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By Ambarish Ghosh, Chitralekha Ghatak, Tanumaya Mitra, Tarun Sengupta, Sajib Das, Sankar Kumar Nath

"Currently construction of important structures like bridges, flyovers and high rise buildings in and around Kolkata are in full swing. These structures have mostly pile or well foundations. The design methodology and construction techniques are being employed keeping in view both the safety and economy of the project. The data presented in this investigation have been taken from Geotechnical Investigation report of Component B in connection with construction of Extradosed Cable Stayed Bridge over River Hooghly in Hooghly and Nadia district of West Bengal, India. The investigation site is located within close proximity of Eocene Hinge Zone which is being taken as the principal contributor of Earthquakes in and around Kolkata. Considering the importance of the project detailed and exhaustive geotechnical investigation has been carried out and site specific response spectra have been generated for analysis and design of the bridge. This paper presents site specific response spectra, liquefaction analysis and comparison of lateral load carrying capacity of pile using Winkler approach and IS 2911 guidelines.INTRODUCTIONPile foundations are used to transfer the load of the super structure through soft soil deposit to deeper bearing stratum by means of skin friction or end bearing or both. Pile foundations are regarded as a safe alternative for supporting structures in seismic areas and have been used for this purpose in non-liquefying as well as liquefying soils. But their design in case of potentially liquefiable soil is quite different from that of non liquefiable soil. In liquefiable soil the progressive buildup of excess pore water pressure will cause stiffness degradation and loss of strength which in turn will induce additional shear force and bending moment in the pile. The mechanism of pile behavior in liquefying soil has been investigated by several investigators in the recent years based on observations of pile performance during earthquakes and studies in the centrifuge and Shake Table tests. Exhaustive geotechnical investigation has been carried out along the proposed alignment of the Extradosed Cable Stayed Bridge i.e., along Baropara, Bansberia ROB, Ishwar Gupta Bridge, Saraswati River to collect disturbed as well as undisturbed soil sample, to develop average soil profile and to determine the design parameters. The proposed project site is very close to Eocene Hinge Zone, which is basically a strike slip fault, capable of generating an earthquake of Mw 6.7. Thus it is evident that the proposed Bridge needs to be designed considering the adverse geo-hydrological condition as well as the earthquake aspects needing special attention following the state-of-the-art technology as guided by relevant codes and published literatures. Considering the soil profile of these locations ground response analysis has been carried out using equivalent linear method to determine the site amplification. Site specific response spectra have been developed for the four zones and zone factors have been determined. The computed zone factors are 0.198g, 0.195g, 0.195g and 0.20g for the four zones respectively, much higher than the zone factor 0.16g, which is for zone III, as stipulated in IS 1893:2002."

Jan 1, 2015

By Kessi E. Zicko, Eric A. Hackenberg, Paul J. Lewis

"Following snow melt and spring rains in 2011, a landslide measuring approximately 600 feet long and 300 feet in slope length occurred within the southbound roadway embankment of a heavily travelled 2-lane divided highway in North Central Pennsylvania. Driven steel piles were designed to stabilize the embankment slope. Factors affecting the selected stabilization technique included an adjacent reservoir, wetlands, the length and depth of the failure plane, extent of glacial lake deposits, excess pore pressures in the foundation soils, and an area of archaeological interest. Field reconnaissance and subsurface explorations including borings, instrumentation, geophysics, and laboratory testing indicated that glacial lake deposits were present in the toe region of the embankment. Instrumentation proved key in measuring excess pore pressures and in locating the failure plane, and geophysics was utilized to estimate the extent of the soft glacial lake deposits and to estimate pile lengths. The existing condition of the embankment was modeled in computer slope stability analyses, which were also used to help assign soil parameters. Significant costs were associated with constructing a berm due to the impacts on adjacent site features. Therefore, multiple rows of driven steel H-piles were designed for installation along the toe of the embankment. The design lateral load in the piles was based on slope stability analyses, and the pile size and number of piles were based on lateral pile computations with modified p-y curves to account for installing piles in an active landslide. The relationship between the factors of safety from slope stability and the LRFD pile design was significant in determining pile loads for lateral analyses.INTRODUCTIONA landslide developed along the lower portion of the southbound embankment of State Route 15 in Tioga County, Pennsylvania. The road passes through a steep valley and is located along the southern extent of the Tioga Reservoir. Although no damage to S.R. 15 was attributed to this landslide, the close proximity of the slide to the road posed a concern for the long-term stability of this section of roadway.This paper presents a summary of the site history; the subsurface conditions based on borings, instrumentation, a geophysical survey, and laboratory testing; slope stability analyses including alternatives assessment; and the pile design.SITE HISTORYS.R. 15 was originally located in the valley along the Tioga River and traversed through the towns of Tioga and Mansfield. Although the reason is unknown, it is interesting to note that Old S.R. 15 curved away from the river in the area of the landslide. In the mid 1970’s, S.R. 15 was relocated to the eastern hillside prior to construction of the Tioga-Hammond Reservoir by the U.S. Army Corps of Engineers. The relocated highway was constructed in stages. Two lanes of relocated S.R. 15 were initially constructed to carry one lane of northbound and one lane of southbound traffic. At this same time, the majority of the fill was placed for two future lanes immediately to the west, which would eventually allow for two lanes in each direction. The two eastern lanes would then carry northbound traffic after completion of the two southbound lanes to the west."

Jan 1, 2015

By William G. Ryan, David S. Graham, Dan A. Brown, Rich A. Lamb, Paul J. Axtell

"The St. Croix River Crossing project on the Minnesota-Wisconsin border has been in the process of planning and public debate for two decades, with several changes in alignment. During the course of the earlier planning process in 1995, a drilled shaft load test was performed to obtain preliminary design information. There were some difficulties in maintaining stability within the weak sandstone bearing formation, and the measured axial resistance was relatively low. Subsequent experience by the Minnesota Department of Transportation with similar weak sandstones on the I-35W project suggests that improved construction techniques using modern drilling fluids may offer opportunities for improved performance. During final design in 2012 a second load test program was performed of a full scale test shaft constructed using polymer drilling fluids. The stability of the socket excavation in the weak sandstone appeared to be greatly improved and the measured axial resistance significantly higher.This case history illustrates the excellent performance that drilled shafts can provide in even relatively weak sandstone bedrock as well as the profound influence on axial resistance associated with the construction techniques used. The improved resistance values obtained by the new load test with more recent construction technology allowed the foundation scheme to be substantially optimized with respect to the number and size of required drilled shafts, reducing the size, cost, and risk of the coffercells and footings.IntroductionThe Minnesota Department of Transportation (MnDOT) has awarded the first phase of a bridge construction project that will cross the St. Croix River between Oak Park Heights, MN and St Joseph, WI. The first phase construction contract involves building the river pier substructures including groups of drilled shafts beneath each tower leg. A general location of the bridge project is provided in Figure 1.Prior to award of the construction contract, two separate design-phase axial load tests were performed on non-production drilled shafts with rock sockets. Both tests were static, bottom-up tests using the Osterberg Cell (O-cell). The first test was performed in 1995 when final design and construction was thought to be imminent. After years of public debate and literally, an act of Congress, design of the project was finally restarted and a second load test performed in 2012. The 1995 test was conducted on the Minnesota bank approximately 900 ft southwest of the St. Croix River bank. The 2012 test was conducted in the river about 2,100 ft northeast of the1995 test location. A plan-view of the project indicating the test program locations relative to the bridge alignment is provided in Figure 2."

Jan 1, 2015

By Richard Stone, Rouzbeh Afsharhasani, Moses Karakouzian

"Caliche, a hardened sedimentary deposit of calcium carbonate that occurs worldwide, generally in arid or semiarid regions, is frequently encountered in Las Vegas, Nevada. The presence of a caliche layer in a soil profile affects the response of deep foundations to axial load. This paper studies the stiffening effect of caliche layers on the elastic settlement of a pile foundation. In order to evaluate the response in a layered soil-caliche profile, finite element analyses were performed on a typical-sized single pile and a pile group, both having constant diameter and length of the pile. The results indicate that the stiffening effect from the caliche is noteworthy, and a layer with a relative thickness of at least one pile width, regardless of its location, reduces the pile settlement for both single piles and group of piles systems by at least 50%.IntroductionThe presence of cemented materials in the soil profile influences the settlement response of foundations. One type of cemented material that can be found in arid places around the world is a sedimentary deposit of calcium carbonate called caliche. Caliche, a hardened sedimentary deposit of calcium carbonate, is common in arid and semi-arid urban areas, such as Las Vegas, Nevada (Wyman, et al. 1993).Caliche is mostly observed in lacustrine, river, and alluvial fan deposits (Jr.C.C 1970). It is also found in Central and Western Australia, the Kalahari Desert, the High Plains of the Western U.S., and the Sonoran Desert of the U.S. and Mexico.Some conditions required for the formation of caliche are that country or basement rocks must be a carbonate type, carbonate must be present in the soil zone of the area, climate regime is semi-arid to arid, there exists widespread capillary activity, and carbon dioxide (CO2) is present in the environment. As a result, caliche occurs as a product of the carbonization process (Atabey, Atabey and Kara 1998). In such areas where foundations are constructed on thin rock layers (caliche), special geotechnical design conditions should be considered, particularly if the supporting rock layer is underlain by a weaker material."

Jan 1, 2015

By Swaminathan Srinivasan, Aaron J. Muck

"When an opportunity arises to combine state-of-the-art concepts with advanced modeling tools, engineers need to take what they know and apply forward thinking to geotechnical solutions to promote the state-ofpractice. Such an opportunity was seized during the design and construction of the Great American Tower in Cincinnati, Ohio. The forty-one story Great American Tower at Queen City Square – currently the tallest building in Cincinnati – has not only changed the downtown skyline, it is also contributing to the advancement of the state-of-the-art use of auger cast-in-place (ACIP) piles as settlement reducers. Predicted settlements of a traditional mat foundation were excessive, and the costs and construction time associated with traditional ACIP piles extending to bedrock were not preferred. A mat supported on a limited number of ACIP piles, with the piles primarily acting as settlement reducers, was evaluated as the preferred foundation type.Promoting the unique soil-structure interaction of the foundation system with confidence required the use of sophisticated numerical modeling tools. Traditional standard penetration test boring data (SPT) was initially used to develop a numerical analysis of the soil-structure interaction using FLAC 3D software. The model was further modified with cone penetration (CPT) and pressuremeter testing (PMT), along with actual load test results on several ACIP pile elements of varying lengths, but all tipping above bedrock. Through a combined design team effort, and detailed numerical modeling analysis, ACIP piles were recommended for reducing mat foundation settlement. Instrumentation during and post-construction confirmed design assumptions and predictions. Integrating sound geotechnical concepts, and using advanced geotechnical analysis and design methods, traditional mat and ACIP pile foundations were successfully integrated into a unique foundation support system.INTRODUCTIONThe Great American Tower at Queen City Square in Cincinnati, Ohio is located within a region dissected by historical geologic deviances associated with the meander of the Ohio River and glacial progression/recession. Combining a challenging geology, with the development of a high-rise office building afforded the design team an opportunity to combine state-of-the-art soil-structure interaction concepts and method with traditional geotechnical engineering concepts. Such a combination required a variety of field tests, collaboration with the design team and owner, and geotechnical-structural modeling during the design phase. During construction, in addition to materials testing and observation, a variety of instrumentation systems were employed. Together, the data was used to corroborate the design model and make adjustments during construction and further substantiate design assumptions following construction."

Jan 1, 2015

By Adegbenjo Adewale Oladapo, Ibitoye Simeon Ademola, Ladiipo Olufemi Akinbiyi, Adegbola Adekunle Amos, Adeboje Taiwo Bode, Raji Fatai Olasunkanmi

The combined effects of the addition of Silicon (Si) as alloying element and low temperature annealing on the tensile properties of 70/30 brass with Nickel (Ni) and Iron (Fe) contaminants is investigated in this paper. Melts of cartridge brass were made to which 0, 0.5, 1, 2, 3 and 4 wt % of Si was added. These were sand cast into rods of 600 mm by 10 mm diameter and were thereafter machined into standard tensile test samples. Some of these samples were annealed in a muffle furnace at temperatures of 250, 300, 350, 400 and 450 oC respectively and the others were used as control. Subsequently, all the heat treated and non heat treated samples were subjected to tensile tests on a Hounsfield Extensometer and the load – extension plots retrieved were analyzed. Microstructural characterizations of the samples were carried out using Accu-Scope Optical Microscope. The results showed that cartridge brasses subjected to alloying and annealing treatments had improved tensile and yield strengths. However, the tensile properties were increased and maintained within acceptable limits at stress relieve annealing temperatures.

Jan 1, 2015

By Junfu Chen, Jiann-Yang Hwang, Yong Zhou, Lijun Lu, Likun Lia, Jixiong Liu

The sheet-like NiS-ZnS heterostructured composites were prepared by the microwave hydrothermal. The fabrication of the heterojunctions broadened the range of light response of ZnS. The photoexcited electrons of ZnS migrated to the redox potential of NiS/Ni2S under visible light irradiation, which can facilitate the effective separation of photogenerated electrons and holes in space. The visible photocatalytic activity towards hydrogen production for NiS/ZnS nanosheet heterostructed composites without co-catalyst achieved 0.28 mmol h–1, and the quantum efficiency was up to 18.6% under the wavelength with 420 nm visible light irradiation.

Jan 1, 2015

By S. Yin, A. Bogno, H. Henein, P. Natzke

Impulse Atomization (IA) (a single fluid atomization technique) was used to rapidly solidify Al- 4.5wt%Cu and Al-4.5wt%Cu-0.4wt%Sc under argon atmosphere. In addition to the IA-generated droplets, the same technique was used to produce strips by Spray Deposition (SD) of the same alloys on a copper substrate with and without oil coating. The rapid solidification microstructures were analyzed using Scanning Electron Microscopy (SEM). From the SEM images, the amount of eutectic and the secondary dendrite arm spacing (SDAS) were measured. These SDAS results lead to the estimation of cooling rate. The eutectic fraction coupled with the metastable extension of the solidus and liquidus lines of Al-Cu (Sc) phase diagram lead to the estimation of primary and eutectic undercoolings. A comparison of the solidification path of the droplets and the strips was done as well as the analysis of the effects of scandium.

Jan 1, 2015

By Jian Li, P. Liu, R. Zhang and J. Lo

In the past decades, focused ion beam (FIB) has evolved into a powerful microscope that provides capabilities that no other microscopes can offer. The combination of high-resolution imaging and stress-free ion beam cross sectioning provides valuable microstructure information both at the specimen surface and beneath. FIB techniques are also the preferred method to prepare site-specific transmission electron microscope (TEM) specimens. CanmetMATERIALS owns a world-class microscopy facility, where advanced microscopy work provides strong supports to research programs that cover a wide range of subject areas. This paper is aimed to provide a few practical examples of FIB applications in microstructure characterizations that include cross-sectioning and imaging, serial sectioning, and advanced TEM specimen preparation in materials research at CanmetMATERIALS.

Jan 1, 2015

By Fuming Wang, Lifu Hu, Changrong Li, Ruipeng Pang

The solidification structure of 430 ferritic stainless steel has been calculated in the solidification process by using 3D-CAFE model under the condition of water cooling. The calculated results consistent with those obtained from experiment. Under watercooling condition, the solidification structure consists of chilled layer, columnar grain zone, transition zone and equiaxed grain zone

Jan 1, 2015

By Thenepalli Thriveni, Ch. Ramakrishna, Yujin Jegal, Ji Whan Ahn, Jyothi Rajesh Kumar

In alumina production or alumina refining, bauxite is converted to alumina (aluminium oxide) The rare-earth elements (REEs) are a group of 17 chemically similar metallic elements (15 lanthanides, including scandium and yttrium). Rare earth elements play a key role in many industrial applications, petroleum refining, clean energy, automobile, electronics, and defense applications. These rare earths are essential to the success of green technologies. China today controls more than 95 percent of the rare-earth supplies and nearly all rare-earth refining and after 2009 year rare earths crisis raises due to China’s export restrictions and growing internal demand for rare earth elements. The extraction of gallium and yttrium from Korean red mud (KC red mud) by selective acid leaching was explored. The recovery of gallium and yttrium from a leach solution of the Korean red mud using solvent extraction was studied. A number of extractants were investigated for the extraction of those mentioned two rare earth elements and also we proposed a flow sheet of rare earth elements respectively. The toxic heavy metals presented in KC red mud were removed by CO2 stabilization.

Jan 1, 2015

By Duclerc Fernandes Parra, Washington Luiz Oliani, Christiano Gianesi Bastos Andrade, Ademar Benevolo Lugão, Danilo Marin Fermino, Francisco R. Valenzuela Diaz

This work concerns the study of the effect of discarded bond paper on the mechanical behavior of polypropylene/organophilic clay nanocomposites. A brown polycationic bentonite from the state of Paraíba, Brazil, was treated with sodium carbonate to transform it into a bentonite that swells in water and then treated with hexadecyltrimethylammonium ammonium chloride to transform it into a bentonite that swells in organic liquids. Polypropylene with 3 % polypropylene graft compatibilizer (PP-g-AM) was mixed with 1 % and 2 % by weight of discarded bond paper and with 1% and 2% by weight of organophilic clay using a twin-screw extruder. The specimens were prepared by the injection process. The clay as received and after organophilization was characterized by XRD, SEM, and capacity of swelling in water and in organic solvents. The nanocomposite specimens were characterized by XRD and thermal analysis. The mechanical behavior of the injected specimens was evaluated by strength, flexural and impact tests. The nanocomposites showed improved mechanical properties compared with the polymer without filler.

Jan 1, 2015

By Enrui Dai, Weibing Chen, Bin Yang, Wenhui Ma, Haisheng Fang, Hui Wang

LiMn0.8Fe0.2PO4/C composite was prepared by an improved solid-state method and the effect of calcination temperature on properties of the obtained materials was investigated. The results showed that increasing calcination temperature from 600 to 700 oC improved the performance of the LiMn0.8Fe0.2PO4/C due to enhanced crystallinity and increased conductivity, but further increase in calcination temperature to 800 oC led to degraded performance due to particle growth and decrease in porosity. Therefore, the LiMn0.8Fe0.2PO4/C composite prepared at 700 oC exhibited the best electrochemical performance, and could deliver a high capacity of 152 mAh g−1 at 0.1 C, 147 mAh g−1 at 1 C and 114 mAh g−1 at 10 C. In addition, the performance of the LiMn0.8Fe0.2PO4/C and LiMn0.8Fe0.19Mg0.01PO4/C was compared when they were obtained at the optimum calcination temperature.

Jan 1, 2015

By Jun Miao, Kang Liu, Jilai Xue, Jun Zhu

CO2 emissions must be reduced by at least 50 % by 2050, and hence the technical solutions to capture and convert CO2 into value–added products should be considered. A Cobalt(III) Schiff base complex (Salen–Co(III)) has been investigated as a catalyst for synthesis of cyclic carbonate from CO2 and epichlorohydrin(ECH) with tetrabutylammonium bromide (TBAB) as co–catalyst. To recover Salen–Co(III) for the next cycling operation, it was immobilized onto zeolite 13X through excessive impregnation method. The immobilized catalyst was characterized using XRD, SEM, BET and ICP–AES techniques. Catalytic tests showed that yield of cyclic carbonate reached 90 % using 0.5 mol % Salen–Co(III) at ambient conditions. The immobilized Salen–Co(III) exhibited better catalytic activity than the homogenous one when used at the first cycle, but the yield decreased by some 20 % after five cycles.

Jan 1, 2015

By Onwukamike, Onyedika G. O, Ogwuegbu M. O. C., K., Onyenehide C

A detailed mineralogical and elemental characterization of a lead (Pb) ore deposit from Ishiagu, Ebonyi State, Nigeria was carried out with XRD, SEM-EDX, and ICP-OES based mappingtechniques. The results show that the most dominant and valuable metal is lead (Pb = 95.02%, mass fraction). The main mineral is galena. Ilmenite and sphalerite occur as minors, which account for 2.71% and 0.80% respectively. Elements like Al, Ca, Mg, Ti, Na, Mn, Si and Sn occurred in trace amounts and are disseminated in the entire ore body.The surface and interrelations of the crystals were examined with x-ray mapping and the result shows the pattern of dissemination of the minerals within the ore body.

Jan 1, 2015

By Patrice Chartrand, Halvor Dalaker, Philippe Ouzilleau

A size-dependant thermodynamical model for the carbon-hydrogen previously developed by Ouzilleau et al. [1] has been expanded here to include chemisorption of methyl groups. Gibbsenergy minimalisation calculations using FACTSAGE software on this model indicates that hydrogen bonding through methyl groups is energetically favoured as an intermediate between bonding as monoatomic hydrogen to edge hexagons (which is more favourable) and as monoatomic hydrogen to corner hexagons (which is less favourable). The model has also been applied to methane decomposition and oxide reduction using natural gas. A C-H solid solution as a thermodynamic description of the solid carbon phase influences calculations of carbon activity in metastable methane, and gives different results than when using graphite.

Jan 1, 2015

By Jianguo Yin, Wenqiang Yang, Xiaoli Yuan, Juan An, Wentang Xia

Low grade iron ore with phosphorus (LGIOWP), a raw and wasted industrial solid material was used as an adsorbent to remove Pb(II) from wastewater. The effects of initial pH value, adsorptive time, initial Pb(II) concentration, adsorptive temperature and LGIOWP dosage on the Pb(II) removal efficiency were studied. The results show that the Pb(II) removal efficiencies exceed 99.4% and Pb(II) concentrations are less than 0.30 mg/L under the conditions of pH value 7.0, adsorptive temperature 50 oC, adsorptive time 30 min, initial Pb(II) concentration 100 mg/L, particle size <0.25 mm, adsorbent dosage 5 g/L and stirring speed 260 r/min. After Pb(II) removal reaction, the Pb(II) concentrations of wastewater completely accord with the requirement of national discharge standards of pollutants from lead and zinc industries (GB 25466-2010) (TPb= 0.5 mg/L) in China. Therefore, it can be concluded that LGIOWP is a new low-cost adsorbent which is suitable for the adsorption of Pb(II) from wastewater.

Jan 1, 2015

By G. L. Pedroti

With the development of industrial processes and the consequent emergence of numerous products that quickly become necessities, industrial activity has acquired an essential character today. Although its importance is unquestionable, industrial activity is responsible for generating quite a large number of residues, with different shapes and characteristics. It has been observed, in particular the grits (Kraft process in the cellulose industry) and the residue from the processing of granite. And, given the importance of Portland cement as a building material, its vast employment and waste properties that resemble components of the clinker, it was decided to produce cementitious compounds from these industrial wastes. The residues were subjected to mineralogical, chemical, physical and morphological. And, the mixing ratio between the residues in the 70% and 30% grits residue granite was sintered at 1250 ° C furnaces to burn threshold of 6 hours forming new compounds observing tri-calcium aluminate and di-calcium silicate that are compounds found in portland cement.

Jan 1, 2015

By C. G. Bastos Andrade, V. F. Justo, F. R. Valenzuela-Diaz, M. G. S. Valenzuela, C. M. Matos, C. Volzone

For industrial use, the smectite clays are usually treated with inorganic acid of high concentration at temperatures under boiling point, which provide the bentonite´s bleaching power. In the present paper, a sample of brown smectite from Paraiba, Brazil, was submitted to treatment under moderate conditions (90°C, reaction times of 1, 6, 12, 18 and 24hours in close reactor, concentration of the aqueous solution of hydrochloric acid 1.5M, clay/acid solution ratio of 1g/10mL), aiming to reduce impurities, responsible for the color of the clay, without causing significant changes in their structure. The samples were characterized by scanning electron microscopy (SEM), energy dispersive X-ray detector (EDS), stereomicroscopy, Cation Exchange Capacity (CEC), Thermal Analysis (TG/DTA), and X-ray diffraction (XRD). It was observed a bleaching in samples with time of 12h to 18h. With the DRX was possible to monitor the peak intensity of the clay structure and the sample with 12 hours of treatment was not significantly altered its crystalline structure, maintaining the peak clay at d(001). The most pronounced changes in the bleaching occurred within the first 12 hours of acid treatment. Thus, clay can be used in products with high added value.

Jan 1, 2015

By G. Plenge, M. Brittan

"Plant design parameters for gold extraction, leach residence time and cyanide consumption are generally determined from standard bench-scale bottle roll or agitation leach tests. The application of laboratory data to process design has essentially evolved from the testing of oxide or low cyanide-consuming ores. Such scale-up factors may not be appropriate for ores that deplete cyanide and oxygen since this interferes with gold extraction kinetics. High cyanide-consuming ores also exacerbate the differences between the conditions applicable to small batch tests and large continuous operations. Testing a reactive high-sulfide South American ore deposit necessitated the re-evaluation of conventional bench-scale cyanidation procedures. Pulp density can be a major factor affecting the results for plant design purposes and should be treated as a test work variable. As with high clay-bearing ore, where pulp viscosity can hinder mass transfer, minimizing the influence of test equipment on gold extraction kinetics may require low pulp densities. This introduces interpretative complexity since cyanide consumption changes as a function of pulp density. Activated carbon also consumes cyanide, so its effect has to be accounted for in the case of carbon-in-leach (CIL) or carbon-in-pulp (CIP) plant flowsheets. Since cyanide is an expensive reagent, often a major component of plant operating costs, it is important that the scale-up of cyanide consumption from laboratory to plant be representative. The traditional method of reporting cyanide consumption in bench-scale testing is questioned since it takes credit for residual free cyanide in leach tails. The projected plant consumption may be better estimated by using the total cyanide addition in a laboratory test. We propose a test work protocol that categorizes the cyanide consumption into its components but requires more extensive testing to generate design data. The ultimate validation of scale-up factors used by project engineers requires rigorous bench-scale versus commercial plant comparative data. Such data are not readily available.IntroductionMajor factors in the design of a gold processing plant are gold recovery, leach residence time and cyanide consumption. These parameters are important determinants of project revenue and costs and, thereby, potentially of project financial viability. Estimates of the associated design criteria for a commercial plant are normally generated from laboratory cyanidation, carbon-in-leach (CIL) or carbon-in-pulp (CIP) tests using standard procedures (Angove, 2005). The key question is whether the standard laboratory test work procedures developed historically for low reagent consuming ores are appropriate for ores that are highcyanide and oxygen consumers.The present paper examines test procedural factors that can influence the test work results and, therefore, their interpretation for design scale-up purposes. The study refers in particular to a high cyanide-consuming sulfide ore. The ore was being tested to develop scoping level engineering design criteria for a proposed project in South America."

Jan 1, 2015