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By E. A. Brocchi, P. K. Jena

Complete extraction of copper from Salobo chalcopyrite concentrate can be achieved in less than 10 minutes by chlorination of the dry concentrate with Cl2 at 450 degrees C and in 5 minutes by chlorination of an aqueous slurry containing 5 wt% concentrate at 30 degrees C. In general, slurry chlorination appears to be faster than dry chlorination. The kinetics of dry chlorination of copper sulphide are controlled by an adsorption mechanism with an activation energy of 6.1 kcal/mole. The rate is independent of chlorine partial pressure when pCl2 exceeds 0.4 atm. In slurry chlorination the dissolution of copper sulphide follows a topochemical reaction model and the rate of chlorination decreases with increase in pulp density and also temperature. Dissolved chlorine appears to take part in the reaction in atomic or ionic form.

Jan 4, 1992

Discussion at the Midland Institute of Mining, Civil, and Mechanical Engineers' general meeting held in Leeds, March 21st, 1916, with T. Beach, vice-president, in the chair, of a paper published in Trans. Inst. Min. Engrs., 1916, vol. L., page 509, comprised a written contribution by O'Shea L.T.

Dec 1, 1916

By T. Sharma, T. C. Rao

Laboratory studies have been carried out on acid leaching as a possible route for the extraction of potassium from glauconitic sandstone. Leaching efficiencies with sulphuric, hydrochloric and nitric acids were investigated. The effects on potassium dissolution of temperature, concentration and type of acid, stirring speed and leaching time were also studied. The results show that it is possible to recover 87.5, 93 and 85% potassium with 5 M H2SO4, HCl and HNO3, respectively. During the initial stages of the sulphuric acid leaching process the chemical reaction at the mineral surface is the rate determining step, whereas during the later stages diffusion through the product layer is rate-controlling. Overall, the process follows a mixed-control model that includes both chemical reaction and diffusion. The activation energy for the dissolution of K was found to be in the range 25.79-106 kJ/mol.

Jan 12, 1992

By A. Ludkin

The paper presents the history of the occurrence of spontaneous combustion in the north area, together with the associated problems. These are examined and a description is given of the methods used to combat the danger, including the use of modern scientific instrumentation. Detailed reference is made to the underground trials with pack injection and sealant coatings which were carried out at Seafield Colliery following the formation of a working group to assess the performance, in the same underground conditions, of (1) sandbagging, (2) pack injection, (3) surface coating. Based on these trials, an improved and more economical method of prevention has been established. There is, however, still scope for further improvement in techniques which would take into account the problems of gradient, transport, manpower and cost.

May 23, 1905

By Winmill T. F.

Among the various theories proposed to account for the spontaneous ignjtion of coal, one which has at times been very strongly held is that the initial heating is due to the oxidation of iron pyrites. From the results described in this paper, it is possible to calculate roughly the rate of spontaneous heating of a specimen of finely-divided pyrites, on the assumption that all the heat developed is used in raising the temperature of the pyrites, and that none is lost. It is clear that where finely-divided pyrites occurs in considerable proportion among coal, it may be the chief factor in originating combustion, but that pyrites can only be the cause of a heating when it is present in considerable proportion, and in a very finely-divided state

Dec 1, 1916

By M. L. Schmulian

"The Windarra nickel deposits display many of the characteristics that typify Archaean volcanic peridotite-associated nickel sulphide ores of Western Australia. The Fe-Ni-Cu sulphide mineralization, which comprises dominantly disseminated sulphides, occurs at the base of a differentiated ultramafic volcanic pile grading upwards from massive meta-peridotitic flows to thin, locally spinifex-textured meta-picritic units. The entire mafic-ultramafic belt has been subjected to mid-amphibolite- facies metamorphism. The ore-bearing ultramafic is immediately underlain by dominantly sulphide-facies banded iron formation (BIF), which commonly contains nickel sulphides adjacent to its contact with mineralized ultramafic. BIF-hosted ores are formed both by physical remobilization of ultramafic-hosted sulphides and by migration of Ni and Cu into pre-existing iron sulphides.At Mt. Windarra the mineralization comprises eight steeply dipping, steeply plunging elongate oreshoots, which display a marked parallelism with major and minor fold structures in the underlying BIF. Seven of the shoots occur at or close to the base of the ultramafic pile, and are hosted by at least three overlapping flows. The zone of overlap occurs at the northern end of each flow, where picritic ultramafic, representing a dominantly liquid portion of the flow, occupies the basal contact. A gross south- north ultramafic flow direction is inferred. The eighth shoot occurs in a stratigraphically higher position within the ultramafic sequence.At South Windarra at least two overlapping mineralized flows occupy the basal contact, the ore zone having a strike extent three to four times its downdip extent. There is no obvious structural control to the mineralization."

Jan 1, 1984

By H. L. Willett

Wrapping up the symposium, covers incidence of spontaneous combustion in British mines, assessment of liability to spontaneous combustion, precautions, rate of advance, starting a line of a coalface, local heatings at roadsides, burying packs, coal headings, retreating longwall, detection and sealant coatings.

May 23, 1905

By P. A. Rossouw, G. A. Fourie

The correction to the paper published in Trans. IMM A, vol.105, 1996, p.A162-A165 stresses that figs. 4 and 5 had been interchanged, reproduces them with their correct captions for clarity and encourages readers to comment on the Delft proposal

Jun 19, 1905

By R. F. Bell, Schultz

The paper briefly discusses the nature of spontaneous heating in mines in the Doncaster area, in the period immediately before 1967 and steps taken to prevent and treat such outbreaks. The changes that led to the increased rates of advice of Barnsley Seam faces since 1967 are listed and the effects of these increased rates on the frequency and location of spontaneous combustion are discussed. The change in methods of control required by the increased rate of advance of the faces and the changes in location of outbreaks are described. Some typical heating situations are evaluated. The methods described include the use of air sealants, water gels for filling of voids in wastes, the balancing of pressures across heating areas by pressure chambers, booster fans, and the resiting of air separation doors, and the sealing of air-ways by flooding. The authors discuss the influence of mine layouts on the risks of spontaneous combustion and advocate that future plans should be designed to limit the number of districts at risk when heatings occur.

May 23, 1905

It was intended to show a film on Dust Suppression in the South Wales Coal-mines. Unfortunately, owing to a breakdown, only a small portion of the film was shown.

Jan 1, 1947

By N. Djordjevic

It is commonly accepted that the strength of rock measured from small samples tends to give unrealistically high estimates of the strength of larger samples, in situ blocks of rock or the rock mass in situ. The Weibull theory of the statistical strength of material provides a possible means for calculation of the strength of large rock volumes, based on the routine testing of small samples. Application of the Weibull approach to estimation of the strength of Moura coal showed an encouraging agreement with experimental results and the method was also applied to hard-rock andesitic and porphyry ore from Bajo de la Alumbrera, Argentina

Jun 21, 1905

By NA NA

Listing safety award winners, £I43M has been added to proceeds from coal privatisation in the year to March 1997, bringing total revenues to over £1.3bn, some company news in brief.

Jan 8, 1997

By D G. Oldfield

Pall has developed and supplied to several airlines cabin air libers to provide clean air for passengers and crew in flight, while reducing airline operating costs. Most of today's modern commercial passenger aircrafts employ cabin air recirculation as a means of reducing operating costs. With large numbers of passengers being subject to an increasing proportion of recirculated air for hours at a time, the matter of cabin air quality, with particular respect to the health effects on passengers and crew, has to be addressed. Commercial pressure will ensure that the airlines and aircraft manufacturers will not revert back to the total fresh air systems of the 1960s and 1970s. In fact, feasibility studies are already being undertaken to look at increasing the proportion of recirculated air to 80% and above. With the application of specialist nitration technologies. Pall is able to ensure that the requirements for economy are met whilst ensuring that the air is effectively rendered as 'fresh air’ each time it is recirculated.

Jan 9, 1996

By S. Y. Ezz

Report of discussion at February, 1971, IMM general meeting (Chairman : M. J. Cahalan, President) of a paper published in Transactions/ Section C (Mineral Processing & Extractive Metallurgy), vol. 79, September, 1970, pp. C226-C233 with contributions by Wild R. and Astier J. on fluidised bed reduction of iron ore fines

Dec 1, 1971

Discussion of the papers with a written contribution and authors' written replies.

Jan 1, 1947

By G. D. Nicholls

There have been very few attempts to isolate the various factors that contribute to the overall imprecision of geochemical analytical procedures, due in part to the difficulty of distinguishing between them. The technique of spark source mass spectrography permits a ready distinction between the contributions to overall precision from sampling error and instrumental and other errors. With conventional methods of sample preparation for this technique sampling difficulties are responsible for 80-90 per cent of the overall imprecision. Examination of the probable location of the major difficulties in sample preparation indicates that the preliminary stage of grinding, mixing and extraction of a first aliquot (about 1/100 of the original sample) is generally perfectly adequate. The difficulty lies in the subsequent stages of sample preparation. Dry mixing techniques are unlikely to give good precision if the sub-samples actually examined by the analytical technique are less than 10 mg in amount. Solution techniques are less prone to sampling difficulty. Fusion techniques, unless conducted with great care, can produce more difficulty than dry mixing. Sample preparation is critical to the success of many analytical procedures. Selection of appropriate sample preparation techniques requires just as much care as the selection of techniques for the actual analysis.

Dec 1, 1971

"Prior to the publication of the General Report of the Miners' Phthisis Prevention Committee of South Africa in 1916 little attention was paid to the dust hazard and the necessity for its suppression in the underground workings of the Broken Hill mines. Such precautions as were observed for the elimination of dust were related rather to the prevention of lead poisoning, which, in the early days of Broken Hill when large tonnages of lead carbonate ore were being won, was rather prevalent. Ventilation and hygiene followed the general practice in this and most foreign countries.This paper covers incidence and action since 1918, considering medical aspects and operating aspects. "

Jan 1, 1947

By G. B. Hooper, G. A. Ferguson

The technical capabilities and user-friendliness of the major computer-aided mining design software systems are reviewed. Recent experiences with three systems are outlined to indicate the practical problems that arise. The examples were: Microlynx software from Lynx Geosystems at the Great Dyke platinum mine in Zimbabwe; Lynx software from Lynx Geosystems at a copper mine in central Africa; and PC-MINE software from Gemcom Services at an open-pit gold project in Western Australia. Difficulties in the use of mining design software has led to an alternative approach. Falconbridge, Canada, has developed an integrated mine-planning system on a CAD platform that encompasses ore reserve estimation, stope design, development layout and survey control. Future directions of computer-aided mining design using this basis are discussed. A major advantage of using mainstream software packages, such as spreadsheets, databases and CAD programs, is that most engineers and geologists are experienced in handling such systems in the normal course of their work.

Jan 12, 1992

By W. R. Donaghue, R. L. Robinson, C. Scott

Whilst spontaneous combustion has never been considered a major problem in south Durham, certain collieries in the area have a history of heatings and precautions are essential. Three collieries are affected - Shotton, Vane Tempest and Seaham - and in the case of the last two, there are huge areas of high quality coal to work under conditions where spontaneous combustion is a real hazard. The seam being extracted has an immediate roof in goaf left by the incomplete extraction of a contiguous seam worked before the turn of the century. The presence of residual coal stocks and old roadways and cavities adds to the difficulty of preventing unwanted air movement. The main preventive measures adopted are the construction of airtight gateside packs and the use of sprayed surface coatings in the gate. Sampling systems and sampling points are described and, in particular the field of continuous monitoring from the surface is examined. The resulting possibility of a quantitative as well as qualitative assessment of the preventative measures required is discussed.

May 23, 1905

Discussion at the North of England Institute of Mining and Mechanical Engineers' general meeting held in Newcastle-upon-Tyne, 8th April 1916, on the paper published in Trans. I.Min.E., vol.LI, 1916, p.72-90, included written contributions on size and gauge standardisation by Lupton A., Peck W.R., Dean S., Mayer R.W. and Ashworth J., with the author's written response, and by Bulman H.F. and Brown M.

Dec 1, 1916