

Jan 1, 1998

By David R. Jessey

An ore microscopic and geochemical study of the nickel-cobalt occurrence in the Southeast Missouri Mining District has revealed several significant relationships. Siegenite [(Ni,Co)3S4] is the dominant nickel-cobalt sulfide in the ores, however, several other members of the thiospi¬nel group (AB2S4) occur: carrollite (CuCo2S4), nickelean carrollite [(Co,Ni,Cu)3S4], fletcherite [Cu(Ni,Co)2S4] and polydymite (Ni 3S4). In addition, bravoite [(Ni,Fe)S2], vaesite (NiS2), millerite (NiS) and gersdorffite (NiAsS) are present. Thiospinel composition varies dramatically within the district. Paragenetic studies have shown that the stratigraphically lowest thiospinels are the most cobalt-copper-rich. A detailed ore microscopic study of the AMAX Lead Company Buick mine has also shown significant changes in mineralogical association, texture and grain size of the siegenite along the north-south strike of the major ore bodies. Siegenite commonly replaces and veins chalcopyrite and is subsequently replaced by sphalerite. Less commonly, siegenite and chalcopyrite are observed to form linear replacements along sphalerite grain boundaries. The grain size of the siegenite varies markedly, but in a predictable north-south pattern that is consistent with a genetic model formulated from geo-chemical data. The compositional as well as textural trends displayed by the thiospinel mineralization could be exploited to optimize recovery of any or all thiospinels of economic interest.

Jan 1, 1981

By M. M. Tilman

As part of ongoing research to improve mine safety, the Bureau of Mines conducted research on the corrosion of friction rock stabilizer steels in five Missouri lead and iron mine waters. Electrochemical corrosion tests, including evaluation of pitting tendency, were performed on two types of high-strength, low-alloy (HSLA) steels and galvanized steel in four Missouri lead mine waters and one Missouri iron mine water. The tests were conducted at in-mine water temperatures in both air-saturated and deaerated waters. Static, weight-loss corrosion tests were also conducted on HSLA steel specimens in the five Missouri mine waters for 2,900-h duration at average in-mine water temperatures and air-dissolved oxygen contents of 6 to 7 ppm. Corrosion rates determined by the weight-loss tests were roughly comparable with rates determined electrochemically in deaerated waters containing 0.3 to 0.5 ppm dissolved oxygen content. Passivation of specimen (nongalvanized) surfaces in air-saturated waters resulted in very low electrochemically deter- mined corrosion rates. Pitting-tendency was generally higher for both HSLA steels in air-saturated waters than in deaerated waters. Galvanized steel generally exhibited higher tendency to pitting in the deaerated waters than in the aerated mine waters.

Jan 1, 1985

By John L. Shafer

A process for the conversion of stibnite (Sb2Sj) concentrates, crude antimony oxide, or metal to a pure cubic antimonous oxide (senarmontite) has been developed on a laboratory scale. The conversion of stibnite to senarmontite has been piloted. The high purity of the final product is the result of forming antimony trichloride as a low temperature distillable intermediate. To obtain the antimony trichloride the stibnite, or crude oxide is slurried in molten antimony trichloride and reacted with gaseous hydrogen chloride. Antimony metal is oxidized to the trichloride with chlorine. The hydrogen sulfide produced from the hydro- chlorination of stibnite can be upgraded to a strength of 95% or greater for further treatment. The crude antimony trichloride is separated from the gangue by a preliminary evaporation and then is fractionally distilled and the trichloride distillate has less than 50ppm of arsenic and lead combined (the most troublesome impurities in antimony processing). The purified antimony trichloride is then hydrolyzed with sodium or ammonium hydroxide to produce the cubic form of antimonous oxide (senarmontite) to the exclusion of the rhombic form (valentinite) which is photosensitive. The advantage of this process is the ability to treat a wide range of antimony ores, concentrates, and metal to yield a high purity oxide in a controllable range of particle sizes.

Jan 1, 1975