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By D. Gorc, T. M. Fraser, Z. T. Nikic, R. Pesalj

"Mount Polley is an alkalic porphyry copper-gold deposit of Lower Jurassic age within the Quesnel terrane in south-central British Columbia. The silica-saturated Mount Polley intmsive complex is assumed to be coeval with volcanic rocks of similar composition in the Nicola Group in which it was emplaced. Other intmsions and some of the volcanic rocks in the Mount Polley area are silicaundersaturated and contain feldspathoids.The Mount Polley deposit is characterized by multiple intrusions that vary from diorite to crowded plagioclase porphyry to monzonite. Intmsion breccias are associated with some of the intmsive phases. Abundant hydrothermal breccias occur on the margins and above plagioclase porphyry intmsions. These breccias provide the main host for mineralization and are associated with the highest concentrations of copper and gold. The breccias are subdivided into four distinct types based on the dominant hydrothermal mineral in the matrix. Actinolite breccia is developed in an elongate zone within the core of the Central zone and grades laterally and vertically into biotite breccia to the southeast. Magnetite breccia is irregularly distributed and is relatively sparse throughout the deposit and albite breccia is dominant in the West zone. Pervasive and vein-related alteration correlates with the breccia types. The core of the hydrothermal system at Mount Polley is subdivided into three zones: actinolite, biotite and K-feldspar-albite. The margins of the core zone are overprinted by a discontinuous zone of calc-silicate minerals. This intermediate zone passes outward into propylitic alteration. Mineralization is most prominent within hydrothermal breccias and is generally present as disseminations, blebs within the matrix and abundant veins. Mineralization is associated with a chalcopyrite-magnetite-bornite assemblage in the core of the deposit passing out into magnetite-pyrite-chalcopyrite. Relatively constant copper to gold ratios suggest that both metals were precipitated under similar conditions.Hydrothermal breccias are genetically related to the emplacement of the crowded plagioclase porphyry melt. Crystallization of the melt was probably accompanied by volatile/aqueous exsolution, forming a water saturated carapace. Decompression of the chamber in response to magma withdrawal, fracture propagation and possible fault movement allowed hydrothermal brecciation to occur at the apex and margins of the intmsion. Alteration and mineralization appears to have been controlled by fluids migrating away from the plagioclase porphyry."

Jan 1, 1995

By W. R. Tyson

IT HAS BEEN KNOWN for many years that alloy steels can become brittle when tempered in the range of 350-600°C, or cooled slowly after heating to higher temperatures. The metallurgical literature reveals that blacksmiths were aware as early as 1883 that water quenching was necessary after heat treatment above 600°C to avoid brittleness. It has also been known for years that the problem is associated with trace impurities; a paper in the Journal of the Iron and Steel Institute of 1894 refers to the brittle, faceted fractures that occur in steels containing arsenic, phosphorus or sulphur. However, definitive investigation of the mechanism of embrittlement has been possible only within the last decade with the introduction of new experimental techniques to investigate surfaces, especially Auger electron spectroscopy. It is now possible to study in detail the chemistry of surfaces with a resolution of an atomic layer or two, and enormous progress has been made recently in studying the segregation of impurities to grain boundaries by exposing the boundaries by fracture inside the microscope. A clear picture of the processes occurring and their interpretation is now emerging, as was particularly clear at the recent 1977 ASM Materials Science Seminar on Interfacial Segregation held in Chicago in October. Recent research in this area has pointed the way for commercial exploitation of this new knowledge and experimental technology. It is the purpose of this article to trace progress in understanding temper embrittlement and to indicate other areas where control of interfacial segregation and its effects can be important in metallurgical applications.

Jan 1, 1978

By A. Danaei, A. McLean, M. Barati, C. Ravindran

"The aluminum industry generates about 90 million tonnes of red mud each year. Previous research shows it could be utilized as a refining flux with a high capacity to absorb phosphorus and sulphur from hot metal in the steel industry. The present study was undertaken to evaluate the melting properties of such fluxes, as it affects the effectiveness of the flux. The results show that the melting behavior of red mud is strongly affected by lime addition and the characteristic melting/softening temperatures reach minimum VALUES (at 32.7 wt% CaO. From these findings, a correlation was established between melting behavior and optical basicity. This allows one to adjust the composition of the flux based on the process requirements. INTRODUCTIONThe aluminum industry generates about 90 million tonnes of bauxite residues each year. This residue is usually red in color because it contains a substantial amount of iron oxide. The red mud, as it is called, is a solid waste with a high concentration of sodium oxide, high pH (10 to 13), and high alkalinity, and thus is harmful to many forms of life. Traditionally, the material is stored in large tailings ponds within the plant’s vicinity (Power, Grafe, & Klauber, 2009). Development of solutions for safe disposal or preferably using this residue for other industrial processes or applications could help restore polluted locations and eliminate a negative impact on the environment (Haake, 1988; Power et al., 2009; Yan & Xuegong, 2010).The mineralogy and chemical composition of red mud depends on the quality of the bauxite and refining process parameters. In general, it consists of iron oxide (Fe2O3), aluminum oxide (Al2O3), titanium oxide (TiO2), sodium oxide (Na2O), silicon oxide (SiO2), and calcium oxide (CaO) (Power et al., 2009). Like most ores and soils, bauxite can contain trace quantities of metals such as arsenic, beryllium, cadmium, chromium, lead, manganese, mercury, nickel, and naturally-occurring radioactive materials, such as thorium and uranium. Most of these trace elements stay in the residue (Power et al., 2009)."

Jan 1, 2012

By S. Banisi, E. Arghavani, A. Akbari, Gh. A. Parsapour, S. Darvish Tafvizi

The new copper processing plant of the Sarcheshmeh copper complex consists of two parallel circuits. After a primary crushing, the ore is sent to a SAG mill and the product is further ground in a ball mill. The overflow of the hydrocyclones is fed to a flotation circuit which contains 8 rougher tank cells (RCS130), 3 cleaner cells (RCS50), 5 scavenger cells (RCS50) and a 4 x 12 m flotation column as recleaner. The circuit was initially designed to process a feed containing 0.8% Cu, but because of the ore type change, the feed grade decreased to 0.6% Cu. This resulted in a reduction of final concentrate grade and recovery from 28 and 85.5% to 24 and 84.4%, respectively. Based on the original design, the copper and silica recovery in the cleaner cells should be 69 and 55%, respectively, but these values increased to 85 and 75% because of a higher retention time. The rather high silica recovery (i.e., 75%) was found to be the main source of the lower final concentrate grade. In order to reduce the retention time of particles in the cleaner cell from 13.7 to 6.9 min, the rougher concentrates of two parallel circuits were fed to only one cleaner-scavenger and regrind circuit. This modification increased the cleaner and final concentrate grade from 15.1 and 24.5% to 17 and 26%, respectively. To prevent a possible reduction in the copper recovery, the froth depth in the scavenger cells was reduced. The overall outcome of the circuit modification was evaluated to be a 10% reduction in the energy consumption without any loss in the overall copper recovery.

Jan 1, 2016

By J. Petit, P. Girard, A-M. Gilbert, D. Faucher

L&apos;annee 2000 a été une année stratégique et significative pour l&apos; Aluminerie de Bécancour dans la réduction des gaz a effets de serre. L&apos; équipe s&apos; etait donne comme defi un jour d&apos;arriver a l&apos;objectif de zero effet d&apos;anode dans les sa11es de cuve (720 cuves au total). Le cha11enge s&apos;averait tres ambitieux car la fa<;on d&apos;alimenter une cuve d&apos;electrolyse pour obtenir son maximum de rendement faraday est de travailler le plus pres possible de l&apos;effet d&apos;anode pour eviter l&apos;embourbement de ce11es-ci. Ceci signifie que techniquement nous a11ons en moyenne, quotidiennement, 12500 fois pres de l&apos;effet d&apos;anode sur !&apos;ensemble de nos 720 cuves qui produisent aujourd&apos;hui environ 405 000 tonnes d&apos;aluminium liquide annuellement. Des 695 kg equivalent en C02 par tonne d&apos;aluminium produite en moyenne annue11ement, de 1990 a 2000, nous en sommes rendus ace jour a environ 35 kg equivalent en C02 par tonne produite. Nous sommes pres d&apos; atteindre notre objectif mais les demiers gains sont plus difficiles a atteindre. Les strategies d&apos;automatisme et d&apos;informatique, incluant l&apos;aspect de !&apos;implication humaine sur les bonnes pratiques de travail sur les cuves d&apos;electrolyse, sont les cles de ces resultats.

Jan 1, 2006

By J. Lee

A monolithic caisson is one of the major structural components commonly used in the construction of docks, breakwaters, and container terminal quay walls. Since the structure of monolithic caissons is typical and somewhat simple, its design process is also typical and repetitive, but still time consuming. To reduce the total time and enhance productivity, we developed a parametric model in Revit to automatically generate a 3D model of a monolithic caisson. It is designed to generate the Revit model of a caisson with concrete body and reinforcing bars. The size of caisson, the number of reinforcing bars, and the space between reinforcing bars are automatically changed when users update parameters. This paper presents how we developed this parametric family in Revit for monolithic caisson design and how it would enhance its design process.

Aug 1, 2013

By W W. Moorhouse

A survey of recent literature indicates that sulphides occur in the volcanic rocks of the Archean, or in sedimentary rocks intercalated with the volcanic rocks. The thick sedimentary sections are generally poor in sulphides. Thus, the widespread pyrite and pyrrhotite mineralization in the Archean may be largely of volcanic origin. Introduction I N this paper, commercial base-metal deposits will not be considered, as they are dealt with in other papers of the Symposium. Instead, attention will be focused on those sulphides, often associated with graphitic argillites or tuffs, which have appeared in such embarrassing abundance in electromagnetic surveys of Archean areas. The data on which the paper is based are drawn from recent reports of the Ontario Department of Mines, the Quebec Department of Natural Resources and the Geological Survey of Canada. The information available from these sources is unfortunately limited, because sulphides commonly occur in sheared rocks, such as black argillites and tuffs, which rarely form conspicuous outcrops, and may not be exposed at all. Thus, in the absence of geophysical information, even detailed mapping may fail to reveal the presence of sulphide-rich rocks.

Jan 1, 1965

By C. M. Campbell

Canadian newspapers from coast to coast, have been, for months, denouncing those articles entitled, "The Whisper of Death," which have been appearing in the Montreal Star. I have not read these articles as the newspapers do not print them; they just denounce them or class them as jokes. Apparently they think that they are not suitable for the ordinary Canadian to read. It appears, however, that the Star has said that unless we balance our budget, and that soon, we shall be bankrupt. That seems to me like common sense, though the Victoria Times says editorially that the Star claims will "shortly find a place in the joke column". In this editorial the Times quotes with much enthusiasm from the Quebec Telegraph. "Canada," says the Telegraph, "is all right. Her natural resources are so vast that no one need worry. Her future possibilities are limitless; her assets beyond figures". Does it not seem like the limit of nonsense for a country that is not paying its running expenses to make such pretensions? After fifty-five years of Confederation and much talk of national status we are still sponging on the mother country for our external defense; we still allow the hard pressed tax-payer in the old land to shoulder the entire burden. We even now refuse to accept able-bodied working-men from that small and overcrowded country and yet blatently talk of limitless resources.

Jan 1, 1923

By D. Royston

In SAG mills fed with a variety of ore types, hard packing between the shell lifters can come and go depending on rock type and rock size distribution and the presence of a binder. Packing can appear in all sizes of SAG mills, and can be tenacious. High ball impact forces (depending on ball size) in larger mills may compact and encourage packing. Packing can have a negative impact on milling performance and a change in shell liner design may be required to remove it. However shell liner design changes need to be managed with care to ensure liner reliability. In smaller mills control of packing can extend shell plate wear-life and may help to maintain milling performance in fixed-speed mills through the liner wear-cycle.

Jan 1, 2012

By James J. Holmes

ACCIDENT prevention as we know and understand it today is of comparatively recent origin. As a matter of fact, the Industrial Accident Prevention Association of Ontario, which is the oldest organization of its kind in the Dominion, celebrated its thirtieth anniversary only this year. On the other hand, one could say that the history of accident prevention is almost the history of mankind itself. In a general sense, every forward step that man has made throughout the centuries has been largely due to two things: (1) a desire for increased comfort, and (2) the need for safety; and, always, the need for safety has taken precedence over the desire for comfort. While it is true that hundreds of volumes have been published, dealing with the many aspects of accident prevention work, you cannot go to a library and pick out a book that has all the answers in it. Such a book has never been published-we are still looking for some of the answers. However, a good deal of real progress has been made.

Jan 1, 1945

By G. Titichoca

Modification of the blasting process considers that any increase in the energy consumption generates greater benefits if done in the later stages (associated with a larger decrease in energy consumption). Therefore, although the blasting cost is doubled, generating a greater proportion of fines in addition to a weaker ore (because with greater loads and appropriate distribution of explosives a greater number of internal cracks is generated), the reduction of the unit cost that occurs in the grinding stages (SAG and ball mills) generates a positive balance in the overall size reduction process. Codelco Chile, Division Andina, has developed an extensive experimental plan to evaluate the concept of blasting modification applying greater energy. This was implemented in two stages, each including a specific mine sector: La Union and Don Luis. This paper reviews the experience of implementing such blasting modifications at the La Union mine and its impact on the design concepts and the operation of the SAG mill plant

Jan 1, 2007

By R. R. Montigny

A brief description is given of the history, location and geology of the Granisle Copper Limited operation on Copper I land in Babine Lake. Detailed information is given with regard to pit design, planning, drilling, blasting, excavation and haulage. Equipment maintenance and mining costs are also presented.

Jan 1, 1971

By J. E. McMenamin, R. B. Hall

"With the emphasis in the past decade on larger and more efficient equipment for open-pit operations, the Normandie mine of the Asbestos Corporation has followed the trend, switching from the smaller type of percussion drills to down-the-hole rigs. One 5 Y2 -in. percussion drill is still in use, but is limited to a ""smooth blasting"" role or to the control of the slope on final benches.In keeping with the times, an attempt was made to eliminate, as much as possible, the use of high explosives and to maximize the percentage of ammonium nitrate -fuel oil mixture. As the concentration of ground water increased with increased mining depths, small pumps were initially employed for the dewatering of boreholes. This proved unsuccessful, and a hole-blowing rig was built and a conversion to plastic liners made. The acquisition of a bulk-mix AN-FO truck has permitted the changeover from an AN premix to an ammonium nitrate prill -fuel oil combination at the borehole."

Jan 1, 1966

By Eldon L. Brown

Location and History The Sherritt Gordon property is located in northwestern Manitoba, about 100 miles north of The Pas and 40 miles northeast of Flin Flon. It is connected with the Manitoba Northern railway, which runs from The Pas to Flin Flon by a branch line, 42 miles in length. The location of the property is shown on the sketch-map, Figure 2. The ore deposit was first discovered by Philip Sherlett, a Cree Indian, in 1922. In 1924 Sherlett&apos;s claims lapsed and the ground was re-staked by Carl Sherritt and Dick Madole, and was optioned by them to J. P. Gordon in the summer of 1925. Gordon re-optioned the property successively to three well-known mining groups, one of which did some surface trenching .and put down 28 shallow diamond-drill holes before dropping their option. In the latter part of 1927, a Company known as Sherritt Gordon Mines, Limited, was formed to take over the property, and preparations were made for systematic development work. Preliminary Development In order to fill-in gaps left by the original drilling, a light diamond-drill outfit was flown-in to the property from the Hudson Bay railway in the early fall of 1927. Ten shallow holes were put down before freeze-up .and a considerable amount of surface trenching was completed. Based on the results of the surface trenching and the shallow diamond-drilling, an extensive development campaign was outlined. A winter road, 90 miles in length, was cut from mileage 55 on the Hudson Bay railway, and during the winter of 1927-28 a total of 2,600 tons of freight was hauled-in to the property. This freight included four complete diamond-drill outfits, two complete mining plants, building material for two sets of camps, and supplies for one year&apos;s operations, including 105,000 gallons of fuel-oil for Diesel engines.

Jan 1, 1933

"Previous studies on the effect of polytetrafluoroethylene addition during chalcopyrite leaching under conditions similar to those of the CESL process have reportedly resulted in complete leaching of the copper without the need for grinding of the flotation concentrate. However, these studies employed a pulp density of only 1% and finely sized PTFE particle that required the use of high impeller rotation rates that are not sustainable at an industrial scale. This paper explores the performance of 1/8” diameter balls of PTFE, that readily sink in the leach solution, on leaching performance at impeller rotation rates and ore pulp densities more typical of industrial practice. Possible routes for separation of the PTFE from the leach residues and their regeneration for recycling back to the leaching stage are also discussed.INTRODUCTIONChalcopyrite, CuFeS2, is the most important primary sulfide source of copper. While pyrometallurgical smelting of chalcopyrite remains the only widely accepted route for treating chalcopyrite concentrates, several medium temperature pressure oxidation processes are claimed to be economically feasible (Muir & McDonald, 2007). Among these, the CESL process has been extensively piloted and demonstrated at the prototype scale. The overall process chemistry of the CESL process may be summarized as follows (Marsden & Wilmot, 2007):4CuFeS2 + 5O2 + 4H2SO4 ? 4Cu2+ + 4SO4 2- + 2Fe2O3 + 8S0 + 4H2O (1)4CuFeS2 + 17O2 + 2H2SO4 ? 4Cu2+ + 10SO4 2- + 4Fe3+ + 2H2O (2)Though copper extractions of over 95 % are achieved, the CESL process requires extra grinding of the concentrate (Muir & McDonald, 2007). This is because leaching is conducted at temperatures around 150 °C, where the elemental sulfur produced is molten and grows thicker on the mineral’s surfaces as oxidation progresses, creating an increasingly large barrier for mass transport. In addition, the sulfur is sticky and tends to cause the mineral particles to agglomerate, effectively halting further oxidation of the particles that end up embedded within the agglomerates. Consumable surfactants, such as ligin sulfonate, have been shown to be effective at avoiding agglomeration, but they are not effective at removing sulfur from the minerals. Hence, their use does not obviate the need for fine grinding."

Jan 1, 2012

By L. Janku, G. Hancox, M. Villenueve, C. Massey

Wellington lies in a seismically active area 150 km from a subduction zone and in the vicinity of several active faults, which poses a risk to its infrastructure and inhabitants. One of these major faults, the Wellington Fault, runs through the centre of the city and across several lifelines, including the natural gas pipeline and the freshwater pipeline. The first settlement in the area was severely damaged in 1848, soon after its establishment, by an earthquake of approximate magnitude Mw 7.4 - 7.5 (Grapes, Little, & Downes, 1998). In 1855, another earthquake of magnitude Mw 8.2 generated by a nearby fault uplifted the eastern part of the current Wellington area and caused several landslides in the surrounding hills (Grapes & Downes, 1997). The Central Business District lies in the area of a sedimentary basin and partly on reclaimed land. Many residential areas, as well as some vital infrastructure, however, lie on or along the slopes in the surrounding hills. The bedrock in the area comprises predominantly the Torlesse greywacke of Permian – Late Triassic age. The greywacke is tilted to a steep angle, intensively faulted and fractured (Cook, 2001). Even though several studies in the past assessed the seismic risk in the area (e.g. Brabhaharan, Hancox, Perrin, & Dellow, 1994), the studies either focussed solely on the area of the sedimentary basin or based their assessment of the hilly terrain purely on slope morphology (slope angle). Previous studies have shown that slope shape and contrasting materials in the slope can amplify earthquake ground motions, such factors are typically called site effects (e.g. Geli, Bard, & Jullien, 1988). Any attempt to systematically quantify the site effects and consequent seismic response of the slopes and use it to predict the consequences of the next large-magnitude earthquake, has not yet been carried out. In this extended abstract we outline the methodology of a PhD research project, focussed on investigating the site effects on the slopes around Wellington and on creating representative numerical models of ‘characteristic’ Wellington slopes and materials. This extended abstract presents the methodology adopted for the assessment using the Te Ahumairangi Hill site as an example.

Jan 1, 2015

By Perry L. Christian

"Mana/ta Coal Ltd. 's Costello Mine, located seven kilometres east of Estevan, Saskatchewan, has been operating at the present location since 1960. During the past twenty-three years, annual production of lignite coal has averaged 590 000 tonnes. The coal is used for power generation and for industrial and domestic use. Markets, operating techniques, facilities in place and reclamation are discussed. Introduction The Costello Mine (formerly the Klimax Mine) is located in southeastern Saskatchewan, approximately 210 kilometres southeast of Regina and 5 kilometres from the United States' border, as shown in Figure 1. The present mine, 7 kilometres east of the city of Estevan, has been operating since 1960. The history, however, of the Costello Mine and of the Estevan Coalfield dates from the initial settling of the area in the 1880s. Mining initially consisted of burrowing into the side of the Souris River Valley or other hillsides where the coal seam was exposed. Eventually, slopes were put down in the Estevan/Bienfait area and vigorous underground activity existed. In the late 1920s surface strip mining was introduced. The use of strip mining progressed to the point where it completely replaced underground mining in the 1950s and it is the only method in use today. During the past 23 years annual production has averaged 590 000 tonnes. The lowest production was in 1960 when the mine was starting up at 167 000 tonnes and the highest production was in 1977 when production was 1 509 000 tonnes. The Costello Mine controls approximately 11 400 hectares of mineral rights in the Estevan area. This is made up of 4 900 hectares of freehold coal and 6 500 hectares of leases. The area forms a large, irregular shaped configuration. Most holdings are contiguous and adjacent. The mine also owns some 8 400 hectares of surface rights. The lands under the Costello Mine's surface rights control, which are not being used in the mining operation, are leased to local farmers and ranchers. This ensures that the land is used to its full potential, both before and after mining."

Jan 1, 1985

By P. Rosario

"Current industry practice for HPGR assessment and sizing relies on conducting a series of tests using pilot-scale machines with roll diameters of 700 mm to 1000 mm. Substantial amounts of sample are required for such pilot test programs, typically 1 to 10 tonnes of the sample is needed depending on the level of study and complexity of the resource. Collection of large quantities of representative samples during the early stage development is challenging and expensive, thus significantly hinders the HPGR technology from being incorporated into early-stage designs. A robust and reliable laboratory test is therefore needed to allow a fair consideration of HPGR for early stage projects. With support from the Canadian Mineral Industry Research Organization (CAMIRO), the NBK Institute of Mining Engineering at the University of British Columbia (UBC) developed a suite of Piston Press bench-scale tests that correlated to pilot and full scale HPGR operating information (Davaanyam, 2015; Davaanyam et al, 2015; McClintock, 2018). The Piston Press Tests (PPTs) are capable of assessing the HPGR technology at the scoping, pre-economic analysis (PEA), and pre-feasibility (PFS) stages of project development. This paper will briefly describe the theory on which the PPTs are based, and then presents a case study conducted for a copper deposit to show how the PPTs are being used for scoping and pre-feasibility level studies. Specifically, the PPTs are being used to provide information for preliminary sizing and selection of an HPGR and to assess the effect of ore variability on HPGR performance. The results are also applied to developing HPGR circuit designs and can be incorporated in simulation so that optimum design parameters can be selected.INTRODUCTION It is widely accepted that high pressure grinding rolls (HPGRs) offer a viable energy-efficient solution for the modern comminution flowsheet design. Table 1 summarizes selected examples of HPGR applications in the hard rock mining industry. The main benefits of HPGRs are energy savings which leads to lower operating costs, and its stable operating characteristics that can better cope with variations in ore hardness when compared to the conventional SAG mill-based comminution circuits."

Jan 1, 2019

By George Langford

Introduction The manufacture of ductile beryllium is one of the most interesting problems confronting the metallurgist today, and one which becomes more acutely in need of resolution as the uses for beryllium increase. Beryllium belongs to the hexagonal group of metals along with zinc, magnesium, and cadmium. The melting point of the metal is about l,280°C. ± 5°C. Due to its brittleness, the metal&apos;s chief use is as an alloying agent in copper and iron. The very low absorption coefficient of beryllium for x-rays makes the metal ideal for x-ray windows, and, similarly, because of its low capture cross-section for neutrons, the metal holds a preferred position in the field of nuclear physics. Modern x-ray diffraction methods were responsible for explaining the mechanism whereby zinc metal, although brittle when cast, could be made ductile at room temperature. The diffraction patterns of zinc and magnesium indicated the importance of the parts played by recrystallization and preferred orientation in this mechanism. It was with this in mind that an Investigation into the recrystallization and preferred orientation of beryllium was undertaken. The investigation, after a series of experiments were conducted involving cold-working and annealing, yielded the recrystallization temperature curve for beryllium. Both the texture of preferred orientation and the effect of recrystallization on this texture when subjected to compressive stresses were also determined. W. A. Alexander, J. K. Swinton and L. M. Pidgeon, in their investigation on The Recrystallization Temperature of Beryllium (C.I.M., Trans., Vol. L, 1947, pp. 657-664), utilized the Brinell ball as a means of cold straining the metal. Sufficient strain was developed to estimate the recrystallization curve for the metal. However, in order to determine the lowest recrystallization curve, as well as to develop a preferred orientation structure, larger deformation than that possible with a Brinell ball was required. The plastic deformation of beryllium can be carried out at an elevated temperature above 700°C. Above 850°C., the metal is quite ductile and can be readily compressed or extruded.

Jan 1, 1948

By A. G. Scobie

THE research laboratory of this Company was recently faced with the problem of determining trace amounts of tungsten in a series of classifier sands. A spectrographie survey revealed the feasibility of using this instrument in the final evaluation, but a check of the common methods in use for the isolation of tungsten (3, 4) showed these methods to give incomplete separation for trace amounts. An investigation into the possibility of modifying these procedures, or developing others, was thus indicated. ASSAY PROCEDURE Weigh 10 grams of 200-mesh ore or concentrate into a 400-ml. beaker, wet the sample well with about 20 ml. of water, and add 100 ml. of hydrochloric acid. Cover, digest at 60° to 70° C. for about 1 hour, and then boil down to approximately 25 ml. Cool, add 25 ml. of hydrochloric acid and 10 ml. of nitric acid, and again boil to former volume. Add 20-ml. portions of nitric acid with successive boiling clown until chemical action is complete. Then add 20-ml. portions of hydrochloric acid until all nitric acid is removed. Take nearly to dryness on a law-temperature hot plate, but do not bake. Take up in 10 ml. of hydrochloric acid and 20 ml. of water and heat on a law-temperature hot plate until all iron goes into solution. Dilute to 200 ml. and heat to just below boiling. Stir in pulp of about half of a No. 41 Whatman filter paper (12.5-cm.) and continue digestion on plate with occasional stirring for 15 to 20 minutes.

Jan 1, 1943