Search Documents

By Ruediger Holz, Tommaso Settimo, Luciano Vignolo

Optimized CAPEX, OPEX, new products, yield and product quality in new process equipment as well as by upgrading of existing facilities are the key factors for success and profitable operation. For this, innovation in processes and design is crucial. Danieli can support their clients by offering innovative and well-thought-out process equipment and upgrade solutions. In 2018, Danieli has put into operation a complete cold processing complex in Turkey, which includes a new continuous pickling tandem mill featuring latest generation of market oriented technologies. In this line, dedicated to run a broad range of size and grades (IF to AHSS as DP1000), the highly efficient Turboflow® pickling process was selected. This technology already proved its efficiency and ability in former applications handling ultra-thin gauges at speeds even exceeding 400 m/min in the pickling tanks. The 5-stand 6-high OSRT tandem mill features important developments, like actuators to improve significantly strip flatness and a special air knife arrangement on the tandem mill exit side to generate perfect strip surface cleanliness. In galvanizing lines, the zinc pot is the most effective area to reduce costs in operation and consumables and increase the product quality. Danieli has spent significant efforts in developing most advanced technology for the wiping process. A fully integrated system solution has been designed to perform a wiping process with high quality, economy, accuracy and productivity. Center part is the newly developed X-Jet / Compact X-Jet air knife, added by new generation electromagnetic stabilizer as well as robotic systems to reduce human intervention and health risks in this area. This technological package is ideal also for upgrade of existing lines, typically generating a return of investment less than 1 year. On top, Danieli has developed advanced automation systems including L2 and L1 controls to achieve outstanding product performances.

Oct 1, 2019

By Breno Totti Maia

This work was a continuous and multidisciplinary development. Through studies of the blowing process and its parameters results, evolutions, improvements and adjustments were made on the lance’s hot face with Slagless® technology, as well in the process parameters and mitigating actions of the projection of materials out of the converter. The main results are the increase in the nozzle’s life with a “record mark” of 1785 heats, and water leakage occurrence in the cartridge decreased considerably reaching the mark of one year without any occurrence.

Oct 30, 2017

By Douglas Glenn Stalheim

Production of structural steel with a minimum yield strength of 700 Mpa produced as hot rolled coil has become increasingly popular due to cost considerations when compared to quench and temper equivalent product. This grade when produced as hot rolled coil requires the use of microalloy precipitation strengthening mechanisms. This is typically a combination of niobium and titanium microalloys. While the metallurgical concept of structural steel precipitation strengthening mechanisms has been well researched and published, actual implementation into the production process can be very challenging. In addition to achieving a minimum yield strength of 700 Mpa, in many applications additional mechanical property attributes of formability as measured by hole expansion testing along with low temperature toughness properties are now required. Achieving a balance of all the mechanical properties in a stable and repeatable performance in production using microalloy precipitation strengthening mechanisms further increases the challenges. This paper will discuss the metallurgical/process strategies required to successfully produce 700 Mpa minimum yield strength hot rolled structural steel coil. In addition, the role and goals of both niobium and titanium in this product design will be presented.

Oct 30, 2017

By Andreas Jungbauer

Two Arvedi ESP plants going into operation in 2015 will allow a Chinese steel producer to better serve the extremely attractive local and export markets for high-quality, thin-gauge strip products. The energy consumption and the related costs are reduced by up to 45% compared to conventional casting and rolling processes. This also means a major reduction in CO2 emissions. The new plants are designed for an annual production capacity of 2 x 2.55 million tons of high-quality, ultra-thin, hot-rolled strip products with widths of up to 1,600 mm and thicknesses down to 0.8 mm. The project scope also features a comprehensive training and assistance package for plant start-up and operations by personnel from the existing ESP plant at Acciaieria Arvedi SpA, Italy. The plant setup, the trainings and assistance program as well as latest results from the ESP plant in Italy will be presented. While this project is under execution three further ESP lines have been ordered by the same customer summing up now to five ESP lines at the same location.

Jul 30, 2018

By Marco Antonio Meggiolaro

Notches are preferential sites for fatigue and for environmentally assisted cracking (EAC) initiation. Semi-empirical notch sensitivity factors have been used for a long time to quantify notch effects on fatigue design. Recently, this concept has been mechanically modeled using techniques which properly consider the notch tip stress gradient influence on the fatigue behavior of mechanically short cracks. This model properly calculates such values from the basic fatigue resistances of the material, its fatigue limit and crack growth threshold, considering the characteristics of the notch geometry and of the loading, without the need for any adjustable parameter. Such criteria to estimate notch sensitivity and tolerable short cracks on fatigue have been extended to EAC conditions and verified by proper tests. In its simplest version, the criterion for the maximum tolerable stress under EAC conditions uses the resistances to crack initiation and to large crack propagation and the characteristic short crack size under EAC, considering the crack size and stress intensity factor. Moreover, the tolerance to short cracks under fatigue and under EAC conditions can be unified in an extended Kitagawa-Takahashi diagram, a new and potentially very useful tool for material selection tasks.

Aug 8, 2018

By Mario González Ramírez

The safe transport of sour gas requires steels with enhanced hydrogen induced cracking (HIC) resistance. Centerline segregation bands of high hardness microconstituents and non-metallic inclusions are the heterogeneities usually linked to HIC failures in pipeline steels. Full-scale production heats of a new low Mn, Nb microalloyed steel were produced by different steel mills aiming at the application in sour gas environments. The new alloy design provides both effective strengthening and control of sulphide inclusions. Coil microstructure consisted of fine grained ferrite with a small volume fraction of uniformly dispersed eutectoid aggregates. Most importantly the microstructure was uniform in both the longitudinal and transverse directions and exhibited exceptional consistency. Samples from this steel were submitted to HIC testing according to NACE standards TM0284-2003 without any sign of cracking. The results, so far, confirm that this new alloy design provides the unique opportunity to economically produce a high strength pipe steel grade with improved sour service resistance for the linepipe industry.

Aug 8, 2018

By Daniel Wild, Tobias Scheffer, Marvin Laugwitz, Martin Jochum

Leveling is a standard process in the rolling mill to eliminate flatness deviations. The process layout is based on models and the leveling result depends on the accuracy of the material parameters in these models. Even small deviations from the correct assumptions can have a major effect on the final flatness. Thus, after leveling the products may look optically flat, but subsequent to a final cutting process springback occurs due to residual stresses. The objective of this work is to analyze the influence of material parameters and gravity on the flatness after leveling. To evaluate the sensitivity of the process, an FE parameter study is exerted that reveals the influence of fluctuations in material properties in the case that the leveling setup is fixed. Gravity is neglected to not conceal flatness deviations. Examples of this study are rerun in a further step under consideration of gravity to also analyze its influence on the resulting flatness and residual stresses. Finally, to analyze the consequence of the residual stresses, all information of the plate from the previous step are transferred while gravity is suppressed to prompt springback. This study revealed that slight deviations of the material properties can lead to uneven plates in simulations where gravity is not considered. If gravity is taken into account, the unevenness is concealed and the plate seems flat. A springback simulation of the same plate shows that strong residual stresses are still present and would lead to unevenness if e.g. the plate were cut.

Oct 1, 2019

By J. Bas A. F. Smeulders

Traditional laboratory lubrication tests, including those for cold rolling lubricants often involve measurement of neat oils. To achieve increased levels of test severity, such tests are often carried out at high temperatures and prolonged durations. However, we found that the levels of lubricant degradation and wear in these tests can be much higher than in the field. Moreover, steel rolling is not done with neat oils, but with emulsions, where the presence of water influences film formation, surface chemistry and oil composition in the roll bite. To better approach the situation in the field, and thus to be able to develop rolling oils with improved lubrication performance, several lubrication tests were developed for emulsions: direct measurement of film formation and measurement of Stribeck curves, in which the emulsions can be assessed in terms of their boundary lubrication and elastohydrodynamic behaviour. The key innovation is that also another test method was developed, which focuses on boundary lubrication and wear, and the role of extreme pressure and anti-wear additives. Realistic levels of test severity are achieved in the tribometer by mimicking frictional power intensities and flash temperatures for typical cold rolling or tinplate mills. Test conditions can be adapted according to the mill stand or pass number and other cold rolling process parameters. The emulsions are kept at normal operational temperature. Clear differences could be observed between emulsions of various concentration and composition. The viability of the method is illustrated by a number of field cases, in which a good correlation is demonstrated between the laboratory tests and the performance in a pilot or production mill.

Jul 30, 2018

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Douglas Glenn Stalheim

The demands for improved mechanical properties in hot rolled long products are increasing as the expectations of global Standards and construction designer’s increase. Cost constraints limit the excessive use of expensive alloys to meet these expectations. In addition, depending on the mill, equipment can limit what can be realized to meet the increasing expectations. The most effective way to meet the increasing expectations for improved mechanical properties of optimum strength and ductility is through producing steel with as fine as possible uniform cross sectional grain size in the “as-rolled” condition. The best solution to the development of this fine and uniform cross sectional grain size is to develop a cost effective alloy design coupled with proper metallurgical process control implemented into an existing mill’s equipment capability and layout. In other words, properly bringing together alloy, metallurgy, process control and existing equipment capabilities to develop an optimum product that can meet the increasing demands of the construction designer. This paper is designed to give a solid understanding of the production and metallurgical requirements to achieve a grain size in “as-rolled” long products that is as fine as possible within the limitations of the process and production parameters of the individual plant.

Jul 30, 2018

By Dagoberto Brandão Santos, Kairo de Barros Guimarães, Túlio Magno Füzessy de Melo

The effect of the cooling conditions on the microstructure and hardness of a Dual Phase hot-rolled steel 800 MPa strength was investigated. Simulations of the cooling conditions using a dilatometer were carried out from samples of a hot rolled coil with variations of the intermediary temperature from 620 to 740°C, isothermal holding time between 1 and 10 s and coiling temperature between 50 and 400°C. In addition, two CCT (Continuous Cooling Transformation) diagrams were developed to evaluate the effect of the isothermal holding time on the phase transformations of the remaining austenite. It was observed that the intermediary temperature has a strong influence on the kinetics of the phase transformation, as well as the isothermal holding time influences the amount of ferrite formed and, consequently, the final microstructure and hardness of the material. The coiling temperature did not cause significant changes in the amount and morphology of the ferrite, but a gradual replacement of martensite with bainite was observed, which, in addition to the self-tempering effect, contributed to the hardness reduction.

Oct 1, 2019

By Pedro Cunha Alves, Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Julio Aníbal Morales Pereira

The capacity of steelmaking slags (CaO-SiO2-Al2O3-MgO) on inclusion removal from liquid steel was investigated through experimental conditions. Laboratory experiments with slag and steel samples (with inclusion population known) were performed using a vertical electric resistance furnace at 1600 ºC. After the melting experiments, slag and steel samples were separated and analyzed regarding their chemical composition and inclusion population evolution. The capacity of slags on inclusion removal was evaluated based on the thermodynamics (solid and liquid phases proportion, phase composition and effective viscosity of slags) calculated using the FactSageTM 7.2. Results indicated that changes in the composition of slags (regarding CaO/SiO2 e Al2O3) presented effects on the steel cleanliness. The total inclusion density decreased in all steel samples and the removal of inclusions by slags shows a tendency to improve as their viscosity decreases (< 0.23 Pa.s).

Oct 1, 2019

By Fábio Dian Murari, Antônio Adel dos Santos

The effect of reheating temperature of slabs on the precipitates dissolution and mechanical properties of Ti-Nb microalloyed steel was investigated in pilot scale. It was verified, by means of transmission electron microscopy, a significant decrease in precipitates formed during the solidification of the steel as the reheating temperature increased from 1100°C to 1200°C. No significant changes in size and shape of the precipitates were observed with further temperature increase up to 1280°C. In line with the precipitates dissolution behavior, an increase in strength was observed with the elevation of the reheating temperature up to 1200°C, due in part to the reprecipitation of fine Nb-rich precipitates during the hot rolling. At 1200°C the presence of deformed ferrite on the microstructure contributed to the additional increase in strength. After reheating above 1200°C up to 1280°C, a decrease in strength of the rolled plates was noticed. This effect has been credited to the absence of deformed ferrite grains and also to a small increase in the low angle grain boundaries size. The results were in agreement with Thermo-Calc and Dictra simulations.

Oct 1, 2019

By Bernhard Hiebl

Global trends that are constantly challenging the iron and steel producers are related to worsening of the iron ore grades, higher substitution rates of main iron ores to cheaper raw materials due to economic pressure and increased environmental standards. Changing the raw materials in an operating plant can significantly influence the sintering or pelletizing process. Adjusting all process parameters to regain stable and high productive operation takes considerable time and causes production losses. Furthermore changes in raw materials lead to variations in the process gas flows and emission concentrations.Therefore SVAI developed two models for numerical simulation of sintering process and pelletizing process. Amongst others the models are based on Ergun equation and include chemical reactions of the related process. For already operating plants the simulations shall predict changes of the process parameters when raw materials are exchanged or when operational parameters are varied. Furthermore the simulations give advantageous information for the design of green field plants and allow the simulation of different plant configurations.The objective of this paper is to demonstrate what the latest developments are in these numerical simulations and what Siemens VAI is doing to overcome the remaining challenges in this field.

Aug 2, 2018

By Hormando Leocadio, CWM van der Geld, Julio Cesar Passos

Impinging water jets promote high heat flux extraction rate. Steel industry widely employs the process for accurate temperature control to improve the microstructure and to ensure adequate mechanical properties. The range of surface temperatures, heat fluxes and cooling rates are very large, which makes it important to obtain an accurate value of the heat transfer coefficient. This paper presents an experimental and numerical study of the heat transfer behavior of a high temperature (450°C - 900°C) steel plate cooled by a water jet at 20°C to 70°C. High-speed imaging (up to 20,000 fps) within water jet impingement zone allowed the characterization of the boiling regimes in the early stages of cooling. The effects of initial temperature, water jet temperature and velocity on the heat transfer coefficient were analyzed by inverse heat conduction method that predicts the heat flux and temperature on the top surface from temperatures measured with thermocouples inserted in test plate. Heat transfer is strongly affected by the initial temperature of the hot steel, water jet temperature and, less intensely, by jet velocity. High cooling rates start when liquid water is in direct contact with surface temperatures above 700°C.The results will contribute to the enhancement of the temperature cooling control on the runout table and cooling model employed at Usiminas Hot Strip Mill.

Oct 1, 2019

By Gerhard Finstermann, Ichiro Maeno, Takehiko Saito, Hironori Shimogama, Konrad Krimpelstätter

Automobile manufacturers are developing Electrified Vehicles with light steel body structure designs that reduce mass and therefore greenhouse gas emissions over the vehicle’s entire life cycle. This raises the demand for the production and development of Advanced and Ultra High-Strength Steels (AHSS / UHSS) and Electrical Steels with increased permeability and reduced core loss to improve energy conversion efficiency. To meet this requirements the steel market is tending towards new generations of AHSS with improved formability (3rd generation AHSS) and high-silicon steels with higher strength and thinner products. With this growing demand for advanced high-strength steels and electrical steels, producers are faced with a unique and interesting challenge in producing materials that strain or exceed the capabilities of existing mill equipment and automation designed to produce low- to medium-carbon sheet. While specialty steel producers have known for decades how to process special high-strength steels and thinner gauges, this equipment typically does not offer the yield and productivity desired by the market, necessitating innovation in re-engineering existing equipment to meet the market demands more economically than new construction. In the case of cold rolling, this can be supported through variable roll geometries, more effective roll-gap lubrication technologies, application of strip heaters (Warm Rolling) to reduce risk for edge crack propagation and strip breaks as well as continuous rolling managed by state-of-the-art automation technologies.

Oct 1, 2019

By João Luiz do Vale

In standard wear tests, such as pin on disk (ASTM-G99) or block on ring (ASTM-G77), the apparatus simulates conditions that are often different from a machine element real application. Therefore, for an accurate investigation of a tribological application, it is essential to test the real condition in which there are similarities as: geometry, contact details, force application mode, materials, among others. It emphasizes that for studies involving polymeric materials it becomes extremely relevant. Thus, the Laboratory of Surfaces and Contact (LASC) at UTFPR developed an apparatus for sliding bearing on shaft test. In that equipment, loads are applied by a dead-weight system and the frictional force is measured on a load cell. The apparatus operating ranges for load added to the dead weight system and rotation shaft are from 0.2 to 5.0 kgf and from 260 to 3500 rpm, respectively. This paper presents a detailed evaluation of such apparatus, which includes free-body diagrams analysis and a deduction to obtain an equation for the kinetic friction coefficient. Also, the standard measurement uncertainties of a caliper, an electronic scale, and a cell load were determined. It was verified that the kinetic friction coefficient equation is dependent on the apparatus geometry, the applied load, and the frictional force value. Additionally, through the statistical significance analysis it was concluded that some terms in the equation were not significant. Finally, through the application of the error propagation theory in the kinetic friction coefficient equation, the standard measurement uncertainty of the apparatus which showed a value nearby 0.002 along the operating range of the apparatus was obtained.

Jul 31, 2018

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the virgin condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 69 to 258 MPa producing rupture times varying from 8 to about 4908 h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results mentioned in literature for the same material in the virgin condition.

Aug 16, 2017

By Ivênio de Oliveira Teixeira

Grelhas constituem o fundo móvel dos setores da esteira sem fim das máquinas de sinterização. Diferentes tipos de materiais têm sido utilizados para a fabricação dessas peças, desde aços resistentes ao calor e inoxidáveis até ferros fundidos de alta resistência, tendo como parâmetro de controle a perda de massa ou redução da espessura das grelhas. A necessidade do aumento do ritmo operacional das sinterizações ao longo dos anos tem levado ao aumento da substituição de grelhas, contrapondo ao aumento da produtividade das sinterizações. Desta forma, a adequação da resistência ao desgaste abrasivo e a minimização de transformações microestruturais em função as condições de utilização dos materiais desses componentes mecânicos têm sido alvo do desenvolvimento de materiais para essa aplicação. Nesse trabalho é discutido o desenvolvimento de materiais aplicados em grelhas de sinterização, visando o aumento da sua vida útil, a partir do melhor entendimento dos mecanismos de degradação e da realização de ensaios laboratoriais de desgaste abrasivo, corrosão a quente e fadiga térmica. Dentre cinco alternativas avaliadas, a concepção de material com matriz ferrítica e adição de elementos químicos formadores de carbonetos mais estáveis a elevadas temperaturas e formação de camada mais aderente de óxidos apresentou melhores resultados, gerando uma perspectiva de aumento da vida útil da ordem de pelo menos três vezes em relação à condição atual.

Aug 16, 2017

By Paulo Sérgio Moreirar

A caracterização do tamanho de grão austenítico prévio dos aços é importante, pois a partir desta investigação é possível estimar parâmetros metalúrgicos que repercutirão na qualidade final do produto. Desenvolver métodos para a revelação do contorno de grão prévio se faz necessário, porém, muitas pesquisas apontam para a complexidade destes métodos. Este trabalho se propõe a avaliar diferentes técnicas de contraste para revelar o contorno de grão austenítico prévio dos aços ABNT 1045 e ABNT 4340. Foram utilizadas três técnicas para revelar o contorno de grão austenítico prévio, sendo: ataque químico, ataque térmico e têmpera superficial. Destacam-se o ataque térmico e a têmpera superficial como métodos inovadores. O ataque químico foi realizado em três condições, variando-se a composição de ácido clorídrico adicionado ao reativo a base de ácido pícrico. O ataque térmico foi realizado em duas condições, em atmosfera inerte e em atmosfera oxidante/inerte. A técnica de têmpera superficial consistiu em austenitizar e promover um tratamento térmico de têmpera com restrições na taxa de resfriamento, promovendo um efeito de transformação bainitica nos contornos de grãos austeníticos prévios. Pôde-se concluir que a técnica mais eficiente para os aços estudados foi o ataque químico a base de ácido pícrico. As técnicas de ataque térmico e têmpera superficial se mostraram eficientes para o aço ABNT 1045, apresentando potencial de melhoria metodológica para outros tipos de aços.

Aug 16, 2017